CN101721337A - Cosmetic containing Rosa setate X R. rugosa extract - Google Patents

Abstract

The invention relates to a cosmetic containing a Rosa setate X R. rugosa extract, which comprises the following components in percentage by weight: 35-45 percent of mixture of the Rosa setate X R. rugosa extract and NaCl, 10-12 percent of AES, 0.8-1.3 percent of aluminum magnesium silicate, 0.9-1.2 percent of xanthan gum, 10-15 percent of Rosa setate X R. rugosa pollen and the balance of deionized water. Meanwhile, the invention also discloses a preparation method of the cosmetic. By adopting the Rosa setate X R. rugosa extract which has stable performance and is abundant in various nutrient components, such as vitamin, amino acid, flavone, and the like as an additive of the cosmetic, the cosmetic has the obvious effect in aspects of nutritionally moisturizing human skin, promoting skin metabolism, softening the skin, inhibiting pigmentation and resisting aging.

Description

A kind of cosmetics that contain the Rose grievances extract

Technical field

The present invention relates to a kind of cosmetics, relate in particular to a kind of cosmetics that contain the Rose grievances extract.

Background technology

Market research shows, consumer begins favor and buys organic cosmetics at present, and some consumers are because skin self than factors such as sensitivities, is tending towards natural, organic, safety to the demand of cosmetics; And medium injure conducting vigorous propaganda of skin to synthesis of chemicals, and demand and the market sale share of further impelling natural organic to make up product progressively increase.

Make up in the product raw materials for production at numerous natural organics, Flos Rosae Rugosae receives much concern.Flos Rosae Rugosae is the perennial evergreen or the fallen leaves property shrub of Rosaceae Rosa, and is at west general designation Rose, Chinese then different lifting manipulation and differentiations such as Flos Rosae Rugosae, Flos Rosae Multiflorae, Mo Hong and Chinese rose are arranged.Flos Rosae Rugosae sweet in the mouth, little hardship, warm in nature, the function that liver-smoothing, qi-regulating, regulating menstruation by adjusting the flow of blood are arranged, can be used for treating stomachache due to hyperactive liver-QI attacking the stomach, lack of appetite vomiting and nausea, menoxenia, fall and pounce on the pain of injury, its root has the effect with blood, regulating menstruation, leukorrhagia stopping, cures mainly menoxenia, leukorrhagia, traumatic injury, rheumatic arthralgia.In recent years, both at home and abroad the Flos Rosae Rugosae effective ingredient is studied, find to contain multiple nutritional components such as polyphenol, flavone, 18 seed amino acids (comprising 8 seed amino acids that human body is necessary) and vitamin C in the Flos Rosae Rugosae, pharmacological research shows the effect that it has stronger antioxidation, removes free radical simultaneously.

It is the cosmetics of raw material production with the Bulgarian Rose that many moneys are arranged in the market, but the Rose grievances few people shows any interest of one of main rose variety of conduct China plantation.Rose grievances (Rosa stertata * Rosa rugosa Yuet Ku) is the Hybrid of Chinese Flos Rosae Rugosae and cognate Flos Rosae Multiflorae, and the cultivation history in more than 200 year is arranged, and mainly cultivates in Yongdeng County, Gansu misery area because of it and gains the name.Annual late May blooms, and about about 25 days of florescence was the representative of Luzhou-flavor Flos Rosae Rugosae.Though both at home and abroad Rose grievances is possessed some special knowledge in recent years, degree of depth deficiency, also unmanned at present the concern with the Rose grievances is the cosmetics research and development of raw material.

Summary of the invention

Technical problem to be solved by this invention provides the cosmetics that contain the Rose grievances extract of a kind of Pear Power, crease-resistant, delaying decrepitude of skin and moisture-keeping efficacy.

Another technical problem to be solved by this invention provides a kind of preparation method that contains the cosmetics of Rose grievances extract.

For addressing the above problem, a kind of cosmetics that contain the Rose grievances extract of the present invention, it is characterized in that: these cosmetics comprise the mixture, 10～12% polyoxyethylenated alcohol sodium sulfate (AES), 0.8～1.3% Magnesiumaluminumsilicate of the Rose grievances extract that accounts for gross weight 35～45% and NaCl, 0.9～1.2% HANSHENGJIAO, 10～15% Rose grievances pollen, and its surplus is a deionized water.

These cosmetics also comprise 0.1～0.3% the poly-aminopropyl acid guanidine that accounts for gross weight, 0.5～5% citric acid.

The mixture of described Rose grievances extract and NaCl is meant the sea salt of the quality adding 20% that will press flower behind the roguing of cup-shaped Rose grievances flower, the calyx of deflorating respectively and 2～4 times water, after reflux, extract,, filtration, get supernatant, the product of gained behind the concentrated supernatant (wherein Rose grievances extract content is 8～15%, and NaCl content is 85～92%).

The mass concentration of described AES is 70%.

Described Rose grievances pollen is meant the sea salt of the quality adding 20% that will press flower behind the roguing of cup-shaped Rose grievances flower, the calyx of deflorating respectively and 2～4 times water, the product of gained behind the colored slag drying after reflux, extract,, the filtration, pulverizing, mistake 40 mesh sieves.

A kind ofly prepare the aforesaid method that contains the cosmetics of Rose grievances extract, it may further comprise the steps:

(1) by each raw material of proportioning weighing;

(2) AES, HANSHENGJIAO are put into deionized water, the heating for dissolving postcooling obtains lysate to room temperature;

(3) add other raw material respectively in lysate, stirring gets final product.

The present invention compared with prior art has the following advantages:

1, the present invention is transparent uniform liquid, and is free from foreign meter, detects the requirement (referring to table 1) that meets sense organ, physics and chemistry and microbiological indicator by QB1994-2004 " People's Republic of China's light industry industry standard---bath shampoo ".

Table 1: the every index testing result of the present invention

Project	Testing result
		Outward appearance	Color and luster is even, does not have obvious impurity and stain
Abnormal smells from the patient	The Rose grievances odor type
		Gross activity thing (%)	??14-18
??PH(25℃)	??4.8-5.7
		Arsenic (in As)/(mg/kg)	Do not have
Heavy metal (in Pb)	Do not have
		Hydrargyrum (in Hg)/(mg/kg)	Do not have

2, because the present invention has adopted stable performance, be rich in the additive (referring to table 2, table 3) of the Rose grievances extract of nutritional labelings such as multivitamin, aminoacid, flavone as cosmetics, thus the present invention to the nourishing and moisturizing of human skin, promote skin metabolism, softening skin, inhibition pigmentation and defying age aspect to have remarkable result.

Table 2: nutritional labeling analysis result in the Rose grievances extract

Protein	Crude fat	Total sugar	Vitamin C	Total flavones
					??11.80％	??12.70％	??19.30％	??444.65mg/100g	??2.99％

Table 4: amino acid analysis result in the Rose grievances extract

Aminoacid	Content (%)
		Aspartic Acid	??0.55
Threonine	??1.7
		Serine	??0.6
Glutamic acid	??1.3
		Proline	??1.15
Glycine	??0.07
		Alanine	??0.47
Valine	??0.27
		Methionine	??0.06
Isoleucine	??0.135
		Leucine	??0.14
Tyrosine	??0.065
		Phenylalanine	??0.205
Lysine	??0.21
		Histidine	??0.07
Arginine	??0.065
		Cystine	??0.07
Total amount	??7.2

3, the present invention and the common commercially available cosmetics that do not contain Rose grievances extract and Rose grievances wax are compared experiment, the result shows that the present invention has tangible skin care effect.

Select 50 routine experimenters, its left hand back of the body smear the present invention clean the back with clear water clean, the right hand back of the body smears cleaning back, commercially available prod and cleans with clear water, every day 1 time, after 30 days, it is obviously comparatively pale than right hand butt skin softness, lubricious, exquisiteness and the colour of skin to observe experimenter's left hand butt skin, and skin elasticity and vigor obviously increase.

4, raw material of the present invention is easy to get, and technology is simple, is easy to suitability for industrialized production.

The specific embodiment

Reagent: mass concentration is that 70% AES, Magnesiumaluminumsilicate, poly-aminopropyl acid guanidine are U.S.'s Qi Chemical Manufacture difficult to understand; HANSHENGJIAO is that Zibo is along reaching bio tech ltd production; Citric acid is the production of neat safe chemical industry company limited.Mentioned reagent is cosmetics-stage.

1 one kinds of cosmetics that contain the Rose grievances extract of embodiment, contain the Rose grievances extract of gross weight 35% and the mixture of NaCl, 10% AES, 0.8% Magnesiumaluminumsilicate, 0.9% HANSHENGJIAO, 10% Rose grievances pollen, its surplus is a deionized water.

Wherein: the mixture of Rose grievances extract and NaCl is meant and will puts into the round-bottomed flask of 5000ml behind the roguing of cup-shaped Rose grievances flower, the calyx of deflorating, the quality of pressing flower respectively adds 20% sea salt and 2～4 times water, connect condensing tube, use water condensation, electricity consumption hot tap heating round-bottomed flask extracts liquid return and got extracting solution in 3～4 hours, obtains crude extract with filtered through gauze; Get supernatant after crude extract filtered with buchner funnel, the R206D type Rotary Evaporators distilling under reduced pressure of adopting Shensheng Science ﹠ Tech. Co., Ltd., Shanghai to produce, be concentrated into pasty state, the desk-top air dry oven of producing with Yongxing drying equipment factory of 9023A type is dried promptly down at 95～105 ℃ at last.

Also can before reflux, extract,, handle with the ultrasonic cell disruption instrument assisted extraction earlier.

Rose grievances pollen is meant to be pulverized the colored slag after filtering after drying down at 95～105 ℃ with the desk-top air dry oven of 9023A type in the mixture process of extracting Rose grievances extract and NaCl, and the product of gained behind 40 mesh sieves.

A kind of preparation contains the method for the cosmetics of Rose grievances extract, and it may further comprise the steps:

(1) by each raw material of proportioning weighing;

(2) AES, HANSHENGJIAO are added in the deionized water, heating in water bath in the HS6-A electric-heated thermostatic water bath that 40～60 ℃ of Huangshi medical apparatus and instruments factories produce, dissolving back postcooling obtains lysate to room temperature fully;

(3) add other raw material respectively in lysate, the speed with 3000 rev/mins in the accurate motor stirrer of JJ-1 that Hua Cheng Katyuan experimental apparatus factory produces stirs 15min, and it is evenly got final product.

2 one kinds of cosmetics that contain the Rose grievances extract of embodiment contain 38% Rose grievances extract and the mixture of NaCl, 11% AES, 0.9% Magnesiumaluminumsilicate, 1.0% HANSHENGJIAO, 12% Rose grievances pollen, and its surplus is a deionized water.

Other is with embodiment 1.

3 one kinds of cosmetics that contain the Rose grievances extract of embodiment contain 42% Rose grievances extract and the mixture of NaCl, 12% AES, 1.1% Magnesiumaluminumsilicate, 1.1% HANSHENGJIAO, 13% Rose grievances pollen, and its surplus is a deionized water.

Other is with embodiment 1.

4 one kinds of cosmetics that contain the Rose grievances extract of embodiment contain 45% Rose grievances extract and the mixture of NaCl, 12% AES, 1.3% Magnesiumaluminumsilicate, 1.2% HANSHENGJIAO, 15% Rose grievances pollen, and its surplus is a deionized water.

Other is with embodiment 1.

5 one kinds of cosmetics that contain the Rose grievances extract of embodiment, contain mixture, 12% AES, 1.3% Magnesiumaluminumsilicate, 1.2% HANSHENGJIAO, the 15% Rose grievances pollen of 45% Rose grievances extract and NaCl, 0.1% poly-aminopropyl acid guanidine, 0.5% citric acid, its surplus is a deionized water.

Other is with embodiment 1.

6 one kinds of cosmetics that contain the Rose grievances extract of embodiment, contain mixture, 12% AES, 1.3% Magnesiumaluminumsilicate, 1.2% HANSHENGJIAO, the 15% Rose grievances pollen of 45% Rose grievances extract and NaCl, 0.2% poly-aminopropyl acid guanidine, 3% citric acid, its surplus is a deionized water.

Other is with embodiment 1.

7 one kinds of cosmetics that contain the Rose grievances extract of embodiment, contain mixture, 12% AES, 1.3% Magnesiumaluminumsilicate, 1.2% HANSHENGJIAO, the 15% Rose grievances pollen of 45% Rose grievances extract and NaCl, 0.3% poly-aminopropyl acid guanidine, 5% citric acid, its surplus is a deionized water.

Other is with embodiment 1.

Claims (6)

1. cosmetics that contain the Rose grievances extract, it is characterized in that: these cosmetics comprise the mixture, 10～12% polyoxyethylenated alcohol sodium sulfate, 0.8～1.3% Magnesiumaluminumsilicate of the Rose grievances extract that accounts for gross weight 35～45% and NaCl, 0.9～1.2% HANSHENGJIAO, 10～15% Rose grievances pollen, and its surplus is a deionized water.

2. a kind of cosmetics that contain the Rose grievances extract as claimed in claim 1 is characterized in that: these cosmetics also comprise 0.1～0.3% the poly-aminopropyl acid guanidine that accounts for gross weight, 0.5～5% citric acid.

3. a kind of cosmetics that contain the Rose grievances extract as claimed in claim 1, it is characterized in that: the mixture of described Rose grievances extract and NaCl is meant the sea salt of the quality adding 20% that will press flower behind the roguing of cup-shaped Rose grievances flower, the calyx of deflorating respectively and 2～4 times water, after reflux, extract,, filtration, get supernatant, the product of gained behind the concentrated supernatant.

4. a kind of cosmetics that contain the Rose grievances extract as claimed in claim 1 is characterized in that: the mass concentration of described polyoxyethylenated alcohol sodium sulfate is 70%.

5. a kind of cosmetics that contain the Rose grievances extract as claimed in claim 1, it is characterized in that: described Rose grievances pollen is meant the sea salt of the quality adding 20% that will press flower behind the roguing of cup-shaped Rose grievances flower, the calyx of deflorating respectively and 2～4 times water, the product of gained behind the colored slag drying after reflux, extract,, the filtration, pulverizing, mistake 40 mesh sieves.

6. one kind prepares the method that contains the cosmetics of Rose grievances extract as claimed in claim 1 or 2, and it may further comprise the steps:

(1) by each raw material of proportioning weighing;

(2) polyoxyethylenated alcohol sodium sulfate, HANSHENGJIAO are put into deionized water, the heating for dissolving postcooling obtains lysate to room temperature;

(3) add other raw material respectively in lysate, stirring gets final product.