CN101525249A - Preparation method of middle temperature blue and white porcelain - Google Patents
Preparation method of middle temperature blue and white porcelain Download PDFInfo
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- CN101525249A CN101525249A CN200910114989A CN200910114989A CN101525249A CN 101525249 A CN101525249 A CN 101525249A CN 200910114989 A CN200910114989 A CN 200910114989A CN 200910114989 A CN200910114989 A CN 200910114989A CN 101525249 A CN101525249 A CN 101525249A
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Abstract
The invention relates to a preparation method of blue and white porcelain, in particular to a preparation method of a middle temperature blue and white porcelain product fired in a middle temperature oxidation atmosphere. The preparation method of the blue and white porcelain sequentially comprises the following steps: (1) preparing mud cakes; (2) press forming; (3) drying the mud cakes; and (4) directly sticking stained cotton paper printed with a sapphire blue color material on ground blank replenished with water, filling the color material, glazing, and once firing into products at the firing temperature of 1180-1250 DEG C for 6-10 hours in an oxidation atmosphere. Compared with products obtained by high temperature reducing flame with traditional color material, blank and glaze formulas, the product obtained by middle temperature oxidizing flame with a sapphire blue color, blank and glaze formula has the advantages of shorter firing time, lower firing temperature and more beautiful appearance, thus saving energy and improving industrial production efficiency.
Description
Technical field:
The present invention relates to the preparation method of bule and white porcelain.The preparation method of the middle temperature bule and white porcelain goods that warm oxidizing atmosphere is burnt till particularly.
Background technology:
Bule and white porcelain all has been to burn till in reducing flame atmosphere for about 1320 ℃ at high temperature since being born, and is reduced into iron protoxide and is Bluish white because of containing ferric oxide in base, the glaze, form in vain in the characteristic of general green grass or young crops.The colour generation of blue and white colorant forms first, bright, clear respectively towards each generation blue and white porcelain in different poses and with different expressions because itself component glaze colours different and that set each other off are different.This kind process for calcining produces the porcelain district in south comparatively in vogue, especially take Jing Dezhen, Liling is representative.
High-temperature oxydation flame process for calcining produces the porcelain district and generally uses in the north, contained iron oxide, manganese oxide are yellow because failing to reduce in base, the glaze, so need other the interpolation in the physics depigmenting agent to form light gray with yellow, whole structure is beautiful not as reducing flame.The high-temperature firing energy resource consumption is big in addition.
Summary of the invention:
Technical scheme of the present invention is as follows:
The preparation method of warm bule and white porcelain in a kind of, wherein: following steps are arranged successively:
On the blank of mill base, moisturizing, directly pasting the cotton paper marble paper of printing with sapphire blue color material, the material that colors in, glazing, 1 ℃～1 ℃ of firing temperature, in the oxidizing atmosphere, 6～10 hours conditions of firing time are adorned burnt product next time.
In the preparation method of warm bule and white porcelain goods, wherein:, have the following steps successively: (1) preparation mud cake before the blank of mill base, moisturizing; (2) compression moulding; (3) dry moulded pottery not yet put in a kiln to bake.
In the preparation method of warm blue and white porcelain goods, wherein: the component of described glaze comprises by weight: SiO
262～67 parts; Al
2O
38.5～11.5 parts; Fe
2O
30.08～0.15 part; 8.0～11.5 parts of CaO; 2.0～3.5 parts of MgO; K
23.5～4.5 parts of O; Na
21.0～2.0 parts of O; 1.0～2.5 parts of ZnO; Li
20～0.3 part of O; IL4.55～6.35 part; SiO wherein
2Be that nanoscale and diameter are that two kinds of conventional particles form by diameter, the SiO of nano-scale particle wherein
21～5 part, all the other are the SiO of conventional granulates
2
The normally calcareous transparent of glaze that obtains by prescription of the present invention.
In the preparation method of warm blue and white porcelain goods, wherein: the component of sapphire blue color material comprises by weight: SiO
234.48～43.06 parts; Al
2O
311.46～12.69 parts; B
2O
36.68～7.59 parts; Co
2O
313.97～19.78 parts; Fe
2O
33.00～5.12 parts; 3.24～6.79 parts of CaO; 1.30～2.21 parts of MgO; 0.86～1.27 part of BaO; 1.00～4.57 parts of CuO; 1.18～2.92 parts of MnO; 7.65～9.18 parts of K Na O.
In the preparation method of warm blue and white porcelain goods, wherein: the component of blank comprises by weight: SiO
265～70 parts; Al
2O
318～22 parts; Fe
2O
30.2～0.5 part; 0.1～1.0 part of CaO; 0.1～1.0 part of MgO; K
22.9～3.5 parts of O; Na
21.4～2.0 parts of O; Li
20～0.5 part of O; IL.5.3～6.5 part.
In the preparation method of warm blue and white porcelain goods, wherein: middle temperature blue and white porcelain adopts under the glaze and decorates, the cotton paper stained paper pasting that lines are printed with sapphire blue color material is transferred on the mold, color lump is with the combined decoration method that colors in and expect.
In the preparation method of warm blue and white porcelain goods, wherein: goods once fill burning with refractory slab, support or saggar in roller kilns, shuttle kiln and tunnel cave.
Loss on ignition in the normally ceramic porcelain of the IL field, loss on ignition are meant crystallization moisture content and the loss on ignition of organic matters matter under warm-up mode in the pug, and IL does not influence the quality of product usually.
Advantage of the present invention is as follows:
In warm bule and white porcelain passed on the decoration technique of the Jing Dezhen bule and white porcelain of one of world culture art rarity, comprise decal paper, the material that colors in, beat color limit etc., incorporated modern technology in producing porcelain, the present invention is owing to having adopted special sapphire blue color material and base, glaze formula, the method that warm oxydizing flame burns till fast in can adopting, the state basic policy that meets energy-conserving and environment-protective creates characteristic sapphire blue bule and white porcelain goods.
Adopt sapphire blue color material of the present invention and base, glaze formula, the product that middle temperature oxidizing flame obtains and traditional color material and base, glaze formula, the product that the high-temperature oxydation flame obtains is compared, and adopts firing time of the present invention shorter, and firing temperature is lower, and outward appearance is also more beautiful.Thereby saved the energy, also improved industrial production efficient.Concrete advantage is as follows with the form contrast:
| Project | Conventional high-temperature blue and white porcelain | Warm blue and white porcelain in of the present invention |
| Temperature | About 1320 ℃ | 1 ℃～125 ℃ |
| Flame | Reducing flame | Oxidizing flame |
| Firing time | 18～24 hours | 6～10 hours |
| The defective that produces easily | Easily smoking, violate yellow, blue and white color and luster is inconsistent | Be not easy smoking, the inconsistent sensation of no color and luster |
Specific embodiment:
Embodiment 1
The preparation method of warm bule and white porcelain in a kind of, wherein: following steps are arranged successively:
(1) preparation mud cake; (2) compression moulding; (3) dry moulded pottery not yet put in a kiln to bake; (4) on the blank of mill base, moisturizing, directly pasting the cotton paper marble paper of printing with sapphire blue color material, the material that colors in, glazing, 1 ℃～1 ℃ of firing temperature, in the oxidizing atmosphere, 6～10 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO
262～67 parts; Al
2O
38.5～11.5 parts; Fe
2O
30.08～0.15 part; 8.0～11.5 parts of CaO; 2.0～3.5 parts of MgO; K
23.5～4.5 parts of O; Na
21.0～2.0 parts of O; 1.0～2.5 parts of ZnO; Li
20～0.3 part of O; 4.55～6.35 parts of IL; SiO wherein
2Be that nanoscale and diameter are that two kinds of conventional particles form by diameter, the SiO of nano-scale particle wherein
21～5 part, all the other are the SiO of conventional granulates
2
Wherein: the component of sapphire blue color material comprises by weight: SiO
234.48～43.06 parts; Al
2O
311.46～12.69 parts; B
2O
36.68～7.59 parts; Co
2O
313.97～19.78 parts; Fe
2O
33.00～5.12 parts; 3.24～6.79 parts of CaO; 1.30～2.21 parts of MgO; 0.86～1.27 part of BaO; 1.00～4.57 parts of CuO; 1.18～2.92 parts of MnO; 7.65～9.18 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO
265～70 parts; Al
2O
318～22 parts; Fe
2O
30.2～0.5 part; 0.1～1.0 part of CaO; 0.1～1.0 part of MgO; K
22.9～3.5 parts of O; Na
21.4～2.0 parts of O; Li
20～0.5 part of O; 5.3～6.5 parts of IL.
Embodiment 2
The preparation method of warm bule and white porcelain in a kind of, 1 ℃ of firing temperature, in the oxidizing atmosphere, 10 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO
262 parts; Al
2O
38.5 part; Fe
2O
30.08 part; 8.0 parts of CaO; 2.0 parts of MgO; K
23.5 parts of O; Na
21.0 parts of O; 1.0 parts of ZnO; Li
20 part of O; 4.55 parts of IL; SiO wherein
2Be that nanoscale and diameter are that two kinds of conventional particles form by diameter, the SiO of nano-scale particle wherein
21 part, all the other are the SiO of conventional granulates
261 parts.
Wherein: the component of sapphire blue color material comprises by weight: SiO
234.48 part; Al
2O
311.46 part; B
2O
36.68 part; Co
2O
313.97 part; Fe
2O
33.00 part; 3.24 parts of CaO; 1.30 parts of MgO; 0.86 part of BaO; 1.00 parts of CuO; 1.18 parts of MnO; 7.65 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO
265 parts; Al
2O
318 parts; Fe
2O
30.2 part; 0.1 part of CaO; 0.1 part of MgO; K
22.9 parts of O; Na
21.4 parts of O; Li
20 part of O; 5.3 parts of IL.
All the other are with embodiment 1.
Embodiment 3
The preparation method of warm bule and white porcelain in a kind of, 1 ℃ of firing temperature, in the oxidizing atmosphere, 6 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO
267 parts; Al
2O
311.5 part; Fe
2O
30.15 part; 11.5 parts of CaO; 3.5 parts of MgO; K
24.5 parts of O; Na
22.0 parts of O; 2.5 parts of ZnO; Li
20.3 part of O; 6.35 parts of IL; SiO wherein
2Be that nanoscale and diameter are that two kinds of conventional particles form by diameter, the SiO of nano-scale particle wherein
25 parts, all the other are the SiO of conventional granulates
262 parts.
Wherein: the component of sapphire blue color material comprises by weight: SiO
243.06 part; Al
2O
312.69 part; B
2O
37.59 part; Co
2O
319.78 part; Fe
2O
35.12 part; 6.79 parts of CaO; 2.21 parts of MgO; 1.27 parts of BaO; 4.57 parts of CuO; 2.92 parts of MnO; 9.18 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO
270 parts; Al
2O
322 parts; Fe
2O
30.5 part; 1.0 parts of CaO; 1.0 parts of MgO; K
23.5 parts of O; Na
22.0 parts of O; Li
20.5 part of O; 6.5 parts of IL.
All the other are with embodiment 1.
Embodiment 4
The preparation method of warm bule and white porcelain in a kind of, 1120 ℃ of firing temperatures, in the oxidizing atmosphere, 8 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO
263 parts; Al
2O
39.5 part; Fe
2O
30.12 part; 9.5 parts of CaO; 2.5 parts of MgO; K
23.9 parts of O; Na
21.5 parts of O; 1.5 parts of ZnO; Li
20.2 part of O; IL5.25 part; SiO wherein
2Be that nanoscale and diameter are that two kinds of conventional particles form by diameter, the SiO of nano-scale particle wherein
23 parts, all the other are the SiO of conventional granulates
260 parts.
Wherein: the component of sapphire blue color material comprises by weight: SiO
242.01 part; Al
2O
311.89 part; B
2O
36.99 part; Co
2O
315.28 part; Fe
2O
34.22 part; 4.29 parts of CaO; 1.77 parts of MgO; 0.89 part of BaO; 2.22 parts of CuO; 1.92 parts of MnO; 8.68 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO
269 parts; Al
2O
321 parts; Fe
2O
30.3 part; 0.8 part of CaO; 0.6 part of MgO; K
23.2 parts of O; Na
21.8 parts of O; Li
20.3 part of O; 5.8 parts of IL.
All the other are with embodiment 1.
Embodiment 5
The preparation method of warm bule and white porcelain in a kind of, 1190 ℃ of firing temperatures, in the oxidizing atmosphere, 9 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO
262 parts; Al
2O
311.5 part; Fe
2O
30.15 part; 11.5 parts of CaO; 2.0 parts of MgO; K
24.5 parts of O; Na
21.0 parts of O; 2.5 parts of ZnO; Li
20.3 part of O; 4.55 parts of IL; SiO wherein
2Be that nanoscale and diameter are that two kinds of conventional particles form by diameter, the SiO of nano-scale particle wherein
21 part, all the other are the SiO of conventional granulates
261 parts.
Wherein: the component of sapphire blue color material comprises by weight: SiO
234.48 part; Al
2O
312.69 part; B
2O
37.59 part; Co
2O
319.78 part; Fe
2O
33.00 part; 6.79 parts of CaO; 1.30 parts of MgO; 1.27 parts of BaO; 4.57 parts of CuO; 2.92 parts of MnO; 9.18 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO
270 parts; Al
2O
318 parts; Fe
2O
30.2 part; 0.1 part of CaO; 1.0 parts of MgO; K
22.9 parts of O; Na
22.0 parts of O; Li
20.5 part of O; 5.3 parts of IL.
All the other are with embodiment 1.
Embodiment 6
The preparation method of warm bule and white porcelain in a kind of, 1210 ℃ of firing temperatures, in the oxidizing atmosphere, 7 hours conditions of firing time are adorned burnt product next time.
Wherein: the component of glaze comprises by weight: SiO
267 parts; Al
2O
38.5 part; Fe
2O
30.08 part; 8.0 parts of CaO; 3.5 parts of MgO; K
23.5 parts of O; Na
22.0 parts of O; 1.0 parts of ZnO; Li
20.3 part of O; 6.42 parts of IL; SiO wherein
2Be that nanoscale and diameter are that two kinds of conventional particles form by diameter, the SiO of nano-scale particle wherein
25 parts, all the other are the SiO of conventional granulates
262 parts.
Wherein: the component of sapphire blue color material comprises by weight: SiO
243.06 part; Al
2O
311.46 part; B
2O
36.68 part; Co
2O
313.97 part; Fe
2O
35.12 part; 3.24 parts of CaO; 2.21 parts of MgO; 0.86 part of BaO; 4.57 parts of CuO; 1.18 parts of MnO; 7.65 parts of K Na O.
Wherein: the component of blank comprises by weight: SiO
265 parts; Al
2O
322 parts; Fe
2O
30.5 part; 1.0 parts of CaO; 0.1 part of MgO; K
23.5 parts of O; Na
21.4 parts of O; 6.5 parts of IL.
All the other are with embodiment 1.
Claims (7)
1, the preparation method of warm bule and white porcelain in a kind of, it is characterized in that: following steps are arranged successively: on the blank of mill base, moisturizing, directly pasting the cotton paper marble paper of printing with sapphire blue color material, material colors in, glazing, 1 ℃～1 ℃ of firing temperature, in the oxidizing atmosphere, 6～10 hours conditions of firing time are adorned burnt product next time.
2, the preparation method of warm bule and white porcelain goods in as claimed in claim 1 is characterized in that: before the blank of mill base, moisturizing, have the following steps successively: (1) preparation mud cake; (2) compression moulding; (3) dry moulded pottery not yet put in a kiln to bake.
3, the preparation method of warm blue and white porcelain goods in as claimed in claim 1 or 2, it is characterized in that: the component of glaze comprises by weight: SiO
262～67 parts; Al
2O
38.5～11.5 parts; Fe
2O
30.08～0.15 part; CaO8.0～11.5 part; MgO2.0～3.5 part; K
2O3.5～4.5 part; Na
2O1.0～2.0 part; ZnO1.0～2.5 part; Li
2O0～0.3 part; IL4.55～6.35 part; SiO wherein
2Be that nanoscale and diameter are that two kinds of conventional particles form by diameter, the SiO of nano-scale particle wherein
21～5 part, all the other are the SiO of conventional granulates
2
4, the preparation method of warm blue and white porcelain goods in as claimed in claim 1 or 2 is characterized in that: the component of sapphire blue color material comprises by weight: SiO
234.48～43.06 parts; Al
2O
311.46～12.69 parts; B
2O
36.68～7.59 parts; Co
2O
313.97～19.78 parts; Fe
2O
33.00～5.12 parts; CaO3.24～6.79 part; MgO1.30～2.21 part; BaO0.86～1.27 part; CuO1.00～4.57 part; MnO1.18～2.92 part; 7.65～9.18 parts of K Na O.
5, the preparation method of warm blue and white porcelain goods in as claimed in claim 1 or 2, it is characterized in that: the component of blank comprises by weight: SiO
265～70 parts; Al
2O
318～22 parts; Fe
2O
30.2～0.5 part; CaO0.1～1.0 part; MgO0.1～1.0 part; K
2O2.9～3.5 part; Na
2O1.4～2.0 part; Li
2O0～0.5 part; IL.5.3～6.5 part.
6, the preparation method of warm blue and white porcelain goods in as claimed in claim 2 is characterized in that: middle temperature blue and white porcelain adopts under the glaze and decorates, and the cotton paper stained paper pasting that lines are printed with sapphire blue color material is transferred on the mold, and color lump is with the combined decoration method that colors in and expect.
7, the preparation method of warm bule and white porcelain goods in as claimed in claim 2, it is characterized in that: goods are once adorned burning with refractory slab, support or saggar in roller kiln, shuttle kiln and tunnel furnace.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009101149898A CN101525249B (en) | 2009-03-04 | 2009-03-04 | Preparation method of middle temperature blue and white porcelain |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009101149898A CN101525249B (en) | 2009-03-04 | 2009-03-04 | Preparation method of middle temperature blue and white porcelain |
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| Publication Number | Publication Date |
|---|---|
| CN101525249A true CN101525249A (en) | 2009-09-09 |
| CN101525249B CN101525249B (en) | 2011-09-14 |
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ID=41093346
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009101149898A Expired - Fee Related CN101525249B (en) | 2009-03-04 | 2009-03-04 | Preparation method of middle temperature blue and white porcelain |
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| CN102417346A (en) * | 2011-08-26 | 2012-04-18 | 钦州市华夏太极泉坭兴陶艺有限责任公司 | Preparation technology of blue-and-white Nixing ceramics |
| CN102464488A (en) * | 2010-11-04 | 2012-05-23 | 福建省泉州龙鹏集团有限公司 | Medium-temperature-oxidized high-whiteness blue jade porcelain and preparation method thereof |
| CN103183525A (en) * | 2013-03-29 | 2013-07-03 | 深圳市永丰源瓷业有限公司 | Blue-and-white pigment used in bone china and fabricating technology for blue-and-white bone china |
| CN103936461A (en) * | 2014-04-04 | 2014-07-23 | 安徽青花坊瓷业股份有限公司 | Blue and white porcelain shaft material formula |
| CN104744078A (en) * | 2015-03-31 | 2015-07-01 | 马健 | Firing technique of blue-and-white underglaze red |
| CN106738238A (en) * | 2016-12-10 | 2017-05-31 | 彭良泉 | A kind of preparation method of blue and white porcelain |
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| JP3399650B2 (en) * | 1994-08-11 | 2003-04-21 | 邦雄 平石 | Heat and oxidation resistant coating method |
| JP2860262B2 (en) * | 1995-03-28 | 1999-02-24 | 日本碍子株式会社 | Method of firing glazed porcelain |
| CN1165122A (en) * | 1997-02-03 | 1997-11-19 | 景德镇市宇宙瓷业有限公司 | High-temp. |
| CN1253124A (en) * | 1998-10-29 | 2000-05-17 | 淄博通博高档骨质瓷有限责任公司 | Green porcelain glaze and process for preparing products of green porcelain glaze |
| CN101244950A (en) * | 2008-03-27 | 2008-08-20 | 湖南华联瓷业有限公司 | Method for manufacturing middle-temperature ceramics for daily use crackle glaze |
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- 2009-03-04 CN CN2009101149898A patent/CN101525249B/en not_active Expired - Fee Related
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| CN102464488A (en) * | 2010-11-04 | 2012-05-23 | 福建省泉州龙鹏集团有限公司 | Medium-temperature-oxidized high-whiteness blue jade porcelain and preparation method thereof |
| CN102417346A (en) * | 2011-08-26 | 2012-04-18 | 钦州市华夏太极泉坭兴陶艺有限责任公司 | Preparation technology of blue-and-white Nixing ceramics |
| CN102417346B (en) * | 2011-08-26 | 2013-07-03 | 钦州市华夏太极泉坭兴陶艺有限责任公司 | Preparation technology of blue-and-white Nixing ceramics |
| CN103183525A (en) * | 2013-03-29 | 2013-07-03 | 深圳市永丰源瓷业有限公司 | Blue-and-white pigment used in bone china and fabricating technology for blue-and-white bone china |
| CN103183525B (en) * | 2013-03-29 | 2014-07-30 | 深圳市永丰源瓷业有限公司 | Blue-and-white pigment used in bone china and fabricating technology for blue-and-white bone china |
| CN103936461A (en) * | 2014-04-04 | 2014-07-23 | 安徽青花坊瓷业股份有限公司 | Blue and white porcelain shaft material formula |
| CN104744078A (en) * | 2015-03-31 | 2015-07-01 | 马健 | Firing technique of blue-and-white underglaze red |
| CN106738238A (en) * | 2016-12-10 | 2017-05-31 | 彭良泉 | A kind of preparation method of blue and white porcelain |
| CN106865986A (en) * | 2017-02-14 | 2017-06-20 | 尹念党 | A kind of brilliant just alabaster material and preparation method and application |
| CN108274598A (en) * | 2017-12-07 | 2018-07-13 | 苏州物非物文化创意有限公司 | A kind of production method of ceramics colouring |
| CN108903157A (en) * | 2018-08-08 | 2018-11-30 | 阮舒涵 | Blue and white porcelain jewelry processing method and necklace, ear nail, ring |
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| CN101525249B (en) | 2011-09-14 |
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