CN104818455A - Processing method of self-sterilizing angstrom-scale functional protective thin film layer - Google Patents

Processing method of self-sterilizing angstrom-scale functional protective thin film layer Download PDF

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CN104818455A
CN104818455A CN201510227733.3A CN201510227733A CN104818455A CN 104818455 A CN104818455 A CN 104818455A CN 201510227733 A CN201510227733 A CN 201510227733A CN 104818455 A CN104818455 A CN 104818455A
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material
amy
functional
self
sterilizing
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CN201510227733.3A
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Chinese (zh)
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戴明光
曾德洪
陈浩
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苏州融睿纳米复材科技有限公司
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Priority to CN201510227733.3A priority Critical patent/CN104818455A/en
Publication of CN104818455A publication Critical patent/CN104818455A/en

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Abstract

The invention discloses a processing method of a self-sterilizing angstrom-scale functional protective thin film layer. The processing method includes following steps: quality inspection of raw materials, vacuumizing treatment to a vacuum device, plasma cleaning treatment, plasma modification treatment, hardened angstrom-scale material stacking treatment, self-sterilizing angstrom-scale material stacking treatment, cooling and vacuum-breaking treatment and quality inspection of a finish product. The processing method can be used for preparing the protective thin film layer product of which the surface has multiple functions comprising self-sterilization, antifouling, fingerprint proofing and water proofing and the like. The functional protective thin film layer can satisfy special user requirements, is free of scratches, base material exposure, falling, scratching and the like problem on surface after long-period contact operation, and can satisfy the special user requirements in all aspects.

Description

自杀菌埃米功能防护薄膜层制程工艺 Since functional bactericidal Amy pellicle layer process technology

技术领域 FIELD

[0001] 本发明属于真空薄膜加工领域,具体地涉及一种自杀菌埃米功能防护薄膜层制程工艺。 [0001] The present invention belongs to the field of vacuum film processing, in particular, to a self-sterilizing Amy functional pellicle layer process technology.

背景技术 Background technique

[0002] 当前真空薄膜的玻璃或陶瓷在表面的各种硬度及功能,都采用“真空制程工艺方式”或是“真空加上表面UV涂层制程工艺方式”。 [0002] Current glass or ceramic vacuum film hardness and various functional surfaces, use the "vacuum process technology embodiment" or "vacuum UV plus surface coating process technology mode." 该工艺生产成本较低,工艺属于新型或是与传统相互搭配。 The process low production cost, the conventional technology is a new type or with each other.

[0003] 但是,当前市场上的薄膜层产品中还没有具有自杀菌功能。 [0003] However, the current products on the market film layer also has no self-sterilizing function. 然而由于长时间的使用,薄膜层上容易滋生细菌等,不能满足特殊客户的需求。 However, due to prolonged use, easy to breed bacteria and other thin film layer, can not meet the special needs of customers.

发明内容 SUMMARY

[0004] 本发明目的是:提供一种自杀菌埃米功能防护薄膜层制程工艺,可以获得成品表面具有自杀菌、防污、防指纹、防水等多种功能防护薄膜层产品。 [0004] The object of the present invention are: to provide a self-sterilizing Amy functional pellicle layer process technology, it is possible to obtain finished surface having a self-sterilization, anti-fouling, anti-fingerprint, water and other functions pellicle layer products.

[0005] 本发明的技术方案是: [0005] aspect of the present invention is:

一种自杀菌埃米功能防护薄膜层制程工艺,包括以下步骤: A self-sterilizing Amy functional pellicle layer process technology, comprising the steps of:

a.原材料质量检验:对原材料的加工表面划痕、外观洁净度进行质量检查; . A quality inspection of raw materials: surface scratches on the processing of raw materials, the appearance of cleanliness QA;

b.真空设备抽真空处理:将符合规格要求的原材料安置在工装治具上,送入真空设备内进行抽真空后得到材料A; . B vacuuming vacuum equipment: The raw materials meet the specifications placed on the fixture, into the material A to give after vacuum evacuation device;

c.电浆清洗处理:将材料A送入电浆离子源设备内,同时冲入第一工作气体,设定预设压力值进行清洗处理后得到材料B; . C Plasma cleaning: A material fed into the plasma ion source device, while the working gas into the first, set a default value after pressure washing treatment to obtain a material B;

d.电浆改质处理:在改质埃米材料区冲入第一工作气体,电子枪通过高电压电流,产生的电子束能量偏转至埃米材料,使得埃米材料由固态转变为气态分子状在材料B表面形成薄膜层,得到材料C; d plasma reforming treatment: Amy into the material in the modified region of the first working gas, high voltage current through the electron gun, the electron beam is deflected to the energy generating Amy material, such Amy material solid to gaseous molecular shape a thin film layer formed on the surface in the material B, C to give material;

e.加硬埃米材料堆栈处理:在加硬功能埃米材料区冲入第二工作气体,电子枪产生的电子束能量偏转至加硬功能埃米材料区的埃米材料上,使得埃米材料由固态转变为气态分子状,埃米材料不断沉积到材料C上,得到材料D; e hardening process the material stack Amy: on the electron beam energy into the second working gas, the electron gun Amy functional hardening material region is deflected to produce stiffening material region Amy Amy functional materials, such materials Amy from the solid to gaseous molecular shape, Amy material continuously deposited onto the material C, giving the D material;

f.自杀菌埃米材料堆栈处理:在功能埃米材料区冲入第二工作气体,电子枪产生的电子束能量偏转至功能埃米材料区的埃米级活性T1或者Ag上,使得埃米级活性T1或者Ag由固态转变为气态分子状,埃米级活性T1或者Ag不断沉积到材料D上,得到材料E; Since the material stack Amy f sterilization process: a second electron beam energy into the working gas, the electron gun Amy functional material region is deflected to produce functional Amy Amy grade active material region on T1 or Ag, such that the level Amy T1 or activity of a Ag solid to gaseous molecular Amy activity level T1 or Ag is deposited continuously onto the material D, E obtained material;

g.冷却破真空处理:材料E冷却后,破真空取出; . G breaking the vacuum cooling process: Material E After cooling, remove the vacuum break;

h.成品质量检验:将材料E进行检查合格后即得到成品。 h finished product quality inspection: The material E after passing inspection to be finished.

[0006] 优选的,所述第一工作气体为氩气。 [0006] Preferably, the first working gas is argon.

[0007] 优选的,所述第二工作气体为氩气、氧气、氮气。 [0007] Preferably, the second working gas is argon, oxygen, nitrogen.

[0008] 优选的,所述原材料为塑胶材料、玻璃或者陶瓷。 [0008] Preferably, the material is a plastic material, glass or a ceramic.

[0009] 优选的,所述步骤d、e中的埃米材料为下列材料的任一种埃米级材料:Si02、活性T1、A1203、ZrO2λ Nb2O50 [0009] Preferably, said step d, e Amy material is any one of the following materials Amy grade material: Si02, active T1, A1203, ZrO2λ Nb2O50

[0010] 本发明的优点是: [0010] The advantage of the present invention are:

1、长期进行接触操作时,表面没有划痕、露底材、脱落、划伤现象等,全都能满足特殊客户的需求。 1, long-term contact operation, no scratches the surface, exposed substrate, falling, scratches and other phenomena, all can meet specific customer needs.

[0011] 2、外观颜色可控,没有偏黄,可以灵活变化客户需求的颜色。 [0011] 2, color control, no yellow, the flexibility to change the color of customer needs.

[0012] 3、工艺生产过程稳定,生产过程自动化控制不良率较低,制程良率高。 [0012] 3. The process of stable production process, the production process automation low defect rate, good rate process. 由一台设备完成整个制程,没有转换设备取放、搬运、储藏等,不会造成毛肩粉尘的吸附问题。 Done by a piece of equipment throughout the manufacturing process, no conversion pick and place equipment, handling, storage, etc., will not cause problems wool shoulder adsorption dust.

[0013] 4、成品表面可以获得具有自杀菌功能(绿脓肝菌、金黄色葡萄球菌、大肠杆菌、肺炎杆菌及流感菌)。 [0013] 4, can be obtained from the finished surface sterilization function (aeruginosa coli, Staphylococcus aureus, Escherichia coli, Klebsiella pneumoniae and influenza strain). 还可以获得具有防污、防指纹、防水等多种功能防护薄膜层产品。 Also can be obtained an antifouling, anti-fingerprint, water and other functions pellicle layer products.

附图说明 BRIEF DESCRIPTION

[0014] 下面结合附图及实施例对本发明作进一步描述: [0014] Example embodiments of the present invention will be further described in conjunction with the accompanying drawings and the following:

图1为本发明自杀菌埃米功能防护薄膜层制程工艺的流程图。 FIG 1 is a flowchart of process technology since the protective film layer Amy sterilization function of the present invention.

具体实施方式 Detailed ways

[0015] 为使本发明的目的、技术方案和优点更加清楚明了,下面结合具体实施方式并参照附图,对本发明进一步详细说明。 [0015] To make the objectives, technical solutions, and advantages of the present invention will become apparent from the following embodiments and with reference to specific embodiment with reference to the accompanying drawings, the present invention is described in further detail. 应该理解,这些描述只是示例性的,而并非要限制本发明的范围。 It should be understood that these descriptions are exemplary only, and are not intended to limit the scope of the invention. 此外,在以下说明中,省略了对公知结构和技术的描述,以避免不必要地混淆本发明的概念。 In the following description, description is omitted for well-known structures and techniques, in order to avoid unnecessarily obscuring the concepts of the present invention.

[0016] 实施例1: [0016] Example 1:

如图1所示,一种自杀菌埃米功能防护薄膜层制程工艺,包括以下步骤: 1, a self-sterilizing Amy functional pellicle layer process technology, comprising the steps of:

a.玻璃材料质量检验:对玻璃材料的加工表面划痕、外观洁净度进行质量检查; . A glass material quality test: scratches on the processing surface, the appearance of cleanliness QA glass material;

b.真空设备抽真空处理:将符合规格要求的玻璃材料安置在工装治具上,送入真空设备内进行抽真空后得到材料A; . B vacuuming vacuum equipment: a glass material will meet the specifications placed on the fixture, a vacuum device into the material A to give after evacuation;

c.电浆清洗处理:将材料A送入电浆离子源设备内,同时冲入氩气,设定预设压力值进行清洗处理后得到材料B; . C Plasma cleaning: A material fed into the ion source plasma equipment, into the argon pressure set a default value after the cleaning process to obtain a material B;

d.电浆改质处理:在改质埃米材料区冲入氩气,电子枪通过高电压电流,产生的电子束能量偏转至埃米级S12,使得埃米级S12由固态转变为气态分子状在材料B表面形成薄膜层,得到材料C; d plasma reforming treatment: Amy material into the region in the modified argon, high-voltage current through the electron gun, the electron beam is deflected to the energy generating Amy stage S12, S12 such that a level Amy solid to gaseous molecular shape a thin film layer formed on the surface in the material B, C to give material;

e.加硬埃米材料堆栈处理:在加硬功能埃米材料区冲入氩气,电子枪产生的电子束能量偏转至加硬功能埃米材料区的埃米级活性T1上,使得埃米级活性T1由固态转变为气态分子状,埃米级活性T1不断沉积到材料C上,得到材料D; e hardening process the material stack Amy: argon into the functional Amy stiffening material region, electron beam energy generated by an electron gun to deflect the angstrom level functional activity T1 Amy stiffening material region so Amy stage T1 active from a solid into a gaseous molecular shape, Amy stage T1 continuously deposited onto the active material C, giving the D material;

f.自杀菌埃米材料堆栈处理:在功能埃米材料区冲入氩气,电子枪产生的电子束能量偏转至功能埃米材料区的埃米级Ag上,使得埃米级Ag由固态转变为气态分子状,埃米级Ag不断沉积到材料D上,得到材料E;在步骤f中,可以把预需要得到的各种功能埃米材料,一直不断沉积到材料E上,形成多种功能性的薄膜层。 Since the material stack Amy f sterilization process: Amy into the argon functional material region, electron beam energy generated by an electron gun to deflect the angstrom level Ag Amy functional material region so Amy stage from a solid into Ag gaseous molecular Amy Ag level continuously deposited onto the material D, E to give material; in step f, the various features may be needed to get the pre-Amy materials has been continuously deposited onto the material E, form various functional film layers. 例如具有防污、防指纹、防水等功能。 For example, anti-fouling, anti-fingerprint, water and other functions.

[0017] g.冷却破真空处理:材料E冷却后,破真空取出; . [0017] g breaking vacuum cooling process: Material E After cooling, remove the vacuum break;

h.成品质量检验:将材料E进行检查合格后即得到成品。 h finished product quality inspection: The material E after passing inspection to be finished.

[0018] 实施例2: 如图1所示,一种高硬度埃米防护薄膜层制程工艺,包括以下步骤: [0018] Example 2: as shown, a high-hardness Amy pellicle film processing process 1, as shown in FIG comprising the step of:

a.陶瓷材料质量检验:对陶瓷材料的加工表面划痕、外观洁净度进行质量检查; . A ceramic material quality test: scratches on the processed surface of the ceramic material, the appearance of cleanliness QA;

b.真空设备抽真空处理:将符合规格要求的陶瓷材料安置在工装治具上,送入真空设备内进行抽真空后得到材料A; . B vacuuming vacuum equipment: meet the specifications of a ceramic material disposed on the fixture, into the material A to give after vacuum evacuation device;

c.电浆清洗处理:将材料A送入电浆离子源设备内,同时冲入氩气,设定预设压力值进行清洗处理后得到材料B; . C Plasma cleaning: A material fed into the ion source plasma equipment, into the argon pressure set a default value after the cleaning process to obtain a material B;

d.电浆改质处理:在改质埃米材料区冲入氩气,电子枪通过高电压电流,产生的电子束能量偏转至埃米级Al2O3,使得埃米级Al2O3由固态转变为气态分子状在材料B表面形成薄膜层,得到材料C; d plasma reforming treatment: Amy material into the region in the modified argon, high-voltage current through the electron gun, the electron beam is deflected to the energy generating stage Amy Al2O3, Al2O3 such that angstrom level from a solid state into a gaseous molecular a thin film layer formed on the surface in the material B, C to give material;

e.加硬埃米材料堆栈处理:在加硬功能埃米材料区冲入氮气,电子枪产生的电子束能量偏转至加硬功能埃米材料区的埃米级ZrO2I,使得埃米级ZrO 2由固态转变为气态分子状,埃米级ZrO2F断沉积到材料C上,得到材料D; e hardening process the material stack Amy: nitrogen flushed Amy functional hardening material region, the electron beam energy generated by an electron gun to deflect Amy Amy functional level ZrO2I stiffening material region, so that the ZrO 2 level Amy solid to gaseous molecular shape, Amy ZrO2F level off the material to be deposited C, giving the D material;

f.自杀菌埃米材料堆栈处理:在功能埃米材料区冲入氧气,电子枪产生的电子束能量偏转至功能埃米材料区的埃米级活性T1上,使得埃米级活性T1由固态转变为气态分子状,埃米级活性T1不断沉积到材料D上,得到材料E;在步骤f中,可以把预需要得到的各种功能埃米材料,一直不断沉积到材料E上,形成多种功能性的薄膜层。 Since the material stack Amy f sterilization process: Amy into the oxygen functional material region, an electron gun to generate the electron beam energy is deflected to the angstrom level functional Amy active material region of T1, such that T1 Amy active level transition from solid gaseous molecular Amy stage T1 continuously deposited onto the active materials D, E to give material; in step f, the various features may be needed to get the pre-Amy materials has been continuously deposited onto the material E, form various functional film layer. 例如具有防污、防指纹、防水等功能。 For example, anti-fouling, anti-fingerprint, water and other functions.

[0019] g.冷却破真空处理:材料E冷却后,破真空取出; . [0019] g breaking vacuum cooling process: Material E After cooling, remove the vacuum break;

h.成品质量检验:将材料E进行检查合格后即得到成品。 h finished product quality inspection: The material E after passing inspection to be finished.

[0020] 实施例3: [0020] Example 3:

如图1所示,一种自杀菌埃米功能防护薄膜层制程工艺,包括以下步骤: 1, a self-sterilizing Amy functional pellicle layer process technology, comprising the steps of:

a.ABS材料质量检验:对ABS材料的加工表面划痕、外观洁净度进行质量检查; Material quality inspection a.ABS: machining scratches on the surface, the appearance of cleanliness QA ABS material;

b.真空设备抽真空处理:将符合规格要求的ABS材料安置在工装治具上,送入真空设备内进行抽真空后得到材料A; . B vacuuming vacuum equipment: meet the specifications of the ABS material is disposed on the fixture, into the material A to give after vacuum evacuation device;

c.电浆清洗处理:将材料A送入电浆离子源设备内,同时冲入氩气,设定预设压力值进行清洗处理后得到材料B; . C Plasma cleaning: A material fed into the ion source plasma equipment, into the argon pressure set a default value after the cleaning process to obtain a material B;

d.电浆改质处理:在改质埃米材料区冲入氩气,电子枪通过高电压电流,产生的电子束能量偏转至埃米级Nb2O5,使得埃米级Nb2O5由固态转变为气态分子状在材料B表面形成薄膜层,得到材料C; d plasma reforming treatment: Amy material into the region in the modified argon, high-voltage current through the electron gun, the electron beam is deflected to the energy generating stage Amy Nb2O5, Nb2O5 such angstrom level from a solid state into a gaseous molecular a thin film layer formed on the surface in the material B, C to give material;

e.加硬埃米材料堆栈处理:在加硬功能埃米材料区冲入氧气,电子枪产生的电子束能量偏转至加硬功能埃米材料区的埃米级S12I,使得埃米级S1 2由固态转变为气态分子状,埃米级S12F断沉积到材料C上,得到材料D; e hardening process the material stack Amy: into the oxygen functional Amy stiffening material region, the electron beam energy generated by an electron gun to deflect Amy Amy functional level S12I stiffening material region, so that the Amy stage S1 2 solid to gaseous molecular shape, S12F angstrom level off the material to be deposited C, giving the D material;

f.自杀菌埃米材料堆栈处理:在功能埃米材料区冲入氩气,电子枪产生的电子束能量偏转至功能埃米材料区的埃米级活性T1上,使得埃米级活性T1由固态转变为气态分子状,埃米级活性T1不断沉积到材料D上,得到材料E;在步骤f中,可以把预需要得到的各种功能埃米材料,一直不断沉积到材料E上,形成多种功能性的薄膜层。 Since the material stack Amy f sterilization process: the argon into the functional area Amy material, an electron beam energy of the electron gun is deflected to produce functional Amy Amy grade active material region T1, such that T1 from solid grade active Amy converted to the gaseous molecular Amy stage T1 continuously deposited onto the active materials D, E to give material; in step f, the various features may be needed to get the pre-Amy materials has been continuously deposited onto the material E, forming a plurality of kinds of functional thin film layer. 例如具有防污、防指纹、防水等功能。 For example, anti-fouling, anti-fingerprint, water and other functions.

[0021] g.冷却破真空处理:材料E冷却后,破真空取出; . [0021] g breaking vacuum cooling process: Material E After cooling, remove the vacuum break;

h.成品质量检验:将材料E进行检查合格后即得到成品。 h finished product quality inspection: The material E after passing inspection to be finished.

[0022] 需要说明的是,本发明的制程工艺的原材料还可以为其它塑胶材料。 [0022] Incidentally, the raw material of the process technology of the present invention may also be other plastics materials. 第二工作气体,实际需求功能状况搭配为氩气、氧气、氮气。 A second working gas, with the actual needs of the functional status of argon, oxygen, nitrogen. 步骤d、e中的埃米材料包括S1 2、活性T1、Al203、Zr02、Nb205中的一种埃米级材料,以先后不同次序堆栈。 Step d, e Amy material comprises one of S1 2, the activity of T1, Al203, Zr02, Nb205 the Amy grade material, have a different stack order.

[0023] 应当理解的是,本发明的上述具体实施方式仅仅用于示例性说明或解释本发明的原理,而不构成对本发明的限制。 [0023] It should be appreciated that the above-described embodiments of the present invention are provided for illustrative or explain the principles of the present invention, not to limit the present invention. 因此,在不偏离本发明的精神和范围的情况下所做的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。 Thus, made without departing from the spirit and scope of the present invention any modification, equivalent replacement, or improvement, it should be included within the scope of the present invention. 此外,本发明所附权利要求旨在涵盖落入所附权利要求范围和边界、或者这种范围和边界的等同形式内的全部变化和修改例。 Furthermore, the claims appended hereto are intended to cover the scope of this embodiment and all changes and modifications within the boundary of equivalents of the appended claims and the range boundaries, or request.

Claims (5)

1.一种自杀菌埃米功能防护薄膜层制程工艺,其特征在于,包括以下步骤: a.原材料质量检验:对原材料的加工表面划痕、外观洁净度进行质量检查; b.真空设备抽真空处理:将符合规格要求的原材料安置在工装治具上,送入真空设备内进行抽真空后得到材料A; c.电浆清洗处理:将材料A送入电浆离子源设备内,同时冲入第一工作气体,设定预设压力值进行清洗处理后得到材料B ; d.电浆改质处理:在改质埃米材料区冲入第一工作气体,电子枪通过高电压电流,产生的电子束能量偏转至埃米材料,使得埃米材料由固态转变为气态分子状在材料B表面形成薄膜层,得到材料C; e.加硬埃米材料堆栈处理:在加硬功能埃米材料区冲入第二工作气体,电子枪产生的电子束能量偏转至加硬功能埃米材料区的埃米材料上,使得埃米材料由固态转变为气态分子状,埃米材料不断 1. A self-sterilizing Amy functional pellicle layer process technology, characterized by comprising the steps of: a quality inspection of raw materials: machining scratches on the surface, the appearance of the raw material cleanliness QA; B vacuum apparatus was evacuated. processing: the raw materials meet the specifications placed on the fixture, into the material a to give after vacuum evacuation equipment; c plasma cleaning: the material a is fed into the ion source plasma equipment, into the after working gas to obtain a first set value preset pressure cleaning material B; d plasma reforming treatment: first operating gas into the electron gun in the modified region Amy material by a high voltage current, generated electrons beam energy is deflected to Amy material, such Amy material solid to gaseous molecular form a thin film layer on the surface of the material B, to obtain a material C; e hardening process the material stack Amy: red in the stiffening material region functional Amy the second process gas, the energy of the electron beam generated by an electron gun to deflect the material stiffening Amy Amy functional material region so Amy material solid to gaseous molecular shape, material continuously Amy 沉积到材料C上,得到材料D; f.自杀菌埃米材料堆栈处理:在功能埃米材料区冲入第二工作气体,电子枪产生的电子束能量偏转至功能埃米材料区的埃米级活性T1或者Ag上,使得埃米级活性T1或者Ag由固态转变为气态分子状,埃米级活性T1或者Ag不断沉积到材料D上,得到材料E ; g.冷却破真空处理:材料E冷却后,破真空取出; h.成品质量检验:将材料E进行检查合格后即得到成品。 Depositing onto the material C, giving the material D; f from the material stack Amy sterilization process: working gas into the second functional region Amy material, an electron beam energy of the electron gun is deflected to produce functional material region Amy Amy stage the active T1 or Ag, or such Ag T1 Amy grade active from a solid into a gaseous molecular shape, Amy activity level T1 or Ag is deposited continuously onto the material D, E to give material; breaking the vacuum cooling process G: material E cooling after breaking the vacuum extraction; product quality inspection H: E material after passing inspection to be finished.
2.根据权利要求1所述的自杀菌埃米功能防护薄膜层制程工艺,其特征在于,所述第一工作气体为氩气。 The self-sterilizing Amy functional pellicle film processing process according to claim 1, wherein said first working gas is argon.
3.根据权利要求1所述的自杀菌埃米功能防护薄膜层制程工艺,其特征在于,所述第二工作气体为氩气、氧气、氮气。 The self-sterilizing Amy functional pellicle film processing process according to claim 1, wherein said second working gas is argon, oxygen, nitrogen.
4.根据权利要求1所述的自杀菌埃米功能防护薄膜层制程工艺,其特征在于,所述原材料为塑胶材料、玻璃或者陶瓷。 The self-sterilizing Amy functional pellicle film processing process according to claim 1, wherein said material is a plastic material, glass or a ceramic.
5.根据权利要求1所述的自杀菌埃米功能防护薄膜层制程工艺,其特征在于,所述步骤d、e中的埃米材料为下列材料的任一种埃米级材料:Si02、S性Ti0、Al203、Zr02、Nb205。 Since according to claim Amy functional bactericidal pellicle film processing process of Claim 1, wherein said step d, e Amy material is any one of the following materials Amy grade material: Si02, S of Ti0, Al203, Zr02, Nb205.
CN201510227733.3A 2015-05-07 2015-05-07 Processing method of self-sterilizing angstrom-scale functional protective thin film layer CN104818455A (en)

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