CN101356208B - 液态、储存稳定、含碳二亚胺和/或脲酮亚胺基团的有机异氰酸酯的制备方法 - Google Patents
液态、储存稳定、含碳二亚胺和/或脲酮亚胺基团的有机异氰酸酯的制备方法 Download PDFInfo
- Publication number
- CN101356208B CN101356208B CN2006800506337A CN200680050633A CN101356208B CN 101356208 B CN101356208 B CN 101356208B CN 2006800506337 A CN2006800506337 A CN 2006800506337A CN 200680050633 A CN200680050633 A CN 200680050633A CN 101356208 B CN101356208 B CN 101356208B
- Authority
- CN
- China
- Prior art keywords
- acid amides
- silylated
- carbodiimide
- isocyanate
- catalyzer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
- C08G18/78—Nitrogen
- C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/02—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only
- C08G18/025—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only the polymeric products containing carbodiimide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C267/00—Carbodiimides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D229/00—Heterocyclic compounds containing rings of less than five members having two nitrogen atoms as the only ring hetero atoms
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/02—Polymeric products of isocyanates or isothiocyanates of isocyanates or isothiocyanates only
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
- C08G18/78—Nitrogen
- C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
- C08G18/797—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing carbodiimide and/or uretone-imine groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/20—Compounding polymers with additives, e.g. colouring
- C08J3/22—Compounding polymers with additives, e.g. colouring using masterbatch techniques
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Polyurethanes Or Polyureas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102006000822A DE102006000822A1 (de) | 2006-01-05 | 2006-01-05 | Verfahren zur Herstellung flüssiger, lagerstabiler Carbodiimid- und/oder Uretonimingruppen aufweisender organischer Isocyanate |
| DE102006000822.7 | 2006-01-05 | ||
| PCT/EP2006/012553 WO2007077000A2 (de) | 2006-01-05 | 2006-12-27 | Verfahren zur herstellung flüssiger, lagerstabiler carbodiimid- und/oder uretonimingruppen aufweisender organischer isocyanate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101356208A CN101356208A (zh) | 2009-01-28 |
| CN101356208B true CN101356208B (zh) | 2011-09-07 |
Family
ID=37895819
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2006800506337A Expired - Fee Related CN101356208B (zh) | 2006-01-05 | 2006-12-27 | 液态、储存稳定、含碳二亚胺和/或脲酮亚胺基团的有机异氰酸酯的制备方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US7714148B2 (https=) |
| EP (1) | EP1971623B1 (https=) |
| JP (1) | JP2009522419A (https=) |
| KR (1) | KR20080091472A (https=) |
| CN (1) | CN101356208B (https=) |
| AT (1) | ATE443090T1 (https=) |
| DE (2) | DE102006000822A1 (https=) |
| ES (1) | ES2331380T3 (https=) |
| PT (1) | PT1971623E (https=) |
| WO (1) | WO2007077000A2 (https=) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102006000825A1 (de) * | 2006-01-05 | 2007-07-12 | Bayer Materialscience Ag | Verfahren zur Herstellung flüssiger, lagerstabiler Carbodiimidgruppen aufweisender organischer Isocyanate |
| DE102006000833A1 (de) * | 2006-01-05 | 2007-07-12 | Bayer Materialscience Ag | Verfahren zur Herstellung flüssiger, lagerstabiler Carbodiimid- und/oder Uretonimingruppen aufweisender organischer Isocyanate |
| CN102718683B (zh) * | 2012-06-05 | 2014-08-06 | 万华化学集团股份有限公司 | 一种制备低色数异氰酸酯的方法及由其制得的异氰酸酯 |
| US10633476B2 (en) | 2015-02-26 | 2020-04-28 | Covestro Deutschland Ag | Method for producing a composition comprising polycarbodiimide having improved storage stability |
| CN109790269B (zh) * | 2016-10-14 | 2022-06-14 | 旭化成株式会社 | 异氰酸酯组合物、异氰酸酯组合物的制造方法以及异氰酸酯聚合物的制造方法 |
| KR102129159B1 (ko) * | 2017-09-15 | 2020-07-01 | 주식회사 엘지화학 | 저색수 카바졸 화합물의 제조방법 |
| CN116057102A (zh) * | 2020-08-07 | 2023-05-02 | 巴斯夫欧洲公司 | 己内酰胺改性的液体mdi及其在聚氨酯中的用途 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5202358A (en) * | 1991-05-28 | 1993-04-13 | Bayer Aktiengesellschaft | Process for the preparation of liquid storable organic isocyanates containing carbodiimide and/or uretone imine groups and their use for the preparation of polyurethane plastics |
| CN1789241A (zh) * | 2005-12-12 | 2006-06-21 | 拜尔材料科学股份公司 | 液态、储存稳定、色指数低、含有碳二亚胺和/或脲酮亚胺基团的有机异氰酸酯的制备方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2853473A (en) * | 1956-08-27 | 1958-09-23 | Du Pont | Production of carbodiimides |
| DE2537685C2 (de) * | 1975-08-23 | 1989-04-06 | Bayer Ag, 5090 Leverkusen | Verfahren zur teilweisen Carbodiimidisierung der Isocyanatgruppen von organischen Polyisocyanaten |
| DE2606419A1 (de) * | 1976-02-18 | 1977-08-25 | Basf Ag | Lagerbestaendige, fluessige carbodiimidgruppen aufweisende polyisocyanate und verfahren zu ihrer herstellung |
| DE4302697A1 (de) * | 1993-02-01 | 1994-08-04 | Bayer Ag | Verfahren zur Herstellung organischer Carbodiimide und ihre Verwendung als Kunststoff-Stabilisatoren |
| US6120699A (en) * | 1998-09-21 | 2000-09-19 | Basf Corporation | Storage stable methylene bis(phenylisocyanate) compositions |
| US6362247B1 (en) * | 2000-05-08 | 2002-03-26 | Rohm And Haas Company | Method of improving stability of aromatic polycarbodiimides |
| DE10201241A1 (de) * | 2002-01-15 | 2003-07-24 | Bayer Ag | Katalysator |
| DE102004033849A1 (de) * | 2004-07-13 | 2006-02-16 | Bayer Materialscience Ag | Verfahren zur Herstellung flüssiger, lagerstabiler Carbodiimid- und/oder Uretonimingruppen aufweisender organischer Isocyanate mit niedriger Farbzahl |
| DE102004060038A1 (de) * | 2004-12-14 | 2006-06-22 | Bayer Materialscience Ag | Verfahren zur Herstellung flüssiger, lagerstabiler Carbodiimid- und/oder Uretonimingruppen aufweisender organischer Isocyanate mit niedriger Farbzahl |
| DE102006000825A1 (de) * | 2006-01-05 | 2007-07-12 | Bayer Materialscience Ag | Verfahren zur Herstellung flüssiger, lagerstabiler Carbodiimidgruppen aufweisender organischer Isocyanate |
| DE102006000833A1 (de) * | 2006-01-05 | 2007-07-12 | Bayer Materialscience Ag | Verfahren zur Herstellung flüssiger, lagerstabiler Carbodiimid- und/oder Uretonimingruppen aufweisender organischer Isocyanate |
| DE102006002158A1 (de) * | 2006-01-17 | 2007-07-19 | Bayer Materialscience Ag | Verfahren zur Herstellung flüssiger, lagerstabiler Carboddimid- und/oder Uretonimingruppen aufweisender organischer Isocyanate |
-
2006
- 2006-01-05 DE DE102006000822A patent/DE102006000822A1/de not_active Withdrawn
- 2006-12-27 KR KR1020087019153A patent/KR20080091472A/ko not_active Ceased
- 2006-12-27 DE DE502006004896T patent/DE502006004896D1/de active Active
- 2006-12-27 EP EP06841179A patent/EP1971623B1/de not_active Not-in-force
- 2006-12-27 AT AT06841179T patent/ATE443090T1/de not_active IP Right Cessation
- 2006-12-27 WO PCT/EP2006/012553 patent/WO2007077000A2/de not_active Ceased
- 2006-12-27 PT PT06841179T patent/PT1971623E/pt unknown
- 2006-12-27 CN CN2006800506337A patent/CN101356208B/zh not_active Expired - Fee Related
- 2006-12-27 ES ES06841179T patent/ES2331380T3/es active Active
- 2006-12-27 JP JP2008548949A patent/JP2009522419A/ja not_active Withdrawn
-
2007
- 2007-01-03 US US11/649,001 patent/US7714148B2/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5202358A (en) * | 1991-05-28 | 1993-04-13 | Bayer Aktiengesellschaft | Process for the preparation of liquid storable organic isocyanates containing carbodiimide and/or uretone imine groups and their use for the preparation of polyurethane plastics |
| CN1789241A (zh) * | 2005-12-12 | 2006-06-21 | 拜尔材料科学股份公司 | 液态、储存稳定、色指数低、含有碳二亚胺和/或脲酮亚胺基团的有机异氰酸酯的制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE502006004896D1 (de) | 2009-10-29 |
| CN101356208A (zh) | 2009-01-28 |
| US7714148B2 (en) | 2010-05-11 |
| US20070155939A1 (en) | 2007-07-05 |
| JP2009522419A (ja) | 2009-06-11 |
| EP1971623A2 (de) | 2008-09-24 |
| KR20080091472A (ko) | 2008-10-13 |
| WO2007077000A2 (de) | 2007-07-12 |
| DE102006000822A1 (de) | 2007-07-12 |
| PT1971623E (pt) | 2009-11-02 |
| EP1971623B1 (de) | 2009-09-16 |
| WO2007077000A3 (de) | 2008-02-21 |
| ES2331380T3 (es) | 2009-12-30 |
| ATE443090T1 (de) | 2009-10-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| REG | Reference to a national code |
Ref country code: HK Ref legal event code: DE Ref document number: 1126804 Country of ref document: HK |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20110907 Termination date: 20121227 |
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