CN101514042B - Method for preparing humic acid fish and veterinary drug preparations by traditional Chinese medicine residues - Google Patents
Method for preparing humic acid fish and veterinary drug preparations by traditional Chinese medicine residues Download PDFInfo
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- CN101514042B CN101514042B CN2009100586708A CN200910058670A CN101514042B CN 101514042 B CN101514042 B CN 101514042B CN 2009100586708 A CN2009100586708 A CN 2009100586708A CN 200910058670 A CN200910058670 A CN 200910058670A CN 101514042 B CN101514042 B CN 101514042B
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- chinese medicine
- medicine slag
- humic acid
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Abstract
The invention provides a method for preparing humic acid fish and veterinary drug preparations by traditional Chinese medicine residues, comprising the following steps: the traditional Chinese medicine residues are cooled after the decoction by water to be below 38 DEG C, compound beneficial microorganism bacteria are added in the traditional Chinese medicine residues for mixing according to the proportion of 3-10Kg of the compound beneficial microorganism bacteria for each ton of the traditional Chinese medicine residues, then a nitrogen source is added into the traditional Chinese medicine residues which are mixed with the compound beneficial microorganism bacteria according to the proportion of 3-80Kg of the nitrogen source for each ton of the traditional Chinese medicine residues, themixture is sealed for 10-40 days after even mixing, the external temperature thereof is maintained between 15 to 38 DGE C, the mixed traditional Chinese medicine residues after the maturity are addedinto alkaline compound liquid, supernatant fluid is taken out, and a finished product with the humic acid content of being not less than 50 percent is prepared by concentration and drying. The methodhas simplicity, low cost and high humic acid content, thereby turning waste into treasure.
Description
Technical field:
The present invention is relevant with the method for preparing fish, veterinary drug preparation, and especially to prepare the method for humic acid fish, veterinary drug preparation relevant with Chinese medicine slag.
Background technology:
The processing of Chinese medicine slag at present is to adopt the subterranean method of people of burying, and takes up an area of and polluted water, and abundant humic acid matrix-based resource is arranged in the Chinese medicine slag, imbeds underground, also very unfortunate.
Humic acids in the existing fish medicine is to extract from top layer coal or marsh mud, the coal resource exhaustion, and owing to the wet land protection policy, also forbidden from the mud of marsh, to extract humic acids.
The nineties, fish, medicine humic acids were extracted in discussion from straw stalk, leaves, at first were with straw stalk, leaves fragmentation, steaming and decocting, made its fibrosis, and complex process has increased production cost greatly.
Summary of the invention:
The objective of the invention is in order to overcome above deficiency the method that provide that a kind of manufacture method is simple, cost is low, humic acids content height, the Chinese medicine slag of turning waste into wealth prepares humic acid fish, beastly Chinese medicine preparation.
The object of the present invention is achieved like this:
The present invention prepares humic acid fish, the method of veterinary drug preparation, this method is that the Chinese medicine slag that will boil through decocting cools to below 38 ℃, the beneficial microorganism bacterium calculating adding in Chinese medicine slag that is compounded with that adds 3～10Kg by Chinese medicine slag per ton is compounded with the beneficial microorganism bacterium, mix, add 3～80Kg urine source by Chinese medicine slag per ton again and calculate adding urine source in being mixed with the Chinese medicine slag that is compounded with the beneficial microorganism bacterium, behind the mix homogeneously airtight 10～40 days, its external temperature is remained between 15～38 ℃, after waiting to become thoroughly decomposed, mixing Chinese medicine slag after will becoming thoroughly decomposed is put into alkaline complex liquid, takes out supernatant, concentrates, drying makes the finished product of humic acids content 〉=50%.
The above-mentioned beneficial microorganism bacterium that is compounded with is made up of following component by weight percentage:
Yeast 10～20,
Lactobacillus 5～20,
Acetic acid bacteria 5～20,
Photosynthetic bacteria 5～20,
Bacillus subtilis 5～20,
Whiterot fungi 10～30.
The above-mentioned beneficial microorganism bacterium that is compounded with should be qualified through the safety detection of health and epidemic prevention station above the provincial level.
Above-mentioned nitrogenous source is amine carbonate, carbamide, at least a in the chick excrement of fermentation maturity.
Above-mentioned alkaline complex liquid is the complex liquid of sodium hydroxide or potassium hydroxide or oxyammonia and sodium hydrogen phosphate and water.
Above-mentioned mixing Chinese medicine slag airtight winter time is 30～40 days, is respectively in spring, autumn 15～25 days, and be 10～20 days summer.
Mixing Chinese medicine slag after will becoming thoroughly decomposed in the above-mentioned method is put in people's alkalescence complex liquid and is soaked, stirred 12～48 hours, takes out supernatant.
Mixing Chinese medicine slag after will becoming thoroughly decomposed in the above-mentioned method is put in the people alkalescence complex liquid through microwave and/or ultrasonic Treatment 15～60 minutes, takes out supernatant, fulvic acid content 〉=60% in the finished product that makes.
Chinese medicine slag in the inventive method is pulverized in decocting process, and fiber is softening, so simplified production procedure greatly, has reduced production cost.The fish that process the inventive method is produced, humic acids content 〉=50% in the veterinary drug preparation.Through a large amount of tests, prove that fish, veterinary drug humic acids preparation that the inventive method is produced are used for fosterly planting fish, can be in 1 hour with the heavy metal flocculation sediment, with hydrogen sulfide, pesticide residue and organic phosphates: as P
2(SO
4)
3Complexation reduces the infringement to Fish of poisonous, harmful substance, is of value to health after people's ichthyophagy.The fish that the inventive method is produced, veterinary drug humic acids preparation have facilitation to the useful thing growth of supporting one's family (as the algae thing of supporting one's family).
Manufacture method of the present invention is simple, and production cost is low, and humic acids content height is turned waste into wealth, and is beneficial to health.
The specific embodiment:
Embodiment 1:
The fresh Chinese medicine slag (water content is more than 50%) of coming out of the stove after decocting boils Radix Ophiopogonis is cooled to about 35 ℃ naturally, by Chinese medicine slag per ton add 5Kg be compounded with the beneficial microorganism bacterium calculate the safety detection that in Chinese medicine slag, adds through Sichuan Province health and epidemic prevention station qualified be compounded with the beneficial microorganism bacterium, mix, the chick excrement (or amine carbonate/or carbamide) that adds the 50Kg fermentation maturity by medicinal residues per ton calculates and add the chick excrement of fermentation maturity (or amine carbonate/or carbamide) in being mixed with the medicinal residues that are compounded with the beneficial microorganism bacterium again, pack into behind the mix homogeneously in the Polywoven Bag, heap was deposited airtight 10～40 days, its external temperature is remained between 15～38 ℃, after waiting to become thoroughly decomposed, mixing Chinese medicine slag after will becoming thoroughly decomposed inclines for soaking in alkaline complex liquid 12～48 hours in concrete floor or the simple and easy pond of plastics, stir repeatedly, take out supernatant, concentrate, spray drying makes the finished product of humic acids content 〉=50%.
The above-mentioned beneficial microorganism bacterium that is compounded with is made up of following component by weight percentage:
Yeast 20,
Lactobacillus 15,
Acetic acid bacteria 15,
Photosynthetic bacteria 10,
Bacillus subtilis 10,
Whiterot fungi 30.
The alkalescence complex liquid is that weight is 2% the sodium hydroxide of alkaline complex liquid gross weight and the complex liquid of 0.1N sodium hydrogen phosphate and water.
Mixing Chinese medicine slag airtight winter time is 30～40 days, and spring, autumn are 15～25 days, and be 10～20 days summer.
Embodiment 2:
The fresh Chinese medicine slag (water content 30% or more) of Folium Camelliae sinensis after decocting boils cooled to about 35 ℃ naturally, by Chinese medicine slag per ton add 4Kg be compounded with the beneficial microorganism bacterium calculate the safety detection that in Chinese medicine slag, adds through Sichuan Province health and epidemic prevention station qualified be compounded with the beneficial microorganism bacterium, mix, add the 5Kg amine carbonate by medicinal residues per ton again and in being mixed with the medicinal residues that are compounded with the beneficial microorganism bacterium, add accumulation deposit in the hermetic container of packing into behind the amine carbonate mix homogeneously, airtight 10～40 days, its external temperature is remained between 15～38 ℃, after waiting to become thoroughly decomposed, mixing medicinal residues after will becoming thoroughly decomposed are put in people's alkalescence complex liquid, microwave treatment ultrasonic Treatment 15 minutes again after 15 minutes, get supernatant, concentrate, spray drying makes the finished product of humic acids content 〉=50%, wherein fulvic acid content＞60%.
The above-mentioned beneficial microorganism bacterium that is compounded with is made up of following component by weight percentage:
Yeast 20,
Lactobacillus 15,
Acetic acid bacteria 15,
Photosynthetic bacteria 20,
Bacillus subtilis 20,
Whiterot fungi 10.
Above-mentioned alkaline complex liquid is the complex liquid of 2% potassium hydroxide and 0.1N sodium hydrogen phosphate and water.
Above-mentioned mixing Chinese medicine slag airtight winter time is 30～40 days, and spring, autumn are 15～25 days, and be 10～20 days summer.
Claims (6)
1. Chinese medicine slag prepares humic acid fish, the method of veterinary drug preparation, this method is that the Chinese medicine slag that will boil through decocting cools to below 38 ℃, the beneficial microorganism bacterium calculating adding in Chinese medicine slag that is compounded with that adds 3～10Kg by Chinese medicine slag per ton is compounded with the beneficial microorganism bacterium, mix, add the calculating of 3～80Kg nitrogenous source by Chinese medicine slag per ton again and in being mixed with the Chinese medicine slag that is compounded with the beneficial microorganism bacterium, add nitrogenous source, behind the mix homogeneously airtight 10～40 days, its external temperature is remained between 15～38 ℃, after waiting to become thoroughly decomposed, mixing Chinese medicine slag after will becoming thoroughly decomposed is put into alkaline complex liquid, take out supernatant, concentrate, drying makes the finished product of humic acids content 〉=50%, is compounded with the beneficial microorganism bacterium and is made up of following component by weight percentage:
Yeast 10～20,
Lactobacillus 5～20,
Acetic acid bacteria 5～20,
Photosynthetic bacteria 5～20,
Bacillus subtilis 5～20,
Whiterot fungi 10～30.
2. Chinese medicine slag as claimed in claim 1 prepares the method for humic acid fish, veterinary drug preparation, it is characterized in that nitrogenous source is amine carbonate, carbamide, at least a in the chick excrement of fermentation maturity.
3. Chinese medicine slag as claimed in claim 1 or 2 prepares the method for humic acid fish, veterinary drug preparation, it is characterized in that alkaline complex liquid is the complex liquid of sodium hydroxide or potassium hydroxide or oxyammonia and sodium hydrogen phosphate and water.
4. Chinese medicine slag as claimed in claim 1 or 2 prepares the method for humic acid fish, veterinary drug preparation, and it is characterized in that mixing Chinese medicine slag airtight winter time is 30～40 days, is respectively in spring, autumn 15～25 days, and be 10～20 days summer.
5. Chinese medicine slag as claimed in claim 1 or 2 prepares the method for humic acid fish, veterinary drug preparation, it is characterized in that the mixing Chinese medicine slag after becoming thoroughly decomposed is put into alkaline complex liquid to be soaked, stirred 12～48 hours, takes out supernatant.
6. Chinese medicine slag as claimed in claim 1 or 2 prepares the method for humic acid fish, veterinary drug preparation, it is characterized in that the mixing Chinese medicine slag after becoming thoroughly decomposed is put into alkaline complex liquid through microwave and/or ultrasonic Treatment 15～60 minutes, takes out supernatant.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100586708A CN101514042B (en) | 2009-03-23 | 2009-03-23 | Method for preparing humic acid fish and veterinary drug preparations by traditional Chinese medicine residues |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2009100586708A CN101514042B (en) | 2009-03-23 | 2009-03-23 | Method for preparing humic acid fish and veterinary drug preparations by traditional Chinese medicine residues |
Publications (2)
| Publication Number | Publication Date |
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| CN101514042A CN101514042A (en) | 2009-08-26 |
| CN101514042B true CN101514042B (en) | 2010-12-29 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2009100586708A Expired - Fee Related CN101514042B (en) | 2009-03-23 | 2009-03-23 | Method for preparing humic acid fish and veterinary drug preparations by traditional Chinese medicine residues |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104017755A (en) * | 2014-05-20 | 2014-09-03 | 郑州市三维配电设备有限公司 | Medicinal-residue fermentation bacterial group and medicinal-residue fermentation technology |
| CN106241998B (en) * | 2016-09-26 | 2019-02-19 | 重庆工商大学 | A method of natural composite flocculation agent is prepared with Chinese medicine dreg |
| CN109576333A (en) * | 2018-12-06 | 2019-04-05 | 成都大学 | A method of fulvic acid is prepared using Salvia miltiorrhiza stem and the dregs of a decoction |
| CN111036647B (en) * | 2019-12-12 | 2021-07-27 | 安徽省农业科学院水产研究所 | Freshwater fish viscera recycling method based on mixed strain solid state fermentation |
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Address after: 610066 Sichuan Provincial Academy of Agricultural Sciences, Jinjiang District Province, Sichuan Province, Lion Hill Road, No. 4, Institute of agricultural products processing Patentee after: Song Yan Address before: 610100, No. 588, east route, Longquan Economic Development Zone, Chengdu, Sichuan Patentee before: Song Yan |
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Granted publication date: 20101229 Termination date: 20200323 |