CN101550533A - Antistatic optical substrate preparation method - Google Patents

Antistatic optical substrate preparation method Download PDF

Info

Publication number
CN101550533A
CN101550533A CNA200910111751XA CN200910111751A CN101550533A CN 101550533 A CN101550533 A CN 101550533A CN A200910111751X A CNA200910111751X A CN A200910111751XA CN 200910111751 A CN200910111751 A CN 200910111751A CN 101550533 A CN101550533 A CN 101550533A
Authority
CN
China
Prior art keywords
substrate
film layer
refractive index
electrostatic
coating materials
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CNA200910111751XA
Other languages
Chinese (zh)
Other versions
CN101550533B (en
Inventor
杨敏男
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
XIAMEN MELLAN OPTOELECTRONICS TECHNOLOGY Co Ltd
Original Assignee
XIAMEN MELLAN OPTOELECTRONICS TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by XIAMEN MELLAN OPTOELECTRONICS TECHNOLOGY Co Ltd filed Critical XIAMEN MELLAN OPTOELECTRONICS TECHNOLOGY Co Ltd
Priority to CN200910111751XA priority Critical patent/CN101550533B/en
Publication of CN101550533A publication Critical patent/CN101550533A/en
Application granted granted Critical
Publication of CN101550533B publication Critical patent/CN101550533B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Landscapes

  • Surface Treatment Of Optical Elements (AREA)
  • Physical Vapour Deposition (AREA)

Abstract

The invention discloses an antistatic optical substrate preparation method, pertaining to the lens coated optics manufacturing technology. The method includes: cleaning the substrate and then placing in a fine vacuum machine whose vacuum degree is pumped to1*10 [-5] Torr to 5*10 [-5] Torr, depositing a film with alternated high refractivity film layer and low refractivity coating film layer in sequence on the substrate, and then evaporating a super water proof coating material WR5 and then evaporating and placing on the film layer in molecular status to form a new layer of film (wherein, the film thickness is 120-220nm), and then removing the substrate to form an antistatic optical substrate. The optical lens can play an antistatic (electrostatic isolation) role, which is not liable to adsorb dust and can remain cleanly and sanitary for a long time.

Description

The optical substrate preparation method of anti-electrostatic
Technical field
The present invention discloses a kind of optical substrate preparation method of anti-electrostatic, belongs to glasses lens plated optics manufacturing technology field.
Background technology
Static is a kind of objective spontaneous phenomenon, and the mode of generation is multiple, as contact, friction etc.The electrostatic characteristics be high-voltage, low electric weight, little electric current and action time short characteristics.It is the abbreviation of Electro-Static discharge that static discharges.When two kinds of materials, and though be by pressure or by friction contact separately after, the electronics surface of material of will dissociating, thus produce the static district.The material surface that electronics reduces is positive polarity, and the material surface of band excess electron is electronegativity, these two kinds of charged materials can attract the material of paripheral zone opposite charges so that electrically neutralization, if charged materials is an electroconductibility, then static charge very soon can be by material transfer to ground, if material is in press charged, then static charge can be transferred to machine surface.If material is an isolator, then static charge can be missed later on gradually at several hrs, a few week even some months.Electrostatics is mainly studied the static utilisation technology, and as electrostatic precipitation, xerox, static biological effect etc., main is the electrostatic protection technology.Static can be described as ubiquitous in our daily life, on our body and just have very high electrostatic potential on every side, several kilovolts even several ten thousand volts.May know from experience less than the pass by carpet static of chemical fibre of, people at ordinary times approximately is 35000 volts, about 7000 volts of the plastics specification sheets of browsing, and for some responsive instruments, this voltage may be fatal harm.
At present, static electricity on human body's safeguard system mainly contains ESD-preventive wrist strap, the ankle band, and compositions such as working suit, footgear, cap, gloves or fingerstall have static and reveal, functions such as neutralization and shielding.The at present common optical base-substrate through plated film easily adsorbs dust, and the optical base-substrate that does not also have on the market to occur by plated film plays anti-static effect.
Summary of the invention
At the deficiencies in the prior art, the invention provides a kind of optical substrate preparation method of reasonable in design, the simple anti-electrostatic of technology, can play the effect of anti-electrostatic through the optical base-substrate of this processing, and be difficult for the absorption dust, can keep clean the long period.
The present invention is achieved by the following technical solutions:
A kind of optical substrate preparation method of anti-electrostatic, its step is as follows:
After substrate cleans up, be positioned over vacuum tightness and be evacuated to 1x10 -5Torr is to 5x10 -5In the high vacuum board of Torr, evaporation high refractive index film layer and low-refraction coatings alternative rete successively on substrate, then the state of super waterproof Coating Materials WR5 evaporation back with molecule steamed in thin film layer, form new WR5 rete, this WR5 thicknesses of layers is at 120-220nm, and the optical base-substrate of formation anti-electrostatic takes out substrate.
Described low-index film of one deck at least and the mutual interference mutually of one deck high refractive index layer.
Described high refractive index Coating Materials is tantalum pentoxide (Ta 2O 5), titanium dioxide (TiO 2), five oxidation Tritanium/Trititanium (Ti 3O 5) wherein any one, in the mode of resistive heating or electron beam gun flow of emitted electrons with above-mentioned high refractive index Coating Materials tantalum pentoxide (Ta 2O 5), titanium dioxide (TiO 2), five oxidation Tritanium/Trititanium (Ti 3O 5) after wherein any evaporation, steaming on substrate with the state of molecule, form a high refractive index layer.
Described low-index material is silicon-dioxide (SiO 2), in the mode of resistive heating or electron beam gun flow of emitted electrons with low-refraction Coating Materials silicon-dioxide (SiO 2) evaporation back steaming on thin film layer with the state of molecule, forms a low refractive index film layer.
Described super waterproof Coating Materials WR5 is evaporated the back in the mode of resistive heating or electron beam gun flow of emitted electrons and is steaming in thin film layer with the state of molecule, forms new one deck rete, this thicknesses of layers 120-220nm.
Described substrate is a kind of in acryl (AC) substrate, PC polycarbonate substrate (Polycarbonate), nylon (Nylon) substrate, the CR-39 substrate.
After any substrate in the materials such as AC, PC, Nylon, CR-39 cleaned up, be positioned over vacuum tightness then and be evacuated to 3.0*10 at least -5In the high vacuum board of handkerchief, in the mode of resistive heating or electron beam gun flow of emitted electrons with high refractive index Coating Materials Ta 2O 5, TiO 2, Ti 3O 5After wherein any evaporation, steaming on substrate, forming a high refractive index layer with the state of molecule, again in the mode of resistive heating or electron beam gun flow of emitted electrons with low-refraction Coating Materials SiO 2Is steaming on high refractive index layer with the state of molecule the evaporation back, forms a low refractive index film layer, at least one floor height specific refractory power and the mutual interference mutually of one deck low-index film.In the mode of resistive heating or electron beam gun flow of emitted electrons the state of super waterproof Coating Materials WR5 evaporation back with molecule steamed in thin film layer, forming new one deck rete, thicknesses of layers is being 120-220nm.Super waterproof Coating Materials WR5 is produced by Merck KGaA company, buys in city's field energy at present, and this Coating Materials is bragged about and had good waterproof effect.
The present invention has following advantage: common product through plated film, easily adsorb dust, and through this product processed, can play the effect of anti-electrostatic, and be difficult for the absorption dust, can make eyeglass keep clean, sanitary the long period.
Description of drawings
Fig. 1 is a process flow sheet of the present invention.
Embodiment
The invention will be further described below in conjunction with accompanying drawing:
Embodiment: structure as shown in Figure 1, a kind of optical substrate preparation method of anti-electrostatic, its technology is as follows: cleaning substrate--is placed on substrate on the tool (shelf of fixed substrate) that--tool is put into the vacuum board, and--the vacuum board is evacuated down to certain condition, and--coating process (detailed process is as follows)--board lose heart--takes out substrate.
Coating process: after substrate cleans up, be positioned over vacuum tightness and be evacuated to 1x10 -5Torr is to 5x10 -5In the high vacuum board of Torr, evaporation high refractive index film layer and low-refraction coatings alternative rete successively on substrate, then the state of super waterproof Coating Materials WR5 evaporation back with molecule steamed in thin film layer, form new one deck rete, and the thickness of the new rete of this WR5 is being 120-220nm, takes out substrate and forms the optical base-substrate of anti-electrostatic.
Above-mentioned at least one floor height refractivity film layer and the mutual interference mutually of one deck low-index film.Wherein, the high refractive index Coating Materials is tantalum pentoxide (Ta 2O 5), titanium dioxide (TiO 2), five oxidation Tritanium/Trititanium (Ti 3O 5) wherein any one, in the mode of resistive heating or electron beam gun flow of emitted electrons with above-mentioned high refractive index Coating Materials tantalum pentoxide (Ta 2O 5), titanium dioxide (TiO 2), five oxidation Tritanium/Trititanium (Ti 3O 5) after wherein any evaporation, steaming on substrate with the state of molecule, form a high refractive index layer.Low-index material is SiO 2, in the mode of resistive heating or electron beam gun flow of emitted electrons with low-refraction Coating Materials SiO 2Is steaming on thin film layer with the state of molecule the evaporation back, forms a low refractive index film layer.
Super waterproof Coating Materials WR5 is evaporated the back in the mode of resistive heating or electron beam gun flow of emitted electrons and is steaming in thin film layer with the state of molecule, forms new one deck rete, and thicknesses of layers is at 120-220nm.
Substrate is a kind of in acryl (AC) substrate, PC polycarbonate substrate (Polycarbonate), nylon (Nylon) substrate, the CR-39 substrate.
After any substrate in the materials such as AC, PC, Nylon, CR-39 cleaned up, be positioned over vacuum tightness then and be evacuated to 1x10 -5Torr is to 5x10 -5Torr, the high vacuum board in, in the mode of resistive heating or electron beam gun flow of emitted electrons with high refractive index Coating Materials Ta 2O 5, TiO 2, Ti 3O 5After wherein any evaporation, steaming on substrate, forming a high refractive index layer with the state of molecule, again in the mode of resistive heating or electron beam gun flow of emitted electrons with low-refraction Coating Materials SiO 2Is steaming on thin film layer with the state of molecule the evaporation back, forms a low refractive index film layer, at least one floor height specific refractory power and the mutual interference mutually of one deck low-index film.In the mode of resistive heating or electron beam gun flow of emitted electrons the state of super waterproof Coating Materials WR5 evaporation back with molecule steamed in thin film layer, forming new one deck rete, WR5 tunic layer thickness is at 120-220nm.
The present invention has following advantage: common product through plated film, easily adsorb dust, and through this product processed, can play the effect of anti-electrostatic, and be difficult for the absorption dust, can keep clean the long period.
Below be concrete experimental data: (used electrostatic test instrument is the COSMI brand SC-STD series that Taiwan produces)
The contrast reference table:
Figure A20091011175100071
The above record only for utilizing the embodiment of this origination techniques content, anyly is familiar with modification, the variation that this skill person uses this creation to do to do, and all belongs to the claim of this creation opinion, and is not limited to those disclosed embodiments.

Claims (6)

1, a kind of optical substrate preparation method of anti-electrostatic is characterized in that step is as follows:
After substrate cleans up, be positioned over vacuum tightness and be evacuated to 1 * 10 -5Torr to 5 * 10 -5In the high vacuum board of Torr, evaporation high refractive index film layer and low refractive index film layer alternative rete successively on substrate, then the state of super waterproof Coating Materials WR5 evaporation back with molecule steamed in thin film layer, form a new WR5 rete, this WR5 thicknesses of layers is 120-220nm, takes out substrate and forms the optical base-substrate of anti-electrostatic.
2, the optical substrate preparation method of anti-electrostatic according to claim 1 is characterized in that: described at least one floor height refractivity film layer and the mutual interference mutually of one deck low-index film.
3, the optical substrate preparation method of anti-electrostatic according to claim 1 is characterized in that: described high refractive index Coating Materials is tantalum pentoxide (Ta 2O 5), titanium dioxide (TiO 2), five oxidation Tritanium/Trititanium (Ti 3O 5) wherein any one, in the mode of resistive heating or electron beam gun flow of emitted electrons with above-mentioned high refractive index Coating Materials tantalum pentoxide (Ta 2O 5), titanium dioxide (TiO 2), five oxidation Tritanium/Trititanium (Ti 3O 5) after wherein any evaporation, steaming on substrate with the state of molecule, form a high refractive index layer.
4, the optical substrate preparation method of anti-electrostatic according to claim 1 is characterized in that: described low-index material is silicon-dioxide (SiO 2), in the mode of resistive heating or electron beam gun flow of emitted electrons with low-refraction Coating Materials silicon-dioxide (SiO 2) evaporation back steaming on thin film layer with the state of molecule, forms a low refractive index film layer.
5, the optical substrate preparation method of anti-electrostatic according to claim 1, it is characterized in that: described super waterproof Coating Materials WR5 is evaporated the back in the mode of resistive heating or electron beam gun flow of emitted electrons and is steaming in thin film layer with the state of molecule, form new one deck rete, thicknesses of layers is being 120-220nm.
6, the optical substrate preparation method of anti-electrostatic according to claim 1 is characterized in that: described substrate is a kind of in acryl (AC) substrate, PC polycarbonate substrate (Polycarbonate), nylon (Nylon) substrate, the CR-39 substrate.
CN200910111751XA 2009-05-07 2009-05-07 Antistatic optical substrate preparation method Active CN101550533B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN200910111751XA CN101550533B (en) 2009-05-07 2009-05-07 Antistatic optical substrate preparation method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN200910111751XA CN101550533B (en) 2009-05-07 2009-05-07 Antistatic optical substrate preparation method

Publications (2)

Publication Number Publication Date
CN101550533A true CN101550533A (en) 2009-10-07
CN101550533B CN101550533B (en) 2011-04-13

Family

ID=41155016

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200910111751XA Active CN101550533B (en) 2009-05-07 2009-05-07 Antistatic optical substrate preparation method

Country Status (1)

Country Link
CN (1) CN101550533B (en)

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102732844A (en) * 2012-07-12 2012-10-17 中国科学院光电技术研究所 Design method of coating uniformity correction baffle plate of spherical optical element on planetary rotating fixture of vacuum coating machine
CN102787301A (en) * 2012-07-23 2012-11-21 中国科学院光电技术研究所 Baffle plate design method for controlling film thickness distribution of conical optical element in film-coating planetary system
CN104419893A (en) * 2013-08-29 2015-03-18 江苏远大光学科技有限公司 Coating method for waterproof film of spectacle lens
CN104498876A (en) * 2014-12-25 2015-04-08 江西昌佳鑫科技有限公司 Vacuum coating method of camera cover plate
CN104561899A (en) * 2014-12-25 2015-04-29 江西昌佳鑫科技有限公司 Vacuum coating camera cover plate and preparation method thereof
CN104818456A (en) * 2015-05-07 2015-08-05 苏州融睿纳米复材科技有限公司 Processing technology of a high-hardness angstrom-scale functional protective thin film layer
CN104818455A (en) * 2015-05-07 2015-08-05 苏州融睿纳米复材科技有限公司 Processing method of self-sterilizing angstrom-scale functional protective thin film layer
CN105444116A (en) * 2015-12-31 2016-03-30 奥特路(漳州)光学科技有限公司 Multifunctional lampshade and manufacturing method thereof
CN105734499A (en) * 2016-04-21 2016-07-06 三明福特科光电有限公司 Preparation method of corrosion resisting and permeability increasing waterproof film
CN105785590A (en) * 2016-05-20 2016-07-20 四川梅塞尔科技有限公司 Preparation method and products for color-changing wearable self-cleaning concave lens
CN110468378A (en) * 2019-09-12 2019-11-19 西安邮电大学 A kind of preparation method of densification five oxidation two tantalum film
CN110484869A (en) * 2019-07-11 2019-11-22 湖北久之洋红外系统股份有限公司 A kind of mildew resistant moistureproof optical thin film and preparation method thereof
CN115061226A (en) * 2022-04-19 2022-09-16 深圳菲比特光电科技有限公司 Large-angle ultralow-reflection film forming method

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102953041B (en) * 2012-10-24 2014-07-02 中国科学院光电技术研究所 Baffle plate design method for controlling film thickness distribution of spherical optical element in coating machine planetary system

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1006825B (en) * 1985-06-14 1990-02-14 兵器工业部第二○五研究所 Process and uses of plating hardfilm for optical plastic lens
KR20030012506A (en) * 2001-08-01 2003-02-12 삼성코닝 주식회사 Anti-reflective and anti-static multi-layer thin film for display device
CN100491584C (en) * 2005-09-22 2009-05-27 中国科学院半导体研究所 Method for preparing different refractivity film layer
CN201035166Y (en) * 2007-04-17 2008-03-12 厦门虹泰光学有限公司 Complex structure for nights drive glasses lens
CN101363919A (en) * 2007-08-09 2009-02-11 大立光电股份有限公司 Plastic optical assembly multilayer film vacuum evaporation method and imaging assembly thereof

Cited By (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102732844B (en) * 2012-07-12 2014-05-07 中国科学院光电技术研究所 Design method of coating uniformity correction baffle plate of spherical optical element on planetary rotating fixture of vacuum coating machine
CN102732844A (en) * 2012-07-12 2012-10-17 中国科学院光电技术研究所 Design method of coating uniformity correction baffle plate of spherical optical element on planetary rotating fixture of vacuum coating machine
CN102787301A (en) * 2012-07-23 2012-11-21 中国科学院光电技术研究所 Baffle plate design method for controlling film thickness distribution of conical optical element in film-coating planetary system
CN102787301B (en) * 2012-07-23 2014-03-26 中国科学院光电技术研究所 Baffle plate design method for controlling film thickness distribution of conical optical element in film-coating planetary system
CN104419893A (en) * 2013-08-29 2015-03-18 江苏远大光学科技有限公司 Coating method for waterproof film of spectacle lens
CN104498876B (en) * 2014-12-25 2017-02-08 江西昌佳鑫科技有限公司 Vacuum coating method of camera cover plate
CN104498876A (en) * 2014-12-25 2015-04-08 江西昌佳鑫科技有限公司 Vacuum coating method of camera cover plate
CN104561899A (en) * 2014-12-25 2015-04-29 江西昌佳鑫科技有限公司 Vacuum coating camera cover plate and preparation method thereof
CN104561899B (en) * 2014-12-25 2017-08-11 江西昌佳鑫科技有限公司 Vacuum coating shooting epicranial plate and preparation method thereof
CN104818456A (en) * 2015-05-07 2015-08-05 苏州融睿纳米复材科技有限公司 Processing technology of a high-hardness angstrom-scale functional protective thin film layer
CN104818455A (en) * 2015-05-07 2015-08-05 苏州融睿纳米复材科技有限公司 Processing method of self-sterilizing angstrom-scale functional protective thin film layer
CN105444116A (en) * 2015-12-31 2016-03-30 奥特路(漳州)光学科技有限公司 Multifunctional lampshade and manufacturing method thereof
CN105734499A (en) * 2016-04-21 2016-07-06 三明福特科光电有限公司 Preparation method of corrosion resisting and permeability increasing waterproof film
CN105734499B (en) * 2016-04-21 2018-06-26 三明福特科光电有限公司 A kind of preparation method of corrosion-resistant anti-reflection waterproof membrane
CN105785590A (en) * 2016-05-20 2016-07-20 四川梅塞尔科技有限公司 Preparation method and products for color-changing wearable self-cleaning concave lens
CN105785590B (en) * 2016-05-20 2018-10-26 四川梅塞尔科技有限公司 A kind of preparation method and product of the wear-resisting automatically cleaning concave lens of discoloration
CN110484869A (en) * 2019-07-11 2019-11-22 湖北久之洋红外系统股份有限公司 A kind of mildew resistant moistureproof optical thin film and preparation method thereof
CN110484869B (en) * 2019-07-11 2021-07-16 湖北久之洋红外系统股份有限公司 Mildew-proof and damp-proof optical film and preparation method thereof
CN110468378A (en) * 2019-09-12 2019-11-19 西安邮电大学 A kind of preparation method of densification five oxidation two tantalum film
CN115061226A (en) * 2022-04-19 2022-09-16 深圳菲比特光电科技有限公司 Large-angle ultralow-reflection film forming method

Also Published As

Publication number Publication date
CN101550533B (en) 2011-04-13

Similar Documents

Publication Publication Date Title
CN101550533B (en) Antistatic optical substrate preparation method
AU704597B2 (en) Electrically conductive anti-reflection coating
CN104081229B (en) Optical goods and manufacture method thereof
JP4314623B2 (en) Transparent conductive laminate and touch panel
CN110537116A (en) Anti-reflection member and its manufacturing method
FR2793889B1 (en) TRANSPARENT SUBSTRATE WITH ANTI-REFLECTIVE COATING
CN102346266A (en) Optical article and method for manufacturing the same
MX2010009557A (en) Transparent substrate with anti-reflection coating.
KR20120002577A (en) Light-emitting member, plastic lens for glasses, and production method therefor
TW201331960A (en) Transparent conductive film
JP3464785B2 (en) Improved anti-reflective composites
Khan et al. Antireflective coatings with enhanced adhesion strength
WO2022014568A1 (en) Optical film with anti-fouling layer
JP2016164680A (en) Optical lens having antistatic coating
JP2010140008A (en) Optical article and method for manufacturing the same
TWI588517B (en) Optical element
JP2003098306A (en) Antireflection film
CN109811308A (en) A kind of ITO process for making conducting membrane
CN209861332U (en) Electronic product and transparent cover plate
JP2022079332A (en) Optical film with antifouling layer
US20150083465A1 (en) Transparent conductive substrate, and method for manufacturing same
JP7378679B1 (en) Optical film with antifouling layer and method for producing the same
JPH07209501A (en) Wear-resistant optical part for preventing charging and manufacture thereof
CN115867436B (en) Laminate body
TW202336250A (en) Optical film with antifouling layer and method for manufacturing same

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant