CN101657403B - 用于回收二氯代醇的多级方法和设备 - Google Patents

用于回收二氯代醇的多级方法和设备 Download PDF

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Publication number
CN101657403B
CN101657403B CN200880011724.9A CN200880011724A CN101657403B CN 101657403 B CN101657403 B CN 101657403B CN 200880011724 A CN200880011724 A CN 200880011724A CN 101657403 B CN101657403 B CN 101657403B
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CN
China
Prior art keywords
liquid
mixture
dichlorohydrins
esters
distillation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN200880011724.9A
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English (en)
Chinese (zh)
Other versions
CN101657403A (zh
Inventor
丹·蒂托维迪奥耶奥
安德烈·梅伦诺夫
克里斯蒂安·D·克诺佩尔
布鲁斯·D·胡克
阿尼尔·梅赫塔
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Global Technologies LLC
Blue Cube IP LLC
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Dow Global Technologies LLC
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Publication date
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Publication of CN101657403A publication Critical patent/CN101657403A/zh
Application granted granted Critical
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Expired - Fee Related legal-status Critical Current
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C07C29/82—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation by azeotropic distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/146—Multiple effect distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/36—Azeotropic distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/38—Steam distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/34—Halogenated alcohols
    • C07C31/36—Halogenated alcohols the halogen not being fluorine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/34—Halogenated alcohols
    • C07C31/42—Polyhydroxylic acyclic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
CN200880011724.9A 2007-04-12 2008-04-11 用于回收二氯代醇的多级方法和设备 Expired - Fee Related CN101657403B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US92310807P 2007-04-12 2007-04-12
US60/923,108 2007-04-12
PCT/US2008/059968 WO2008128004A1 (en) 2007-04-12 2008-04-11 Multi-stage process and apparatus for recovering dichlorohydrins

Publications (2)

Publication Number Publication Date
CN101657403A CN101657403A (zh) 2010-02-24
CN101657403B true CN101657403B (zh) 2014-07-30

Family

ID=39651380

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200880011724.9A Expired - Fee Related CN101657403B (zh) 2007-04-12 2008-04-11 用于回收二氯代醇的多级方法和设备

Country Status (7)

Country Link
US (1) US8664453B2 (enExample)
EP (1) EP2137121A1 (enExample)
JP (1) JP2010523698A (enExample)
KR (1) KR20100016452A (enExample)
CN (1) CN101657403B (enExample)
TW (1) TWI432407B (enExample)
WO (1) WO2008128004A1 (enExample)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008128004A1 (en) 2007-04-12 2008-10-23 Dow Global Technologies Inc. Multi-stage process and apparatus for recovering dichlorohydrins
WO2008128014A1 (en) * 2007-04-12 2008-10-23 Dow Global Technologies Inc. Process and apparatus for vapor phase purification during hydrochlorination of multi-hydroxylated aliphatic hydrocarbon compounds
KR20090130123A (ko) * 2007-04-12 2009-12-17 다우 글로벌 테크놀로지스 인크. 다이클로로하이드린의 공비 회수를 위한 방법 및 장치
WO2008128010A1 (en) * 2007-04-12 2008-10-23 Dow Global Technologies Inc. Process and apparatus for recovery of dichlorohydrins via codistillation
TW200906776A (en) * 2007-04-12 2009-02-16 Dow Global Technologies Inc Conversion of a multihydroxylated-aliphatic hydrocarbon or ester thereof to a chlorohydrin
JP2011516553A (ja) 2008-04-09 2011-05-26 ダウ グローバル テクノロジーズ リミティド ライアビリティ カンパニー ジクロロヒドリン類を回収する多段法及び装置
CN102471196A (zh) 2009-07-03 2012-05-23 阿克佐诺贝尔化学国际公司 制备二氯丙醇的方法
JP5226710B2 (ja) * 2010-02-01 2013-07-03 三井造船株式会社 高粘度重合液中の揮発性物質回収装置
US9192877B2 (en) 2010-12-10 2015-11-24 Angus Chemical Company Apparatus and process for using a nitroalkane as an entrainer for azeotropic removal of water from aqueous acid solution
US9180384B2 (en) 2010-12-10 2015-11-10 Dow Global Technologies Llc Apparatus and process for using olefin as an azeotropic entrainer for isolating 1,3-DICHLORO-2-propanol from a 2,2′-oxybis (1-chloropropane) waste stream
KR101489098B1 (ko) 2012-01-25 2015-02-02 아사히 가세이 케미칼즈 가부시키가이샤 분리 방법
EP2708525A1 (en) * 2012-09-12 2014-03-19 Solvay SA Process of stripping a liquid medium
CN104761433B (zh) * 2015-04-01 2018-07-20 中国天辰工程有限公司 用于甘油法ech回收二氯丙醇及催化剂的设备和工艺
CN113329799B (zh) * 2019-01-25 2023-04-25 博里利斯股份公司 用于从聚合物反应混合物中分离挥发性化合物的分离装置和方法
US12453930B2 (en) 2021-04-02 2025-10-28 Natural Extraction Systems, LLC Products and methods related to the distillation of molecules from aerosols
WO2022212898A1 (en) * 2021-04-02 2022-10-06 Natural Extraction Systems, LLC Compositions for low-temperature distillation of high-boiling-point molecules

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4634784A (en) * 1984-06-04 1987-01-06 Showa Denko Kabushiki Kaisha Process for production of epichlorohydrin
CN1882522A (zh) * 2003-11-20 2006-12-20 索尔维公司 从甘油生产二氯丙醇的方法,甘油最终来自生物柴油生产中动物脂肪的转化
EP1752435A1 (en) * 2003-11-20 2007-02-14 SOLVAY (Société Anonyme) Process for producing dichloropropanol from glycerol , the glycerol coming eventualy from the manufacture of biodiesel
EP1762556A1 (en) * 2005-05-20 2007-03-14 SOLVAY (Société Anonyme) Process for producing dichloropropanol from glycerol

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE197308C (enExample)
GB9602680D0 (en) * 1996-02-09 1996-04-10 Ici Plc Distillation process
CZ20032346A3 (cs) 2003-09-01 2005-04-13 Spolek Pro Chemickou A Hutní Výrobu,A.S. Způsob přípravy dichlorpropanolů z glycerinu
CN102516205B (zh) 2004-07-21 2016-05-04 兰科知识产权有限责任公司 多羟基化脂族烃或其酯向氯醇的转化
US8173823B2 (en) * 2005-05-20 2012-05-08 Solvay (Société Anonyme) Method for making an epoxide
WO2008128010A1 (en) * 2007-04-12 2008-10-23 Dow Global Technologies Inc. Process and apparatus for recovery of dichlorohydrins via codistillation
WO2008128004A1 (en) 2007-04-12 2008-10-23 Dow Global Technologies Inc. Multi-stage process and apparatus for recovering dichlorohydrins

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4634784A (en) * 1984-06-04 1987-01-06 Showa Denko Kabushiki Kaisha Process for production of epichlorohydrin
CN1882522A (zh) * 2003-11-20 2006-12-20 索尔维公司 从甘油生产二氯丙醇的方法,甘油最终来自生物柴油生产中动物脂肪的转化
EP1752435A1 (en) * 2003-11-20 2007-02-14 SOLVAY (Société Anonyme) Process for producing dichloropropanol from glycerol , the glycerol coming eventualy from the manufacture of biodiesel
EP1762556A1 (en) * 2005-05-20 2007-03-14 SOLVAY (Société Anonyme) Process for producing dichloropropanol from glycerol

Also Published As

Publication number Publication date
EP2137121A1 (en) 2009-12-30
JP2010523698A (ja) 2010-07-15
CN101657403A (zh) 2010-02-24
TWI432407B (zh) 2014-04-01
US8664453B2 (en) 2014-03-04
WO2008128004A1 (en) 2008-10-23
US20100137652A1 (en) 2010-06-03
TW200904786A (en) 2009-02-01
KR20100016452A (ko) 2010-02-12

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Address after: American Michigan

Patentee after: Dow Global Technologies Llc

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Patentee before: Dow Global Technologies Inc.

TR01 Transfer of patent right

Effective date of registration: 20151224

Address after: American Michigan

Patentee after: BLUE CUBE IP LLC

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Patentee before: Dow Global Technologies Llc

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140730

Termination date: 20170411

CF01 Termination of patent right due to non-payment of annual fee