CN101507734A - Deer-bone serial processing method - Google Patents
Deer-bone serial processing method Download PDFInfo
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- CN101507734A CN101507734A CNA2009101317130A CN200910131713A CN101507734A CN 101507734 A CN101507734 A CN 101507734A CN A2009101317130 A CNA2009101317130 A CN A2009101317130A CN 200910131713 A CN200910131713 A CN 200910131713A CN 101507734 A CN101507734 A CN 101507734A
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Abstract
The invention provides a method for serial processing of deer bone. Products such as deer bone powder, deer bone oil, crystalline particles extracted from the deer bone, deer bone collagen particles and the like, are prepared through the processing treatment to the deer bone such as water boiling, separation, freeze drying and the like. The method can extract effective ingredients and keep active substances of marrow not destroyed, greatly improve the efficacy, and avoid the waste caused by single processing at the same time. The products, namely the crystalline particles extracted from the deer bone and the deer bone collagen particles have efficacies of resisting fatigue, improving the immunity and the like. The deer bone powder has functions of supplementing calcium, strengthening tendons and bones, activating blood and supplementing qi, resisting senility and the like. The products have the special effect of comprehensive treatment on osteoporosis, cervical spondylosis, lumbar vertebra disease, arthritis and the like, can promote bone healing to traumatic fracture, and can be fully absorbed and utilized by bone. The deer bone products after the processing can become novel raw materials in the fields such as food, health care products and the like.
Description
Technical field
The present invention relates to bio-pharmaceuticals, functional food and health product production and processing technical field.
Background technology
China is the country that produces the deer most species in the world.Deer belongs to the animal of Cervidae, and the whole world has 17 and belongs to, 38 kinds, wherein have 10 belong to, 18 kinds once produced or still produced now in China.In other words, the deer of China accounts for over half that world deer belongs to, account for world's deer kind nearly half.The areas such as the Northeast, northwest, Hebei and Sichuan of China all are the main culture zones of deer.Along with the human living standard improves gradually, the value of researchs such as the medical science of Os Cervi, pharmacy and health care aspect is come into one's own.
Os Cervi is the side-product in the deer slaughtering process, usually is used for the animal protein feed additive.Along with people further discover, contain the necessary material of collagen protein, proteoglycan, calcium phosphate, calcium carbonate, various trace elements and bone metabolism in the Os Cervi.How the active substance composition in the Os Cervi being extracted and keep the bone marrow active substance not to be destroyed, increase substantially effect, is the difficult problem that this area is never captured.
Summary of the invention
The objective of the invention is the abundant development and utilization of Os Cervi resource, provide a kind of the deer-bone serial method for processing.
Processing method provided by the invention, can be with collagen protein, the proteoglycan that contains in the Os Cervi, active substance compositions such as calcium phosphate, calcium carbonate, various trace elements and the necessary material of bone metabolism propose and keep the bone marrow active substance not to be destroyed, and increase substantially effect.
The present invention further separates the heterogeneity of Os Cervi by the decocting in water processing to Os Cervi, reaches the purpose that branch extracts, fully utilizes.
Method provided by the invention can be processed into Os Cervi deer bone powder, Os Cervi oil, Os Cervi extraction crystalline particle, deer-bone collagenous granule.
Processing method of the present invention comprises the steps:
(1) gets bright Os Cervi by processing of classifying such as excellent bone, skulls;
(2) Os Cervi of classification is put and carried out high temperature (100 ℃) decocting in water in the container, isolate water cooking liquid; Circulate three times, add clear water at every turn; Merge three times water cooking liquid; Os Cervi and water cooking liquid preserve separately that separation obtains is standby;
(3) clean, dry after isolated Os Cervi being removed the foreign material such as going up remaining meat muscle of boning, then exsiccant Os Cervi is pulverized, sterilized, what obtain at last is deer bone powder.
(4) water cooking liquid with step (2) concentrates, and three layers of upper, middle and lowers are divided in the cooling back, and the upper strata is the animal oil part; The middle level is amber paste; Lower floor is mixture such as broken bone, meat.
(5) after being concentrated, the upper strata in the step (4) obtains Os Cervi oil; After the middle level concentrates this product is carried out lyophilizing and handle, obtain Os Cervi and extract crystalline particle;
(6) after-filtration is heated in the lower floor in the step (4), concentrate, lyophilizing obtains deer-bone collagenous granule.
The preferred version of processing method provided by the invention is:
(1) gets bright Os Cervi and clean, carry out deeply with cutter, make and expose bone marrow, classify by excellent bone, skull etc. then.
(2) sorted Os Cervi is packed in the stainless-steel pan, add the 3-8 times of water yield (volume ratio) and carried out 100 ℃ of decocting in water 8 hours, isolate water cooking liquid; Circulate three times, add clear water at every turn; Merge three times water cooking liquid; Os Cervi and water cooking liquid preserve separately that separation obtains is standby;
(3) clean, dry after isolated Os Cervi being removed the foreign material such as going up remaining meat muscle of boning, then exsiccant Os Cervi is pulverized, sterilization, what obtain at last is deer bone powder.
(4) with step (2) but water cooking liquid be concentrated to volume with the hydrogen pot and no longer change, cooling, concentrated solution can be divided into three layers of upper, middle and lowers, separates, the upper strata is the animal oil part; The middle level is amber paste; Lower floor is mixture such as broken bone, meat.
(5) with step (4) but in the upper strata concentrate with the hydrogen pot and remove moisture and obtain Os Cervi oil; After but the middle level concentrates with the hydrogen pot, this product at-20 ℃ of precooling 3-4 hours, is carried out lyophilizing then and handled 24 hours, obtain Os Cervi and extract crystalline particle;
(6) lower floor in the step (4) is heated to 100 ℃ of after-filtration, but reuse hydrogen pot concentrate, this product at-20 ℃ of precooling 3-4 hours, is carried out lyophilizing then and handled 24 hours, obtain deer-bone collagenous granule.
The more preferably scheme of processing method provided by the invention is:
(1) gets bright Os Cervi and clean, carry out deeply with electronic deep cutter, make and expose bone marrow, classify by excellent bone, skull etc. then, be respectively charged in the rustless steel hurdle and (be provided with partition in the rustless steel shelves, the hurdle is divided into several zones, similar Os Cervi is placed in the same zone).
(2) the rustless steel hurdle of sorted Os Cervi will be housed, place in the stainless-steel pan, and add the 3-8 times of water yield (volume ratio) and carried out 100 ℃ of decocting in water 8 hours, isolate water cooking liquid; Circulate three times, add clear water at every turn; Merge three times water cooking liquid; Os Cervi and water cooking liquid preserve separately that separation obtains is standby;
(3) clean, utilize CT-1 type electric-controlled type hot air circulation drying machine drying after isolated Os Cervi being removed the foreign material such as going up remaining meat muscle of boning, utilize WL-100 type pulverizing mill to pulverize to exsiccant Os Cervi then, sterilization, what obtain at last is deer bone powder.
(4) with step (2) but water cooking liquid be concentrated to volume with the hydrogen pot and no longer change, cooling, concentrated solution can be divided into three layers of upper, middle and lowers, separates, the upper strata is the animal oil part; The middle level is amber paste; Lower floor is mixture such as broken bone, meat.
(5) with step (4) but in the upper strata concentrate with the hydrogen pot and remove moisture and obtain Os Cervi oil; After but the middle level concentrates with the hydrogen pot, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and carried out lyophilizing processing 24 hours, obtain Os Cervi and extract crystalline particle;
(6) lower floor in the step (4) is heated to 100 ℃ of after-filtration, but reuse hydrogen pot concentrate, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and is carried out lyophilizing and handled 24 hours, obtain deer-bone collagenous granule.
Os Cervi among the present invention can be the skeleton of animal in deer family Cervus nippon Temminck or Cervus elaphus linnaeus, as the skull of the skull of Cervus nippon Temminck, spine, bones of limbs etc. or Cervus elaphus linnaeus, spine, bones of limbs etc.
Processing method provided by the invention can propose the active substance composition and maintenance bone marrow active substance is not destroyed, and increases substantially effect, has avoided the waste that single processing caused simultaneously.It is as follows that the deer bone powder Os Cervi oil Os Cervi that the Flos Mume Os Cervi prepares with this processing method extracts the deer-bone collagenous particulate main nutrient composition content of crystalline particle:
Project zinc ug/g magnesium mg/g calcium mg/g copper ug/g manganese ug/g ferrum ug/g phosphorus mg/g
Deer bone powder 105.16 6.24 235.59 4.47 9.51 190.84 100.74
Deer-bone collagenous granule 48.03 0.93 8.01 34.59 6.51 326.74 6.18
Os Cervi extracts crystalline particle 55.38 0.49 5.11 32.58 3.28 55.97 5.39
Title deer bone powder % Os Cervi extracts the deer-bone collagenous granule % of crystalline particle %
Aspartic acid 1.52 3.58 4.96
Serine 0.51 2.51 3.62
Threonine 0.84 3.18 4.26
Glutamic acid 2.91 9.68 11.36
Glycine 5.62 2.76 2.78
Alanine 2.87 2.32 2.56
Cystine 0.46 4.21 4.98
Valine 0.76 4.56 5.03
Methionine 0.21 2.35 2.56
Isoleucine 0.44 2.78 2.91
Leucine 1.11 4.65 4.98
Tyrosine 0.21 1.89 2.18
Phenylalanine 0.79 3.25 3.45
Lysine 0.95 3.46 3.95
Histidine 0.32 2.74 2.89
Arginine 1.93 2.35 2.56
Proline 3 .17 4.95 5.31
Amount to 24.62 61.22 70.34
Os Cervi fatty acid oil relative amount %
Myristic acid C14:0 0.97
Palmic acid C16:0 25.00
The Petiolus Trachycarpi monoenoic acid
C16:1 1.36
Stearic acid C18:0 19.44
Oleic acid C18:1 37.57
Linoleic acid C18:2 10.96
Linolenic acid C18:3 0.47
Eicosapentaenoic acid
C20:5 0.6
Clupanodonic acid
C22:5 0.06
Product Os Cervi of the present invention extracts crystalline particle and deer-bone collagenous granule has effects such as resisting fatigue, raising immunity.Deer bone powder has supplement calcium, bone and muscle strengthening, the QI invigorating of invigorating blood circulation, the anti-ageing effect of waiting for a long time.The special-effect that osteoporosis, cervical spondylosis, lumbar spondylosis, arthritis etc. is had Comprehensive Treatment; Can promote knitting to traumatic fracture, can fully be absorbed by skeleton.Processing method provided by the invention, cost is low, is convenient to produce.
Content of the present invention is not limited in an embodiment, and embodiment is just for better explanation the present invention.Processing method of the present invention is applicable to all bone processing of deer.Can become novel material with this method in fields such as food, health product through the Os Cervi product after processing.
The specific embodiment
Embodiment 1
The spine 10Kg that gets bright Cervus nippon Temminck cleans, and carries out deeply with electronic deep cutter, makes and exposes bone marrow, and in the stainless steel square pot of packing into, adding is the water of 3 times of amounts of spine volume, 100 ℃ of decocting in water 8 hours; Circulate three times, add commensurability clear water at every turn, merge three times water cooking liquid; Separate bone and water cooking liquid, preserve separately is standby.
Clean, utilize CT-1 type electric-controlled type hot air circulation drying machine drying after the spine of isolated Cervus nippon Temminck removed the foreign material such as going up remaining meat muscle of boning, utilize WL-100 type pulverizing mill to pulverize to exsiccant Os Cervi then, sterilization, what obtain at last is Cervus nippon Temminck bone meal.
But being concentrated to volume with the hydrogen pot, the water cooking liquid of Cervus nippon Temminck spine no longer changes, cooling, and concentrated solution can be divided into three layers of upper, middle and lowers, separates, and the upper strata is the animal oil part, but removes moisture and obtain the Cervus nippon Temminck animal oil with the hydrogen pot is concentrated; The middle level is amber paste, but after using the hydrogen pot to concentrate, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and carried out lyophilizing processing 24 hours, obtains the Flos Mume Os Cervi and extracts crystalline particle; Lower floor is mixture such as broken bone, meat, be heated to 100 ℃ of after-filtration, but reuse hydrogen pot concentrate, with this product at-20 ℃ of precooling 3-4 hours, put into the full-automatic lyophilizing machine of CRYODOS type then and carry out lyophilizing processing 24 hours, obtain Cervus nippon Temminck ossein granule.
Embodiment 2
The skull 1Kg that gets bright Cervus nippon Temminck cleans, and carries out deeply with electronic deep cutter, makes and exposes bone marrow, and in the stainless steel square pot of packing into, the adding volume is the water of the amount of 4 times of skulls, 100 ℃ of decocting in water 8 hours; Circulate three times, add commensurability clear water at every turn, merge three times water cooking liquid; Separate bone and water cooking liquid, preserve separately is standby.
Clean, utilize CT-1 type electric-controlled type hot air circulation drying machine drying after the skull of isolated Cervus nippon Temminck removed the foreign material such as going up remaining meat muscle of boning, utilize WL-100 type pulverizing mill to pulverize to exsiccant Os Cervi then, the evacuation packing is carried out in sterilization, and what obtain at last is Cervus nippon Temminck bone meal.
But being concentrated to volume with the hydrogen pot, the water cooking liquid of deer flower deer skull no longer changes, cooling, and concentrated solution can be divided into three layers of upper, middle and lowers, separates, and the upper strata is the animal oil part, but removes moisture and obtain the Cervus nippon Temminck animal oil with the hydrogen pot is concentrated; The middle level is amber paste, but after using the hydrogen pot to concentrate, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and carried out lyophilizing processing 24 hours, obtains the Flos Mume Os Cervi and extracts crystalline particle; Lower floor is mixture such as broken bone, meat, be heated to 100 ℃ of after-filtration, but reuse hydrogen pot concentrate, with this product at-20 ℃ of precooling 3-4 hours, put into the full-automatic lyophilizing machine of CRYODOS type then and carry out lyophilizing processing 24 hours, obtain Cervus nippon Temminck ossein granule;
Embodiment 3
The bones of limbs 10Kg that gets bright Cervus nippon Temminck cleans, and carries out deeply with electronic deep cutter, makes and exposes bone marrow, and in the stainless steel square pot of packing into after deep, the adding volume is the water of the amount of 4 times of bones of limbs, 100 ℃ of decocting in water 8 hours; Circulate three times, add commensurability clear water at every turn, merge three times water cooking liquid; Separate bone and water cooking liquid, preserve separately is standby.
Clean, utilize CT-1 type electric-controlled type hot air circulation drying machine drying after the bones of limbs of isolated Cervus nippon Temminck removed the foreign material such as going up remaining meat muscle of boning, utilize WL-100 type pulverizing mill to pulverize to exsiccant Os Cervi then, sterilization, carry out the evacuation packing, what obtain at last is Cervus nippon Temminck bone meal.
But being concentrated to volume with the hydrogen pot, the water cooking liquid of deer flower deer bones of limbs no longer changes, cooling, and concentrated solution can be divided into three layers of upper, middle and lowers, separates, and the upper strata is the animal oil part, but removes moisture and obtain the Cervus nippon Temminck animal oil with the hydrogen pot is concentrated; The middle level is amber paste, but after using the hydrogen pot to concentrate, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and carried out lyophilizing processing 24 hours, obtains the Flos Mume Os Cervi and extracts crystalline particle; Lower floor is mixture such as broken bone, meat, be heated to 100 ℃ of after-filtration, but reuse hydrogen pot concentrate, with this product at-20 ℃ of precooling 3-4 hours, put into the full-automatic lyophilizing machine of CRYODOS type then and carry out lyophilizing processing 24 hours, obtain Cervus nippon Temminck ossein granule;
Embodiment 4
The spine 10Kg that gets bright Cervus elaphus linnaeus cleans, and carries out deeply with electronic deep cutter, makes and exposes bone marrow, and in the stainless steel square pot of packing into after deep, the adding volume is the water of the amount of 6 times of spines, 100 ℃ of decocting in water 8 hours; Circulate three times, add commensurability clear water at every turn, merge three times water cooking liquid; Separate bone and water cooking liquid, preserve separately is standby.
Clean, utilize CT-1 type electric-controlled type hot air circulation drying machine drying after the spine of isolated Cervus elaphus linnaeus removed the foreign material such as going up remaining meat muscle of boning, utilize WL-100 type pulverizing mill to pulverize to exsiccant Os Cervi then, the evacuation packing is carried out in sterilization, and what obtain at last is Cervus elaphus linnaeus bone meal.
But being concentrated to volume with the hydrogen pot, the water cooking liquid of Cervus elaphus linnaeus spine no longer changes, cooling, and concentrated solution can be divided into three layers of upper, middle and lowers, separates, and the upper strata is the animal oil part, but removes moisture and obtain the Cervus elaphus linnaeus animal oil with the hydrogen pot is concentrated; The middle level is amber paste, but after using the hydrogen pot to concentrate, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and carried out lyophilizing processing 24 hours, obtains Cervus elaphus Linnaeas bone and extracts crystalline particle; Lower floor is mixture such as broken bone, meat, be heated to 100 ℃ of after-filtration, but reuse hydrogen pot concentrate, with this product at-20 ℃ of precooling 3-4 hours, put into the full-automatic lyophilizing machine of CRYODOS type then and carry out lyophilizing processing 24 hours, obtain the Cervus elaphus Linnaeas bone collagen particle;
Embodiment 5
The skull 5Kg that gets bright Cervus elaphus linnaeus cleans, and carries out deeply with electronic deep cutter, makes and exposes bone marrow, and in the stainless steel square pot of packing into after deep, the adding volume is the water of the amount of 7 times of skulls, 100 ℃ of decocting in water 8 hours; Circulate three times, add commensurability clear water at every turn, merge three times water cooking liquid; Separate bone and water cooking liquid, preserve separately is standby.
Clean, utilize CT-1 type electric-controlled type hot air circulation drying machine drying after the skull of isolated Cervus elaphus linnaeus removed the foreign material such as going up remaining meat muscle of boning, utilize WL-100 type pulverizing mill to pulverize to exsiccant Os Cervi then, the evacuation packing is carried out in sterilization, and what obtain at last is Cervus elaphus linnaeus bone meal.
But being concentrated to volume with the hydrogen pot, the water cooking liquid of Cervus elaphus linnaeus skull no longer changes, cooling, and concentrated solution can be divided into three layers of upper, middle and lowers, separates, and the upper strata is the animal oil part, but removes moisture and obtain the Cervus elaphus linnaeus animal oil with the hydrogen pot is concentrated; The middle level is amber paste, but after using the hydrogen pot to concentrate, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and carried out lyophilizing processing 24 hours, obtains Cervus elaphus Linnaeas bone and extracts crystalline particle; Lower floor is mixture such as broken bone, meat, be heated to 100 ℃ of after-filtration, but reuse hydrogen pot concentrate, with this product at-20 ℃ of precooling 3-4 hours, put into the full-automatic lyophilizing machine of CRYODOS type then and carry out lyophilizing processing 24 hours, obtain the Cervus elaphus Linnaeas bone collagen particle;
Embodiment 6
The bones of limbs 2Kg that gets bright Cervus elaphus linnaeus cleans, and carries out deeply with electronic deep cutter, makes and exposes bone marrow, and in the stainless steel square pot of packing into after deep, the adding volume is the water of the amount of 8 times of bones of limbs, 100 ℃ of decocting in water 8 hours; Circulate three times, add commensurability clear water at every turn, merge three times water cooking liquid; Separate bone and water cooking liquid, preserve separately is standby.
Clean, utilize CT-1 type electric-controlled type hot air circulation drying machine drying after the bones of limbs of isolated Cervus elaphus linnaeus removed the foreign material such as going up remaining meat muscle of boning, utilize WL-100 type pulverizing mill to pulverize to exsiccant Os Cervi then, the evacuation packing is carried out in sterilization, and what obtain at last is Cervus elaphus linnaeus bone meal.
But being concentrated to volume with the hydrogen pot, the water cooking liquid of Cervus elaphus linnaeus bones of limbs no longer changes, cooling, and concentrated solution can be divided into three layers of upper, middle and lowers, separates, and the upper strata is the animal oil part, but removes moisture and obtain the Cervus elaphus linnaeus animal oil with the hydrogen pot is concentrated; The middle level is amber paste, but after using the hydrogen pot to concentrate, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and carried out lyophilizing processing 24 hours, obtains Cervus elaphus Linnaeas bone and extracts crystalline particle; Lower floor is mixture such as broken bone, meat, be heated to 100 ℃ of after-filtration, but reuse hydrogen pot concentrate, with this product at-20 ℃ of precooling 3-4 hours, put into the full-automatic lyophilizing machine of CRYODOS type then and carry out lyophilizing processing 24 hours, obtain the Cervus elaphus Linnaeas bone collagen particle.
Embodiment 7
(1) gets bright Os Cervi and clean, carry out deeply with electronic deep cutter, make and expose bone marrow, classify by excellent bone, skull etc. then, be respectively charged in the rustless steel hurdle and (be provided with partition in the rustless steel shelves, the hurdle is divided into several zones, similar Os Cervi is placed in the same zone).
(2) the rustless steel hurdle that sorted Os Cervi will be housed places in the stainless-steel pan, and the water that adds volume and be the amount of 3 times of Os Cervi volumes carried out 100 ℃ of decocting in water 8 hours, isolated water cooking liquid; Circulate three times, add clear water at every turn; Merge three times water cooking liquid; Os Cervi and water cooking liquid preserve separately that separation obtains is standby;
(3) clean, utilize CT-1 type electric-controlled type hot air circulation drying machine drying after isolated Os Cervi being removed the foreign material such as going up remaining meat muscle of boning, utilize WL-100 type pulverizing mill to pulverize to exsiccant Os Cervi then, sterilization, what obtain at last is deer bone powder.
(4) with step (2) but water cooking liquid be concentrated to volume with the hydrogen pot and no longer change, cooling, concentrated solution can be divided into three layers of upper, middle and lowers, separates, the upper strata is the animal oil part; The middle level is amber paste; Lower floor is mixture such as broken bone, meat.
(5) with step (4) but in the upper strata concentrate with the hydrogen pot and remove moisture and obtain Os Cervi oil; After but the middle level concentrates with the hydrogen pot, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and carried out lyophilizing processing 24 hours, obtain Os Cervi and extract crystalline particle;
(6) lower floor in the step (4) is heated to 100 ℃ of after-filtration, but reuse hydrogen pot concentrate, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and is carried out lyophilizing and handled 24 hours, obtain deer-bone collagenous granule.
Embodiment 8
(1) gets bright Os Cervi and clean, carry out deeply with electronic deep cutter, make and expose bone marrow, classify by excellent bone, skull etc. then, be respectively charged in the stainless-steel pan.
(2) adding volume is that the water of the amount of 3 times of Os Cervi volumes carried out 100 ℃ of decocting in water 8 hours, isolates water cooking liquid; Circulate three times, add clear water at every turn; Merge three times water cooking liquid; Os Cervi and water cooking liquid preserve separately that separation obtains is standby;
(3) clean, utilize CT-1 type electric-controlled type hot air circulation drying machine drying after isolated Os Cervi being removed the foreign material such as going up remaining meat muscle of boning, utilize WL-100 type pulverizing mill to pulverize to exsiccant Os Cervi then, sterilization, what obtain at last is deer bone powder.
(4) with step (2) but water cooking liquid be concentrated to volume with the hydrogen pot and no longer change, cooling, concentrated solution can be divided into three layers of upper, middle and lowers, separates, the upper strata is the animal oil part; The middle level is amber paste; Lower floor is mixture such as broken bone, meat.
(5) with step (4) but in the upper strata concentrate with the hydrogen pot and remove moisture and obtain Os Cervi oil; After but the middle level concentrates with the hydrogen pot, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and carried out lyophilizing processing 24 hours, obtain Os Cervi and extract crystalline particle;
(6) lower floor in the step (4) is heated to 100 ℃ of after-filtration, but reuse hydrogen pot concentrate, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and is carried out lyophilizing and handled 24 hours, obtain deer-bone collagenous granule.
Above embodiment, or not within the spirit and principles in the present invention not all only for the purpose of description in order to restriction the present invention, any modification of being done, be equal to replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (6)
1, a kind of to the deer-bone serial method for processing, it is characterized in that comprising the steps:
(1) getting bright Os Cervi classifies;
(2) Os Cervi of classification is put in the container, 100 ℃ of decocting in water are isolated water cooking liquid; Circulate three times, add clear water at every turn; Merge three times water cooking liquid; Os Cervi and water cooking liquid preserve separately is standby;
(3) Os Cervi that obtains is upward cleaned, dries behind the remaining foreign material except that boning, then exsiccant Os Cervi is pulverized, sterilized, obtain the deer bone powder product;
(4) water cooking liquid with step (2) concentrates, and three layers of upper, middle and lowers are divided in the cooling back, and the upper strata is the animal oil part; The middle level is amber paste; Lower floor is mixture such as broken bone, meat;
(5) after being concentrated, the upper strata in the step (4) obtains Os Cervi oil; After the middle level concentrates this product is carried out lyophilizing and handle, obtain Os Cervi and extract crystalline particle;
(6) after-filtration is heated in the lower floor in the step (4), concentrate, lyophilizing is handled, and gets deer-bone collagenous granule.
2, method according to claim 1 is characterized in that described step (1) is: get bright Os Cervi and clean, carry out deeply with cutter, make and expose bone marrow, classify then.
3, method according to claim 1 is characterized in that described step (2) is: sorted Os Cervi is packed in the stainless-steel pan, and adding volume ratio was the water that Os Cervi volume 3-8 doubly measures, in 100 ℃ of decocting in water 8 hours.
4, method according to claim 1 is characterized in that described step (5) is: with step (4) but in the upper strata concentrate with the hydrogen pot and remove moisture and obtain Os Cervi oil; After but the middle level concentrates with the hydrogen pot, this product at-20 ℃ of precooling 3-4 hours, is carried out lyophilizing then and handled 24 hours, obtain Os Cervi and extract crystalline particle.
5, method according to claim 1 is characterized in that described step (6) is: the lower floor in the step (4) is heated to 100 ℃, filters, but reuse hydrogen pot concentrates, this product at-20 ℃ of precooling 3-4 hours, is carried out lyophilizing then and handled 24 hours, obtain deer-bone collagenous granule.
6, method according to claim 1 is characterized in that comprising the steps
(1) get bright Os Cervi and clean, carry out deeply with electronic deep cutter, make and expose bone marrow, classification is then packed Os Cervi in the rustless steel hurdle into, is provided with partition in the rustless steel shelves, and the hurdle is divided into several zones, and similar Os Cervi is placed in the same zone;
(2) the rustless steel hurdle of Os Cervi will be housed, and place in the stainless-steel pan, adding volume is the water that Os Cervi volume 3-8 doubly measures, and 100 ℃ of decocting in water 8 hours are isolated water cooking liquid; Circulate three times, add clear water at every turn; Merge three times water cooking liquid; Os Cervi and water cooking liquid preserve separately that separation obtains is standby;
(3) isolated Os Cervi is upward cleaned, utilizes CT-1 type electric-controlled type hot air circulation drying machine drying behind the foreign material except that boning, utilize WL-100 type pulverizing mill to pulverize to exsiccant Os Cervi then, sterilization, what obtain at last is deer bone powder;
(4) with step (2) but water cooking liquid be concentrated to volume with the hydrogen pot and no longer change, cooling, concentrated solution can be divided into three layers of upper, middle and lowers, separates, the upper strata is the animal oil part; The middle level is amber paste; Lower floor is mixture such as broken bone, meat;
(5) with step (4) but in the upper strata concentrate with the hydrogen pot and remove moisture and obtain Os Cervi oil; After but the middle level concentrates with the hydrogen pot, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and carried out lyophilizing processing 24 hours, obtain Os Cervi and extract crystalline particle;
(6) lower floor in the step (4) is heated to 100 ℃ of after-filtration, but reuse hydrogen pot concentrate, this product at-20 ℃ of precooling 3-4 hours, is put into the full-automatic lyophilizing machine of CRYODOS type then and is carried out lyophilizing and handled 24 hours, obtain deer-bone collagenous granule.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101803738A (en) * | 2010-03-24 | 2010-08-18 | 郑彬 | Method for preparing deer bone frozen powder by ultrasonic degradation |
| CN103251065A (en) * | 2013-05-14 | 2013-08-21 | 吉林大学 | Domesticated sika deer bone meal as well as preparation method thereof and sika deer bone chewable tablet prepared from bone meal |
| CN106880839A (en) * | 2015-12-14 | 2017-06-23 | 吉林省东鳌鹿业集团有限公司 | A kind of deer osteocomma and preparation method thereof |
| CN110115385A (en) * | 2018-02-05 | 2019-08-13 | 常州英莱克斯生物工程有限公司 | A kind of strength osteocomma increasing bone density and its production method |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103843970B (en) * | 2012-11-30 | 2015-05-20 | 闫云霞 | Production method for preparing ossein oligopeptide meal, bone oil and bone meal |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100389679C (en) * | 2006-06-21 | 2008-05-28 | 山东师范大学 | A deer bone granule |
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2009
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101803738A (en) * | 2010-03-24 | 2010-08-18 | 郑彬 | Method for preparing deer bone frozen powder by ultrasonic degradation |
| CN101803738B (en) * | 2010-03-24 | 2012-04-18 | 郑彬 | Method for preparing deer bone frozen powder by ultrasonic degradation |
| CN103251065A (en) * | 2013-05-14 | 2013-08-21 | 吉林大学 | Domesticated sika deer bone meal as well as preparation method thereof and sika deer bone chewable tablet prepared from bone meal |
| CN106880839A (en) * | 2015-12-14 | 2017-06-23 | 吉林省东鳌鹿业集团有限公司 | A kind of deer osteocomma and preparation method thereof |
| CN110115385A (en) * | 2018-02-05 | 2019-08-13 | 常州英莱克斯生物工程有限公司 | A kind of strength osteocomma increasing bone density and its production method |
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