CN101390596B - Production method of debitterized honey pomelo meal fiber - Google Patents
Production method of debitterized honey pomelo meal fiber Download PDFInfo
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- CN101390596B CN101390596B CN2008101564129A CN200810156412A CN101390596B CN 101390596 B CN101390596 B CN 101390596B CN 2008101564129 A CN2008101564129 A CN 2008101564129A CN 200810156412 A CN200810156412 A CN 200810156412A CN 101390596 B CN101390596 B CN 101390596B
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- sweet shaddock
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Abstract
A debittering honeyed shaddock dietary fiber production method takes the mesocarp of honeyed shaddock pulp as the raw material; after being washed and disinfected, the mesocarp of honeyed shaddock pulp is debittered with soy milk; the debittered mesocarp of honeyed shaddock pulp is beaten, ground, fermented, processed through colloidal grind and filtered; the obtained residue is dried and ultrafinely crushed to get ultrafine dietary fiber powders; the obtained filtrate is vacuum-condensed and spray-dried to get spray-dried dietary fiber powders; and the two types of dietary fiber powders are mixed so as to get the debittering honeyed shaddock dietary fiber finished product. The invention takes the mesocarp of honeyed shaddock pulp as the raw material and uses soy milk as the debittering agent of the mesocarp of honeyed shaddock pulp to make full use of the plant enzyme contained in the soy milk to effectively reduce the content of bitter principle aurantiamarin of the mesocarp of honeyed shaddock pulp; based on measurement, the content of aurantiamarin in the mesocarp of debittered honeyed shaddock pulp is significantly reduced, so that the debittering effect is obvious.
Description
Technical field
The present invention relates to the preparation method of sweet shaddock deep processed product, be specifically related to the preparation method of debitterized honey pomelo meal fiber.
Background technology
Shaddock claims sweet shaddock again, is the ripening fruits of rutaceae evergreen fruit trees teak, and the meat of shaddock and Pi Junhan are rich in the dried immature fruit of citron orange, carrotene, B family vitamin, vitamin C, natural complex, P, mineral matter, carbohydrate and volatile oil.Effects such as that shaddock has is hypoglycemic, hypotensive, fat-reducing, beauty treatment often ediblely can play good health-care effect.Current, shaddock is based on the fresh fruit sale, is subjected to seasonal effect big and added value is low.And in preserved fruit of shaddock and preparation method thereof, the debitterize technology is crucial.Naringin is the bitter principle that contains in the shaddock, and along with the resting period is long more, the content of naringin raises, and bitter taste increases the weight of, and has a strong impact on its eating mouth feel.Chinese patent CN98112546 " food of shaddock skin and preparation method thereof ", wherein the debitterize technical method of shaddock is to use saline solution 1%-1.5%, and post rinse is boiled in the heating of shaddock skin.Utilize the method boiling time short, bitter taste removes unclean; Boiling time is long, and the shaddock skin is well-done, and product is difficult for being shaped, and the nutritional labeling warp of shaddock high temperature for a long time heats and loses.The shaddock ascolichen contains high fiber, can promote enterogastric peristalsis, digests having indigestion, plays the effect of toxin-expelling and face nourishing.There is no sweet shaddock meat capsule clothing goods up to now comes out.
Summary of the invention
The present invention is directed to above-mentioned employing saline solution carries out the shortcoming that the food and preparation method thereof of debitterize gained shaddock skin exists and improves to shaddock, provide another that shaddock or sweet shaddock are carried out the method for debitterize, providing a kind of on the basis of this method is the preparation method of the debitterized honey pomelo meal fiber of raw material with shaddock or sweet shaddock.
Technical scheme of the present invention is as follows:
A kind of preparation method of debitterized honey pomelo meal fiber is characterized in that comprising being prepared as follows step:
(1), the preliminary treatment of sweet shaddock fresh fruit: after sweet shaddock fresh fruit cleans, with sweet shaddock belt leather cavernous body, sweet shaddock meat, sweet shaddock meat capsule ginning outturn from;
(2), raw material sterilization: the ClO 2 solution that is 150-200ppm with sweet shaddock meat capsule clothing concentration soaked 3-6 minutes, cleaned to dry, and sweet shaddock meat capsule clothing is sterilized;
(3), make soymilk: with defibrination behind the soybeans soaking, high-pressure homogeneous homogenate becomes soymilk, and protein content is 1.2-5%;
(4), raw material debitterize: step (2) gained sterilization raw material with the soymilk of weight ratio 1:2-3, in 2-4 hours debitterizes of 55-66 ℃ of insulations, is obtained debittering honey pomelo meat capsule clothing;
(5), clean: debittering honey pomelo meat capsule clothing is cleaned No. 2-3 times the dewaterer dehydration with clear water;
(6), secondary sterilization: the debittering honey pomelo meat capsule clothing after clean drying is a secondary sterilization 3-6 minutes in the ClO 2 solution solution of 150-200ppm in concentration, cleans to dry;
(7), enzymolysis is ground in making beating: will clean the sweet shaddock meat capsule clothing that dries and drop into beater, the water making beating that adds its weight ratio 10%, again slurry is ground, add capsule clothing weight ratio after grinding and be 1%-1.5%, enzyme activity is the cellulase of 300u/ml, in 45 ℃-55 ℃, pH value 4.5-5.5, enzymolysis 1.5-3.5 hours, in 75 ℃-85 ℃, be incubated 10-15 minutes enzymes that go out behind the enzymolysis, obtain enzymolysis capsule clothing slurries;
(8), the glue mill filters: through colloid mill glue mill, filter glue mill back with enzymolysis capsule clothing slurries;
(9), ultramicro grinding: step (8) gained filter residue is dried to water content below 5%, through ultramicro grinding, obtains the dietary fiber powder of ultramicro grinding;
(10), vacuum concentrates: step (8) gained filtrate vacuum is concentrated, and vacuum is 0.070.08mpa; Concentrate under the condition that temperature is 70-80 ℃, reach 25%-30% to solid content;
(11), spray-drying: step (10) gained concentrate is carried out spray-drying, and spray-dired EAT is 155 ℃-185 ℃, and leaving air temp is 85 ℃-95 ℃, obtains spray-dired dietary fiber powder;
(12), mix: step (9) is mixed with step (11) gained dietary fiber powder, obtain the debitterized honey pomelo meal fiber finished product.
Main points of the present invention are to adopt sweet shaddock meat capsule clothing as raw material and adopt the debitterize agent of soymilk as sweet shaddock meat capsule clothing raw material, utilize the phytoenzyme that contains in the soymilk to effectively reduce the content of the bitter principle-aurantiin of sweet shaddock meat capsule clothing.The debittering honey pomelo meat capsule clothing that obtains after measured and low by the content of its contained aurantiin of debitterized honey pomelo meal fiber that makes is obtained significant de-bittering effect.
The specific embodiment:
Below concrete enforcement of the present invention is described:
Embodiment 1
After fresh fruit honey shaddock is cleaned, with sweet shaddock belt leather cavernous body, sweet shaddock meat, sweet shaddock meat capsule ginning outturn from; 5kg honey shaddock meat capsule clothing is that the ClO 2 solution of 150ppm soaked 3 minutes with 10kg concentration, cleans drying, and sweet shaddock meat capsule clothing is sterilized; Behind the soybean defibrination, high-pressure homogeneous homogenate becomes soymilk, measures its Protein content according to a conventional method 1.2%; Sweet shaddock meat capsule clothing after the sterilization is put in the 10kg soymilk, in 2 hours debitterizes of 55 ℃ of insulations; Sweet shaddock meat capsule clothing behind the debitterize is cleaned No. 2 times the centrifugal dehydrator dehydration with clear water; Sweet shaddock meat capsule clothing after clean drying is a secondary sterilization 3 minutes in the ClO 2 solution solution of 180ppm in concentration, cleans to dry; Adding 0.5kg water mixes with sweet shaddock meat capsule clothing through secondary sterilization and drops into beater and pull an oar, again slurry is ground, adding the 50g enzyme activity after grinding is the 300u/ml cellulase, in 45 ℃, pH value 4.5 enzymolysis 1.5 hours, in 10 minutes enzymes that go out of 75 ℃ of insulations, obtain enzymolysis honey shaddock meat capsule clothing slurries behind the enzymolysis;
Enzymolysis honey shaddock meat capsule clothing slurries are through colloid mill glue mill, and glue mill back is crossed 100 order screen packs and filtered; The filter residue that obtains is dried to water content below 5%, through ultramicro grinding, obtains the dietary fiber powder of ultramicro grinding; The filtrate that obtains is through 0.07mpa, the solid content that is concentrated to concentrate under 70 ℃ the condition reaches 25%, concentrate pumps into spray dryer and carries out spray-drying, EAT is 155 ℃ during spray-drying, leaving air temp is 85 ℃, during spraying centrifuge speed 8000r/ minute, obtain spray-dired dietary fiber powder; The dietary fiber powder and the spray-dired dietary fiber powder of above-mentioned ultramicro grinding are mixed, become the debitterized honey pomelo meal fiber finished product.
Embodiment 2
After fresh fruit honey shaddock is cleaned, with sweet shaddock belt leather cavernous body, sweet shaddock meat, sweet shaddock meat capsule ginning outturn from; 10kg honey shaddock meat capsule clothing is that the ClO 2 solution of 180ppm soaked 4 minutes with 25kg concentration, cleans drying, and sweet shaddock meat capsule clothing is sterilized; Behind the soybean defibrination, high-pressure homogeneous homogenate becomes soymilk, measures its Protein content according to a conventional method 3%; Sweet shaddock meat capsule clothing after the sterilization is put in the 25kg soymilk, in 3 hours debitterizes of 60 ℃ of insulations; Sweet shaddock meat capsule clothing behind the debitterize is cleaned No. 2 times the centrifugal dehydrator dehydration with clear water; Sweet shaddock meat capsule clothing after clean drying is a secondary sterilization 4 minutes in the ClO 2 solution solution of 200ppm in concentration, cleans to dry; Adding 1kg water mixes with sweet shaddock meat capsule clothing through secondary sterilization and drops into beater and pull an oar, again slurry is ground, add the cellulase that the 120g enzyme activity is 300u/mkg after grinding, in 50 ℃, pH value 5.0 enzymolysis 2.5 hours, in 12 minutes enzymes that go out of 80 ℃ of insulations, obtain enzymolysis honey shaddock meat capsule clothing slurries behind the enzymolysis;
Enzymolysis honey shaddock meat capsule clothing slurries are through colloid mill glue mill, and glue mill back is crossed 100 order screen packs and filtered; The filter residue that obtains is dried to water content below 5%, through ultramicro grinding, obtains the dietary fiber powder of ultramicro grinding; The filtrate that obtains is through 0.08mpa, the solid content that is concentrated to concentrate under 75 ℃ the condition reaches 27%, concentrate pumps into spray dryer and carries out spray-drying, EAT is 170 ℃ during spray-drying, leaving air temp is 90 ℃, during spraying centrifuge speed 9000r/ minute, obtains spray-dired dietary fiber powder; The dietary fiber powder and the spray-dired dietary fiber powder of above-mentioned ultramicro grinding are mixed, become the debitterized honey pomelo meal fiber finished product.
Embodiment 3
After fresh fruit honey shaddock is cleaned, with sweet shaddock belt leather cavernous body, sweet shaddock meat, sweet shaddock meat capsule ginning outturn from.100kg honey shaddock meat capsule clothing is that the ClO 2 solution of 200ppm soaked 6 minutes with 300kg concentration, cleans drying, and sweet shaddock meat capsule clothing is sterilized; Behind the soybean defibrination, high-pressure homogeneous homogenate becomes soymilk, measures its Protein content according to a conventional method 5%; Sweet shaddock meat capsule clothing after the sterilization is put among the 300kg soymilk 300kg, in 4 hours debitterizes of 66 ℃ of insulations; Sweet shaddock meat capsule clothing behind the debitterize is cleaned No. 3 times the centrifugal dehydrator dehydration with clear water; Sweet shaddock meat capsule clothing after clean drying is a secondary sterilization 6 minutes in the ClO 2 solution solution of 180ppm in concentration, cleans to dry; Adding 10kg water mixes with sweet shaddock meat capsule clothing through secondary sterilization and drops into beater and pull an oar, again slurry is ground, add the cellulase that the 1.5kg enzyme activity is 300u/mkg after grinding, in 55 ℃, pH value 5.5 enzymolysis 3.5 hours, in 15 minutes enzymes that go out of 85 ℃ of insulations, obtain enzymolysis honey shaddock meat capsule clothing slurries behind the enzymolysis;
Enzymolysis honey shaddock meat capsule clothing slurries are through colloid mill glue mill, and glue mill back is crossed 100 order screen packs and filtered; The filter residue that obtains is dried to water content below 5%, through ultramicro grinding, obtains the dietary fiber powder of ultramicro grinding; The filtrate that obtains is through 0.08mpa, the solid content that is concentrated to concentrate under 80 ℃ the condition reaches 30%, concentrate pumps into spray dryer and carries out spray-drying, EAT is 185 ℃ during spray-drying, leaving air temp is 95 ℃, during spraying centrifuge speed 10000r/ minute, obtains spray-dired dietary fiber powder; The dietary fiber powder and the spray-dired dietary fiber powder of above-mentioned ultramicro grinding are mixed, become the debitterized honey pomelo meal fiber finished product.
Before the honey shaddock meat capsule clothing debitterize with debitterize after the content measuring value of the content of contained aurantiin and the contained aurantiin of debitterized honey pomelo meal fiber finished product see the following form 1 (with reference to Pharmacopoeia of People's Republic of China 2005 editions: the assay method of the naringin content of Fructus Aurantii is tested).
Table 1 measuring naringin content value (%)
Claims (1)
1. the preparation method of a debitterized honey pomelo meal fiber is characterized in that comprising being prepared as follows step:
(1), the preliminary treatment of sweet shaddock fresh fruit: after sweet shaddock fresh fruit cleans, with sweet shaddock belt leather cavernous body, sweet shaddock meat, sweet shaddock meat capsule ginning outturn from;
(2), raw material sterilization: the ClO 2 solution that is 150-200ppm with sweet shaddock meat capsule clothing concentration soaked 3-6 minute, cleaned to dry, and sweet shaddock meat capsule clothing is sterilized;
(3), make soymilk: with defibrination behind the soybeans soaking, high-pressure homogeneous homogenate becomes soymilk, and protein content is 1.2-5%;
(4), raw material debitterize: step (2) gained sterilization raw material with the soymilk of weight ratio 1: 2-3, in 2-4 hour debitterize of 55-66 ℃ of insulation, is obtained debittering honey pomelo meat capsule clothing;
(5), clean: debittering honey pomelo meat capsule clothing is cleaned 2-3 time the dewaterer dehydration with clear water;
(6), secondary sterilization: the debittering honey pomelo meat capsule clothing after clean drying is in the ClO 2 solution solution of 150-200ppm secondary sterilization 3-6 minute in concentration, cleans to dry;
(7), enzymolysis is ground in making beating: will clean the sweet shaddock meat capsule clothing that dries and drop into beater, the water making beating that adds its weight ratio 10%, again slurry is ground, adding capsule clothing weight ratio after grinding is that 1%-1.5%, enzyme activity are the cellulase of 300u/ml, in 45 ℃-55 ℃, and pH value 4.5-5.5, enzymolysis 1.5-3.5 hour, in 75 ℃-85 ℃, be incubated the 10-15 minute enzyme that goes out behind the enzymolysis, obtain enzymolysis capsule clothing slurries;
(8), the glue mill filters: through colloid mill glue mill, filter glue mill back with enzymolysis capsule clothing slurries;
(9), ultramicro grinding: step (8) gained filter residue is dried to water content below 5%, through ultramicro grinding, obtains the dietary fiber powder of ultramicro grinding;
(10), vacuum concentrates: step (8) gained filtrate vacuum is concentrated, and vacuum is 0.07-0.08MPa; Concentrate under temperature 70-80 ℃ the condition, reach 25%-30% to solid content;
(11), spray-drying: step (10) gained concentrate is carried out spray-drying, and spray-dired EAT is 155 ℃-185 ℃, and leaving air temp is 85 ℃-95 ℃, obtains spray-dired dietary fiber powder;
(12), mix: step (9) is mixed with step (11) gained dietary fiber powder, obtain the debitterized honey pomelo meal fiber finished product.
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| CN2008101564129A CN101390596B (en) | 2008-10-15 | 2008-10-15 | Production method of debitterized honey pomelo meal fiber |
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Families Citing this family (9)
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| CN101897452B (en) * | 2010-06-30 | 2013-01-02 | 集美大学 | Fermentation production method of grapefruit juice debitterizing enzyme |
| CN102150850B (en) * | 2011-01-12 | 2012-12-19 | 胡枝清 | Debitterized pomelo peel processed powder |
| CN103598596A (en) * | 2013-11-07 | 2014-02-26 | 南昌大学 | Functional food containing ginger dietary fiber |
| CN103932085A (en) * | 2014-04-14 | 2014-07-23 | 马建华 | Method for extracting grapefruit fibers |
| CN104223122B (en) * | 2014-09-05 | 2018-10-23 | 广东梅州市富柚生物科技有限公司 | Golden-pomelo dietary fiber and preparation method thereof |
| CN104293862A (en) * | 2014-09-19 | 2015-01-21 | 北京利晟新能生物科技中心（有限合伙） | Method for preventing material in enzymolysis tank from precipitation |
| CN108497147A (en) * | 2018-02-10 | 2018-09-07 | 荔浦县万家兴果蔬专业合作社 | A kind of processing method of pomelo peel preserved fruit |
| CN110584081A (en) * | 2019-09-29 | 2019-12-20 | 广州沃邦生物科技有限公司 | Salad sauce premixed flour and preparation method thereof |
| CN111972673A (en) * | 2020-08-25 | 2020-11-24 | 杨李益 | Grapefruit whole fruit cellulose powder and production method and application thereof |
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|---|---|---|---|---|
| CN1056401A (en) * | 1990-05-15 | 1991-11-27 | 成都科技大学 | The method of the residue of sweet orange through removing bitterness and squeezing manufacturing fruit powder |
| CN1060766A (en) * | 1990-10-25 | 1992-05-06 | 凌石 | The processing method of orange peel food |
| CN1241372A (en) * | 1998-07-10 | 2000-01-19 | 湖南省江永潇湘食品有限公司 | Shaddock rind food and its preparation |
| CN1943453A (en) * | 2006-11-01 | 2007-04-11 | 湖南省农产品加工研究所 | Method for removing orange skin by enzyme |
-
2008
- 2008-10-15 CN CN2008101564129A patent/CN101390596B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1056401A (en) * | 1990-05-15 | 1991-11-27 | 成都科技大学 | The method of the residue of sweet orange through removing bitterness and squeezing manufacturing fruit powder |
| CN1060766A (en) * | 1990-10-25 | 1992-05-06 | 凌石 | The processing method of orange peel food |
| CN1241372A (en) * | 1998-07-10 | 2000-01-19 | 湖南省江永潇湘食品有限公司 | Shaddock rind food and its preparation |
| CN1943453A (en) * | 2006-11-01 | 2007-04-11 | 湖南省农产品加工研究所 | Method for removing orange skin by enzyme |
Non-Patent Citations (1)
| Title |
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| JP平1-91766A 1989.04.11 |
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Effective date of registration: 20091218 Address after: Industrial Development Zone, South Sheng Town, Pinghe County, Fujian, Zhangzhou Province, China: 363701 Applicant after: Fujian Nanhai Food Co., Ltd. Address before: Industrial Development Zone, South Sheng Town, Pinghe County, Fujian, Zhangzhou Province, China: 363701 Applicant before: Fujian Nanhai Food Co., Ltd. Co-applicant before: Gu Jinglin |
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Inventor after: Gu Jinglin Inventor after: Hu Wenxing Inventor after: Lin Shunfa Inventor after: Yang Qingquan Inventor before: Gu Jinglin |
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Free format text: CORRECT: INVENTOR; FROM: GU JINGLIN TO: GU JINGLIN HU WENXING LIN SHUNFA YANG QINGQUAN |
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