CN101507697B - Purple beautyberry mouth wash - Google Patents
Purple beautyberry mouth wash Download PDFInfo
- Publication number
- CN101507697B CN101507697B CN2009100024880A CN200910002488A CN101507697B CN 101507697 B CN101507697 B CN 101507697B CN 2009100024880 A CN2009100024880 A CN 2009100024880A CN 200910002488 A CN200910002488 A CN 200910002488A CN 101507697 B CN101507697 B CN 101507697B
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- China
- Prior art keywords
- beautyberry
- extract
- folium callicarpae
- callicarpae formosanae
- ethanol
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Abstract
The invention discloses beautyberry mouthninse. The beautyberry mouthninse is a liquid which is prepared by a beautyberry extract and commonly used mouthninse components by adopting the prior preparation technology and has a pH value of between 5.5 and 7.5, wherein the beautyberry extract accounts for 0.1 to 10 percent of the total amount (calculated as weight percentage); and the beautyberry extract is prepared by the following steps that: beautyberry powder is boiled by water, the solution is filtered, a filtrate is concentrated and then is subjected to alcohol precipitation by alcohol to obtain a crude extract, the crude extract is dissolved by water, and the obtained solution is removed with impurities and filtered, then is subjected to alcohol precipitation by the alcohol, and is filtered and dried to obtain powder. The invention effectively utilizes effective constituents of beautyberry and adopts preparation technology to prepare the mouthninse which has better therapeutic effect on common diseases in oral cavity such as toothache, ngivitis, periodontitis, gingival bleeding, has obvious functions of clearing heat and diminishing inflammation, stanching, inhibiting bacteria and relieving pain, can be used for adjuvant therapy of oral inflammation, and can also be used for daily oral health care.
Description
Technical field
This invention relates to a kind of functional oral health-care product, and particularly a kind of purple beautyberry mouth wash that contains the extract of Folium Callicarpae Formosanae natural plants is a kind of have good heat clearing and inflammation relieving, hemostatic effect, collutory that mouthfeel is good, easy to use, without any side effects.
Background technology
Folium Callicarpae Formosanae has heat-clearing and toxic substances removing, cooling blood for hemostasis, dephlogistication and promoting nuscle growth, effect such as anticancer, the Callicarpa floristics is various, and various places mainly contain as the plant of medicinal Folium Callicarpae Formosanae at present: Verenaceae plant callicarpa pedunculata, Callicarpa dichotoma, callicarpa cathayana Chang, Radix Callicarpae Giraldii, Callicarpa nudiflora, Folium Callicarpae Macrophyllae, Callicarpa kwangtungensis Chun, entire beautyberry herb, Japanese Folium Callicarpae Formosanae, Folium Callicarpae Longissimae, red autumnal leaves Folium Callicarpae Formosanae, cognate Folium Callicarpae Rubellae, Radix Callicarpae Bodinieri etc.
Along with the raising day by day of living standard, people also improve day by day to the health care consciousness of self, and oral cavity health also is one of them, and oral inflammation is a kind of disease of seeing more, is the multiple disease in oral cavity as diseases such as toothache, gingivitis, periodontitis, gingival hemorrhages.Being used for the medicament of oral disease prevention and control such as buccal tablet, chewing gum, diaphragm etc. at present is difficult to penetrate at teeth space, be difficult to bring into play due therapeutical effect, and the preparation that uses adopts crude extract to make mostly, and effective component content is low and unstable, is difficult to the effect that reaches set.
In the collutory on the existing market majority is a Chinese medicine and western medicine in conjunction with working, and is main functional component with Western medicine, though and some collutorys are arranged based on Chinese medicine ingredients, effect is not very desirable.
Summary of the invention
The purpose of this invention is to provide a kind of purple beautyberry mouth wash that utilizes the Folium Callicarpae Formosanae effective ingredient, have obvious heat clearing and inflammation relieving, hemostasis, antibacterial, analgesic activity, diseases such as the common toothache in oral cavity, gingivitis, periodontitis, gingival hemorrhage are had better curative effect.
The technical solution adopted in the present invention is:
A kind of purple beautyberry mouth wash adopts traditional preparation process technology and the pH value that makes is 5.5～7.5 liquid by Folium Callicarpae Formosanae extract and collutory composition commonly used, and wherein Folium Callicarpae Formosanae extract accounts for 0.1%～10% of total amount by weight percentage.Described Folium Callicarpae Formosanae extract is to get the Folium Callicarpae Formosanae grass meal through decocting in water, filtration, it is 15%～30% that filtrate is concentrated into solid content, then with concentrated solution with 3～8 times concentration more than or equal to 90% ethanol carry out alcohol analyse crude extract, the crude extract water dissolution, remove impurity is filtered, after filtrate transferred PH to 5.5～7.5, carry out alcohol with 3～8 times concentration more than or equal to 90% ethanol and analyse, filter, dry down that powders be Folium Callicarpae Formosanae extract at 50～110 ℃.
Described collutory composition commonly used is Herba Menthae quintessence oil, ethanol, tween 80, PH buffer agent and pure water.
Described PH buffer agent is the mixture of sodium hydroxide and potassium dihydrogen phosphate, wherein counts sodium hydroxide in molar ratio: potassium dihydrogen phosphate is 0: 1～0.5: 1.
Correspondingly, purple beautyberry mouth wash provided by the present invention, be to adopt traditional preparation process technology and the P H-number that makes is 5.5～7.5 liquid by Folium Callicarpae Formosanae extract, Herba Menthae quintessence oil, ethanol, tween 80, PH buffer agent and pure water, wherein each components contents is by weight: Folium Callicarpae Formosanae extract 0.1%～10%, Herba Menthae quintessence oil 0.02%～0.5%, ethanol 2%～25%, tween 80 0.01%～0.35%, PH buffer agent 0.01%～0.05%, surplus are pure water.
The present invention effectively utilizes the effective ingredient of Folium Callicarpae Formosanae, adopt preparation technology to prepare a kind of collutory that diseases such as the common toothache in oral cavity, gingivitis, periodontitis, gingival hemorrhage is had better curative effect, have obvious heat clearing and inflammation relieving, hemostasis, antibacterial, analgesic activity, not only can be used for the auxiliary treatment of oral inflammation, also can be used for daily oral cavity health.
The specific embodiment
The invention will be further described with indefiniteness embodiment below.
One, the extraction of Folium Callicarpae Formosanae extract:
Get Folium Callicarpae Formosanae grass meal water and boil twice, boiled one hour at every turn, it is 20% that merging filtrate is concentrated into solid content; This concentrated solution with 5 times 95% ethanol carry out alcohol analyse crude extract; With the crude extract water dissolution, add precipitant contamination precipitation is removed by filtration, filtrate is transferred P H to 6, carry out alcohol with the ethanol of 4 times concentration 95% and analyse, filter, usefulness washing with alcohol twice, and get dry powder at 60 ℃ of following vacuum dryings.
Two, the preparation of purple beautyberry mouth wash:
1. with mix homogeneously after Herba Menthae quintessence oil, tween, the ethanol weighing.
2. the refining dry powder of Folium Callicarpae Formosanae is mixed with pure water and also fully be dissolved into clear solution.
3. above two kinds of liquid are fully mixed, adding PH buffer agent accent pH value is 6.5.
4. packing enters finished bin after the assay was approved.
Example one
Proportioning by following each component makes purple beautyberry mouth wash according to above-mentioned technology.
Callicarpa nudiflora is made with extra care dry powder: 1%
Herba Menthae quintessence oil: 0.05%
95% ethanol (food stage): 6%
Tween 80: 0.05%
PH buffer agent: 0.02%
Pure water: surplus
Example two
Proportioning by following each component makes purple beautyberry mouth wash according to above-mentioned technology.
Callicarpa nudiflora is made with extra care dry powder: 1.5%
Herba Menthae quintessence oil: 0.1%
95% ethanol (food stage): 10%
Tween 80: 0.1%
PH buffer agent: 0.02%
Pure water: surplus
Claims (2)
1. purple beautyberry mouth wash, it is characterized in that: be to adopt traditional preparation process technology and the pH value that makes is 5.5～7.5 liquid by Folium Callicarpae Formosanae extract, Herba Menthae quintessence oil, ethanol, tween 80, pH buffer agent and pure water, wherein each components contents is by weight: Folium Callicarpae Formosanae extract 0.1%～10%, Herba Menthae quintessence oil 0.02%～0.5%, ethanol 2%～25%, tween 80 0.01%～0.35%, pH buffer agent 0.01%～0.05%, surplus are pure water; Described Folium Callicarpae Formosanae extract is to get the Folium Callicarpae Formosanae grass meal through decocting in water, filtration, it is 15%～30% that filtrate is concentrated into solid content, then with concentrated solution with 3～8 times concentration more than or equal to 90% ethanol carry out alcohol analyse crude extract, the crude extract water dissolution, remove impurity is filtered, after filtrate transferred pH to 5.5～7.5, carry out alcohol with 3～8 times concentration more than or equal to 90% ethanol and analyse, filter, dry down that powders be Folium Callicarpae Formosanae extract at 50～110 ℃.
2. purple beautyberry mouth wash according to claim 1 is characterized in that: described pH buffer agent is the mixture of sodium hydroxide and potassium dihydrogen phosphate, wherein counts sodium hydroxide in molar ratio: potassium dihydrogen phosphate is 0: 1～0.5: 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100024880A CN101507697B (en) | 2009-01-22 | 2009-01-22 | Purple beautyberry mouth wash |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100024880A CN101507697B (en) | 2009-01-22 | 2009-01-22 | Purple beautyberry mouth wash |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101507697A CN101507697A (en) | 2009-08-19 |
| CN101507697B true CN101507697B (en) | 2011-03-23 |
Family
ID=41000336
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009100024880A Expired - Fee Related CN101507697B (en) | 2009-01-22 | 2009-01-22 | Purple beautyberry mouth wash |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101507697B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104127586A (en) * | 2014-08-13 | 2014-11-05 | 陈林旭 | Mouth wash capable of inhibiting gum bleeding and preparation method thereof |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104510666A (en) * | 2013-12-21 | 2015-04-15 | 莫治玲 | Mouthwash for treating gingival bleeding |
| CN104042519A (en) * | 2014-06-30 | 2014-09-17 | 黄树长 | Mouthwash |
| CN104116682B (en) * | 2014-08-13 | 2016-05-25 | 李红 | Compound Japanses beauty-berry grass mouthwash and preparation method thereof |
| CN105497311A (en) * | 2015-12-10 | 2016-04-20 | 韦焜 | Method for preparing mouthwash for treating wind-heat type toothache |
-
2009
- 2009-01-22 CN CN2009100024880A patent/CN101507697B/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104127586A (en) * | 2014-08-13 | 2014-11-05 | 陈林旭 | Mouth wash capable of inhibiting gum bleeding and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101507697A (en) | 2009-08-19 |
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20110323 Termination date: 20210122 |
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| CF01 | Termination of patent right due to non-payment of annual fee |