CN101701138A - Cohesive glue for flexible decorative tile and manufacturing method thereof - Google Patents
Cohesive glue for flexible decorative tile and manufacturing method thereof Download PDFInfo
- Publication number
- CN101701138A CN101701138A CN200910230639A CN200910230639A CN101701138A CN 101701138 A CN101701138 A CN 101701138A CN 200910230639 A CN200910230639 A CN 200910230639A CN 200910230639 A CN200910230639 A CN 200910230639A CN 101701138 A CN101701138 A CN 101701138A
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- CN
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- Prior art keywords
- water
- percent
- glue
- flexible decorative
- decorative tile
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003292 glue Substances 0.000 title claims abstract description 41
- 238000004519 manufacturing process Methods 0.000 title claims abstract 4
- 239000007788 liquid Substances 0.000 claims abstract description 30
- 230000008719 thickening Effects 0.000 claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229920000642 polymer Polymers 0.000 claims abstract description 11
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 7
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 7
- 239000004816 latex Substances 0.000 claims abstract description 6
- 229920000126 latex Polymers 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims description 22
- 239000000839 emulsion Substances 0.000 claims description 17
- 230000004048 modification Effects 0.000 claims description 13
- 238000012986 modification Methods 0.000 claims description 13
- 239000000126 substance Substances 0.000 claims description 13
- 239000003112 inhibitor Substances 0.000 claims description 10
- 230000003647 oxidation Effects 0.000 claims description 10
- 238000007254 oxidation reaction Methods 0.000 claims description 10
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 9
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 9
- 239000006096 absorbing agent Substances 0.000 claims description 9
- 238000004581 coalescence Methods 0.000 claims description 9
- ZRALSGWEFCBTJO-UHFFFAOYSA-N Guanidine Chemical compound NC(N)=N ZRALSGWEFCBTJO-UHFFFAOYSA-N 0.000 claims description 6
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 4
- DAFHKNAQFPVRKR-UHFFFAOYSA-N (3-hydroxy-2,2,4-trimethylpentyl) 2-methylpropanoate Chemical compound CC(C)C(O)C(C)(C)COC(=O)C(C)C DAFHKNAQFPVRKR-UHFFFAOYSA-N 0.000 claims description 3
- 229920002153 Hydroxypropyl cellulose Polymers 0.000 claims description 3
- CHJJGSNFBQVOTG-UHFFFAOYSA-N N-methyl-guanidine Natural products CNC(N)=N CHJJGSNFBQVOTG-UHFFFAOYSA-N 0.000 claims description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 3
- 239000002131 composite material Substances 0.000 claims description 3
- SWSQBOPZIKWTGO-UHFFFAOYSA-N dimethylaminoamidine Natural products CN(C)C(N)=N SWSQBOPZIKWTGO-UHFFFAOYSA-N 0.000 claims description 3
- 239000001863 hydroxypropyl cellulose Substances 0.000 claims description 3
- 235000010977 hydroxypropyl cellulose Nutrition 0.000 claims description 3
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 3
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 3
- -1 lauryl alcohol ester Chemical class 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 229920000609 methyl cellulose Polymers 0.000 claims description 3
- 239000001923 methylcellulose Substances 0.000 claims description 3
- KGRVJHAUYBGFFP-UHFFFAOYSA-N 2,2'-Methylenebis(4-methyl-6-tert-butylphenol) Chemical compound CC(C)(C)C1=CC(C)=CC(CC=2C(=C(C=C(C)C=2)C(C)(C)C)O)=C1O KGRVJHAUYBGFFP-UHFFFAOYSA-N 0.000 claims description 2
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 claims description 2
- MCPKSFINULVDNX-UHFFFAOYSA-N drometrizole Chemical compound CC1=CC=C(O)C(N2N=C3C=CC=CC3=N2)=C1 MCPKSFINULVDNX-UHFFFAOYSA-N 0.000 claims description 2
- 238000010276 construction Methods 0.000 abstract description 3
- 239000000654 additive Substances 0.000 abstract 2
- 239000002562 thickening agent Substances 0.000 abstract 2
- 239000006097 ultraviolet radiation absorber Substances 0.000 abstract 2
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 238000005303 weighing Methods 0.000 description 18
- 239000012467 final product Substances 0.000 description 15
- 238000003756 stirring Methods 0.000 description 15
- 239000011449 brick Substances 0.000 description 8
- 239000000853 adhesive Substances 0.000 description 4
- 230000001070 adhesive effect Effects 0.000 description 4
- 238000012856 packing Methods 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 238000006073 displacement reaction Methods 0.000 description 3
- 231100000252 nontoxic Toxicity 0.000 description 3
- 230000003000 nontoxic effect Effects 0.000 description 3
- 230000009967 tasteless effect Effects 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000004567 concrete Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000012774 insulation material Substances 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 239000011433 polymer cement mortar Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
Landscapes
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention relates to cohesive glue for a flexible decorative tile and a manufacturing method thereof; the cohesive glue is composed of the following raw materials by weight proportion: 0.3-1.5 percent of water-retaining agents, 28-48 percent of water, 0.3-2 percent of thickeners, 48-68 percent of polymer latex, 0-0.35 percent of ultra-violet absorber, 0-0.42 percent of antioxidant, and 0.7-4.2 percent of film-forming additives; the manufacturing method is that: 1-3 percent of the water-retaining agents, 93-97 percent of water and 1-4 percent of the thickeners are mixed to prepare water-holding thickening liquid for spare, and then 94-98 percent of the polymer latex, 0-0.5 percent of the ultra-violet absorber, 0-0.6 percent of the antioxidant and 1-6 percent of the film-forming additives are mixed to prepare polymer film-formation weather-proofing modified liquid for spare, and 30-50 percent of the water-holding thickening liquid and the polymer film-formation weather-proofing modified liquid are formulated to prepare the cohesive glue for the flexible decorative tile. The cohesive glue has the advantages of no taste, no toxicity, high first sticking intensity, low volume weight and rapid construction speed.
Description
Technical field
The present invention relates to a kind of assembly glue and preparation method thereof, particularly a kind of assembly glue that bond buildings outer wall flexible tapestry brick uses and preparation method thereof that is used for.
Background technology
Often there is following common fault in traditional outer wall flexible tapestry brick assembly glue owing to adopting sand-cement slurry or polymer cement mortar to make, being applied on the exterior wall:
1. initial adhesive strength is low, very easily occurs coming off; 2. adhesive mortar can pollute facing tile when constructing, and influences outward appearance; 3. the patch block speed of application is slow, thereby increases construction cost; 4., consumption many (consumption 4Kg/m big because of matrix material unit weight
2), thereby increased the load of gravity torque for the external wall outer insulation material; 5. matrix material is a rigid material, and big with the material temperature variable coefficient difference of flexible decorative facing brick, its bonding interface easily is subjected to displacement under frequent temperature change condition, causes flexible decorative facing brick to come off.
Summary of the invention
The objective of the invention is to want to overcome above-mentioned the deficiencies in the prior art, a kind of new cohesive glue for flexible decorative tile and preparation method thereof is provided, the assembly glue that adopts this method to make, tasteless, nontoxic, the initial adhesive strength height, unit weight is little, consumption is few, speed of application is fast, neither can pollute, brick is subjected to displacement under temperature change situation brick.
For realizing that the technical scheme that above-mentioned purpose of the present invention adopts is: a kind of cohesive glue for flexible decorative tile is characterized in that being made up of following materials of weight proportions: water-holding agent 0.3-1.5%, water 28-48%, thickening material 0.3-2%; Polymer emulsion 48-68%, UV light absorber 0-0.35%, oxidation inhibitor 0-0.42%, film coalescence aid 0.7-4.2%.
Above-mentioned cohesive glue for flexible decorative tile is made as follows:
1. make water-keeping thickening liquid: water-keeping thickening liquid is made by following materials of weight proportions: water-holding agent 1-3%, water 93-97%, thickening material 1-4%;
2. make the weather-proof modification liquid of film forming of polymkeric substance: the weather-proof modification liquid of the film forming of polymkeric substance is made by following materials of weight proportions: polymer emulsion 94-98%, UV light absorber 0-0.5%, oxidation inhibitor 0-0.6%, film coalescence aid 1-6%;
3. assembly glue is composite: the weather-proof modification liquid of the film forming of water-keeping thickening liquid and polymkeric substance is allocated by following weight ratio, makes cohesive glue for flexible decorative tile: the weather-proof modification liquid of the film forming 50-70% of water-keeping thickening liquid 30-50%, polymkeric substance.
Described water-holding agent can adopt at least a in the water-holding agents such as methylcellulose gum MC, hydroxypropylcellulose HPMC, Natvosol, guanidine glue HS-30R.
Described film coalescence aid can adopt at least a in the film coalescence aid such as TEXANOL, lauryl alcohol ester, ethylene glycol monobutyl ether, propylene glycol.
Described thickening material can be with adopting at least a in UH-420, TE-936, the thickening materials such as TT935, ASE-60.
Described water preferably adopts the clean water of PH=7.
Described polymer emulsion can adopt at least a in the emulsions such as pure-acrylic emulsion, benzene emulsion, organosilicon crylic acid latex, acrylic emulsion.
Described oxidation inhibitor can adopt at least a in the oxidation inhibitor such as antioxidant 2246, antioxidant 1010, antioxidant 3114, oxidation inhibitor 4010NA.
Described UV light absorber can adopt at least a in the UV light absorber such as photostabilizer UV-9, UV-531, UV-327, UV-P.
The assembly glue of making according to method of the present invention has following advantage: be white thickness paste before this assembly glue is solidified 1., solidifying the back is tasteless, nontoxic, water white elastomerics, have waterproof, ageing-resistant performance, can not cause color stain flexible decorative facing brick; 2. this assembly glue is high-ductility, elastomer material, and its snappiness is similar with flexible decorative facing brick, can not be subjected to displacement under temperature change situation; 3. this assembly glue initial adhesive strength height; 4. this assembly glue unit weight is little, consumption is few (consumption 0.6Kg/m
2); 5. patch block speed of application fast (stickup, jointing, face glue once survive), construction cost is low; 6. this assembly glue is water-based, tasteless, nontoxic ep-type material.
Embodiment
For describing the present invention in detail, below in conjunction with the concrete example of implementing the present invention is done further detailed description, yet described embodiment should not explain in the mode of restriction.
1, the making of water-keeping thickening liquid:
Take by weighing water-holding agent 1-3%, water 93-97%, thickening material 1-4% by weight percentage, put into reactor, stirring gets final product.
Example: can press column weight amount per-cent and take by weighing raw material:
1., by weight take by weighing the clean water of 1% methylcellulose gum MC, 97%PH=7,2% thickening material UH-420, put into reactor, stirring gets final product.
2., by weight take by weighing the clean water of 3% hydroxypropylcellulose HPMC, 93%PH=7,4% thickening material TE-936, put into reactor, stirring gets final product.
3., by weight take by weighing 2% Natvosol, 97% clean water, 1% thickening material TT935, put into reactor, stirring gets final product.
4., by weight take by weighing 3% guanidine glue HS-30R, 94% clean water, 3% thickening material ASE-60, put into reactor, stirring gets final product.
2, the making of the weather-proof modification liquid of the film forming of polymkeric substance:
Take by weighing polymer emulsion 94-98%, UV light absorber 0-0.5%, oxidation inhibitor 0-0.6%, film coalescence aid 1-6% by weight percentage, put into reactor, stirring gets final product.
Example: can press column weight amount per-cent and take by weighing raw material:
1., by weight take by weighing 94% pure-acrylic emulsion, 0.5% photostabilizer UV-9,0.5% antioxidant 2246,5% film coalescence aid TEXANOL, put into reactor, stirring gets final product.
2., by weight take by weighing 98% benzene emulsion, 0.6% antioxidant 1010,1.4% lauryl alcohol ester, put into reactor, stirring gets final product.
3., by weight take by weighing 96% organosilicon crylic acid latex, 0.3% ultraviolet absorbent UV-531,3.7% ethylene glycol monobutyl ether, put into reactor, stirring gets final product.
4., by weight take by weighing 94% acrylic emulsion, 6% propylene glycol, put into reactor, stirring gets final product.
5., by weight take by weighing 98% organosilicon crylic acid latex, 0.5% UV light absorber UV-327,0.5% antioxidant 3114,1% ethylene glycol monobutyl ether, put into reactor, stirring gets final product.
3, assembly glue is composite:
Take by weighing the weather-proof modification liquid of the film forming 50-70% of prepared water-keeping thickening liquid 30-50%, polymkeric substance by weight percentage, put into reactor, stir, make cohesive glue for flexible decorative tile, packing gets final product.
Example: can press column weight amount per-cent and take by weighing raw material:
1., by weight take by weighing the weather-proof modification liquid 50% of film forming of prepared water-keeping thickening liquid 50%, prepared polymkeric substance, put into reactor, stir, make cohesive glue for flexible decorative tile, packing gets final product.
2., by weight take by weighing the weather-proof modification liquid 70% of film forming of prepared water-keeping thickening liquid 30%, prepared polymkeric substance, put into reactor, stir, make cohesive glue for flexible decorative tile, packing gets final product.
3., by weight take by weighing the weather-proof modification liquid 60% of film forming of prepared water-keeping thickening liquid 40%, prepared polymkeric substance, put into reactor, stir, make cohesive glue for flexible decorative tile, packing gets final product.
The equipment that the present invention produces cohesive glue for flexible decorative tile is universal glassed steel reaction vessels.
Claims (8)
1. cohesive glue for flexible decorative tile is characterized in that being made up of following materials of weight proportions: water-holding agent 0.3-1.5%, water 28-48%, thickening material 0.3-2%; Polymer emulsion 48-68%, UV light absorber 0-0.35%, oxidation inhibitor 0-0.42%, film coalescence aid 0.7-4.2%.
2. according to the described cohesive glue for flexible decorative tile of claim 1, it is characterized in that described water-holding agent adopts at least a in the following raw materials according: methylcellulose gum MC, hydroxypropylcellulose HPMC, Natvosol, guanidine glue HS-30R.
3. according to the described cohesive glue for flexible decorative tile of claim 1, it is characterized in that described film coalescence aid adopts at least a in the following raw materials according: TEXANOL, lauryl alcohol ester, ethylene glycol monobutyl ether, propylene glycol.
4. according to the described cohesive glue for flexible decorative tile of claim 1, it is characterized in that described thickening material adopts at least a in the following raw materials according: UH-420, TE-936, TT935, ASE-60.
5. according to the described cohesive glue for flexible decorative tile of claim 1, it is characterized in that described polymer emulsion adopts at least a in the following raw materials according: pure-acrylic emulsion, benzene emulsion, organosilicon crylic acid latex, acrylic emulsion.
6. according to the described cohesive glue for flexible decorative tile of claim 1, it is characterized in that described oxidation inhibitor adopts at least a in the following raw materials according: antioxidant 2246, antioxidant 1010, antioxidant 3114, oxidation inhibitor 4010NA.
7. according to the described cohesive glue for flexible decorative tile of claim 1, it is characterized in that described UV light absorber adopts at least a in the following raw materials according: photostabilizer UV-9, UV-531, UV-327, UV-P.
8. method of making the described cohesive glue for flexible decorative tile of claim 1 is characterized in that making by following method:
(1), the making of water-keeping thickening liquid: water-keeping thickening liquid is made by following materials of weight proportions: water-holding agent 1-3%, water 93-97%, thickening material 1-4%;
(2), the making of the weather-proof modification liquid of the film forming of polymkeric substance: the weather-proof modification liquid of the film forming of polymkeric substance is made by following materials of weight proportions: polymer emulsion 94-98%, UV light absorber 0-0.5%, oxidation inhibitor 0-0.6%, film coalescence aid 1-6%;
(3), assembly glue is composite: the weather-proof modification liquid of the film forming of water-keeping thickening liquid and polymkeric substance is allocated by following weight ratio, makes cohesive glue for flexible decorative tile: the weather-proof modification liquid of the film forming 50-70% of water-keeping thickening liquid 30-50%, polymkeric substance.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009102306398A CN101701138B (en) | 2009-11-19 | 2009-11-19 | Cohesive glue for flexible decorative tile and manufacturing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009102306398A CN101701138B (en) | 2009-11-19 | 2009-11-19 | Cohesive glue for flexible decorative tile and manufacturing method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101701138A true CN101701138A (en) | 2010-05-05 |
| CN101701138B CN101701138B (en) | 2011-10-19 |
Family
ID=42156066
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009102306398A Active CN101701138B (en) | 2009-11-19 | 2009-11-19 | Cohesive glue for flexible decorative tile and manufacturing method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101701138B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102174847A (en) * | 2011-01-22 | 2011-09-07 | 夏良强 | Weatherable flexible tapestry brick and manufacturing method thereof |
| CN105349065A (en) * | 2015-12-04 | 2016-02-24 | 重庆江北工农化工有限责任公司 | Emulsion adhesive |
| CN106497473A (en) * | 2016-10-21 | 2017-03-15 | 湖北碱克新材料有限公司 | A kind of environment protection type single-component vitrified brick gum and preparation method thereof |
| CN106753076A (en) * | 2015-11-25 | 2017-05-31 | 铂恩塞尔新材料（上海）股份有限公司 | A kind of Environment-friendlywallpaper wallpaper glue material for sticking wallpaper and preparation method thereof |
| CN106893530A (en) * | 2017-04-25 | 2017-06-27 | 无锡市福享天下科技有限公司 | Senior water-proof adhesive |
| CN106978107A (en) * | 2017-04-27 | 2017-07-25 | 无锡市福享天下科技有限公司 | The senior strength adhesive of multipurpose |
| CN109021880A (en) * | 2017-06-10 | 2018-12-18 | 清远楼邦建材科技有限公司 | A kind of waterproofness strong adherence agent |
-
2009
- 2009-11-19 CN CN2009102306398A patent/CN101701138B/en active Active
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102174847A (en) * | 2011-01-22 | 2011-09-07 | 夏良强 | Weatherable flexible tapestry brick and manufacturing method thereof |
| CN106753076A (en) * | 2015-11-25 | 2017-05-31 | 铂恩塞尔新材料（上海）股份有限公司 | A kind of Environment-friendlywallpaper wallpaper glue material for sticking wallpaper and preparation method thereof |
| CN105349065A (en) * | 2015-12-04 | 2016-02-24 | 重庆江北工农化工有限责任公司 | Emulsion adhesive |
| CN106497473A (en) * | 2016-10-21 | 2017-03-15 | 湖北碱克新材料有限公司 | A kind of environment protection type single-component vitrified brick gum and preparation method thereof |
| CN106497473B (en) * | 2016-10-21 | 2019-06-04 | 湖北碱克新材料有限公司 | A kind of environment protection type single-component vitrified brick gum and preparation method thereof |
| CN106893530A (en) * | 2017-04-25 | 2017-06-27 | 无锡市福享天下科技有限公司 | Senior water-proof adhesive |
| CN106978107A (en) * | 2017-04-27 | 2017-07-25 | 无锡市福享天下科技有限公司 | The senior strength adhesive of multipurpose |
| CN109021880A (en) * | 2017-06-10 | 2018-12-18 | 清远楼邦建材科技有限公司 | A kind of waterproofness strong adherence agent |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101701138B (en) | 2011-10-19 |
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Inventor after: Ye Yongjun Inventor after: Xia Liangqiang Inventor after: Niu Chengbin Inventor before: Xia Liangqiang |
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Owner name: YANTAI TONGHUA WATERPROOF + THERMAL INSULATING ENG Free format text: FORMER OWNER: XIA LIANGQIANG Effective date: 20120222 |
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Effective date of registration: 20120222 Address after: Fushan hi tech Zone Yongda Street Yantai city Shandong province 265500 No. 591 Patentee after: Yantai Tonghua Waterproof & Thermal Insulation Engineering Co., Ltd. Address before: Fushan hi tech Zone Yongda Street Yantai city Shandong province 265500 No. 591 Patentee before: Xia Liangqiang |