CN101647812A - Method for extracting deer antler extract continuously and quickly at normal temperature - Google Patents

Method for extracting deer antler extract continuously and quickly at normal temperature Download PDF

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Publication number
CN101647812A
CN101647812A CN200810051079A CN200810051079A CN101647812A CN 101647812 A CN101647812 A CN 101647812A CN 200810051079 A CN200810051079 A CN 200810051079A CN 200810051079 A CN200810051079 A CN 200810051079A CN 101647812 A CN101647812 A CN 101647812A
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China
Prior art keywords
cornu cervi
extract
cervi pantotrichum
extraction
raw material
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CN200810051079A
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Chinese (zh)
Inventor
赵景辉
王英平
潘永岐
孙长伟
赵伟刚
徐志臣
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赵景辉
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Priority to CN200810051079A priority Critical patent/CN101647812A/en
Publication of CN101647812A publication Critical patent/CN101647812A/en
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Abstract

The invention relates to a method for extracting deer antler extract continuously and quickly at normal temperature, which is characterized in that 40 to 70 percent ethanol is used as an extraction solvent, and nutrient substances are continuously extracted from the deer antler at the normal temperature by adopting a high-voltage pulse electric field. The specific process steps comprise material selection, finishing, slicing, crushing, weighing, soaking, standing, extraction (according to the field strength of 20 to 30 kilovolts, the pulse number of 4 to 8 and the solid-liquid ratio of 1 to 10), filtration, compression, drying and packing and product obtaining. The method has the characteristics of novel technique, normal-temperature continuous extraction, high extraction rate, sterilization function in the extraction process, high bioavailability, short extraction time, low cost, and the like.

Description

A kind of method of extracting deer antler extract continuously and quickly at normal temperature
Technical field:
The present invention relates to a kind of method of extracting deer antler extract continuously and quickly at normal temperature, particularly relate to a kind of method that adopts high-voltage pulse electric field from Cornu Cervi Pantotrichum, to extract nutrient substance.
Background technology:
Raise 6,000,000 of deer at present in the world, about 1,000,000 of China artificial breeding produces Cornu Cervi Pantotrichum per year and reaches ten thousand kilograms of 7-8.Compendium of Material Medica record, Cornu Cervi Pantotrichum have spermatogenesis to mend marrow, the Yiyang of nourishing blood, strengthening the tendons and bones, the strong will of QI invigorating, control deafness, tinnitus, sexual impotence, seminal emission, deficiency-cold of uterus, bleeding not during menses and effect that all are deficient.Modern study proves: Cornu Cervi Pantotrichum has to be regulated organism metabolism, physical strength reinforcing, improve hemopoietic function, promotes growth promoter, the human body immunity improving ability, promote function such as various physiological function activities, is one of the famousst and precious animal drugs.
Closed compositions such as phospholipid, glycolipid, glue fat, hormone, fatty acid, aminoacid, protein and inorganic elements in the Cornu Cervi Pantotrichum, still, these compositions are not the special compositions of Cornu Cervi Pantotrichum.The significant active component of Cornu Cervi Pantotrichum is not clear at present.
The antler health-care product are a lot, but kind is less.Mainly contain piece of antler, deer antler wine, pantocrine, pilose antler tea, pantocrin oral liquid, Cornu Cervi Pantotrichum chewing gum etc.Inconvenience is taken and carried to the said goods ubiquity, can not effectively absorb, and can not embody its special efficacy, the not high shortcoming of scientific and technological content.Therefore, with the Cornu Cervi Pantotrichum to be that development of raw materials goes out high in technological content, superior in quality, taste and nutrition are all good, take the high-grade nutrient health care product with high-end health care easy to carry, anti-disease, anti-aging, enhancing immunity, particularly important with the demand that satisfies consumers in general.
Summary of the invention:
The object of the present invention is to provide a kind of method of extracting deer antler extract continuously and quickly at normal temperature, be to adopt high-voltage pulse electric field from Cornu Cervi Pantotrichum, to extract the method for nutrient substance, it is to utilize different molecular to produce the principle of different polarization reactions under the high-strength electric field effect that high-voltage pulse electric field extracts, make act in the solvent fast stripping of effective constituent of pilose antler, realize the purpose of extracts active ingredients by electric field force; It has following characteristics: 1. technology novelty, extraction ratio height, and leaching process has bactericidal action; 2. normal-temperature continuous is extracted; 3. extraction time is short, cost is low.
Technical scheme of the present invention is achieved in that a kind of method of extracting deer antler extract continuously and quickly at normal temperature, it is characterized in that: with 40-70% ethanol serves as to extract solvent, adopts high-voltage pulse electric field normal-temperature continuous from Cornu Cervi Pantotrichum to extract nutrient substance; Concrete processing step is as follows:
(1) selects materials: do not select the Cornu Cervi Pantotrichum damaging by worms, pollute as raw material;
(2) arrangement: with no pyrotechnics is that alcohol burner or electric furnace burn the Cornu Cervi Pantotrichum fine hair, then branch is decomposed;
(3) section: with the Cornu Cervi Pantotrichum microtome Cornu Cervi Pantotrichum crosscut is become the fine and soft sheet of 2-4mm;
(4) pulverize: more than raw material pulverizing to 60 order after will cutting with the Baily pulverizer;
(5) weigh, soak: by material: liquid=1: 10 adds raw material and 40-70% ethanol extraction solvent;
(6) static: as, to place 0.5h restir mixing with raw material and after extracting the stirring solvent mixing;
(7) extract: the raw material after will soaking with liquor pump is continuously pumped in the potential pulse extraction unit, and with field intensity 20-30kv, umber of pulse 4-8 is a parameter extraction, collects extracting solution continuously;
(8) filter: extracting solution is pumped into flame filter press filter;
(9) concentrate: filtrate is carried out vacuum concentration to fluid extract;
(10) drying: fluid extract spray drying or lyophilization are become powder;
(11) packing: in the clean dried chamber, powder packed in the plastic packaging bag, seal, warehouse-in.
Good effect of the present invention is: 1. success is applied to high-voltage pulse electric field in the extraction of pilose antler active composition, for similar research is offered reference.2. realize extract at room temperature and sterilization one, reduced the heat-sensitive substance degraded.3. continuously rapid extraction; Extraction ratio is up to more than 80%, energy-saving and environmental protection, efficient.4. bioavailability height; High in technological content.5. extraction time is short, cost is low.
The specific embodiment:
The present invention will be further described below in conjunction with embodiment:
Embodiment 1:
With 40-70% ethanol serves as to extract solvent, adopts high-voltage pulse electric field normal-temperature continuous from Cornu Cervi Pantotrichum to extract nutrient substance; Concrete processing step is as follows:
(1) selects materials: do not select the Cornu Cervi Pantotrichum damaging by worms, pollute as raw material;
(2) arrangement: with no pyrotechnics is that alcohol burner or electric furnace burn the Cornu Cervi Pantotrichum fine hair, then branch is decomposed;
(3) section: the fine and soft sheet that the Cornu Cervi Pantotrichum crosscut is become 2mm with the Cornu Cervi Pantotrichum microtome;
(4) pulverize: raw material pulverizing to 40 order after will cutting with the Baily pulverizer;
(5) weigh, soak: by material: liquid=1: 10 adds raw material and 40% ethanol extraction solvent;
(6) static: as, to place 0.5h restir mixing with raw material and after extracting the stirring solvent mixing;
(7) extract: the raw material after will soaking with liquor pump is continuously pumped in the potential pulse extraction unit, and with field intensity 20kv, umber of pulse 4 is a parameter extraction, collects extracting solution simultaneously;
(8) filter: extracting solution is pumped into flame filter press filter;
(9) concentrate: filtrate is carried out vacuum concentration to fluid extract;
(10) drying: fluid extract spray drying or lyophilization are become powder;
(11) packing: in the clean dried chamber, powder packed in the plastic packaging bag, seal, warehouse-in.
Embodiment 2:
With 40-70% ethanol serves as to extract solvent, adopts high-voltage pulse electric field normal-temperature continuous from Cornu Cervi Pantotrichum to extract nutrient substance; Concrete processing step is as follows:
(1) selects materials: do not select the Cornu Cervi Pantotrichum damaging by worms, pollute as raw material;
(2) arrangement: with no pyrotechnics is that alcohol burner or electric furnace burn the Cornu Cervi Pantotrichum fine hair, then branch is decomposed;
(3) section: the fine and soft sheet that the Cornu Cervi Pantotrichum crosscut is become 3mm with the Cornu Cervi Pantotrichum microtome;
(4) pulverize: raw material pulverizing to 50 order after will cutting with the Baily pulverizer;
(5) weigh, soak: by material: liquid=1: 10 adds raw material and 50% ethanol extraction solvent;
(6) static: as, to place 0.5h restir mixing with raw material and after extracting the stirring solvent mixing;
(7) extract: the raw material after will soaking with liquor pump is continuously pumped in the potential pulse extraction unit, and with field intensity 25kv, umber of pulse 6 is a parameter extraction, collects extracting solution simultaneously;
(8) filter: extracting solution is pumped into flame filter press filter;
(9) concentrate: filtrate is carried out vacuum concentration to fluid extract;
(10) drying: fluid extract spray drying or lyophilization are become powder;
(11) packing: in the clean dried chamber, powder packed in the plastic packaging bag, seal, warehouse-in.
Embodiment 3:
With 40-70% ethanol serves as to extract solvent, adopts high-voltage pulse electric field normal-temperature continuous from Cornu Cervi Pantotrichum to extract nutrient substance; Concrete processing step is as follows:
(1) selects materials: do not select the Cornu Cervi Pantotrichum damaging by worms, pollute as raw material;
(2) arrangement: with no pyrotechnics is that alcohol burner or electric furnace burn the Cornu Cervi Pantotrichum fine hair, then branch is decomposed;
(3) section: the fine and soft sheet that the Cornu Cervi Pantotrichum crosscut is become 4mm with the Cornu Cervi Pantotrichum microtome;
(4) pulverize: raw material pulverizing to 60 order after will cutting with the Baily pulverizer;
(5) weigh, soak: by material: liquid=1: 10 adds raw material and 70% ethanol extraction solvent;
(6) static: as, to place 0.5h restir mixing with raw material and after extracting the stirring solvent mixing;
(7) extract: the raw material after will soaking with liquor pump is continuously pumped in the potential pulse extraction unit, and with field intensity 30kv, umber of pulse 8 is a parameter extraction, collects extracting solution simultaneously;
(8) filter: extracting solution is pumped into flame filter press filter;
(9) concentrate: filtrate is carried out vacuum concentration to fluid extract;
(10) drying: fluid extract spray drying or lyophilization are become powder;
(11) packing: in the clean dried chamber, powder packed in the plastic packaging bag, seal, warehouse-in.

Claims (1)

1, a kind of method of extracting deer antler extract continuously and quickly at normal temperature is characterized in that: with 40-70% ethanol serves as to extract solvent, adopts high-voltage pulse electric field normal-temperature continuous from Cornu Cervi Pantotrichum to extract nutrient substance; Concrete processing step is as follows:
(1) selects materials: do not select the Cornu Cervi Pantotrichum damaging by worms, pollute as raw material;
(2) arrangement: with no pyrotechnics is that alcohol burner or electric furnace burn the Cornu Cervi Pantotrichum fine hair, then branch is decomposed;
(3) section: the fine and soft sheet that the Cornu Cervi Pantotrichum crosscut is become 2-4mm with the Cornu Cervi Pantotrichum microtome;
(4) pulverize: the raw material pulverizing after will cutting with the Baily pulverizer is to the 40-60 order;
(5) weigh, soak: by material: liquid=1: 10 adds raw material and 40-70% ethanol extraction solvent;
(6) static: as, to place 0.5h restir mixing with raw material and after extracting the stirring solvent mixing;
(7) extract: the raw material after will soaking with liquor pump is continuously pumped in the potential pulse extraction unit, and with field intensity 20-30kv, umber of pulse 4-8 is a parameter extraction, collects extracting solution simultaneously;
(8) filter: extracting solution is pumped into flame filter press filter;
(9) concentrate: filtrate is carried out vacuum concentration to fluid extract;
(10) drying: fluid extract spray drying or lyophilization are become powder;
(11) packing: in the clean dried chamber, powder packed in the plastic packaging bag, seal, warehouse-in.
CN200810051079A 2008-08-15 2008-08-15 Method for extracting deer antler extract continuously and quickly at normal temperature Pending CN101647812A (en)

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CN200810051079A CN101647812A (en) 2008-08-15 2008-08-15 Method for extracting deer antler extract continuously and quickly at normal temperature

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN200810051079A CN101647812A (en) 2008-08-15 2008-08-15 Method for extracting deer antler extract continuously and quickly at normal temperature

Publications (1)

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CN101647812A true CN101647812A (en) 2010-02-17

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102440309A (en) * 2010-10-12 2012-05-09 宜昌三峡玉泉寺茶叶有限公司 Manufacturing process for antler organic tea and preparation thereof
CN103281912A (en) * 2010-12-30 2013-09-04 皇家飞利浦电子股份有限公司 Method and apparatus for decocting ingredients in a solvent

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102440309A (en) * 2010-10-12 2012-05-09 宜昌三峡玉泉寺茶叶有限公司 Manufacturing process for antler organic tea and preparation thereof
CN103281912A (en) * 2010-12-30 2013-09-04 皇家飞利浦电子股份有限公司 Method and apparatus for decocting ingredients in a solvent

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Open date: 20100217