CN101657253B - 大的单晶金刚石 - Google Patents

大的单晶金刚石 Download PDF

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Publication number
CN101657253B
CN101657253B CN2008800121066A CN200880012106A CN101657253B CN 101657253 B CN101657253 B CN 101657253B CN 2008800121066 A CN2008800121066 A CN 2008800121066A CN 200880012106 A CN200880012106 A CN 200880012106A CN 101657253 B CN101657253 B CN 101657253B
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CN
China
Prior art keywords
single crystal
growth
crystal diamond
seed
diamond material
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CN2008800121066A
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English (en)
Chinese (zh)
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CN101657253A (zh
Inventor
C·N·多德格
R·A·斯皮茨
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Element Six Ltd
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Element Six Ltd
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    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B25/00—Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
    • C30B25/02—Epitaxial-layer growth
    • C30B25/18—Epitaxial-layer growth characterised by the substrate
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/06—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies
    • B01J3/062—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies characterised by the composition of the materials to be processed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2203/00—Processes utilising sub- or super atmospheric pressure
    • B01J2203/06—High pressure synthesis
    • B01J2203/0605—Composition of the material to be processed
    • B01J2203/061—Graphite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2203/00—Processes utilising sub- or super atmospheric pressure
    • B01J2203/06—High pressure synthesis
    • B01J2203/0605—Composition of the material to be processed
    • B01J2203/062—Diamond
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2203/00—Processes utilising sub- or super atmospheric pressure
    • B01J2203/06—High pressure synthesis
    • B01J2203/065—Composition of the material produced
    • B01J2203/0655—Diamond
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2203/00—Processes utilising sub- or super atmospheric pressure
    • B01J2203/06—High pressure synthesis
    • B01J2203/0675—Structural or physico-chemical features of the materials processed
    • B01J2203/068—Crystal growth
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/24—Structurally defined web or sheet [e.g., overall dimension, etc.]
    • Y10T428/24942—Structurally defined web or sheet [e.g., overall dimension, etc.] including components having same physical characteristic in differing degree
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/30—Self-sustaining carbon mass or layer with impregnant or other layer

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Nonmetal Cutting Devices (AREA)
CN2008800121066A 2007-03-08 2008-03-07 大的单晶金刚石 Active CN101657253B (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
GBGB0704516.4A GB0704516D0 (en) 2007-03-08 2007-03-08 Diamond
GB0704516.4 2007-03-08
US89492007P 2007-03-15 2007-03-15
US60/894,920 2007-03-15
PCT/IB2008/050851 WO2008107860A2 (en) 2007-03-08 2008-03-07 Large single crystal diamonds

Publications (2)

Publication Number Publication Date
CN101657253A CN101657253A (zh) 2010-02-24
CN101657253B true CN101657253B (zh) 2013-01-23

Family

ID=37988627

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2008800121066A Active CN101657253B (zh) 2007-03-08 2008-03-07 大的单晶金刚石

Country Status (6)

Country Link
US (2) US8574535B2 (https=)
EP (1) EP2125188B1 (https=)
JP (1) JP5522606B2 (https=)
CN (1) CN101657253B (https=)
GB (1) GB0704516D0 (https=)
WO (1) WO2008107860A2 (https=)

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GB0704516D0 (en) 2007-03-08 2007-04-18 Element Six Ltd Diamond
US20090260396A1 (en) * 2008-04-16 2009-10-22 Eitan Broukman Methods for processing ornamental diamonds and corresponding ornamental diamonds
GB0900771D0 (en) * 2009-01-16 2009-03-04 Element Six Ltd Diamond
US20100272627A1 (en) * 2009-04-23 2010-10-28 Chien-Min Sung Multi-Faceted Diamond and Associated Methods
GB201107730D0 (en) * 2011-05-10 2011-06-22 Element Six Ltd Diamond sensors, detectors and quantum devices
EP2791386B1 (en) * 2011-12-16 2018-10-03 Element Six Technologies Limited Large area optical quality synthetic polycrystalline diamond window
KR101299136B1 (ko) * 2012-02-08 2013-08-22 한국과학기술연구원 다이아몬드 열방산체 및 그 제조방법
GB201204533D0 (en) * 2012-03-15 2012-04-25 Element Six Ltd Process for manufacturing synthetic single crystal diamond material
GB201320304D0 (en) * 2013-11-18 2014-01-01 Element Six Ltd Methods of fabricating synthetic diamond materials using microwave plasma actived chemical vapour deposition techniques and products obtained using said
US9823313B2 (en) 2016-01-21 2017-11-21 Lockheed Martin Corporation Diamond nitrogen vacancy sensor with circuitry on diamond
US9835693B2 (en) 2016-01-21 2017-12-05 Lockheed Martin Corporation Higher magnetic sensitivity through fluorescence manipulation by phonon spectrum control
US9910104B2 (en) 2015-01-23 2018-03-06 Lockheed Martin Corporation DNV magnetic field detector
US9910105B2 (en) 2014-03-20 2018-03-06 Lockheed Martin Corporation DNV magnetic field detector
US9817081B2 (en) 2016-01-21 2017-11-14 Lockheed Martin Corporation Magnetometer with light pipe
US9638821B2 (en) 2014-03-20 2017-05-02 Lockheed Martin Corporation Mapping and monitoring of hydraulic fractures using vector magnetometers
US10012704B2 (en) 2015-11-04 2018-07-03 Lockheed Martin Corporation Magnetic low-pass filter
US9541610B2 (en) 2015-02-04 2017-01-10 Lockheed Martin Corporation Apparatus and method for recovery of three dimensional magnetic field from a magnetic detection system
US9853837B2 (en) 2014-04-07 2017-12-26 Lockheed Martin Corporation High bit-rate magnetic communication
US9614589B1 (en) 2015-12-01 2017-04-04 Lockheed Martin Corporation Communication via a magnio
US9557391B2 (en) 2015-01-23 2017-01-31 Lockheed Martin Corporation Apparatus and method for high sensitivity magnetometry measurement and signal processing in a magnetic detection system
US10168393B2 (en) 2014-09-25 2019-01-01 Lockheed Martin Corporation Micro-vacancy center device
CA2945016A1 (en) 2014-04-07 2015-10-15 Lockheed Martin Corporation Energy efficient controlled magnetic field generator circuit
CN106163652B (zh) * 2014-10-11 2019-02-01 河南飞孟金刚石工业有限公司 一种表面粗糙金刚石的合成方法
WO2016190909A2 (en) 2015-01-28 2016-12-01 Lockheed Martin Corporation Magnetic navigation methods and systems utilizing power grid and communication network
BR112017016261A2 (pt) 2015-01-28 2018-03-27 Lockheed Martin Corporation carga de energia in situ
GB2550809A (en) 2015-02-04 2017-11-29 Lockheed Corp Apparatus and method for estimating absolute axes' orientations for a magnetic detection system
CN105327654A (zh) * 2015-10-23 2016-02-17 重庆天宇弘锋新材料科技有限责任公司 一种生命钻石的制备工艺
GB2560283A (en) 2015-11-20 2018-09-05 Lockheed Corp Apparatus and method for closed loop processing for a magnetic detection system
WO2017087014A1 (en) 2015-11-20 2017-05-26 Lockheed Martin Corporation Apparatus and method for hypersensitivity detection of magnetic field
WO2017123261A1 (en) 2016-01-12 2017-07-20 Lockheed Martin Corporation Defect detector for conductive materials
WO2017127098A1 (en) 2016-01-21 2017-07-27 Lockheed Martin Corporation Diamond nitrogen vacancy sensed ferro-fluid hydrophone
GB2562193B (en) 2016-01-21 2021-12-22 Lockheed Corp Diamond nitrogen vacancy sensor with common RF and magnetic fields generator
WO2017127096A1 (en) 2016-01-21 2017-07-27 Lockheed Martin Corporation Diamond nitrogen vacancy sensor with dual rf sources
WO2017127079A1 (en) 2016-01-21 2017-07-27 Lockheed Martin Corporation Ac vector magnetic anomaly detection with diamond nitrogen vacancies
GB2562958A (en) 2016-01-21 2018-11-28 Lockheed Corp Magnetometer with a light emitting diode
US10345396B2 (en) 2016-05-31 2019-07-09 Lockheed Martin Corporation Selected volume continuous illumination magnetometer
US10345395B2 (en) 2016-12-12 2019-07-09 Lockheed Martin Corporation Vector magnetometry localization of subsurface liquids
US10330744B2 (en) 2017-03-24 2019-06-25 Lockheed Martin Corporation Magnetometer with a waveguide
US10338163B2 (en) 2016-07-11 2019-07-02 Lockheed Martin Corporation Multi-frequency excitation schemes for high sensitivity magnetometry measurement with drift error compensation
US10408890B2 (en) 2017-03-24 2019-09-10 Lockheed Martin Corporation Pulsed RF methods for optimization of CW measurements
US10677953B2 (en) 2016-05-31 2020-06-09 Lockheed Martin Corporation Magneto-optical detecting apparatus and methods
US10145910B2 (en) 2017-03-24 2018-12-04 Lockheed Martin Corporation Photodetector circuit saturation mitigation for magneto-optical high intensity pulses
US20170343621A1 (en) 2016-05-31 2017-11-30 Lockheed Martin Corporation Magneto-optical defect center magnetometer
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US10527746B2 (en) 2016-05-31 2020-01-07 Lockheed Martin Corporation Array of UAVS with magnetometers
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US10228429B2 (en) 2017-03-24 2019-03-12 Lockheed Martin Corporation Apparatus and method for resonance magneto-optical defect center material pulsed mode referencing
US10317279B2 (en) 2016-05-31 2019-06-11 Lockheed Martin Corporation Optical filtration system for diamond material with nitrogen vacancy centers
US10359479B2 (en) 2017-02-20 2019-07-23 Lockheed Martin Corporation Efficient thermal drift compensation in DNV vector magnetometry
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US10371765B2 (en) 2016-07-11 2019-08-06 Lockheed Martin Corporation Geolocation of magnetic sources using vector magnetometer sensors
GB201620413D0 (en) * 2016-12-01 2017-01-18 Element Six Tech Ltd Single crystal synthetic diamond material via chemical vapour deposition
US10379174B2 (en) 2017-03-24 2019-08-13 Lockheed Martin Corporation Bias magnet array for magnetometer
US10371760B2 (en) 2017-03-24 2019-08-06 Lockheed Martin Corporation Standing-wave radio frequency exciter
US10338164B2 (en) 2017-03-24 2019-07-02 Lockheed Martin Corporation Vacancy center material with highly efficient RF excitation
US10459041B2 (en) 2017-03-24 2019-10-29 Lockheed Martin Corporation Magnetic detection system with highly integrated diamond nitrogen vacancy sensor
CN107675249B (zh) * 2017-09-08 2020-07-07 西安电子科技大学 单晶金刚石的扩径生长方法
EP4317544A4 (en) * 2021-03-31 2024-08-28 Sumitomo Electric Industries, Ltd. MONOCRYSTALLINE DIAMOND AND DIAMOND COMPOSITE COMPRISING IT
GB202305972D0 (en) * 2023-04-24 2023-06-07 Element Six Tech Ltd Method of manufacturing single crystal diamonds
WO2025182850A1 (ja) * 2024-02-28 2025-09-04 住友電気工業株式会社 ダイヤモンドスピンセンサおよびその製造方法

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EP0136408A1 (en) * 1983-07-01 1985-04-10 Sumitomo Electric Industries Limited Synthetic diamond heat sink
CN88103598A (zh) * 1987-05-08 1988-12-07 住友电气工业株式会社 合成大尺寸金刚石的方法
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Also Published As

Publication number Publication date
GB0704516D0 (en) 2007-04-18
US9034296B2 (en) 2015-05-19
WO2008107860A2 (en) 2008-09-12
US20100119790A1 (en) 2010-05-13
WO2008107860A3 (en) 2008-10-30
JP2010520146A (ja) 2010-06-10
EP2125188A2 (en) 2009-12-02
US20140020620A1 (en) 2014-01-23
CN101657253A (zh) 2010-02-24
EP2125188B1 (en) 2017-11-15
US8574535B2 (en) 2013-11-05
JP5522606B2 (ja) 2014-06-18

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