CN101690546A - Layer chicken feed additive and using method - Google Patents
Layer chicken feed additive and using method Download PDFInfo
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- CN101690546A CN101690546A CN200910153073A CN200910153073A CN101690546A CN 101690546 A CN101690546 A CN 101690546A CN 200910153073 A CN200910153073 A CN 200910153073A CN 200910153073 A CN200910153073 A CN 200910153073A CN 101690546 A CN101690546 A CN 101690546A
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- layer chicken
- feed addictive
- hypericum perforatum
- lucifuge
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- 241000287828 Gallus gallus Species 0.000 title claims abstract description 112
- 238000000034 method Methods 0.000 title claims abstract description 22
- 239000003674 animal food additive Substances 0.000 title abstract description 13
- 244000141009 Hypericum perforatum Species 0.000 claims abstract description 137
- 235000017309 Hypericum perforatum Nutrition 0.000 claims abstract description 115
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 50
- 108010011619 6-Phytase Proteins 0.000 claims abstract description 33
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims abstract description 25
- 229930003268 Vitamin C Natural products 0.000 claims abstract description 25
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 25
- 239000011718 vitamin C Substances 0.000 claims abstract description 25
- 229940085127 phytase Drugs 0.000 claims abstract description 24
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229910021536 Zeolite Inorganic materials 0.000 claims abstract description 11
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims abstract description 11
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- Feed For Specific Animals (AREA)
- Fodder In General (AREA)
Abstract
The invention relates to the technical field of feed additive, in particular to a layer chicken feed additive and a using method. The invention aims to provide a layer chicken feed additive taking hypericum perforatum as the main raw material and a using method, aiming to improve layer chicken productivity, lower egg lipid substance content, improve egg antibiosis and antioxidation performances and prevent and cure poultry bird flu. The layer chicken feed additive of the invention comprises the components of hypericum perforatum extractive, phytase and vitamin C; a carrier can be added in the layer chicken feed additive to form dilute layer chicken feed additive, wherein the carrier adopts one of white carbon black, kieselguhr and zeolite. The using method of the layer chicken feed additive comprises: adding the layer chicken feed additive in layer chicken feed, and evenly mixing the layer chicken feed additive with the layer chicken feed in the no-light environment; sealing and packaging the feed additive; and putting the feed additive in a shady, cool and dry place without light. Layer chicken is fed twice a day, respectively in the morning and in the afternoon.
Description
Technical field
The present invention relates to field of feed additive technology, particularly a kind of feed addictive of layer chicken and using method.
Background technology
Egg is one of human best nutriment, contains a large amount of vitamin and mineral matter in the egg and the protein of high biological value is arranged.For the people, protein quality the best of egg is only second to breast milk, and the amino acid ratio of egg protein is well suited for Human Physiology to be needed, easily be the body absorption, and utilization rate is up to more than 98%, and nutritive value is very high.Calcium, phosphorus, iron and vitamin A content are very high in the egg, the B family vitamin is also very abundant, the vitamin and the trace element that also contain other many kinds of needed by human are children's, old man, puerpera and hepatitis, tuberculosis, anaemia patient, post-operative recovery patient's good tonics.Yet, contain higher triglycerides and T-CHOL in the egg, often eat egg, can cause the cholesterolemia too high levels, cause the generation of the atherosclerotic and the heart, cranial vascular disease, affect human beings'health.In addition, in order to prevent that laying hen is ill and to improve the production performance of laying hen, the enterprise of raising chickens generally adds antibiotic, hormone and chemical synthetic drug in egg feedstuff, easily induce pathogen to produce antibody, medicine fermentoid behind for a long time edible this feed of laying hen, change permeability of cell membrane or plasm metabolic process, thereby drug resistance occurs, and make in the laying hen body and exist medicament residue that human health is caused potential threat.
Chinese herbal medicine is the product of distinctive traditional Chinese medical theory of China and practice, its aboundresources, with a long history.Natural Chinese medicinal herb does not generally have the resistance to the action of a drug or the resistance to the action of a drug is less, and the Chinese herbal medicine immunologic active material can strengthen human body immune function, improve that animal is anti-stress, anti-disease ability, improve breeding performonce fo animals, and has noresidue, is difficult for producing advantages such as drug resistance.In recent years, the experimental study of Chinese herbal medicine in laying hen mainly concentrates on above the various diseases control, and lacking further investigation aspect laying hen egg laying performance and the egg quality.
Hypericum perforatum (Hypericum perforatum L.) is Guttiferae (Guttiferae) perennial herb, all herbal medicine, can clear away heart-fire make eye bright, hemostasia and promoting granulation, regulating menstruation and activating blood, detoxicating, relieving inflammation.Discover that hypericum perforatum has the effect that reduces lipid materials such as animal body inner cholesterol.In addition, its medical value of main active hypericin class material (hypericins) of hypericum perforatum is also very high, be used for anti-melancholy, the effect of inhibition nervous centralis except that clinical, still a kind of promising endogenous photosensitizer is used for tumour photochemodiagnosis and treatment.Current research finds that hypericin has significant anti-DNA, RNA virus function, can directly act on viruses such as bird flu, swine fever, aftosa, disturbs this virus replication, breeding and virus is had strong inhibitory action, begins to be applied to the treatment of AIDS recently.At present, hypericum perforatum is not appeared in the newspapers as feed addictive of layer chicken.
Summary of the invention
The purpose of this invention is to provide a kind of is the feed addictive of layer chicken and the using method of primary raw material with the hypericum perforatum, is intended to improve the laying hen production performance, reduces egg lipid material content, improves the antibiotic antioxygenic property of egg, prevents and treats the poultry bird flu simultaneously.Satisfy breeding layer chicken industry demand to natural green, with low cost, multifunction quick-effect feed addictive.
The technical solution adopted in the present invention is finished in the following way: a kind of feed addictive of layer chicken, the component of this feed addictive of layer chicken comprises Hypericum Perforatum P.E, phytase and vitamin C, and the weight proportion of the component of feed addictive of layer chicken is: 100 parts of Hypericum Perforatum P.Es, 6～17 parts of phytases, 6～17 parts of vitamin Cs.
In order to strengthen the stable and easy to use of additive, can add carrier in above-mentioned feed addictive of layer chicken makes it become the dilution type feed addictive of layer chicken, the weight proportion of the component of dilution type feed addictive of layer chicken is: 100 parts of Hypericum Perforatum P.Es, 6～17 parts of phytases, 6～17 parts of vitamin Cs, 400～600 parts in carrier, wherein, carrier adopts a kind of in white carbon, diatomite, the zeolite powder, optimization be to adopt white carbon as carrier.
The preparation method of feed addictive of layer chicken is:
1, preparation Hypericum Perforatum P.E
The preparation process of Hypericum Perforatum P.E is:
(1) 15～25 centimetres of parts in hypericum perforatum plant top of gathering, harvesting back lucifuge and with 35 ℃～55 ℃ temperature clear water clean, immersion 2～4 hours;
(2) the hypericum perforatum plant after the immersion is removed stem and branch, gets leaf and flower portion, and lucifuge is dried to water content and is lower than percentage by weight 0.05%;
(3) hypericum perforatum leaf after drying and flower portion pulverize with pulverizer, and hypericum perforatum leaf and flower portion pulverize the back and cross 60 mesh sieves;
(4) remove chlorophyll, above-mentioned hypericum perforatum powder put into can dissolve chlorophyllous solvent and mix, at 55 ℃～65 ℃ with ultrasonic wave pulverizer extraction 20～40 minutes, with the chlorophyll in the removal hypericum perforatum powder;
(5) filter extract, residue is put into baking oven under 55 ℃～65 ℃ temperature dry 2～4 hours, the NaOH that adds dried residue percentage by weight 0.1～0.3% in the dry residue, mix the back and add the extraction solvent, under 20 ℃～40 ℃, extracted 20～40 minutes then with ultrasonic wave; After the filtration, extract 55 ℃～65 ℃ ,-0.10～-0.06Mpa condition vacuum concentrates, and reclaims solvent, obtains the pitchy powder, crosses 80 mesh sieves, be used for the Hypericum Perforatum P.E of feed addictive of layer chicken.This Hypericum Perforatum P.E is stored under lucifuge, 0～4 ℃ of condition.
Above all operations step is all operated according under the intensity in lucifuge or than low light.
2, the preparation of feed addictive of layer chicken
The preparation of feed addictive of layer chicken is divided into the preparation of plain edition feed addictive of layer chicken and the preparation of dilution type feed addictive of layer chicken, wherein:
(1) preparation of plain edition feed addictive of layer chicken
Weight proportion by additive component takes by weighing Hypericum Perforatum P.E, phytase and vitamin C, stir, pack the back a kind of plain edition feed addictive of layer chicken.
(2) preparation of dilution type feed addictive of layer chicken
Weight proportion by dilution type feed addictive of layer chicken component takes by weighing Hypericum Perforatum P.E, phytase, vitamin C and carrier, wherein, the vegetable oil that adds vehicle weight percentage 0.5～1% in carrier, vegetable oil adopt a kind of in soya-bean oil, corn oil, peanut oil, cottonseed oil, the rapeseed oil; During preparation, in carrier, add earlier vegetable oil, to be mixed evenly after, add Hypericum Perforatum P.E, vitamin C and phytase successively, mix, pack the back a kind of dilution type feed addictive of layer chicken.
In the preparation method of above-mentioned feed addictive of layer chicken, the used hypericum perforatum plant of preparation Hypericum Perforatum P.E is to adopt the hypericum perforatum that is planted in land for growing field crops, middle part, Zhejiang Province of introducing a fine variety from the Qinling Mountains, the Shaanxi Province wild plant of north slope.
In the preparation method of above-mentioned feed addictive of layer chicken, in the preparation process of Hypericum Perforatum P.E (4), used to dissolve chlorophyllous solvent be a kind of in chloroform, the ether, optimization be to adopt chloroform as dissolving chlorophyllous solvent; As can dissolve chlorophyllous solvent the time, the proportioning of described hypericum perforatum powder and chloroform is: described hypericum perforatum powder 1kg, chloroform 3000ml～8000ml with chloroform.
In the preparation method of above-mentioned feed addictive of layer chicken, in the preparation process of Hypericum Perforatum P.E (5), used extraction solvent is a kind of in methyl alcohol, ethanol, normal propyl alcohol, acetone, the ethyl acetate, optimization be to adopt methyl alcohol as solvent; When extracting solvent, the filtered residue of described drying and the proportioning of methyl alcohol are: the filtered residue 1kg of described drying, methyl alcohol 3000ml～8000ml with methyl alcohol.
The using method of feed addictive of layer chicken of the present invention is:
In the egg feedstuff of 10kg, add plain edition feed addictive of layer chicken 5～10g of the present invention and mix, the operating process lucifuge of trying one's best.In order to keep the effect of additive,＜15 days batch mixings once and pack feed addictive, place shady and cool drying and lucifuge place.
Or in the egg feedstuff of 10kg, add dilution type feed addictive of layer chicken 20～50g of the present invention and mix, the operating process lucifuge of trying one's best.In order to keep the effect of additive,＜15 days batch mixings once and pack feed addictive, place shady and cool drying and lucifuge place.
Giving the laying hen feeding time is respectively to feed once in the morning and afternoon of every day, and the laying hen feeding time of giving of optimization is that 8 of every days and 15 respectively feed once.
Plain edition feed addictive of layer chicken of the present invention can add in the drinking-water of laying hen, and additional proportion is 500mg/kg～1000mg/kg.
Phytase in above-mentioned feed addictive of layer chicken component has the digestibility that can improve elements such as calcium, phosphorus in the laying hen plant feed, alleviates hypericin and reduces the effect that blood calcium causes the egg shell thickness to reduce.
Vitamin C in above-mentioned feed addictive of layer chicken component helps in the laying hen body cholesterol to resolve into cholic acid to excrete, strengthen laying hen body disease-resistant power and defensive enginery, the vitamin C in the feed can prevent that active component is oxidized in the Hypericum Perforatum P.E simultaneously.
Find through experiment: adopt feed addictive of layer chicken of the present invention to feed after 4 weeks, compare with control group (not adding feed addictive of layer chicken of the present invention), each index result is as follows: egg size increase by 2.76%, feedstuff-egg ratio reduce by 3.98%, the egg volume improves 3.80%, and the laying rate of laying hen does not have influence; Yolk SOD content improves 7.43%, and yolk MDA reduces by 35.91%; Laying hen serum and yolk total cholesterol level reduce by 27.92% and 13.79% respectively, and yolk triglyceride content reduces by 16.23%; Egg white lysozyme content improves 11.18%; The laying hen quantity of leucocyte improves 41.84%.So feed addictive of the present invention can improve the laying hen production performance, reduced the breeding production cost, improved the egg oxidation stability, reduced the lipid material content of egg, make egg effectively resist bacterial invasion, strengthen the egg property stability, prolong the egg product period of storage, and improved immunity of layer chicken.
The specific embodiment
Below by embodiment the present invention is made further and to specify, but the invention is not restricted to these embodiment.
Embodiment 1
A kind of feed addictive of layer chicken, the component of this additive comprises Hypericum Perforatum P.E, phytase and vitamin C, the weight proportion of the component of additive is: 100 parts of Hypericum Perforatum P.Es, 6～17 parts of phytases, 6～17 parts of vitamin Cs.
The preparation method of this feed addictive of layer chicken is:
1, preparation Hypericum Perforatum P.E
The preparation process of Hypericum Perforatum P.E is:
(1) 15～25 centimetres of parts in hypericum perforatum plant top of gathering, harvesting back lucifuge is also cleaned, was soaked 2～4 hours with 35 ℃～55 ℃ temperature clear water, wherein, the hypericum perforatum plant is adopted the hypericum perforatum that is planted in land for growing field crops, middle part, Zhejiang Province of introducing a fine variety from the Qinling Mountains, the Shaanxi Province wild plant of north slope;
(2) the hypericum perforatum plant after the immersion is removed stem and branch, gets leaf and flower portion, and lucifuge is dried to water content and is lower than percentage by weight 0.05%;
(3) hypericum perforatum leaf after drying and flower portion pulverize with pulverizer, and hypericum perforatum leaf and flower portion pulverize the back and cross 60 mesh sieves;
(4) remove chlorophyll, above-mentioned hypericum perforatum powder put into can dissolve chlorophyllous solvent and mix, at 55 ℃～65 ℃ with ultrasonic wave pulverizer extraction 20～40 minutes, with the chlorophyll in the removal hypericum perforatum powder;
(5) filter extract, residue is put into baking oven under 55 ℃～65 ℃ temperature dry 2～4 hours, the NaOH that adds dried residue percentage by weight 0.1～0.3% in the dry residue, mix the back and add methyl alcohol, extracted 20～40 minutes with ultrasonic wave under 20 ℃～40 ℃ then, the dry filtered residue and the proportioning of methyl alcohol are: dry filtered residue 1kg, methyl alcohol 3000ml～8000ml; After the filtration, extract 55 ℃～65 ℃ ,-0.10～-0.06Mpa condition vacuum concentrates, and reclaims solvent, obtains the pitchy powder, crosses 80 mesh sieves, be used for the Hypericum Perforatum P.E of feed addictive of layer chicken.This Hypericum Perforatum P.E is stored under lucifuge, 0～4 ℃ of condition.
Above all operations step is all operated according under the intensity in lucifuge or than low light.
2, the preparation of feed addictive of layer chicken
Weight proportion by additive component takes by weighing Hypericum Perforatum P.E, phytase and vitamin C, stir, pack the back a kind of feed addictive of layer chicken.
The using method of feed addictive of layer chicken of the present invention is:
In the egg feedstuff of 10kg, add plain edition feed addictive of layer chicken 5～10g of the present invention and mix, the operating process lucifuge of trying one's best.In order to keep the effect of additive,＜15 days batch mixings once and pack feed addictive, place shady and cool drying and lucifuge place.
Giving the laying hen feeding time is respectively to feed once in the morning and afternoon of every day, and the laying hen feeding time of giving of optimization is that 8 and 15 of every day respectively feed once.
Feed addictive of layer chicken of the present invention is added in the drinking-water of laying hen, additional proportion is 500mg/kg～1000mg/kg.
Embodiment 2
A kind of feed addictive of layer chicken, the component of this additive comprises Hypericum Perforatum P.E, phytase, vitamin C and white carbon, and the weight proportion of the component of additive is: 100 parts of Hypericum Perforatum P.Es, 6～17 parts of phytases, 6～17 parts of vitamin Cs, 400～600 parts of white carbons.
The preparation method of this feed addictive of layer chicken is:
1, preparation Hypericum Perforatum P.E
The preparation process of Hypericum Perforatum P.E is:
(1) 15～25 centimetres of parts in hypericum perforatum plant top of gathering, harvesting back lucifuge is also cleaned, was soaked 2～4 hours with 35 ℃～55 ℃ temperature clear water, wherein, the hypericum perforatum plant is adopted the hypericum perforatum that is planted in land for growing field crops, middle part, Zhejiang Province of introducing a fine variety from the Qinling Mountains, the Shaanxi Province wild plant of north slope;
(2) the hypericum perforatum plant after the immersion is removed stem and branch, gets leaf and flower portion, and lucifuge is dried to water content and is lower than percentage by weight 0.05%;
(3) hypericum perforatum leaf after drying and flower portion pulverize with pulverizer, and hypericum perforatum leaf and flower portion pulverize the back and cross 60 mesh sieves;
(4) remove chlorophyll, above-mentioned hypericum perforatum powder put into can dissolve chlorophyllous solvent and mix, at 55 ℃～65 ℃ with ultrasonic wave pulverizer extraction 20～40 minutes, with the chlorophyll in the removal hypericum perforatum powder;
(5) filter extract, residue is put into baking oven under 55 ℃～65 ℃ temperature dry 2～4 hours, the NaOH that adds dried residue percentage by weight 0.1～0.3% in the dry residue, mix the back and add ethanol, extracted 20～40 minutes with ultrasonic wave under 20 ℃～40 ℃ then, the dry filtered residue and the proportioning of ethanol are: dry filtered residue 1kg, ethanol 3000ml～8000ml; After the filtration, extract 55 ℃～65 ℃ ,-0.10～-0.06Mpa condition vacuum concentrates, and reclaims solvent, obtains the pitchy powder, crosses 80 mesh sieves, be used for the Hypericum Perforatum P.E of feed addictive of layer chicken.This Hypericum Perforatum P.E is stored under lucifuge, 0～4 ℃ of condition.
Above all operations step is all operated according under the intensity in lucifuge or than low light.
2, the preparation of feed addictive of layer chicken
Weight proportion by additive component takes by weighing Hypericum Perforatum P.E, phytase, vitamin C and white carbon, wherein, the vegetable oil that adds vehicle weight percentage 0.5～1% in white carbon, vegetable oil adopt a kind of in soya-bean oil, corn oil, peanut oil, cottonseed oil, the rapeseed oil; During preparation, in white carbon, add earlier vegetable oil, to be mixed evenly after, add Hypericum Perforatum P.E, vitamin C and phytase successively, mix, pack the back a kind of dilution type feed addictive of layer chicken.
The using method of dilution type feed addictive of layer chicken of the present invention is:
In the egg feedstuff of 10kg, add dilution type feed addictive of layer chicken 20～50g of the present invention and mix, the operating process lucifuge of trying one's best.In order to keep the effect of additive,＜15 days batch mixings once and pack feed addictive, place shady and cool drying and lucifuge place.
Giving the laying hen feeding time is respectively to feed once in the morning and afternoon of every day, and the laying hen feeding time of giving of optimization is that 8 and 15 of every day respectively feed once.
Embodiment 3
A kind of feed addictive of layer chicken, the component of this additive comprises Hypericum Perforatum P.E, phytase, vitamin C and diatomite, and the weight proportion of the component of additive is: 100 parts of Hypericum Perforatum P.Es, 6～17 parts of phytases, 6～17 parts of vitamin Cs, 400～600 parts in diatomite.
The preparation method of this feed addictive of layer chicken is:
1, preparation Hypericum Perforatum P.E
The preparation process of Hypericum Perforatum P.E is:
(1) 15～25 centimetres of parts in hypericum perforatum plant top of gathering, harvesting back lucifuge is also cleaned, was soaked 2～4 hours with 35 ℃～55 ℃ temperature clear water, wherein, the hypericum perforatum plant is adopted the hypericum perforatum that is planted in land for growing field crops, middle part, Zhejiang Province of introducing a fine variety from the Qinling Mountains, the Shaanxi Province wild plant of north slope;
(2) the hypericum perforatum plant after the immersion is removed stem and branch, gets leaf and flower portion, and lucifuge is dried to water content and is lower than percentage by weight 0.05%;
(3) hypericum perforatum leaf after drying and flower portion pulverize with pulverizer, and hypericum perforatum leaf and flower portion pulverize the back and cross 60 mesh sieves;
(4) remove chlorophyll, above-mentioned hypericum perforatum powder put into can dissolve chlorophyllous solvent and mix, at 55 ℃～65 ℃ with ultrasonic wave pulverizer extraction 20～40 minutes, with the chlorophyll in the removal hypericum perforatum powder;
(5) filter extract, residue is put into baking oven under 55 ℃～65 ℃ temperature dry 2～4 hours, the NaOH that adds dried residue percentage by weight 0.1～0.3% in the dry residue, mix the back and add normal propyl alcohol, extracted 20～40 minutes with ultrasonic wave under 20 ℃～40 ℃ then, the dry filtered residue and the proportioning of normal propyl alcohol are: dry filtered residue 1kg, normal propyl alcohol 3000ml～8000ml; After the filtration, extract 55 ℃～65 ℃ ,-0.10～-0.06Mpa condition vacuum concentrates, and reclaims solvent, obtains the pitchy powder, crosses 80 mesh sieves, be used for the Hypericum Perforatum P.E of feed addictive of layer chicken.This Hypericum Perforatum P.E is stored under lucifuge, 0～4 ℃ of condition.
Above all operations step is all operated according under the intensity in lucifuge or than low light.
2, the preparation of feed addictive of layer chicken
Weight proportion by additive component takes by weighing Hypericum Perforatum P.E, phytase, vitamin C and diatomite, wherein, the vegetable oil that adds vehicle weight percentage 0.5～1% in diatomite, vegetable oil adopt a kind of in soya-bean oil, corn oil, peanut oil, cottonseed oil, the rapeseed oil; During preparation, in diatomite, add earlier vegetable oil, to be mixed evenly after, add Hypericum Perforatum P.E, vitamin C and phytase successively, mix, pack the back a kind of dilution type feed addictive of layer chicken.
The using method of dilution type feed addictive of layer chicken of the present invention is identical with embodiment 2.
Embodiment 4
A kind of feed addictive of layer chicken, the component of this additive comprises Hypericum Perforatum P.E, phytase, vitamin C and diatomite, and the weight proportion of the component of additive is: 100 parts of Hypericum Perforatum P.Es, 6～17 parts of phytases, 6～17 parts of vitamin Cs, 400～600 parts of zeolite powders.
The preparation method of this feed addictive of layer chicken is:
1, preparation Hypericum Perforatum P.E
The preparation process of Hypericum Perforatum P.E is:
(1) 15～25 centimetres of parts in hypericum perforatum plant top of gathering, harvesting back lucifuge is also cleaned, was soaked 2～4 hours with 35 ℃～55 ℃ temperature clear water, wherein, the hypericum perforatum plant is adopted the hypericum perforatum that is planted in land for growing field crops, middle part, Zhejiang Province of introducing a fine variety from the Qinling Mountains, the Shaanxi Province wild plant of north slope;
(2) the hypericum perforatum plant after the immersion is removed stem and branch, gets leaf and flower portion, and lucifuge is dried to water content and is lower than percentage by weight 0.05%;
(3) hypericum perforatum leaf after drying and flower portion pulverize with pulverizer, and hypericum perforatum leaf and flower portion pulverize the back and cross 60 mesh sieves;
(4) remove chlorophyll, above-mentioned hypericum perforatum powder put into can dissolve chlorophyllous solvent and mix, at 55 ℃～65 ℃ with ultrasonic wave pulverizer extraction 20～40 minutes, with the chlorophyll in the removal hypericum perforatum powder;
(5) filter extract, residue is put into baking oven under 55 ℃～65 ℃ temperature dry 2～4 hours, the NaOH that adds dried residue percentage by weight 0.1～0.3% in the dry residue, mix the back and add acetone, extracted 20～40 minutes with ultrasonic wave under 20 ℃～40 ℃ then, the dry filtered residue and the proportioning of acetone are: dry filtered residue 1kg, acetone 3000ml～8000ml; After the filtration, extract 55 ℃～65 ℃ ,-0.10～-0.06Mpa condition vacuum concentrates, and reclaims solvent, obtains the pitchy powder, crosses 80 mesh sieves, be used for the Hypericum Perforatum P.E of feed addictive of layer chicken.This Hypericum Perforatum P.E is stored under lucifuge, 0～4 ℃ of condition.
Above all operations step is all operated according under the intensity in lucifuge or than low light.
2, the preparation of feed addictive of layer chicken
Weight proportion by additive component takes by weighing Hypericum Perforatum P.E, phytase, vitamin C and zeolite powder, wherein, the vegetable oil that adds vehicle weight percentage 0.5～1% in zeolite powder, vegetable oil adopt a kind of in soya-bean oil, corn oil, peanut oil, cottonseed oil, the rapeseed oil; During preparation, in zeolite powder, add earlier vegetable oil, to be mixed evenly after, add Hypericum Perforatum P.E, vitamin C and phytase successively, mix, pack the back a kind of dilution type feed addictive of layer chicken.
The using method of dilution type feed addictive of layer chicken of the present invention is identical with embodiment 2.
Embodiment 5
A kind of feed addictive of layer chicken, the component of this additive comprises Hypericum Perforatum P.E, phytase, vitamin C and diatomite, and the weight proportion of the component of additive is: 100 parts of Hypericum Perforatum P.Es, 6～17 parts of phytases, 6～17 parts of vitamin Cs, 400～600 parts of zeolite powders.
The preparation method of this feed addictive of layer chicken is:
1, preparation Hypericum Perforatum P.E
The preparation process of Hypericum Perforatum P.E is:
(1) 15～25 centimetres of parts in hypericum perforatum plant top of gathering, harvesting back lucifuge is also cleaned, was soaked 2～4 hours with 35 ℃～55 ℃ temperature clear water, wherein, the hypericum perforatum plant is adopted the hypericum perforatum that is planted in land for growing field crops, middle part, Zhejiang Province of introducing a fine variety from the Qinling Mountains, the Shaanxi Province wild plant of north slope;
(2) the hypericum perforatum plant after the immersion is removed stem and branch, gets leaf and flower portion, and lucifuge is dried to water content and is lower than percentage by weight 0.05%;
(3) hypericum perforatum leaf after drying and flower portion pulverize with pulverizer, and hypericum perforatum leaf and flower portion pulverize the back and cross 60 mesh sieves;
(4) remove chlorophyll, above-mentioned hypericum perforatum powder put into can dissolve chlorophyllous solvent and mix, at 55 ℃～65 ℃ with ultrasonic wave pulverizer extraction 20～40 minutes, with the chlorophyll in the removal hypericum perforatum powder;
(5) filter extract, residue is put into baking oven under 55 ℃～65 ℃ temperature dry 2～4 hours, the NaOH that adds dried residue percentage by weight 0.1～0.3% in the dry residue, mix the back and add ethyl acetate, extracted 20～40 minutes with ultrasonic wave under 20 ℃～40 ℃ then, the dry filtered residue and the proportioning of ethyl acetate are: dry filtered residue 1kg, ethyl acetate 3000ml～8000ml; After the filtration, extract 55 ℃～65 ℃ ,-0.10～-0.06Mpa condition vacuum concentrates, and reclaims solvent, obtains the pitchy powder, crosses 80 mesh sieves, be used for the Hypericum Perforatum P.E of feed addictive of layer chicken.This Hypericum Perforatum P.E is stored under lucifuge, 0～4 ℃ of condition.
Above all operations step is all operated according under the intensity in lucifuge or than low light.
2, the preparation of feed addictive of layer chicken
Weight proportion by additive component takes by weighing Hypericum Perforatum P.E, phytase, vitamin C and zeolite powder, wherein, the vegetable oil that adds vehicle weight percentage 0.5～1% in zeolite powder, vegetable oil adopt a kind of in soya-bean oil, corn oil, peanut oil, cottonseed oil, the rapeseed oil; During preparation, in zeolite powder, add earlier vegetable oil, to be mixed evenly after, add Hypericum Perforatum P.E, vitamin C and phytase successively, mix, pack the back a kind of dilution type feed addictive of layer chicken.
The using method of dilution type feed addictive of layer chicken of the present invention is identical with embodiment 2.
Claims (10)
1. feed addictive of layer chicken, it is characterized in that: the component of this feed addictive of layer chicken comprises Hypericum Perforatum P.E, phytase and vitamin C.
2. a kind of feed addictive of layer chicken according to claim 1 is characterized in that: the weight proportion of the component of feed addictive of layer chicken is: 100 parts of Hypericum Perforatum P.Es, 6～17 parts of phytases, 6～17 parts of vitamin Cs.
3. a kind of feed addictive of layer chicken according to claim 2, it is characterized in that: in feed addictive of layer chicken, add carrier and make it become the dilution type feed addictive of layer chicken, the weight proportion of the component of dilution type feed addictive of layer chicken is: 100 parts of Hypericum Perforatum P.Es, 6～17 parts of phytases, 6～17 parts of vitamin Cs, 400～600 parts in carrier, wherein, the carrier that is added in feed addictive of layer chicken is a kind of in white carbon, diatomite, the zeolite powder.
4. a kind of feed addictive of layer chicken according to claim 3 is characterized in that: the carrier that is added in feed addictive of layer chicken preferably adopts white carbon as the carrier that is added in feed addictive of layer chicken.
5. the preparation method of a kind of feed addictive of layer chicken according to claim 2, it is characterized in that: the preparation process of feed addictive of layer chicken is:
(1) preparation Hypericum Perforatum P.E
1. 15～25 centimetres of parts in hypericum perforatum plant top of gathering, harvesting back lucifuge and with 35 ℃～55 ℃ temperature clear water clean, immersion 2～4 hours;
2. the hypericum perforatum plant after soaking is removed stem and branch, gets leaf and flower portion, and lucifuge is dried to water content and is lower than percentage by weight 0.05%;
3. hypericum perforatum leaf after drying and flower portion pulverize with pulverizer, and hypericum perforatum leaf and flower portion pulverize the back and cross 60 mesh sieves;
4. remove chlorophyll, above-mentioned hypericum perforatum powder is put into to be dissolved chlorophyllous solvent and mix, extracted 20～40 minutes with the ultrasonic wave pulverizer, to remove the chlorophyll in the hypericum perforatum powder at 55 ℃～65 ℃;
5. under the lucifuge condition, filter extract, residue is put into baking oven under 55 ℃～65 ℃ temperature dry 2～4 hours, the NaOH that adds dried residue percentage by weight 0.1～0.3% in the dry residue, mix the back and add the extraction solvent, under 20 ℃～40 ℃, extracted 20～40 minutes then with ultrasonic wave; After the filtration, extract 55 ℃～65 ℃ ,-0.10～-0.06Mpa condition vacuum concentrates, and reclaims solvent, obtain the pitchy powder, cross 80 mesh sieves, be used for the Hypericum Perforatum P.E of feed addictive of layer chicken, this Hypericum Perforatum P.E is stored under lucifuge, 0 ℃～4 ℃ conditions;
(2) preparation of feed addictive of layer chicken
Weight proportion by additive component takes by weighing Hypericum Perforatum P.E, phytase and vitamin C, stir, pack the back a kind of plain edition feed addictive of layer chicken.
6. the preparation method of a kind of dilution type feed addictive of layer chicken according to claim 3 is characterized in that: the preparation process of dilution type feed addictive of layer chicken is:
(1) preparation Hypericum Perforatum P.E
1. 15～25 centimetres of parts in hypericum perforatum plant top of gathering, harvesting back lucifuge and with 35 ℃～55 ℃ temperature clear water clean, immersion 2～4 hours;
2. the hypericum perforatum plant after soaking is removed stem and branch, gets leaf and flower portion, and lucifuge is dried to water content and is lower than percentage by weight 0.05%;
3. hypericum perforatum leaf after drying and flower portion pulverize with pulverizer, and hypericum perforatum leaf and flower portion pulverize the back and cross 60 mesh sieves;
4. remove chlorophyll, above-mentioned hypericum perforatum powder is put into to be dissolved chlorophyllous solvent and mix, extracted 20～40 minutes with the ultrasonic wave pulverizer, to remove the chlorophyll in the hypericum perforatum powder at 55 ℃～65 ℃;
5. under the lucifuge condition, filter extract, residue is put into baking oven under 55 ℃～65 ℃ temperature dry 2～4 hours, the NaOH that adds dried residue percentage by weight 0.1～0.3% in the dry residue, mix the back and add the extraction solvent, under 20 ℃～40 ℃, extracted 20～40 minutes then with ultrasonic wave; After the filtration, extract 55 ℃～65 ℃ ,-0.10～-0.06Mpa condition vacuum concentrates, and reclaims solvent, obtain the pitchy powder, cross 80 mesh sieves, be used for the Hypericum Perforatum P.E of feed addictive of layer chicken, this Hypericum Perforatum P.E is stored under lucifuge, 0 ℃～4 ℃ conditions;
(2) preparation of feed addictive of layer chicken
Weight proportion by dilution type feed addictive of layer chicken component takes by weighing Hypericum Perforatum P.E, phytase, vitamin C and carrier, wherein, the vegetable oil that adds vehicle weight percentage 0.5～1% in carrier, vegetable oil adopt a kind of in soya-bean oil, corn oil, peanut oil, cottonseed oil, the rapeseed oil; During preparation, in carrier, add earlier vegetable oil, to be mixed evenly after, add Hypericum Perforatum P.E, vitamin C and phytase successively, mix, pack the back a kind of dilution type feed addictive of layer chicken.
7. according to the preparation method of claim 5 or 6 described a kind of feed addictive of layer chicken, it is characterized in that: in the preparation method of feed addictive of layer chicken, it is used that to dissolve chlorophyllous solvent be a kind of in chloroform, the ether, what optimize is to adopt chloroform as dissolving chlorophyllous solvent, as can dissolve chlorophyllous solvent the time, the proportioning of described hypericum perforatum powder and chloroform is: described hypericum perforatum powder 1kg, chloroform 3000ml～8000ml with chloroform; Used extraction solvent is a kind of in methyl alcohol, ethanol, normal propyl alcohol, acetone, the ethyl acetate, what optimize is to adopt methyl alcohol as solvent, when extracting solvent, the filtered residue of described drying and the proportioning of methyl alcohol are: the filtered residue 1kg of described drying, methyl alcohol 3000ml～8000ml with methyl alcohol.
8. the using method of a kind of feed addictive of layer chicken according to claim 2, it is characterized in that: in the egg feedstuff of 10kg, add plain edition feed addictive of layer chicken 5～10g of the present invention and mix, the operating process lucifuge of trying one's best, in order to keep the effect of additive,＜15 days batch mixings once, and feed addictive packed, place shady and cool drying and lucifuge place; Giving the laying hen feeding time is respectively to feed once in the morning and afternoon of every day, and the laying hen feeding time of giving of optimization is that 8 of every days and 15 respectively feed once.
9. the using method of a kind of feed addictive of layer chicken according to claim 2 is characterized in that: feed addictive of layer chicken is added in the drinking-water of laying hen, the ratio that adds in the laying hen drinking-water is 500mg/kg～1000mg/kg.
10. the using method of a kind of feed addictive of layer chicken according to claim 3 is characterized in that: add dilution type feed addictive of layer chicken 20～50g of the present invention and mix in the egg feedstuff of 10kg, the operating process lucifuge of trying one's best.In order to keep the effect of additive,＜15 days batch mixings once and pack feed addictive, place shady and cool drying and lucifuge place; Giving the laying hen feeding time is respectively to feed once in the morning and afternoon of every day, and the laying hen feeding time of giving of optimization is that 8 of every days and 15 respectively feed once.
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| CN2009101530733A CN101690546B (en) | 2009-09-29 | 2009-09-29 | Layer chicken feed additive and using method |
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| CN2009101530733A CN101690546B (en) | 2009-09-29 | 2009-09-29 | Layer chicken feed additive and using method |
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| CN101690546B CN101690546B (en) | 2013-02-13 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103976149A (en) * | 2014-04-28 | 2014-08-13 | 彭鸿贰 | Chinese medicine feed additive for avian influenza prevention |
| CN108077574A (en) * | 2017-12-17 | 2018-05-29 | 柳州市象行教育科技有限责任公司 | A kind of feed addictive of layer chicken for improving laying rate and preparation method thereof |
| CN110592056A (en) * | 2019-09-19 | 2019-12-20 | 昆明理工大学 | Phage lyase composite powder and preparation method and application thereof |
| CN112655820A (en) * | 2020-12-16 | 2021-04-16 | 长沙昆博生物科技有限公司 | Feed additive and application thereof |
| RU2806138C1 (en) * | 2022-12-26 | 2023-10-26 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Кубанский государственный аграрный университет имени И.Т. Трубилина" | Feed additive for laying hens |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101181018B (en) * | 2007-12-13 | 2011-05-11 | 济南和美华饲料有限公司 | Hen feedstuff for producing healthy egg |
-
2009
- 2009-09-29 CN CN2009101530733A patent/CN101690546B/en active Active
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103976149A (en) * | 2014-04-28 | 2014-08-13 | 彭鸿贰 | Chinese medicine feed additive for avian influenza prevention |
| CN108077574A (en) * | 2017-12-17 | 2018-05-29 | 柳州市象行教育科技有限责任公司 | A kind of feed addictive of layer chicken for improving laying rate and preparation method thereof |
| CN110592056A (en) * | 2019-09-19 | 2019-12-20 | 昆明理工大学 | Phage lyase composite powder and preparation method and application thereof |
| CN112655820A (en) * | 2020-12-16 | 2021-04-16 | 长沙昆博生物科技有限公司 | Feed additive and application thereof |
| RU2806138C1 (en) * | 2022-12-26 | 2023-10-26 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Кубанский государственный аграрный университет имени И.Т. Трубилина" | Feed additive for laying hens |
| RU2806177C1 (en) * | 2022-12-26 | 2023-10-27 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Кубанский государственный аграрный университет имени И.Т. Трубилина" | Way to increase the productivity of laying hens |
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| CN101690546B (en) | 2013-02-13 |
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