CN101357949A - Extraction method of polysaccharides from morinda officinalis how and application thereof in cigarette - Google Patents
Extraction method of polysaccharides from morinda officinalis how and application thereof in cigarette Download PDFInfo
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- CN101357949A CN101357949A CNA2008101414507A CN200810141450A CN101357949A CN 101357949 A CN101357949 A CN 101357949A CN A2008101414507 A CNA2008101414507 A CN A2008101414507A CN 200810141450 A CN200810141450 A CN 200810141450A CN 101357949 A CN101357949 A CN 101357949A
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Abstract
The invention provides a method for extracting polysaccharides from morinda root and the application of the polysaccharides in cigarettes. The method for extracting the polysaccharides comprises the steps as follows: morinda root is dried, and pulverized into powder of 10 to 100 meshes; the morinda root powder is immersed and extracted by adding water at 50 to 100 DEG C; subsequently, the mixture of the morinda root powder and water is filtered and the filtrate is concentrated; the concentrated filtrate is added to ethanol to ensure the ethanol to account for 80 percent in volume; the mixture of the concentrated filtrate and the ethanol are allowed to be settled out and filtered, thus getting the raw polysaccharides; the raw polysaccharides are put in water for redissolution; a sevag reagent 0.1 to 1 time of the raw polysaccharide solution in volume is added, and is shaken and allowed to be separated into layers; the mixture of the thick sevag and protein on the lower layer is removed; the pH value is adjusted to 9 to 10 with ammonia; oxydol 30 percent of the solution in mass is added slowly until the solution is turned into straw yellow; after the solution is decolored, the solution is condensed before ethanol with the concentration from 95 to 100 percent is added, the volume percentage of the ethanol is kept to be 80 percent; the solution is allowed to be settled out for 24 to 48 hours, thus getting the polysaccharides from morinda root through filtration.
Description
Technical field
The present invention relates to vegetable polysaccharides and extract and use, relate to the extracting method of Root of Medicinal Indian mulberry polysaccharide and the application in cigarette specifically.This The Application of Technology does not change the existing complete processing of cigarette, the aesthetic quality that can improve cigarette, the hazardness of reduction cigarette.
Background technology
Along with the problem of smoking with health more and more receives publicity, the objectionable constituent of sucking security, increase nourishing function, reducing in the cigarette smoke that improve cigarette are the inevitable development trend of cigarette.Therefore occurred as cigarette kinds such as ginseng cigarette, peppermint cigarettes on the market, promptly in pipe tobacco, added the material that genseng, peppermint etc. have unique function or taste.
Root of Medicinal Indian mulberry is a kind of rare Chinese medicine with multiple pharmacologically active, and the Root of Medicinal Indian mulberry polysaccharide can obtain by extracting in the Root of Medicinal Indian mulberry rhizome.Root of Medicinal Indian mulberry has the increase body's immunity, nervous system regulation, endocrine system, hemopoietic function improvement and effect such as antitumor, and the Root of Medicinal Indian mulberry polysaccharide is one of main active ingredient.The research of domestic relevant Root of Medicinal Indian mulberry mainly at chemical constituents determination, aspect such as medical, is not seen the application precedent in tobacco.Forefathers are also doing many work aspect the Root of Medicinal Indian mulberry polysaccharide, mainly concentrate on 1. Root of Medicinal Indian mulberry measurements of the polysaccharide content; 2. the extracting method of Root of Medicinal Indian mulberry polysaccharide; 3. the separation and purification of Root of Medicinal Indian mulberry polysaccharide; The biological activity of 4 Root of Medicinal Indian mulberry polysaccharide.But do not consider different processing condition, as the influence of temperature, solid-liquid ratio, extraction time, cycles of concentration to polysaccharide yield.Hydrogen peroxide is as the discoloring agent of oxidized form, and the extraction purifying that is used for vegetable polysaccharides has report, does not see relevant report as yet but be used for Root of Medicinal Indian mulberry polysaccharide extraction purifying.
Summary of the invention
Purpose of the present invention just is being based on the situation of above-mentioned prior art and is studying at Root of Medicinal Indian mulberry specially, and then a kind of extracting method of Root of Medicinal Indian mulberry polysaccharide and the application in cigarette are provided.The Root of Medicinal Indian mulberry polysaccharide that method of the present invention is extracted can be used for joining on the cigarette shreds, to improve the sucking quality of cigarette, reduces some objectionable constituent in the cigarette mainstream flue gas.And this The Application of Technology does not change the existing complete processing of cigarette, the aesthetic quality that can improve cigarette, the hazardness of reduction cigarette.
Purpose of the present invention can be achieved through the following technical solutions:
The extracting method of Root of Medicinal Indian mulberry polysaccharide of the present invention comprises the steps:
A, will place under 30～70 ℃ of conditions and dry, afterwards it is crushed to 10～100 orders through the Root of Medicinal Indian mulberry of pre-treatment;
B, get certain mass step a gained Medicinal Indianmulberry Root, according to water: material (m/m)=5～50, extraction time is 1～4h under 50～100 ℃ of conditions;
C, filtration, concentrated filtrate are to 1/2～1/10 of former filtrate volume;
D, concentrated solution is joined volume fraction is in 95～100% ethanol, and keeping last alcoholic acid volume fraction is 80%, leaves standstill precipitating 24～48 hours, promptly gets the Root of Medicinal Indian mulberry Crude polysaccharides after the filtration;
E, d step gained Root of Medicinal Indian mulberry Crude polysaccharides is put into water redissolve, be mixed with mass concentration and be 1～10% Crude polysaccharides solution, adding volume again is the sevag reagent of 0.1～1 times of Crude polysaccharides solution, vibration is more than 3 hours, leave standstill more than 12 hours, after treating the solution layering, remove the thick shape sevag and the proteinic mixture of lower floor;
F, will remove proteinic polysaccharide soln and with ammoniacal liquor the pH value is adjusted to 9～10, and under 60 ℃ of conditions, slowly add mass concentration and be 30% hydrogen peroxide, add-on is 1/10～1/5 of a polysaccharide soln volume, and polysaccharide soln becomes faint yellow;
G, step f gained solution decoloured after, concentrate, be concentrated into 1/2～1/10 of step f gained liquor capacity, join volume fraction and be in 95～100% the ethanol, keeping last alcoholic acid volume fraction is 80%, leave standstill precipitating 24～48 hours, and filtered the gained white powder, be Root of Medicinal Indian mulberry polysaccharide finished product.
The pre-treatment of the polysaccharide of Root of Medicinal Indian mulberry described in the present invention is removed reel after comprising washing, rejecting impurity, airing and pulverizing.
With the Root of Medicinal Indian mulberry polysaccharide of the inventive method gained after water dissolution, can be used as cigarette is applied on the cigarette shreds with feed liquid, when burning and sucking cigarette, the flue gas free from extraneous odour can improve fragrance matter, pure and mild degree and sweet sense, improves the oral cavity comfortableness, assorted gas and pungency reduce, dry sensation obtains to a certain degree must improving, and certain medicinal efficacy is arranged, and can reduce the content of some objectionable constituent in the cigarette mainstream flue gas.Concrete usage ratio is: Root of Medicinal Indian mulberry polysaccharide consumption is the 0.001-0.5% of tobacco quality, the Root of Medicinal Indian mulberry polysaccharide is a white powder, soluble in water, during use, it is 1～10% solution that the Root of Medicinal Indian mulberry polysaccharide is made into mass concentration through water dissolution, the Root of Medicinal Indian mulberry polysaccharide soln is added on the pipe tobacco at charging process by spray pattern.
Beneficial effect of the present invention is as follows:
Be added with the cigarette of the prepared Root of Medicinal Indian mulberry polysaccharide of the inventive method, when burning and sucking, can obviously improve the sucking quality of cigarette, improve mouthfeel etc., and can reduce the content of some objectionable constituent in the cigarette mainstream flue gas.The present invention does not change original performance of cigarette, has improved the sucking quality of cigarette, therefore has more the meaning and the value of actual production.
Embodiment
The present invention is described further below with reference to embodiment, but is not restriction the present invention.
Embodiment 1
A, will through washing, removal of impurities, removal particle intermediary reel, dry or dry after Root of Medicinal Indian mulberry, place under 60 ℃ of conditions and dry, afterwards it is crushed to 40 orders;
B, get step a gained Medicinal Indianmulberry Root, according to water: material (m/m)=20: 1, under 70 ℃ of conditions, carry out lixiviate and extract, extraction time is 2h;
C, filtration, concentrated filtrate are to 1/6 of former filtrate volume;
D, concentrated solution is added in the dehydrated alcohol, keeping the alcoholic acid volume fraction is 80%, leaves standstill precipitating 48h after the mixing, promptly gets the Root of Medicinal Indian mulberry Crude polysaccharides after the filtration, and productive rate is 13.8%
E, d step gained Root of Medicinal Indian mulberry Crude polysaccharides is put into water redissolve, be mixed with mass concentration and be 5% solution, add volume again and be 0.8 times of Crude polysaccharides solution sevag reagent [chloroform: propyl carbinol (V: V)=4: 1], vibration is more than 3 hours, leave standstill more than 12 hours, after treating the solution layering, remove the thick shape sevag and the proteinic mixture of lower floor;
F, will remove proteinic polysaccharide soln and with ammoniacal liquor the pH value is adjusted to 9～10, and under 60 ℃ of conditions, slowly add mass concentration and be 30% hydrogen peroxide, and become faint yellowly to polysaccharide soln, add-on is about 1/10 of polysaccharide soln volume;
G, with the solution after the step f gained decolouring, concentrate, be concentrated into 1/4 of step f gained liquor capacity, add dehydrated alcohol, keeping the ethanol volume fraction is 80%, leaves standstill precipitating 48 hours, filters the gained white powder, is Root of Medicinal Indian mulberry polysaccharide finished product.
The Root of Medicinal Indian mulberry polysaccharide of the inventive method gained after water dissolution, is mixed with the cigarette feed liquid, is applied on the cigarette shreds and gets final product; Concrete usage ratio is: Root of Medicinal Indian mulberry polysaccharide consumption is 0.01% of a tobacco quality, and the Root of Medicinal Indian mulberry polysaccharide is white powder, and is soluble in water, and during use, the Root of Medicinal Indian mulberry polysaccharide is mixed with mass concentration after water dissolution be 5% solution, stored refrigerated; The Root of Medicinal Indian mulberry polysaccharide soln is added on the pipe tobacco at charging process by spray pattern.
Embodiment 2
A, will through washing, removal of impurities, removal particle intermediary reel, dry or dry after Root of Medicinal Indian mulberry, place under 60 ℃ of conditions and dry, afterwards it is crushed to 40 orders;
B, get step a gained Medicinal Indianmulberry Root, according to water: material (m/m)=40: 1, under 75 ℃ of conditions, carry out lixiviate and extract, extraction time is 1.5h;
C, filtration, concentrated filtrate are to 1/10 of former filtrate volume;
D, concentrated solution is joined in the dehydrated alcohol, keeping the alcoholic acid volume fraction is 80%, leaves standstill precipitating 48h after the mixing, promptly gets the Root of Medicinal Indian mulberry Crude polysaccharides after the filtration, and productive rate is 13.3%
E, d step gained Root of Medicinal Indian mulberry Crude polysaccharides is put into water redissolve, be mixed with mass concentration and be 5% solution, adding volume again is the sevag reagent [chloroform: propyl carbinol (V/V)=4: 1] of 0.7 times of Crude polysaccharides, vibration is more than 3 hours, leave standstill more than 12 hours, after treating the solution layering, remove the thick shape sevag and the proteinic mixture of lower floor;
F, will remove proteinic polysaccharide soln and with ammoniacal liquor the pH value is adjusted to 9～10, and under 60 ℃ of conditions, slowly add mass concentration and be 30% hydrogen peroxide, polysaccharide soln becomes faint yellow, and add-on is 1/10 of a polysaccharide soln volume;
G, with the solution after the step f gained decolouring, concentrate, be concentrated into 1/4 of step f gained liquor capacity, join in the dehydrated alcohol, keeping the ethanol volume fraction is 80%, leaves standstill precipitating 48 hours, filters the gained white powder, is Root of Medicinal Indian mulberry polysaccharide finished product.
The Root of Medicinal Indian mulberry polysaccharide of the inventive method gained after water dissolution, is mixed with the cigarette feed liquid, is applied on the cigarette shreds and gets final product; Concrete usage ratio is: Root of Medicinal Indian mulberry polysaccharide consumption is 0.1% of a tobacco quality, and the Root of Medicinal Indian mulberry polysaccharide is white powder, and is soluble in water, and during use, the Root of Medicinal Indian mulberry polysaccharide is mixed with mass concentration after water dissolution be 6% solution, stored refrigerated; The Root of Medicinal Indian mulberry polysaccharide soln is added on the pipe tobacco at charging process by spray pattern.
Embodiment 3
A, will through washing, removal of impurities, removal particle intermediary reel, dry or dry after Root of Medicinal Indian mulberry, place under 60 ℃ of conditions and dry, afterwards it is crushed to 40 orders;
B, get step a gained Medicinal Indianmulberry Root, according to water: material=25: 1, under 65 ℃ of conditions, carry out lixiviate and extract, extraction time is 1h;
C, filtration, concentrated filtrate are to 1/8 of former filtrate volume;
D, concentrated solution is joined in the dehydrated alcohol, keeping the ethanol volume fraction is 80%, leaves standstill precipitating 48h after the mixing, promptly gets the Root of Medicinal Indian mulberry Crude polysaccharides after the filtration, and productive rate is 12.9%;
E, d step gained Root of Medicinal Indian mulberry Crude polysaccharides is put into water redissolve, being mixed with mass concentration is 5% solution, add volume again and be 0.7 times of Crude polysaccharides solution sevag reagent [chloroform: propyl carbinol (V: V)=4: 1], vibration is more than 3 hours, leave standstill more than 12 hours, after treating the solution layering, remove the thick shape sevag and the proteinic mixture of lower floor;
F, will remove proteinic polysaccharide soln and with ammoniacal liquor the pH value is adjusted to 9～10, and under 60 ℃ of conditions, slowly add mass concentration and be 30% hydrogen peroxide, polysaccharide soln becomes faint yellow, and add-on is 1/10 of a polysaccharide soln volume;
G, with the solution after the step f gained decolouring, concentrate, be concentrated into 1/4 of step f gained liquor capacity, join in the dehydrated alcohol, keeping the ethanol volume fraction is 80%, leaves standstill precipitating 48 hours, filters the gained white powder, is finished product Root of Medicinal Indian mulberry polysaccharide.
The Root of Medicinal Indian mulberry polysaccharide of the inventive method gained after water dissolution, is mixed with the cigarette feed liquid, is applied on the cigarette shreds and gets final product; Concrete usage ratio is: Root of Medicinal Indian mulberry polysaccharide consumption is 0.2% of a tobacco quality, and the Root of Medicinal Indian mulberry polysaccharide is white powder, and is soluble in water, and during use, the Root of Medicinal Indian mulberry polysaccharide is configured to mass concentration after water dissolution be 7% solution, stored refrigerated; The Root of Medicinal Indian mulberry polysaccharide soln is added on the pipe tobacco at charging process by spray pattern.
Claims (5)
1, a kind of extracting method of Root of Medicinal Indian mulberry polysaccharide is characterized in that: described extracting method comprises the steps:
A, will place under 30～70 ℃ of conditions and dry, afterwards it is crushed to 10～100 orders through the Root of Medicinal Indian mulberry of pre-treatment;
B, get certain mass step a gained Medicinal Indianmulberry Root, according to water: material (m/m)=5～50: 1, extraction time is 1～4h under 50～100 ℃ of conditions;
C, filtration, concentrated filtrate are to 1/2～1/10 of former filtrate volume;
D, concentrated solution is joined volume fraction is in 95～100% ethanol, and keeping last alcoholic acid volume fraction is 80%, leaves standstill precipitating 24～48 hours, promptly gets the Root of Medicinal Indian mulberry Crude polysaccharides after the filtration;
E, d step gained Root of Medicinal Indian mulberry Crude polysaccharides is put into water redissolve, be mixed with mass concentration and be 1～10% Crude polysaccharides solution, adding volume again is the sevag reagent of 0.1～1 times of Crude polysaccharides solution, vibration is more than 3 hours, leave standstill more than 12 hours, after treating the solution layering, remove the thick shape sevag and the proteinic mixture of lower floor;
F, will removing proteinic polysaccharide soln, to transfer pH with ammoniacal liquor be under 9～10,60 ℃ of conditions, slowly adds mass concentration and be 30% hydrogen peroxide, and add-on is 1/10～1/5 of a polysaccharide soln volume, and polysaccharide soln becomes faint yellow;
G, with the solution after the step f gained decolouring, concentrate, be concentrated into 1/2～1/10 of step f gained liquor capacity, join volume fraction and be in 95～100% the ethanol, keeping last alcoholic acid volume fraction is 80%, leave standstill precipitating 24～48 hours, and filtered the gained white powder, be Root of Medicinal Indian mulberry polysaccharide finished product.
2, Root of Medicinal Indian mulberry extraction method of polysaccharides according to claim 1 is characterized in that: the processing in early stage of described Root of Medicinal Indian mulberry comprises washing, rejects impurity, airing, pulverizes, goes reel.
3, Root of Medicinal Indian mulberry extraction method of polysaccharides according to claim 1 is characterized in that: described sevag reagent is chloroform: propyl carbinol (V: V)=4: 1.
4, the application of Root of Medicinal Indian mulberry polysaccharide according to claim 1 in cigarette is characterized in that: Root of Medicinal Indian mulberry polysaccharide consumption is 0.001～0.5% of a tobacco quality, the Root of Medicinal Indian mulberry polysaccharide soln is added on the pipe tobacco at charging process by spray pattern.
5, the application of Root of Medicinal Indian mulberry polysaccharide according to claim 4 in cigarette is characterized in that: the mass concentration of Root of Medicinal Indian mulberry polysaccharide after water dissolution is 1～10%.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2008101414507A CN101357949B (en) | 2008-09-25 | 2008-09-25 | Extraction method of polysaccharides from morinda officinalis how and application thereof in cigarette |
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| CN2008101414507A CN101357949B (en) | 2008-09-25 | 2008-09-25 | Extraction method of polysaccharides from morinda officinalis how and application thereof in cigarette |
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Cited By (10)
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| CN101704900B (en) * | 2009-11-10 | 2011-07-27 | 中国烟草总公司郑州烟草研究院 | Extraction method of cactus polysaccharide and application thereof in cigarettes |
| CN102283434A (en) * | 2010-06-18 | 2011-12-21 | 福建中烟工业公司 | Preparation method of morinda officinalis regenerated thin tablet and application of morinda officinalis regenerated thin tablet prepared by the preparation method in tobacco product |
| CN102351956A (en) * | 2011-08-09 | 2012-02-15 | 朱孟勇 | Extraction method of morindea officinalis polysaccharide |
| CN102793263A (en) * | 2012-08-27 | 2012-11-28 | 福建中烟工业有限责任公司 | Extraction method of tremella water extract concentrate and application of concentrate in tobaccos |
| CN103859582A (en) * | 2014-04-02 | 2014-06-18 | 甘肃烟草工业有限责任公司 | Application of potentilla anserine polysaccharide to cigarettes and preparation method of tobacco material liquid thereof |
| CN103980374A (en) * | 2014-05-20 | 2014-08-13 | 河南中烟工业有限责任公司 | Morinda officinalis polysaccharide, extraction and purification method and application thereof as tobacco humectant |
| CN104119576A (en) * | 2014-06-19 | 2014-10-29 | 无限极（中国）有限公司 | Morinda officinalis and sealwort compound polysaccharide with function of adjusting tumor microenvironment and preparation method and application of morinda officinalis and sealwort compound polysaccharide |
| CN104397872A (en) * | 2014-12-04 | 2015-03-11 | 湖南中烟工业有限责任公司 | Application of pineapple skin polysaccharide in cigarettes |
| CN107118283A (en) * | 2017-05-26 | 2017-09-01 | 广东药科大学 | Morinda officinalis sugar polymers and its production and use |
| CN114190458A (en) * | 2021-12-08 | 2022-03-18 | 海南省农业科学院农产品加工设计研究所 | Compound Mallotus oblongifolius tea polyphenol concentrated powder and preparation method thereof |
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2008
- 2008-09-25 CN CN2008101414507A patent/CN101357949B/en not_active Expired - Fee Related
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101704900B (en) * | 2009-11-10 | 2011-07-27 | 中国烟草总公司郑州烟草研究院 | Extraction method of cactus polysaccharide and application thereof in cigarettes |
| CN102283434A (en) * | 2010-06-18 | 2011-12-21 | 福建中烟工业公司 | Preparation method of morinda officinalis regenerated thin tablet and application of morinda officinalis regenerated thin tablet prepared by the preparation method in tobacco product |
| CN102351956A (en) * | 2011-08-09 | 2012-02-15 | 朱孟勇 | Extraction method of morindea officinalis polysaccharide |
| CN102793263A (en) * | 2012-08-27 | 2012-11-28 | 福建中烟工业有限责任公司 | Extraction method of tremella water extract concentrate and application of concentrate in tobaccos |
| CN103859582A (en) * | 2014-04-02 | 2014-06-18 | 甘肃烟草工业有限责任公司 | Application of potentilla anserine polysaccharide to cigarettes and preparation method of tobacco material liquid thereof |
| CN103859582B (en) * | 2014-04-02 | 2016-04-06 | 甘肃烟草工业有限责任公司 | The preparation method of fern amylose cigarette feed liquid |
| CN103980374A (en) * | 2014-05-20 | 2014-08-13 | 河南中烟工业有限责任公司 | Morinda officinalis polysaccharide, extraction and purification method and application thereof as tobacco humectant |
| CN104119576A (en) * | 2014-06-19 | 2014-10-29 | 无限极（中国）有限公司 | Morinda officinalis and sealwort compound polysaccharide with function of adjusting tumor microenvironment and preparation method and application of morinda officinalis and sealwort compound polysaccharide |
| CN104397872A (en) * | 2014-12-04 | 2015-03-11 | 湖南中烟工业有限责任公司 | Application of pineapple skin polysaccharide in cigarettes |
| CN104397872B (en) * | 2014-12-04 | 2016-01-20 | 湖南中烟工业有限责任公司 | The application of pineapple peel polysaccharide in cigarette |
| CN107118283A (en) * | 2017-05-26 | 2017-09-01 | 广东药科大学 | Morinda officinalis sugar polymers and its production and use |
| CN114190458A (en) * | 2021-12-08 | 2022-03-18 | 海南省农业科学院农产品加工设计研究所 | Compound Mallotus oblongifolius tea polyphenol concentrated powder and preparation method thereof |
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