CN101525249B - Preparation method of middle temperature blue and white porcelain - Google Patents

Preparation method of middle temperature blue and white porcelain Download PDF

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Publication number
CN101525249B
CN101525249B CN2009101149898A CN200910114989A CN101525249B CN 101525249 B CN101525249 B CN 101525249B CN 2009101149898 A CN2009101149898 A CN 2009101149898A CN 200910114989 A CN200910114989 A CN 200910114989A CN 101525249 B CN101525249 B CN 101525249B
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CN101525249A (en
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董克勤
李非柳
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JINGDEZHEN SHENKE SPECIAL PORCELAIN CO Ltd
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JINGDEZHEN SHENKE SPECIAL PORCELAIN CO Ltd
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Abstract

The invention relates to a preparation method of blue and white porcelain, in particular to a preparation method of a middle temperature blue and white porcelain product fired in a middle temperature oxidation atmosphere. The preparation method of the blue and white porcelain sequentially comprises the following steps: (1) preparing mud cakes; (2) press forming; (3) drying the mud cakes; and (4) directly sticking stained cotton paper printed with a sapphire blue color material on ground blank replenished with water, filling the color material, glazing, and once firing into products at the firing temperature of 1180-1250 DEG C for 6-10 hours in an oxidation atmosphere. Compared with products obtained by high temperature reducing flame with traditional color material, blank and glaze formulas, the product obtained by middle temperature oxidizing flame with a sapphire blue color, blank and glaze formula has the advantages of shorter firing time, lower firing temperature and more beautiful appearance, thus saving energy and improving industrial production efficiency.

Description

The preparation method of warm bule and white porcelain in a kind of
Technical field:
The present invention relates to the preparation method of bule and white porcelain.The preparation method of the middle temperature bule and white porcelain goods that warm oxidizing atmosphere is burnt till particularly.
Background technology:
Bule and white porcelain all has been to burn till in reducing flame atmosphere for about 1320 ℃ at high temperature since being born, and is reduced into iron protoxide and is Bluish white because of containing ferric oxide in base, the glaze, form in vain in the characteristic of general green grass or young crops.The colour generation of blue and white colorant forms first, bright, clear respectively towards each generation bule and white porcelain in different poses and with different expressions because of itself component glaze colours different and that set each other off are different.This kind process for calcining produces the porcelain district in south comparatively in vogue, is representative with Jing Dezhen, Liling especially.
High temperature oxidation flame process for calcining produces porcelain district widespread usage in the north, contained ferric oxide, manganese oxide are yellow because of failing to reduce in base, the glaze, so need other the interpolation in the physics depigmenting agent to form light gray with yellow, whole structure is beautiful not as reducing flame.The high-temperature firing energy consumption is big in addition.
Summary of the invention:
Technical scheme of the present invention is as follows:
The preparation method of warm bule and white porcelain in a kind of, wherein: following steps are arranged successively:
On the blank of mill base, moisturizing, directly pasting the cotton paper marble paper of printing with sapphire blue color material, the material that colors in, glazing, 1 ℃～1 ℃ of firing temperature, in the oxidizing atmosphere, 6～10 hours conditions of firing time are adorned burnt product next time.
In the preparation method of warm bule and white porcelain goods, wherein:, have the following steps successively: (1) preparation mud cake before the blank of mill base, moisturizing; (2) compression moulding; (3) dry moulded pottery not yet put in a kiln to bake.
In the preparation method of warm bule and white porcelain goods, wherein: the component of described glaze comprises by weight: SiO 262～67 parts; Al 2O 38.5～11.5 parts; Fe 2O 30.08～0.15 part; 8.0～11.5 parts of CaO; MgO2.0～3.5 part; K 23.5～4.5 parts of O; Na 2O1.0～2.0 part; ZnO1.0～2.5 part; Li 2O0～0.3 part; IL4.55～6.35 part; SiO wherein 2By diameter is that nano level and diameter are two kinds of conventional granulometric composition, the wherein SiO of nano-scale particle 21～5 part, all the other are the SiO of conventional granulates 2
The normally calcareous transparent of glaze that obtains by prescription of the present invention.
In the preparation method of warm bule and white porcelain goods, wherein: the component of sapphire blue color material comprises by weight: SiO 234.48～43.06 parts; Al 2O 311.46～12.69 parts; B 2O 36.68～7.59 parts; Co 2O 313.97～19.78 parts; Fe 2O 33.00～5.12 parts; CaO3.24～6.79 part; MgO1.30～2.21 part; BaO0.86～1.27 part; CuO1.00～4.57 part; MnO1.18～2.92 part; 7.65～9.18 parts of K Na O.
In the preparation method of warm bule and white porcelain goods, wherein: the component of blank comprises by weight: SiO 265～70 parts; Al 2O 318～22 parts; Fe 2O 30.2～0.5 part; CaO0.1～1.0 part; MgO0.1～1.0 part; K 22.9～3.5 parts of O; Na 21.4～2.0 parts of O; Li 2O0～0.5 part; IL.5.3～6.5 part.
In the preparation method of warm bule and white porcelain goods, wherein: middle temperature bule and white porcelain adopts glaze to decorate down, the cotton paper marble paper that lines are printed with sapphire blue color material is pasted and is transferred on the mold, color lump is with the combined decoration method that colors in and expect.
In the preparation method of warm bule and white porcelain goods, wherein: goods are once adorned burning with refractory slab, support or saggar in roller kiln, shuttle kiln and tunnel furnace.
Loss on ignition in the normally ceramic porcelain of the IL field, loss on ignition are meant crystallization moisture content and the loss on ignition of organic matters matter under warm-up mode in the pug, and IL does not influence the quality of product usually.
Advantage of the present invention is as follows:
In warm bule and white porcelain passed on the decoration technique of the Jing Dezhen bule and white porcelain of one of world culture art rarity, comprise decal paper, the material that colors in, beat color limit etc., incorporated modern technology in producing porcelain, the present invention is owing to having adopted special sapphire blue color material and base, glaze formula, the method that warm oxydizing flame burns till fast in can adopting, the state basic policy that meets energy-conserving and environment-protective creates characteristic sapphire blue bule and white porcelain goods.
Adopt sapphire blue color material of the present invention and base, glaze formula, the product that middle temperature oxydizing flame obtains and traditional color material and base, glaze formula, the product that the high temperature oxidation flame obtains is compared, and adopts firing time of the present invention shorter, and firing temperature is lower, and outward appearance is also more beautiful.Thereby saved the energy, also improved industrial production efficient.Concrete advantage is as follows with the form contrast:
Project Conventional high-temperature bule and white porcelain Warm bule and white porcelain in of the present invention
Temperature About 1320 ℃ 1℃～12?5℃
Flame Reducing flame Oxydizing flame
Firing time 18～24 hours 6～10 hours
The defective that is easy to generate Easily smoking, violate yellow, blue and white color and luster is inconsistent Be not easy smoking, the inconsistent sensation of no color and luster
Specific embodiment:
Embodiment 1
The preparation method of warm bule and white porcelain in a kind of, wherein: following steps are arranged successively:
(1) preparation mud cake; (2) compression moulding; (3) dry moulded pottery not yet put in a kiln to bake; (4) on the blank of mill base, moisturizing, directly pasting the cotton paper marble paper of printing with sapphire blue color material, the material that colors in, glazing, 1 ℃～1 ℃ of firing temperature, in the oxidizing atmosphere, 6～10 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO 262～67 parts; Al 2O 38.5～11.5 parts; Fe 2O 30.08～0.15 part; 8.0～11.5 parts of CaO; MgO2.0～3.5 part; K 23.5～4.5 parts of O; Na 2O1.0～2.0 part; ZnO1.0～2.5 part; Li 2O0～0.3 part; 4.55～6.35 parts of IL; SiO wherein 2By diameter is that nano level and diameter are two kinds of conventional granulometric composition, the wherein SiO of nano-scale particle 21～5 part, all the other are the SiO of conventional granulates 2
Wherein: the component of sapphire blue color material comprises by weight: SiO 234.48～43.06 parts; Al 2O 311.46～12.69 parts; B 2O 36.68～7.59 parts; Co 2O 313.97～19.78 parts; Fe 2O 33.00～5.12 parts; CaO3.24～6.79 part; MgO1.30～2.21 part; BaO0.86～1.27 part; CuO1.00～4.57 part; MnO1.18～2.92 part; 7.65～9.18 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO 265～70 parts; Al 2O 318～22 parts; Fe 2O 30.2～0.5 part; CaO0.1～1.0 part; MgO0.1～1.0 part; K 22.9～3.5 parts of O; Na 21.4～2.0 parts of O; Li 2O0～0.5 part; IL5.3～6.5 part.
Embodiment 2
The preparation method of warm bule and white porcelain in a kind of, 1 ℃ of firing temperature, in the oxidizing atmosphere, 10 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO 262 parts; Al 2O 38.5 part; Fe 2O 30.08 part; 8.0 parts of CaO; MgO2.0 part; K 23.5 parts of O; Na 2O1.0 part; ZnO1.0 part; Li 2O0 part; 4.55 parts of IL; SiO wherein 2By diameter is that nano level and diameter are two kinds of conventional granulometric composition, the wherein SiO of nano-scale particle 21 part, all the other are the SiO of conventional granulates 261 parts.
Wherein: the component of sapphire blue color material comprises by weight: SiO 234.48 part; Al 2O 311.46 part; B 2O 36.68 part; Co 2O 313.97 part; Fe 2O 33.00 part; CaO3.24 part; MgO1.30 part; BaO0.86 part; CuO1.00 part; MnO1.18 part; 7.65 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO 265 parts; Al 2O 318 parts; Fe 2O 30.2 part; CaO0.1 part; MgO0.1 part; K 22.9 parts of O; Na 21.4 parts of O; Li 2O0 part; IL5.3 part.
All the other are with embodiment 1.
Embodiment 3
The preparation method of warm bule and white porcelain in a kind of, 1 ℃ of firing temperature, in the oxidizing atmosphere, 6 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO 267 parts; Al 2O 311.5 part; Fe 2O 30.15 part; 11.5 parts of CaO; MgO3.5 part; K 24.5 parts of O; Na 2O2.0 part; ZnO2.5 part; Li 2O0.3 part; IL6.35 part; SiO wherein 2By diameter is that nano level and diameter are two kinds of conventional granulometric composition, the wherein SiO of nano-scale particle 25 parts, all the other are the SiO of conventional granulates 262 parts.
Wherein: the component of sapphire blue color material comprises by weight: SiO 243.06 part; Al 2O 312.69 part; B 2O 37.59 part; Co 2O 319.78 part; Fe 2O 35.12 part; CaO6.79 part; MgO2.21 part; BaO1.27 part; CuO4.57 part; MnO2.92 part; 9.18 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO 270 parts; Al 2O 322 parts; Fe 2O 30.5 part; CaO1.0 part; MgO1.0 part; K 2O3.5 part; Na 2O2.0 part; Li 2O0.5 part; IL6.5 part.
All the other are with embodiment 1.
Embodiment 4
The preparation method of warm bule and white porcelain in a kind of, 1120 ℃ of firing temperatures, in the oxidizing atmosphere, 8 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO 263 parts; Al 2O 39.5 part; Fe 2O 30.12 part; 9.5 parts of CaO; MgO2.5 part; K 23.9 parts of O; Na 2O1.5 part; ZnO1.5 part; Li 2O0.2 part; IL5.25 part; SiO wherein 2By diameter is that nano level and diameter are two kinds of conventional granulometric composition, the wherein SiO of nano-scale particle 23 parts, all the other are the SiO of conventional granulates 260 parts.
Wherein: the component of sapphire blue color material comprises by weight: SiO 242.01 part; Al 2O 311.89 part; B 2O 36.99 part; Co 2O 315.28 part; Fe 2O 34.22 part; CaO4.29 part; MgO1.77 part; BaO0.89 part; CuO2.22 part; MnO1.92 part; 8.68 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO 269 parts; Al 2O 321 parts; Fe 2O 30.3 part; CaO0.8 part; MgO0.6 part; K 23.2 parts of O; Na 21.8 parts of O; Li 2O0.3 part; IL5.8 part.
All the other are with embodiment 1.
Embodiment 5
The preparation method of warm bule and white porcelain in a kind of, 1190 ℃ of firing temperatures, in the oxidizing atmosphere, 9 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO 262 parts; Al 2O 311.5 part; Fe 2O 30.15 part; 11.5 parts of CaO; MgO2.0 part; K 24.5 parts of O; Na 2O1.0 part; ZnO2.5 part; Li 2O0.3 part; IL4.55 part; SiO wherein 2By diameter is that nano level and diameter are two kinds of conventional granulometric composition, the wherein SiO of nano-scale particle 21 part, all the other are the SiO of conventional granulates 261 parts.
Wherein: the component of sapphire blue color material comprises by weight: SiO 234.48 part; Al 2O 312.69 part; B 2O 37.59 part; Co 2O 319.78 part; Fe 2O 33.00 part; CaO6.79 part; MgO1.30 part; BaO1.27 part; CuO4.57 part; MnO2.92 part; 9.18 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO 270 parts; Al 2O 318 parts; Fe 2O 30.2 part; CaO0.1 part; MgO1.0 part; K 2O2.9 part; Na 2O2.0 part; Li 2O0.5 part; IL5.3 part.
All the other are with embodiment 1.
Embodiment 6
The preparation method of warm bule and white porcelain in a kind of, 1210 ℃ of firing temperatures, in the oxidizing atmosphere, 7 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO 267 parts; Al 2O 38.5 part; Fe 2O 30.08 part; 8.0 parts of CaO; MgO3.5 part; K 23.5 parts of O; Na 2O2.0 part; ZnO1.0 part; Li 2O0.3 part; IL6.42 part; SiO wherein 2By diameter is that nano level and diameter are two kinds of conventional granulometric composition, the wherein SiO of nano-scale particle 25 parts, all the other are the SiO of conventional granulates 262 parts.
Wherein: the component of sapphire blue color material comprises by weight: SiO 243.06 part; Al 2O 311.46 part; B 2O 36.68 part; Co 2O 313.97 part; Fe 2O 35.12 part; CaO3.24 part; 2.21 parts of MgO; BaO0.86 part; CuO4.57 part; MnO1.18 part; 7.65 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO 265 parts; Al 2O 322 parts; Fe 2O 30.5 part; CaO1.0 part; MgO0.1 part; K 2O3.5 part; Na 2O1.4 part; IL6.5 part.
All the other are with embodiment 1.

Claims (3)

1. the preparation method of warm bule and white porcelain in a kind is characterized in that: following steps are arranged successively: (1) preparation mud cake; (2) compression moulding; (3) dry moulded pottery not yet put in a kiln to bake; (4) on the blank of mill base, moisturizing, directly pasting the cotton paper marble paper of printing with sapphire blue color material, the material that colors in, glazing, 1120 ℃ of firing temperatures, in the oxidizing atmosphere, 8 hours conditions of firing time are adorned burnt product next time;
Wherein: the component of glaze comprises by weight: SiO 263 parts; Al 2O 39.5 part; Fe 2O 30.12 part; 9.5 parts of CaO; MgO2.5 part; K 2O3.9 part; Na 2O1.5 part; ZnO1.5 part; Li 2O0.2 part; IL5.25 part; SiO wherein 2By diameter is that nano level and diameter are two kinds of conventional granulometric composition, the wherein SiO of nano-scale particle 23 parts, all the other are the SiO of conventional granulates 260 parts;
Wherein: the component of sapphire blue color material comprises by weight: SiO 242.01 part; Al 2O 311.89 part; B 2O 36.99 part; Co 2O 315.28 part; Fe 2O 34.22 part; CaO4.29 part; MgO1.77 part; BaO0.89 part; CuO2.22 part; MnO1.92 part; 8.68 parts of K Na O;
Wherein: the component of blank comprises by weight: SiO 269 parts; Al 2O 321 parts; Fe 2O 30.3 part; CaO0.8 part; MgO0.6 part; K 23.2 parts of O; Na 21.8 parts of O; Li 2O0.3 part; IL5.8 part.
2. the preparation method of warm bule and white porcelain in a kind is characterized in that: following steps are arranged successively: (1) preparation mud cake; (2) compression moulding; (3) dry moulded pottery not yet put in a kiln to bake; (4) on the blank of mill base, moisturizing, directly pasting the cotton paper marble paper of printing with sapphire blue color material, the material that colors in, glazing, 1190 ℃ of firing temperatures, in the oxidizing atmosphere, 9 hours conditions of firing time are adorned burnt product next time;
Wherein: the component of glaze comprises by weight: SiO 262 parts; Al 2O 311.5 part; Fe 2O 30.15 part; 11.5 parts of CaO; MgO2.0 part; K 24.5 parts of O; Na 2O1.0 part; ZnO2.5 part; Li 2O0.3 part; IL4.55 part; SiO wherein 2By diameter is that nano level and diameter are two kinds of conventional granulometric composition, the wherein SiO of nano-scale particle 21 part, all the other are the SiO of conventional granulates 261 parts;
Wherein: the component of sapphire blue color material comprises by weight: SiO 234.48 part; Al 2O 312.69 part; B 2O 37.59 part; Co 2O 319.78 part; Fe 2O 33.00 part; CaO6.79 part; MgO1.30 part; BaO1.27 part; CuO4.57 part; MnO2.92 part; 9.18 parts of KNaO;
Wherein: the component of blank comprises by weight: SiO 270 parts; Al 2O 318 parts; Fe 2O 30.2 part; CaO0.1 part; MgO1.0 part; K 2O2.9 part; Na 2O2.0 part; Li 2O0.5 part; IL5.3 part.
3. the preparation method of warm bule and white porcelain in a kind is characterized in that: following steps are arranged successively: (1) preparation mud cake; (2) compression moulding; (3) dry moulded pottery not yet put in a kiln to bake; (4) on the blank of mill base, moisturizing, directly pasting the cotton paper marble paper of printing with sapphire blue color material, the material that colors in, glazing, 1210 ℃ of firing temperatures, in the oxidizing atmosphere, 7 hours conditions of firing time are adorned burnt product next time;
Wherein: the component of glaze comprises by weight: SiO 267 parts; Al 2O 38.5 part; Fe 2O 30.08 part; 8.0 parts of CaO; MgO3.5 part; K 23.5 parts of O; Na 2O2.0 part; ZnO1.0 part; Li 2O0.3 part; IL6.42 part; SiO wherein 2By diameter is that nano level and diameter are two kinds of conventional granulometric composition, the wherein SiO of nano-scale particle 25 parts, all the other are the SiO of conventional granulates 262 parts;
Wherein: the component of sapphire blue color material comprises by weight: SiO 243.06 part; Al 2O 311.46 part; B 2O 36.68 part; Co 2O 313.97 part; Fe 2O 35.12 part; CaO3.24 part; 2.21 parts of MgO; BaO0.86 part; CuO4.57 part; MnO1.18 part; 7.65 parts of KNaO;
Wherein: the component of blank comprises by weight: SiO 265 parts; Al 2O 322 parts; Fe 2O 30.5 part; CaO1.0 part; MgO0.1 part; K 2O3.5 part; Na 2O1.4 part; IL6.5 part.
CN2009101149898A 2009-03-04 2009-03-04 Preparation method of middle temperature blue and white porcelain Expired - Fee Related CN101525249B (en)

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