CN101654346A - Preparation method of noctilucent sand stone - Google Patents
Preparation method of noctilucent sand stone Download PDFInfo
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- CN101654346A CN101654346A CN200910192307A CN200910192307A CN101654346A CN 101654346 A CN101654346 A CN 101654346A CN 200910192307 A CN200910192307 A CN 200910192307A CN 200910192307 A CN200910192307 A CN 200910192307A CN 101654346 A CN101654346 A CN 101654346A
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Abstract
The invention discloses a preparation method of a noctilucent color sand stone, comprising the following steps: (1) taking a plurality of high-luminousness materials and smashing into high-luminousness materials of 5-200 meshes, and then fine screening to obtain semi-finished product sand materials of 5-140 meshes; (2) adding the semi-finished product sand materials, water and steel balls into a ball mill together or ball-milling to obtain ball-milled sand materials, cleaning the ball-milled sand materials with water and putting in a drying box for drying; (3) adding the dried ball-milled sandmaterials into a stirrer for stirring to prepare mixed materials, and sequentially adding color concentrates, noctilucent powder, a binding agent and a polishing agent during stirring; (4) placing the mixed materials in the drying box for drying to obtain the noctilucent color sand stone. The noctilucent color sand stone prepared by the method has very good noctilucent effect and very rich colorsand is suitable for multiple occasions.
Description
Technical field
The present invention relates to a kind of preparation method of noctilucent sand stone.
Background technology
At present, rostone more and more is subjected to people's welcome, because rostone is a kind of novel finishing material, art painting material, toy for children material and artwork work material, yet common rostone does not have the characteristics of noctilucence, restricted further developing of it.The technology of luminescent powder with the effect that reaches noctilucence also appearred smearing on the rostone surface on the market, yet the luminous effect of the Noctilucent artificial stone that this technology is worked it out is relatively poor, photochromic comparatively single, be unfavorable for making other products, and luminescent powder waterproof scarcely, therefore be not suitable for moist environment yet.
Summary of the invention
The preparation method who the purpose of this invention is to provide a kind of noctilucent sand stone, the noctilucent sand stone luminous effect for preparing is fine, and color is very abundant, is applicable to multiple occasion.
For achieving the above object, technical scheme of the present invention is:
A kind of preparation method of noctilucent sand stone may further comprise the steps:
(1) it is some to get the high transmission rate material, and the high transmission rate material is crushed to 5～200 orders, carries out the fine screen branch again and makes 5～140 order work in-process sand material.
(2) work in-process sand material, water, steel ball are added the ball mill ball milling together and make ball milling sand material, will put into oven for drying after the elutriation totally of ball milling sand material water;
(3) dried ball-milled sand material is added stirrer and stir and make compound, add look essence, luminescent powder, tamanori and rumbling compound in the time of stirring successively;
(4) compound is put into oven for drying, obtain noctilucent sand stone.
Alternatively, in the step of the present invention (1), at first the high transmission rate material is put into jaw crusher during pulverizing and pulverize, be crushed to 5～200 orders with sand shaker then, fine screen timesharing employing multilayer is revolved the sieve apparatus that shakes and is carried out the fine screen branch.
Alternatively, in the step of the present invention (1), described high transmission rate material be quartz sand, calcite, glass, sodium fluoroaluminate, bar wherein one or more.
Alternatively, in the step of the present invention (2), the ball milling time is 4～8 hours, and the weight ratio that steel ball accounts for ball milling sand material is 20～40%, and the weight ratio that water accounts for ball milling sand material is 20～35%.
Alternatively, in the step of the present invention (3), look smart weight ratio with ball milling sand material is 0.005～0.02: 1.
Alternatively, in the step of the present invention (3), the weight ratio of luminescent powder and ball milling sand material is 0.2～0.4: 1; Described luminescent powder is long afterglow luminous powder.
Alternatively, in the step of the present invention (3), the weight ratio that tamanori accounts for compound is 5%～7%; Described tamanori is a unsaturated polyester.
Alternatively, in the step of the present invention (3), the ratio of the weight of the volume of rumbling compound and ball milling sand material is 0.01～0.03: 1; Described rumbling compound is a whiteruss.
Alternatively, in the step of the present invention (3), stirrer is the colour mixture stirrer, and the rotating speed of colour mixture stirrer is 1000～3000 rev/mins, and churning time is 5～30 minutes.
Alternatively, in the step of the present invention (4), baking oven is an automated temperature control oven, and drying time is 3～8 hours, and the temperature during oven dry is 80～120 ℃.
Therefore compared with prior art, the present invention has following beneficial effect:
(1) the present invention adopts the more more common calcite of occurring in nature, quartzite, and high transmission rate materials such as sodium fluoroaluminate, barite, cullet are as raw material, and transmittance and specific refractory power are all very high, the material choice wide range;
(2) unsaturated polyester of the present invention has high adherence, can bonding well luminescent powder and other components, and the prepared noctilucent sand stone that goes out is water insoluble, can be applicable to moist environment, has enlarged use range;
Also added look essence when (3) the present invention adopts luminescent powder, greatly enriched the color kind of noctilucent sand stone with multicolour, very attractive in appearance;
(4) long afterglow luminous powder of the present invention does not comprise the radiativity material, and does not produce the waste gas waste material aborning, can not cause environmental pollution, very environmental protection, and also production process is simple, operation easily, and production cost is lower.
Embodiment
Describe the present invention in detail below in conjunction with specific embodiment, be used for explaining the present invention in this illustrative examples of the present invention and explanation, but not as a limitation of the invention.
Embodiment 1
Prepare noctilucent sand stone according to the following step:
(1) takes by weighing quartz sand, quartz sand is put into jaw crusher pulverize, be crushed to 5～200 orders with sand shaker then, put into multilayer again and revolve the sieve apparatus that shakes and carry out the fine screen branch and make the work in-process sand material that comprises 5～140 order all sizes.
(2) work in-process sand material, water, steel ball were added the ball mill ball milling 5 hours together, make ball milling sand material, wherein to account for the weight ratio of ball milling sand material be 30% to steel ball, and the weight ratio that water accounts for ball milling sand material is 25%, then ball milling sand material water is eluriated totally, put into oven for drying after elutriation is clean fully;
(3) complete dried ball-milled sand material being added the colour mixture stirrer stirs and makes compound, add look essence, long afterglow luminous powder, unsaturated polyester and whiteruss when stirring successively, wherein look smart weight ratio with ball milling sand material is 0.01: 1, the weight ratio of long afterglow luminous powder and ball milling sand material is 0.3: 1, the weight ratio that unsaturated polyester accounts for compound is 6%, the ratio of the weight of the volume of whiteruss and ball milling sand material is 0.02: 1, the rotating speed of colour mixture stirrer is 2000 rev/mins, and churning time is 20 minutes;
(4) compound is put into the automated temperature control oven oven dry and obtained noctilucent sand stone in 6 hours, the temperature during oven dry is 100 ℃.
Embodiment 2
Prepare noctilucent sand stone according to the following step:
(1) takes by weighing calcite, calcite is put into jaw crusher pulverize, be crushed to 5～200 orders with sand shaker then, put into multilayer again and revolve the sieve apparatus that shakes and carry out the fine screen branch and make the work in-process sand material that comprises 5～140 order all sizes.
(2) work in-process sand material, water, steel ball were added the ball mill ball milling 4 hours together, make ball milling sand material, wherein to account for the weight ratio of ball milling sand material be 20% to steel ball, and the weight ratio that water accounts for ball milling sand material is 20%, then ball milling sand material water is eluriated totally, put into oven for drying after elutriation is clean fully;
(3) complete dried ball-milled sand material being added the colour mixture stirrer stirs and makes compound, add look essence, long afterglow luminous powder, unsaturated polyester and whiteruss when stirring successively, wherein look smart weight ratio with ball milling sand material is 0.005: 1, the weight ratio of long afterglow luminous powder and ball milling sand material is 0.2: 1, the weight ratio that unsaturated polyester accounts for compound is 5%, the ratio of the weight of the volume of whiteruss and ball milling sand material is 0.01: 1, the rotating speed of colour mixture stirrer is 1000 rev/mins, and churning time is 30 minutes;
(4) compound is put into the automated temperature control oven oven dry and obtained noctilucent sand stone in 3 hours, the temperature during oven dry is 80 ℃.
Embodiment 3
Prepare noctilucent sand stone according to the following step:
(1) takes by weighing glass, glass is put into jaw crusher pulverize, be crushed to 5～200 orders with sand shaker then, put into multilayer again and revolve the sieve apparatus that shakes and carry out the fine screen branch and make the work in-process sand material that comprises 5～140 order all sizes.
(2) work in-process sand material, water, steel ball were added the ball mill ball milling 8 hours together, make ball milling sand material, wherein to account for the weight ratio of ball milling sand material be 40% to steel ball, and the weight ratio that water accounts for ball milling sand material is 35%, then ball milling sand material water is eluriated totally, put into oven for drying after elutriation is clean fully;
(3) complete dried ball-milled sand material being added the colour mixture stirrer stirs and makes compound, add look essence, long afterglow luminous powder, unsaturated polyester and whiteruss when stirring successively, wherein look smart weight ratio with ball milling sand material is 0.02: 1, the weight ratio of long afterglow luminous powder and ball milling sand material is 0.4: 1, the weight ratio that unsaturated polyester accounts for compound is 7%, the ratio of the weight of the volume of whiteruss and ball milling sand material is 0.03: 1, the rotating speed of colour mixture stirrer is 3000 rev/mins, and churning time is 5 minutes;
(4) compound is put into the automated temperature control oven oven dry and obtained noctilucent sand stone in 8 hours, the temperature during oven dry is 120 ℃.
Embodiment 4
Prepare noctilucent sand stone according to the following step:
(1) takes by weighing sodium fluoroaluminate, sodium fluoroaluminate is put into jaw crusher pulverize, be crushed to 5～200 orders with sand shaker then, put into multilayer again and revolve the sieve apparatus that shakes and carry out the fine screen branch and make the work in-process sand material that comprises 5～140 order all sizes.
(2) work in-process sand material, water, steel ball were added the ball mill ball milling 7 hours together, make ball milling sand material, wherein to account for the weight ratio of ball milling sand material be 24% to steel ball, and the weight ratio that water accounts for ball milling sand material is 32%, then ball milling sand material water is eluriated totally, put into oven for drying after elutriation is clean fully;
(3) complete dried ball-milled sand material being added the colour mixture stirrer stirs and makes compound, add look essence, long afterglow luminous powder, unsaturated polyester and whiteruss when stirring successively, wherein look smart weight ratio with ball milling sand material is 0.018: 1, the weight ratio of long afterglow luminous powder and ball milling sand material is 0.24: 1, the weight ratio that unsaturated polyester accounts for compound is 5.6%, the ratio of the weight of the volume of whiteruss and ball milling sand material is 0.016: 1, the rotating speed of colour mixture stirrer is 1600 rev/mins, and churning time is 25 minutes;
(4) compound is put into the automated temperature control oven oven dry and obtained noctilucent sand stone in 7 hours, the temperature during oven dry is 105 ℃.
Embodiment 5
Prepare noctilucent sand stone according to the following step:
(1) takes by weighing barite, barite is put into jaw crusher pulverize, be crushed to 5～200 orders with sand shaker then, put into multilayer again and revolve the sieve apparatus that shakes and carry out the fine screen branch and make the work in-process sand material that comprises 5～140 order all sizes.
(2) work in-process sand material, water, steel ball were added the ball mill ball milling 5.5 hours together, make ball milling sand material, wherein to account for the weight ratio of ball milling sand material be 32% to steel ball, and the weight ratio that water accounts for ball milling sand material is 32%, with ball milling sand material ditch wash clean, put into oven for drying after elutriation is clean fully then;
(3) complete dried ball-milled sand material being added the colour mixture stirrer stirs and makes compound, add look essence, long afterglow luminous powder, unsaturated polyester and whiteruss when stirring successively, wherein look smart weight ratio with ball milling sand material is 0.018: 1, the weight ratio of long afterglow luminous powder and ball milling sand material is 0.32: 1, the weight ratio that unsaturated polyester accounts for compound is 6.4%, the ratio of the weight of the volume of whiteruss and ball milling sand material is 0.024: 1, the rotating speed of colour mixture stirrer is 2400 rev/mins, and churning time is 18 minutes;
(4) compound is put into the automated temperature control oven oven dry and obtained noctilucent sand stone in 7.5 hours, the temperature during oven dry is 95 ℃.
Embodiment 6
Prepare noctilucent sand stone according to the following step:
(1) be 1: 1: 1 by weight: 1: 1 ratio takes by weighing quartz sand, calcite, glass, sodium fluoroaluminate, barite, putting into jaw crusher pulverizes, be crushed to 5～200 orders with sand shaker then, put into multilayer again and revolve the sieve apparatus that shakes and carry out the fine screen branch and make the work in-process sand material that comprises 5～140 order all sizes.
(2) work in-process sand material, water, steel ball were added the ball mill ball milling 6 hours together, make ball milling sand material, wherein to account for the weight ratio of ball milling sand material be 35% to steel ball, and the weight ratio that water accounts for ball milling sand material is 30%, then ball milling sand material water is eluriated totally, put into oven for drying after elutriation is clean fully;
(3) complete dried ball-milled sand material being added the colour mixture stirrer stirs and makes compound, add look essence, long afterglow luminous powder, unsaturated polyester and whiteruss when stirring successively, wherein look smart weight ratio with ball milling sand material is 0.015: 1, the weight ratio of long afterglow luminous powder and ball milling sand material is 0.35: 1, the weight ratio that unsaturated polyester accounts for compound is 6.5%, the ratio of the weight of the volume of whiteruss and ball milling sand material is 0.025: 1, the rotating speed of colour mixture stirrer is 2500 rev/mins, and churning time is 16 minutes;
(4) compound is put into oven for drying and obtained noctilucent sand stone in 7 hours, the temperature during oven dry is 110 ℃.
More than the technical scheme that the embodiment of the invention provided is described in detail, used specific case herein the principle and the embodiment of the embodiment of the invention are set forth, the explanation of above embodiment only is applicable to the principle that helps to understand the embodiment of the invention; Simultaneously, for one of ordinary skill in the art, according to the embodiment of the invention, the part that on embodiment and range of application, all can change, in sum, this description should not be construed as limitation of the present invention.
Claims (10)
1, a kind of preparation method of noctilucent sand stone is characterized in that this method may further comprise the steps:
(1) it is some to get the high transmission rate material, and the high transmission rate material is crushed to 5～200 orders, carries out the fine screen branch again and makes 5～140 order work in-process sand material;
(2) work in-process sand material, water, steel ball are added the ball mill ball milling together and make ball milling sand material, will put into oven for drying after the elutriation totally of ball milling sand material water;
(3) dried ball-milled sand material is added stirrer and stir and make compound, add look essence, luminescent powder, tamanori and rumbling compound in the time of stirring successively;
(4) compound is put into oven for drying, obtain noctilucent sand stone.
2, the preparation method of a kind of noctilucent sand stone according to claim 1, it is characterized in that: in the described step (1), at first the high transmission rate material being put into jaw crusher during pulverizing pulverizes, be crushed to 5～200 orders with sand shaker then, fine screen timesharing employing multilayer is revolved the sieve apparatus that shakes and is carried out the fine screen branch.
3, the preparation method of a kind of noctilucent sand stone according to claim 1 is characterized in that: in the described step (1), described high transmission rate material be quartz sand, calcite, glass, sodium fluoroaluminate, bar wherein one or more.
4, the preparation method of a kind of noctilucent sand stone according to claim 1 is characterized in that: in the described step (2), the ball milling time is 4～8 hours, and the weight ratio that steel ball accounts for ball milling sand material is 20～40%, and the weight ratio that water accounts for ball milling sand material is 20～35%.
5, the preparation method of the color silicon stone of a kind of noctilucence according to claim 1 is characterized in that: in the described step (3), look smart weight ratio with ball milling sand material is 0.005～0.02: 1.
6, the preparation method of a kind of noctilucent sand stone according to claim 1 is characterized in that: in the described step (3), the weight ratio of luminescent powder and ball milling sand material is 0.2～0.4: 1; Described luminescent powder is long afterglow luminous powder.
7, the preparation method of a kind of noctilucent sand stone according to claim 1 is characterized in that: in the described step (3), the weight ratio that tamanori accounts for compound is 5%～7%; Described tamanori is a unsaturated polyester.
8, the preparation method of a kind of noctilucent sand stone according to claim 1 is characterized in that: in the described step (3), the ratio of the weight of the volume of rumbling compound and ball milling sand material is 0.01～0.03: 1; Described rumbling compound is a whiteruss.
9, the preparation method of a kind of noctilucent sand stone according to claim 1 is characterized in that: in the described step (3), stirrer is the colour mixture stirrer, and the rotating speed of colour mixture stirrer is 1000～3000 rev/mins, and churning time is 5～30 minutes.
10, the preparation method of a kind of noctilucent sand stone according to claim 1 is characterized in that: in the described step (4), baking oven is an automated temperature control oven, and drying time is 3～8 hours, and the temperature during oven dry is 80～120 ℃.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910192307A CN101654346A (en) | 2009-09-11 | 2009-09-11 | Preparation method of noctilucent sand stone |
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| CN200910192307A CN101654346A (en) | 2009-09-11 | 2009-09-11 | Preparation method of noctilucent sand stone |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102464460A (en) * | 2010-11-16 | 2012-05-23 | 王明军 | Colored sand and preparation method thereof |
| CN106583000A (en) * | 2016-12-22 | 2017-04-26 | 浙江叶力机械制造有限公司 | Crushing production line |
| CN108724453A (en) * | 2018-04-27 | 2018-11-02 | 合肥海银杆塔有限公司 | A kind of processing method of self-luminous cement shaft tower |
| CN110436831A (en) * | 2019-06-26 | 2019-11-12 | 河北晨阳工贸集团有限公司 | A kind of lacquer and preparation method thereof |
-
2009
- 2009-09-11 CN CN200910192307A patent/CN101654346A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102464460A (en) * | 2010-11-16 | 2012-05-23 | 王明军 | Colored sand and preparation method thereof |
| CN106583000A (en) * | 2016-12-22 | 2017-04-26 | 浙江叶力机械制造有限公司 | Crushing production line |
| CN108724453A (en) * | 2018-04-27 | 2018-11-02 | 合肥海银杆塔有限公司 | A kind of processing method of self-luminous cement shaft tower |
| CN110436831A (en) * | 2019-06-26 | 2019-11-12 | 河北晨阳工贸集团有限公司 | A kind of lacquer and preparation method thereof |
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Application publication date: 20100224 |