CN113842338B

CN113842338B - Camellia oil skin-moistening oil and preparation method thereof

Info

Publication number: CN113842338B
Application number: CN202111168653.7A
Authority: CN
Inventors: 杨光永; 李祎洁; 田容华; 廖慧慧
Original assignee: Hunan Qinxiang Jiuzhou Biotechnology Co ltd
Current assignee: Hunan Qinxiang Jiuzhou Biotechnology Co ltd
Priority date: 2021-10-08
Filing date: 2021-10-08
Publication date: 2023-08-29
Anticipated expiration: 2041-10-08
Also published as: CN113842338A

Abstract

The invention discloses camellia oil skin-moistening oil and a preparation method thereof, and relates to the technical field of camellia oil skin-moistening oil. The camellia oil skin-moistening oil provided by the invention has faint fragrance and long duration when being rubbed on skin, and the stimulation component in the skin-moistening oil is neutralized, so that the softness of the skin-moistening oil is improved, and the camellia oil skin-moistening oil is suitable for common skin and sensitive skin, and the sensitive skin is rubbed and feels fresh and has no uncomfortable feeling.

Description

Camellia oil skin-moistening oil and preparation method thereof

Technical Field

The invention relates to the technical field of camellia oil skin-moistening oil, in particular to camellia oil skin-moistening oil and a preparation method thereof.

Background

The camellia oil is extracted from camellia seed and is produced by peeling, drying, crushing, boiling, extracting oil and filtering. The tea oil contains no mustard and cholesterol. Experiments show that the content of unsaturated fatty acid in the tea oil is more than 90%, the content of fatty acid is between 80 and 83%, and the content of linolenic acid is between 7 and 13%, especially the rich linolenic acid is necessary for human body and can not be synthesized.

The composition of unsaturated fatty acids in camellia oil is similar to human milk. The linoleic acid and linolenic acid contents are approximately the same as human milk. Is easily absorbed by skin, and can form hydrophobic film on skin surface. It not only can bring softness, lubrication and luster to the skin, but also can effectively inhibit the evaporation of water, prevent the skin from drying, make the dried skin and the hardened cutin layer re-hydrolyze, restore the softness and elasticity of the cutin layer and make the skin soft and smooth, and protect the skin health. Camellia oil also contains natural vitamin E and squalene. Moreover, it has good antioxidant and radical javelin capabilities; at the same time, it is also an antioxidant and membrane stabilizer for the weight of cell membranes. The fatty acid profile of camellia oil is close to that of human skin. Moreover, that is easily absorbed by the skin and has no greasy feel. In addition, the camellia oil is also rich in bactericidal and anti-pyogenic components such as tea polyphenol and tea saponin. Therefore, camellia oil can be used as a raw material for developing excellent cosmetics.

The camellia skin-moistening oil disclosed in the publication No. CN104434643A and a preparation method thereof are characterized in that camellia oil is mixed with C12-15-alkyl benzoate and cyclomethicone in a formula amount, uniformly stirred at normal temperature, then vitamin, isopropyl myristate and essential oil are sequentially added, and continuously and uniformly stirred at normal temperature to obtain the camellia skin-moistening oil, wherein the camellia skin-moistening oil contains natural unsaturated oleic acid, vitamin and other nutrient substances and mineral elements of the camellia oil, and also contains tea polyphenol, tea saponin and other bactericidal and antipruritic components; the skin care cream is capable of nourishing and caring skin, resisting aging, preventing oxidation, being safe and free of stimulation, and being suitable for all dry skin, while moistening and preserving the skin. Most importantly, the preparation process is safe, simple and convenient to operate, and is easy for industrial production.

The camellia oil skin-moistening oil produced by the invention is characterized in that the fragrance is carried by raw materials, the fragrance can be gradually covered in the process of manufacturing, the fragrance lasting capability is not strong enough, and most of sensitive skin is sensitive to camellia oil and additives, and the camellia oil skin-moistening oil cannot be used, so that the user is damaged.

Disclosure of Invention

The invention mainly aims to provide camellia oil skin-moistening oil and a preparation method thereof, which can effectively solve the problems that the fragrance is carried by raw materials in the background art, the fragrance can be gradually covered in the process of preparation, the lasting capability of the fragrance is not strong enough, and most of sensitive skin is sensitive to camellia oil and additives, and the camellia oil skin-moistening oil cannot be used, so that the user is damaged.

In order to achieve the above purpose, the technical scheme adopted by the invention is as follows:

a camellia oil skin-moistening oil, which consists of the following components:

flavoring agent: 30-80% of alcohol, 10-50% of deionized water, 1-5% of fruit extract, 1.5% of essence, 3% of musk, 1.5% of benzyl salicylate, 3% of isopropyl myristate and 1.5% of tea extract;

mild liquid: the preparation method comprises the steps of taking albizia flower extract as a main raw material, and taking water-soluble pearl and seaweed extract as auxiliary materials;

camellia skin-moistening oil primary liquid: 20 parts of camellia oil, 8 parts of caprylic capric triglyceride, 1 part of palmitic acid, 1.5 parts of cetostearyl alcohol, 2 parts of vitamin and 2 parts of essential oil.

A preparation method of camellia oil skin-moistening oil comprises the following steps:

s1, preparing a flavoring agent:

the flavoring agent is prepared from (by weight) ethanol 30-80%, deionized water 10-50%, fruit extract 1-5%, essence 1.5%, moschus 3%, benzyl salicylate 1.5%, isopropyl myristate 3%, and tea extract 1.5% prepared by fermenting semen Maydis as main material;

s2, preparing a mild solution:

the mild liquid is prepared from the following raw materials, namely albizia flower extract serving as a main raw material and water-soluble pearl and seaweed extract serving as auxiliary materials, wherein the mass ratio of the albizia flower extract is as follows: water-soluble pearl: the seaweed extract is 4-6:1-3:2-4, mixing and stirring the raw materials, wherein the stirring temperature is 80 ℃, the stirring time is 2 hours, preserving the heat for 40 minutes after stirring is finished, and cooling to 20 ℃ to obtain a finished product mild liquid;

s3, preparing camellia skin-moistening oil primary liquid:

20 parts of camellia oil, 8 parts of caprylic/capric triglyceride, 1 part of palmitic acid, 1.5 parts of cetostearyl alcohol, 2 parts of vitamin and 2 parts of essential oil are prepared, wherein the weight ratio is 20:8:1:1.5:2:2, adding camellia oil into a stirring container, sequentially adding caprylic capric triglyceride, palmitic acid and cetylstearyl alcohol for 20min, adding vitamin and essential oil for 10min, stirring at 70 ℃ until the camellia oil is dissolved, and obtaining camellia skin-moistening oil primary liquid;

s4, preparing camellia skin-moistening oil:

and sequentially adding the obtained flavoring agent and the mild liquid into the camellia skin-moistening oil primary liquid at a time interval of 1h, and stirring until the flavoring agent and the mild liquid are dissolved in the camellia skin-moistening oil primary liquid to obtain the camellia skin-moistening oil.

The preparation of the flavoring agent in the step S1 comprises the following steps:

s1, adding alcohol obtained by fermenting and deodorizing corn into a reactor, adding musk and benzyl salicylate into a container, stirring and dissolving, and standing at 5 ℃ in a dark place for at least one week;

s2, adding deionized water, fruit extract, tea extract, essence and isopropyl myristate into the solution, stirring and mixing for 3-5 hours at the temperature of minus 10 ℃ and then filtering;

s3, filtering the filtered solution for Chen Hua-30 days at the temperature of 0-20 ℃ in an aging period, and finally filtering and packing the Chen Hua product.

The vitamin is one of D-vitamin E, vitamin E and acetate.

The essential oil is at least one of tangerine essential oil, cypress essential oil, herba Rosmarini officinalis essential oil and myrrh essential oil. Watermelon extract, pomegranate extract, melon extract.

The S4 mountain tea skin-moistening oil primary liquid, the flavoring agent and the mild liquid are in the following proportion: the stirring time is 10h, the stirring temperature is 70 ℃, the stirring and dissolving completion phenomenon is that the liquid is clear, and no obvious precipitate exists after the liquid is left stand for 1 h.

The mild liquid is prepared from the following seaweed extract 5 in percentage by mass: 2:3, comprising the following steps:

s1, crushing coarse materials in the albizia flower extract, soaking, refluxing and extracting with refined oil, and concentrating to obtain albizia flower powder;

s2, crushing the fine materials in the water-soluble pearls to obtain fine powder;

and S3, heating the seaweed extract in a container at 110 ℃, adding the albizia flower powder, continuing heating and stirring until the water vapor in the mixture is reduced to below 2%, stopping heating, finally adding the refined powder, stirring uniformly, placing on a filter cloth, filtering, and obtaining the mild liquid after filtering.

The camellia oil is pressed camellia oil.

Albizia is also called as cotton tree, and lantana flower. Deciduous arbor, summer flower, head inflorescence, valve corolla, stamen, and reddish. The pods were streaked, flat, and not cracked. 4-15 meters high. Developing tree crowns; the small branches have edges and corners, and the tender branches, inflorescences and leaf shafts are fluffed or short and soft. The supporting leaf is in a linear shape and is in a needle shape; the head inflorescences are arranged on the top of the branch to form cone inflorescences; pollen red; calyx tube shape, and flowering period of 6-7 months; the fruit period is 8-10 months.

The comparison experiment of the water-soluble pearl powder and the common pearl powder shows that: the solubility is more than 2000 times, the absorptivity is more than 20 times, meanwhile, the content of the effective components of the water-soluble pearl powder is more abundant, and the trace elements of calcium and protein are hydrolyzed and then measured to contain aspartic acid, threonine, isoleucine, leucine, serine, tyrosine, glutamic acid, phenylalanine and glycine; used in health food, functional beverage, water, and cosmetics; pearl is a medicine and food homologous product in the past, and is worn by the old and the middle-aged people due to its unique effect.

Algae, which are algae grown in the sea, are cryptogamic plants of the plant kingdom, and include several different species of organisms that produce energy by photosynthesis. They are generally considered simple plants and are mainly characterized by: no vascular bundle tissue and no differentiation phenomenon of true positive roots, stems and leaves; no flowering, no fruit or seed; the reproductive organs are not specialized protective tissues, often producing spores or gametes directly from a single cell; and no embryo formation.

Compared with the prior art, the invention has the following beneficial effects:

the camellia emollient oil is prepared by adding a flavoring agent into camellia emollient oil, wherein the flavoring agent is prepared from alcohol, deionized water, a fruit extract, essence, musk, benzyl salicylate and isopropyl myristate which are prepared by fermenting and deodorizing corn as a main raw material, so that fragrance is faint and lasting when the emollient oil is rubbed on skin, and a mild liquid is added into the camellia emollient oil, wherein the mild liquid is prepared from albizia flower extract as a main raw material and water-soluble pearl and seaweed extract as auxiliary materials, so that the stimulating components in the emollient oil are neutralized, the softness of the emollient oil is improved, the emollient oil is suitable for ordinary skin and sensitive skin, and the sensitive skin is rubbed to feel fresh and uncomfortable.

Drawings

In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings that are needed for the description of the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and that other drawings may be obtained according to these drawings without inventive effort for a person skilled in the art.

FIG. 1 is a flow chart of a camellia oil emollient oil and a preparation method thereof;

Detailed Description

The invention is further described in connection with the following detailed description, in order to make the technical means, the creation characteristics, the achievement of the purpose and the effect of the invention easy to understand.

In the description of the present invention, it should be noted that the directions or positional relationships indicated by the terms "upper", "lower", "inner", "outer", "front", "rear", "both ends", "one end", "the other end", etc. are based on the directions or positional relationships shown in the drawings, are merely for convenience of describing the present invention and simplifying the description, and do not indicate or imply that the devices or elements referred to must have a specific direction, be configured and operated in the specific direction, and thus should not be construed as limiting the present invention. Furthermore, the terms "first," "second," and the like, are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.

In the description of the present invention, it should be noted that, unless explicitly specified and limited otherwise, the terms "mounted," "provided," "connected," and the like are to be construed broadly, and may be fixedly connected, detachably connected, or integrally connected, for example; can be mechanically or electrically connected; can be directly connected or indirectly connected through an intermediate medium, and can be communication between two elements. The specific meaning of the above terms in the present invention will be understood in specific cases by those of ordinary skill in the art.

The present invention will be described more specifically below based on examples and comparative examples. It should be noted that these examples do not limit the scope of the present invention.

Example 1

The camellia oil skin-moistening oil comprises the following raw materials in parts by weight per 100 ml: the proportion of the camellia skin-moistening oil primary liquid, the flavoring agent and the mild liquid is as follows: 10:2:1;

the preparation method comprises the following steps:

s1, preparing a flavoring agent:

the flavoring agent is prepared from (by weight) ethanol 50%, deionized water 35%, fruit extract 3.5%, essence 1.5%, moschus 3%, benzyl salicylate 1.5%, isopropyl myristate 3%, and tea extract 1.5% prepared by fermenting semen Maydis as main material;

s2, preparing a mild solution:

the mild liquid is prepared from the following raw materials, namely albizia flower extract serving as a main raw material and water-soluble pearl and seaweed extract serving as auxiliary materials, wherein the mass ratio of the albizia flower extract is as follows: water-soluble pearl: the seaweed extract was 5:2:3, mixing and stirring the raw materials, wherein the stirring temperature is 80 ℃, the stirring time is 2 hours, preserving the heat for 40 minutes after stirring is finished, and cooling to 20 ℃ to obtain a finished product mild liquid;

s3, preparing camellia skin-moistening oil primary liquid:

s4, preparing camellia skin-moistening oil:

The preparation of the flavoring agent in S1 comprises the following steps:

s2, adding deionized water, fruit extract, tea extract, essence and isopropyl myristate into the solution, stirring and mixing for 4 hours at the temperature of minus 10 ℃ and then filtering;

and S3, filtering the filtered solution for Chen Hua days at the temperature of 15 ℃ in an ageing period, and finally filtering and packing the Chen Hua product.

The vitamin is one of D-vitamin E, vitamin E and acetate.

The essential oil is at least one of tangerine essential oil, cypress essential oil, herba Rosmarini officinalis essential oil and myrrh essential oil.

Watermelon extract, pomegranate extract, melon extract.

S4, the proportion of the mountain tea skin-moistening oil primary liquid, the flavoring agent and the mild liquid is as follows: the stirring time is 10h, the stirring temperature is 70 ℃, the stirring and dissolving completion phenomenon is that the liquid is clear, and no obvious precipitate exists after the liquid is left stand for 1 h.

The preparation of the mild liquid comprises the following steps of: 2:3, comprising the following steps:

and S3, heating the seaweed extract in a container at 110 ℃, adding the albizia flower powder, continuously heating and stirring until the water vapor in the mixture is reduced to below 2%, stopping heating, finally adding the refined powder, uniformly stirring, placing the mixture on a filter cloth, filtering, and obtaining the mild liquid after filtering.

The oleum Camelliae Japonicae is squeezed oleum Camelliae Japonicae.

The containing bottle is a plastic bottle or an organic glass reagent bottle, and potassium hydrogen phthalate is used as a reference reagent.

Example 2

Example 2 differs from example 1 in that S1: 30% of alcohol, 50% of deionized water and 5% of fruit extract.

The procedure is as in example 1.

Example 3

Example 3 differs from example 1 in that S1: 80% of alcohol, 10% of deionized water and 1% of fruit extract.

The procedure is as in example 1.

Example 4

Example 4 differs from example 1 in that S2: the mass ratio of the albizia flower extract is as follows: water-soluble pearl: the seaweed extract was 4:1:2.

the procedure is as in example 1.

Example 5

Example 5 differs from example 1 in that S2: the mass ratio of the albizia flower extract is as follows: water-soluble pearl: the seaweed extract was 5:1:2.

the procedure is as in example 1.

Example 6

Example 5 differs from example 1 in that S2: the mass ratio of the albizia flower extract is as follows: water-soluble pearl: the seaweed extract was 6:3:4.

the procedure is as in example 1.

Comparative example 1

Comparative example 1 differs from example 1 in that no flavoring agent was added during the preparation of the camellia emollient oil, and an equal amount of camellia emollient oil primary liquid was added.

The procedure is as in example 1.

Comparative example 2

Comparative example 2 differs from example 1 in that no mild liquid was added and an equal amount of camellia emollient oil primary liquid was added when camellia emollient oil was prepared.

The procedure is as in example 1.

Performance comparison of examples and comparative examples:

table 1 shows the free acid content of the fluorogypsum with a known content of 0.54% determined by the method described in the examples and comparative examples:

as can be seen from the results shown in table 1 above, the camellia emollient oils prepared in examples 1 to 6 were compared with comparative example 1 according to the method of the present invention, the camellia emollient oils prepared in examples 1 to 6 were 5 hours in flavor duration, and the camellia emollient oils prepared in comparative example 1 were 1 hour in flavor duration, the camellia emollient oils prepared in examples 1 to 6 were compared with comparative example 2 in flavor duration, the camellia emollient oils prepared in examples 1 to 6 were free from uncomfortable feeling on sensitive skin, and the camellia emollient oils prepared in comparative example 2 were strong in uncomfortable feeling on sensitive skin, so the effects of examples were excellent, the flavor duration of example 1 was the longest and no uncomfortable feeling on sensitive skin was obtained during the mutual comparison of examples, and the effects of example 1 were better.

The foregoing has shown and described the basic principles and main features of the present invention and the advantages of the present invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and that the above embodiments and descriptions are merely illustrative of the principles of the present invention, and various changes and modifications may be made without departing from the spirit and scope of the invention, which is defined in the appended claims. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims

1. A camellia oil skin-moistening oil is characterized in that: the camellia skin-moistening oil consists of the following components:

mild liquid: the preparation method comprises the steps of taking the albizia flower extract as a main raw material, taking the water-soluble pearl and seaweed extract as auxiliary materials, wherein the mild liquid is prepared from the following albizia flower extract in percentage by mass: water-soluble pearl: the seaweed extract is 4-6:1-3:2-4;

camellia skin-moistening oil primary liquid: 20 parts of camellia oil, 8 parts of caprylic capric triglyceride, 1 part of palmitic acid, 1.5 parts of cetostearyl alcohol, 2 parts of vitamins and 2 parts of essential oil;

the camellia skin-moistening oil primary liquid, the flavoring agent and the mild liquid are in the following proportion: 10:2:1.

2. A preparation method of camellia oil skin-moistening oil is characterized by comprising the following steps: the method comprises the following steps:

s1, preparing a flavoring agent:

s2, preparing a mild solution:

the mild liquid is prepared from the following raw materials, namely albizia flower extract serving as a main raw material and water-soluble pearl and seaweed extract serving as auxiliary materials, wherein the mass ratio of the albizia flower extract is as follows: water-soluble pearl: the seaweed extract is 4-6:1-3:2-4, mixing and stirring the raw materials at 80 ℃ for 2 hours, preserving heat for 40 minutes after stirring, and cooling to 20 ℃ to obtain a finished product mild liquid;

s3, preparing camellia skin-moistening oil primary liquid:

20 parts of camellia oil, 8 parts of caprylic/capric triglyceride, 1 part of palmitic acid, 1.5 parts of cetostearyl alcohol, 2 parts of vitamin and 2 parts of essential oil, wherein the weight ratio of the camellia oil to the caprylic/capric triglyceride is 20:8:1:1.5:2:2, mixing Camellia japonica

Adding oil into stirring container, sequentially adding caprylic capric triglyceride, palmitic acid and cetostearyl alcohol for 20min, adding vitamins and essential oil for 10min, stirring at 70deg.C, and stirring to dissolve to obtain primary solution of camellia skin caring oil;

s4, preparing camellia skin-moistening oil:

3. The method for preparing camellia oil skin-moistening oil according to claim 2, which is characterized in that: the preparation of the flavoring agent in the step S1 comprises the following steps:

s1-1, adding alcohol obtained by fermenting and deodorizing corn into a reactor, adding musk and benzyl salicylate into a container, stirring and dissolving, and standing at 5 ℃ in a dark place for at least one week;

s1-2, adding deionized water, fruit extract, tea extract, essence and isopropyl myristate into the solution, stirring and mixing for 3-5 hours at the temperature of minus 10 ℃, and filtering;

s1-3, aging the filtered solution at the temperature of 0-20 ℃ for 20-30 days, and finally filtering and packing the aged product.

4. The method for preparing camellia oil skin-moistening oil according to claim 2, which is characterized in that: the vitamin is one of D-vitamin E, vitamin E and vitamin E acetate.

5. The method for preparing camellia oil skin-moistening oil according to claim 2, which is characterized in that: the essential oil is at least one of tangerine essential oil, cypress essential oil, herba Rosmarini officinalis essential oil and myrrh essential oil.

6. The method for preparing camellia oil skin-moistening oil according to claim 2, which is characterized in that: the fruit extract comprises at least one of watermelon extract, pomegranate extract and melon extract.

7. The method for preparing camellia oil skin-moistening oil according to claim 2, which is characterized in that:

the stirring time in the step S4 is 10 hours, the stirring temperature is 70 ℃, the phenomenon that stirring and dissolution are completed is that liquid is clear, and no obvious precipitate exists after the liquid is left stand for 1 hour.

8. A method for preparing camellia oil emollient oil according to claim 5, characterized in that: the preparation of the mild liquid comprises the following steps:

s2-1, crushing coarse materials in the albizia flower extract, soaking and reflux-extracting with refined oil, and concentrating to obtain albizia flower powder;

s2-2, crushing the fine materials in the water-soluble pearls to obtain fine powder;

s2-3, heating the seaweed extract in a container at 110 ℃, adding the albizia flower powder, continuously heating and stirring until the water vapor in the mixture is reduced to below 2%, stopping heating, finally adding the refined powder, uniformly stirring, filtering on a filter cloth, and obtaining the mild liquid after filtering.

9. A method for preparing camellia oil emollient oil according to claim 5, characterized in that: the camellia oil is pressed camellia oil.