CN101803738B

CN101803738B - Method for preparing deer bone frozen powder by ultrasonic degradation

Info

Publication number: CN101803738B
Application number: CN2010101582209A
Authority: CN
Inventors: 郑彬; 李丽娟
Original assignee: Individual
Current assignee: Individual
Priority date: 2010-03-24
Filing date: 2010-03-24
Publication date: 2012-04-18
Anticipated expiration: 2030-03-24
Also published as: CN101803738A

Abstract

The invention relates to a health care food and a preparation method thereof, in particular to a method for preparing deer bone frozen powder by ultrasonic degradation. The method comprises the following steps of: cleaning a deer bone without anadesmas, crushing, and adding acetone to remove fat in the deer bone and prepare defatted deer bone powder; grinding the defatted deer powder with a colloid grinder to obtain deer bone slurry of 200-230 meshes; mixing the deer bone slurry and active water to form a suspension; crushing the sufficiently dispersed and emulsified deer bone suspension by an ultrasonic continuous flow cell crusher under stirring to fracture cell membranes and fully release the active substances in the cells; directly sublimating the target drying substance by utilizing a frozen drying and condensing technology to remove moisture, wherein drying by heating is avoided to prevent the inactivation of the active substances of the deer bone in the preparation process. The deer bone frozen powder has complete nutrition and high activity, and the preparation method needs short extraction time, reduces the loss of active substances and improves the utilization rate of the deer bone. The invention has the advantages of simple process, low production cost and shortened production period.

Description

The method of preparing deer bone frozen powder by ultrasonic degradation

Technical field

The present invention relates to a kind of health food and preparation method thereof, specifically a kind of method of preparing deer bone frozen powder by ultrasonic degradation.

Background technology

China carries out the technological relatively backward of intensive processing to the deer bone at present; It is existing that what adopt is the method for traditional high temperature boiling with heated baking pulverizing; The processing method of this heat; Can make active ingredient considerable damage and loss in the deer bone, nutritive value also reduces greatly, particularly the almost whole inactivations of the active material in the deer bone.

Summary of the invention

The objective of the invention is the shortcoming to above-mentioned existence, a kind of good health care effect is provided, the utilization rate of extract is high, and extraction time is short, and the preparation method of being rich in nutrition active material preparing deer bone frozen powder by ultrasonic degradation in the extract.

Technical solution the present invention includes the method for being prepared as follows:

1) the deer bone that will reject manadesma cleans up fragmentation, adds acetone and sloughs the fat in the deer bone, processes the degreasing deer bone powder, and filtrating is reclaimed acetone.The purpose that adds acetone is to slough the fat in the deer bone, makes it not contain cholesterol.

2) 200～230 purpose deer pulp bodies must be through colloid mill.

3) ultrasonic degradation:

A, at first carry out the preparation of active water, add the 0.5g-2g sucrose ester in every 100Kg water;

B, deer pulp body that colloid mill is ground and active water form suspension, addition by weight, active water: deer pulp body=3: 1;

C, deer bone suspension that abundant dispersion and emulsion is good are under stirring condition; Through ultrasonic continuous stream biomixer; Utilize hyperacoustic cavitation principle, the ultrasonic wave that is sent under certain condition makes the deer bone tissue reach the cell grade fragmentation; With membranolysis, intracellular active material fully discharges.Supersonic frequency 15-40KHz, power 1800-3500W, suspension per hour flow are 10Kg, and percentage of damage reaches more than 95%.

4) freeze drying concentrates: the deer bone suspension through ultrasonic degradation in the step 3) to be inserted in the freeze drier material disc, and the freeze drier temperature be≤-50 ℃, operating voltage AC (380 ± 38) V (50 ± 1) HZ, freeze-drying time are taking-up in 16-22 hour; Utilize the freeze drying concentration technique, the dry thing of target is directly distilled under freezing state remove moisture, avoid heat drying to cause the active material inactivation of deer bone.

5) ultra-fine grinding: the material after freeze drying concentrated is crushed to more than 400 orders at micronizer.

6) capsule can.

7) packing.

Using ultrasound cracking technique of the present invention; Its core technology is to utilize hyperacoustic cavitation principle, and the ultrasonic wave that is sent under certain condition causes the hydrone blast; Thereby smash the solid matter of periphery, make institute want the material of fragmentation can reach cell one-level fragmentation.Ultrasonic degradation technology of the present invention makes the deer bone tissue reach the cell grade fragmentation; With membranolysis; Intracellular active material fully discharges; Macro-molecular protein is transformed into the micromolecule polypeptide that can be absorbed by the body, rapidly nutriment in the cell is discharged fully, like collagen, amino acid, organic calcium, auxin, various trace elements.And comprehensive nutrition, activity is high, extraction time is short, has reduced losing of active material, has improved the utilization rate of deer bone.

Deer bone of the present invention is because through colloidal grinding, the material that will grind again is through ultrasonic degradation, so have following advantage:

1, production technology of the present invention and working condition are simple, have greatly reduced production cost, have significantly improved production efficiency, shorten the production cycle.

2, broken through traditional heat and caused nutrient loss, directly the deer pulp body with colloidal grinding flows biomixer, avoids high temperature through ultrasonic continuous, has kept most of active material in the deer bone.

3, the deer pulp body through colloidal grinding flows biomixer through ultrasonic continuous again, makes membranolysis in the tissue, rapidly nutriment in the cell is discharged fully; Nutriment is comprehensive, active high, is easily absorbed by the body.

4, lack process time, reduced losing of active material, improved the utilization rate of deer bone.

5, fully kept being rich in nutrition active material and other nutrients in the extract, this technology has been filled up domestic blank, reaches the international leading level.

The specific embodiment

Raw material sources of the present invention are in passing through the highest authentication of Chinese food---the bright deer bone of organic food authentication.The preparation method comprises the steps:

1) processed of deer bone: the deer bone that will reject manadesma cleans up, and it is broken to get deer bone 5kg, adds 7.5 liters in acetone, fully stirs 2.5 hours, filters, and filter cake in vacuum is dry, processes the degreasing deer bone powder, and filtrating is reclaimed acetone.

2) the utilization whole stainless steel colloid mill of obtaining the production of national patent seven-star dairy products instrument factory makes grinding, emulsification, pulverizing, mixing, dispersion and the homogeneous of material under the effect of complicated power such as high-frequency vibration and high speed vortex, thereby must be 200 purpose deer pulp bodies;

3) ultrasonic degradation:

A, at first carry out the preparation of active water: add the 0.5g sucrose ester in every 25Kg water, sucrose ester is a kind of surfactant, and the purpose of adding is that deer pulp body is evenly disperseed in water better;

B, deer pulp body and the active water that colloid mill is ground form suspension, add 5Kg deer pulp body in every 15Kg water;

C, deer bone suspension that abundant dispersion and emulsion is good are under stirring condition, and through ultrasonic continuous stream biomixer, supersonic frequency 40KHz, power 3500W, suspension per hour flow are 10Kg, and percentage of damage reaches more than 95%.

4) freeze drying concentrates: the pilose antler slurries that will pass through ultrasonic degradation are inserted in the freeze drier material disc, and the freeze drier temperature is-30 ℃, and operating voltage AC380V50HZ, freeze-drying time are taking-up in 20 hours.Can obtain the freeze-dried powder of deer bone.

5) ultra-fine grinding: the freeze-dried powder that will obtain the deer bone utilizes the CWJ micronizer of Zhejiang Province Fengli smash equipment Co., Ltd to be crushed to more than 400 orders.

6) capsule can: 300,000 grades of Clean room cans, qualified micropowders added in the automatic tire bagger fill, it is heavy to survey 1 capsule in per 15 minutes in service, guarantees different qualified of the capsule method of double differences, and the container of packing into is tested.

7) packing:

1. correctly post required label on request.

2. correctly pack on request in corresponding packing box or the packing case, registration is put in storage.

Claims

1. the method for preparing deer bone frozen powder by ultrasonic degradation is characterized in that, comprises the method for being prepared as follows:

1) processed of deer bone: the deer bone that will reject manadesma cleans up fragmentation, adds acetone and sloughs the fat in the deer bone, processes the degreasing deer bone powder;

2) 200～230 purpose deer pulp bodies must be through colloid mill;

3) ultrasonic degradation:

A, at first carry out the preparation of active water: add the 0.5g-2g sucrose ester in every 100Kg water;

C, deer bone suspension that abundant dispersion and emulsion is good are under stirring condition, and through ultrasonic continuous stream biomixer, supersonic frequency 15-40KHz, power 1800-3500W, suspension per hour flow are 10Kg, and percentage of damage reaches more than 95%;

4) freeze drying concentrates: the deer bone suspension through ultrasonic degradation in the step 3) to be inserted in the freeze drier material disc, and the freeze drier temperature be≤-50 ℃, operating voltage AC is: 380 ± 38V, Hz are: 50 ± 1, freeze-drying time is taking-up in 16-22 hour;

5) ultra-fine grinding: the material after freeze drying concentrated is crushed to more than 400 orders at micronizer;

6) capsule can;

7) packing.