CN101210129A - Crackle lacquer, preparing method thereof and spraying method for the same - Google Patents
Crackle lacquer, preparing method thereof and spraying method for the same Download PDFInfo
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- CN101210129A CN101210129A CNA200610063702XA CN200610063702A CN101210129A CN 101210129 A CN101210129 A CN 101210129A CN A200610063702X A CNA200610063702X A CN A200610063702XA CN 200610063702 A CN200610063702 A CN 200610063702A CN 101210129 A CN101210129 A CN 101210129A
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Abstract
The invention relates to a crack lacquer. According to the portion by weight, the lacquer comprises the following components that: 11 to 40 percent of thermoset acrylics, 4 to 20 percent of no-light powder, 0.5 to 26 percent of auxiliary, 2.7 to 33 percent of mixed solvent, and 5 to 15 percent of paint; the crack lacquer has natural grain, good three-dimensional effect and even cracks; the crack effect is beautiful with excellent aging resistance, water resistance and stability; the preparation technique of the crack lacquer of the invention is simple, and the spraying method of the crack lacquer is as follows: priming lacquer is firstly sprayed so as to ensure that the priming lacquer is matched with the crack lacquer; in the spraying process, the temperature difference between the bottom of the crack lacquer and a bottom layer is generated by adopting the high solidity and the high speed of the volatilization of the solvent of the crack lacquer; the priming lacquer of the crack lacquer is cracked by means of the strain of a lacquer film; the greater the color difference between the priming lacquer and the crack lacquer, the better the three-dimensional effect of the crack lacquer and the more obvious the aesthetic perception of the decoration.
Description
Technical field
The present invention relates to a kind of paint, especially relate to the spraying method of a kind of strain indicating lacquer and preparation method thereof and this strain indicating lacquer.
Background technology
In daily life, usually can see that some are coated with ornament through wind, Exposure to Sunlight, drench with rain and big or small nonstandard crackle occurs, strain indicating lacquer is copied this effect and is developed, it can form good crack pattern rapidly at body surface, the crackle texture is even, changeful, have stereoeffect, true to nature naturally, noble elegant, has higher artistic taste, can strengthen the attractive in appearance of coatingsurface, improve ornamentally, be suitable for the surface decoration of indoor furniture and indoor decoration and artwork, give people's allusion, the U.S. of missing old times or old friends is for traditional straight-shade coating provides abundant artistic effect.Present this painting effect is accepted by people gradually and is liked, household that is used for making oneself beautiful and life.
At present, the strain indicating lacquer of preparation is in the majority with nitro-resin, for example the Chinese patent publication number is that CN1580151 discloses a kind of nitro crack lacquer and preparation method thereof, described strain indicating lacquer is made by nitrocellulose, pigment, filler and solvent etc., film forming matter is few in the prescription, and pigment, filler are many, and solvent volatility is big, the stress that self is produced by paint film in the solvent evaporates process makes paint film cracking.Strain indicating lacquer generally all needs with common pyroxylin(e)finish as bottom; In order to protect the crackle coating, also use the zapon varnish Lacquer finish sometimes, but the poor-performing that pyroxylin(e)finish is filmed, such as the poor stability of pyroxylin(e)finish, easily aging under the irradiation of sunlight, weathering resistance is relatively poor, is easy to fade and flavescence paint film adhesion difference etc.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of strain indicating lacquer, and durability of coating is good after this strain indicating lacquer film forming.
Another object of the present invention is to provide a kind of preparation method of strain indicating lacquer, this method technology is simple.
Still a further object of the present invention provides a kind of spraying method of strain indicating lacquer, this method application, and workability is superior.
For achieving the above object, technical scheme of the present invention is: a kind of strain indicating lacquer is provided, and it comprises following component by weight: thermosetting acrylic resin 11-40, mute light powder 4-20, auxiliary material 0.5-26, mixed solvent 2.7-33, pigment 5-15.
Described strain indicating lacquer comprises following component by weight: thermosetting acrylic resin 15-30, mute light powder 5-10, auxiliary material 1-10, mixed solvent 2.7-33, pigment 5-15.
The solid content of described thermosetting acrylic resin is 40-60%,
Described mute light powder is an aerosil, and itself and thermosetting acrylic resin solid content weight ratio are: 1: 0.5-6.
Described auxiliary material comprises one or more compositions in the anti-settling agent of the softening agent of flow agent, 0.1-6 of dispersion agent, the 0.1-5 of 0.1-10 and 0.1-5 by weight.
Described mixed solvent is the mixed solvent that ketone, ethers, ester class and alcohols are formed, and ketone: ethers: ester class: the weight ratio of alcohols is (15-30): (10-20): (20-40): (15-30).
Described ketone is one or more compositions of acetone, butanone, methyl iso-butyl ketone (MIBK), ring ethyl ketone or pimelinketone; Described ethers is one or more compositions of butyl glycol ether, ethylene glycol ethyl ether; One or more compositions that described ester class is ethyl acetate, butylacetate, ethylene glycol ether acetate or 2-Butoxyethyl acetate; Described alcohols is one or more compositions of diacetone alcohol, Virahol, butanols or isopropylcarbinol.
Described mixed solvent is acetone, pimelinketone degree, butyl glycol ether, the mixed solvent that ethyl acetate and diacetone alcohol are formed, acetone, pimelinketone, butyl glycol ether, ethyl acetate and diacetone alcohol count 1.5 by weight: (1-1.5): (2-3): 1.5: 1.
The present invention also provides a kind of preparation method of strain indicating lacquer, it is characterized in that: this method is the auxiliary material mixing with the heat cured acrylic resin of 11-40 weight part and 0.5-26 weight part, make in the mixed solvent that is dispersed in the 2.7-33 weight part, fully mix the pigment of back adding 5-20 weight part, continue to mix, grind, be uniformly dispersed.
The present invention further provides a kind of spraying method of strain indicating lacquer, it is characterized in that: comprise the following steps:
(1) spraying crackle priming paint;
(2) strain indicating lacquer is mixed with an amount of solidifying agent, be adjusted to certain viscosity, stir evenly with thinner;
(3) mixture with (2) step sprays on the crackle priming paint, surface drying 6-8 minute, dries 15-25 minute under 60-80 ℃ of left and right sides condition then;
Described solidifying agent is the isocyanates solidifying agent.
The beneficial effect that the present invention brings is, the present invention adopts the existing nitro crack lacquer in thermoset acrylics strain indicating lacquer and market to compare, vinylformic acid strain indicating lacquer lines nature, and stereoeffect is good, and crackle is even; The crackle effect is attractive in appearance, has excellent resistance to deterioration, and is water-fast and stable; Strain indicating lacquer preparation technology of the present invention is simple, the spraying method of this strain indicating lacquer is to spray priming paint earlier, make it supporting with strain indicating lacquer, utilize strain indicating lacquer self solid content height in spraying process, solvent evaporates is fast, crack the temperature head of lacquer surface and bottom, rely on the tension force effect of paint film, ftracture on crackle priming paint, priming paint and strain indicating lacquer color distinction are big more, the strain indicating lacquer stereoeffect that forms is good more, and ornamental aesthetic feeling is obvious more.
Embodiment
The invention provides a kind of strain indicating lacquer; It comprises following component by weight: thermosetting acrylic resin 11-40; Mute light powder 4-20; Auxiliary material 0.5-26; Mixed solvent 2.7-33; Pigment 5-15.
Auxiliary material of the present invention comprises dispersion agent, flow agent, softening agent and anti-settling agent, and the composition of described flow agent is organically-modified siloxanes or fluorine-carbon modified polyacrylic acid; The composition of described dispersion agent is the polymer copolymerization body that contains the pigment affinity groups; The composition of described softening agent is that dioctyl phthalate (DOP) (DOP) is or/and dibutyl phthalate (DBP).Pigment of the present invention comprises carbon black, organic red, titanium dioxide etc.
Described mute light powder master is an aerosil, mainly is will be used for controlling the size of strain indicating lacquer crackle and ftractureing into degree, and itself and thermosetting acrylic resin contain weight ratio admittedly and be: 1: 0.5-6.
Embodiment 1
Embodiments of the invention provide a kind of strain indicating lacquer, and it comprises following component by weight:
Thermosetting acrylic resin 2850 is 24, pigment 10, and dispersion agent 1.3, anti-settling agent 0.78, flow agent 0.72, softening agent 0.73, mute light powder 10, solvent 25, solidifying agent is an amount of.
Described resin is a thermosetting acrylic resin, and mute light powder is an aerosil, and described solvent is by acetone, pimelinketone, butyl glycol ether, and ethyl acetate and diacetone alcohol are formed, and it counts 1.5: 1.5: 2.5 by weight: 1.5: 1.
Form according to above-mentioned prescription, described strain indicating lacquer adopts following method preparation:
(1) in having the container of agitator, add thermosetting acrylic resin, dispersion agent, softening agent, mute light powder, anti-settling agent, flow agent and mixed solvent stir evenly.
(2) add pigment in the slurries that make, grind to disperse with shredder, it is even to add remaining stirring solvent, filters and promptly gets the strain indicating lacquer finished product.
The strain indicating lacquer lines nature that present embodiment makes, stereoeffect is good, and crackle is even; The crackle effect is attractive in appearance, has excellent resistance to deterioration, and is water-fast and stable.
Embodiment 2
A kind of strain indicating lacquer that embodiments of the invention provide, it comprises following component by weight: thermosetting acrylic resin 2850 is 24, pigment 13, dispersion agent 1.4, anti-settling agent 0.78, flow agent 0.37, softening agent 0.72, mute light powder 8, solvent 25, solidifying agent is an amount of.
Described resin is a thermosetting acrylic resin, and mute light powder is an aerosil, and described solvent is by acetone, pimelinketone, butyl glycol ether, and ethyl acetate and diacetone alcohol are formed, and it counts 1.5: 1: 2 by weight: 1.5: 1.
The preparation method of embodiments of the invention is identical with embodiment 1, and crackle is even, attractive in appearance, but lines is less.
Embodiment 3
A kind of strain indicating lacquer that embodiments of the invention provide, it comprises following component by weight: thermosetting acrylic resin A-371 is 24, pigment 10, dispersion agent 1.4, anti-settling agent 0.78, flow agent 0.36, mute light powder 10, solvent 30, solidifying agent is an amount of.
Described resin is a thermosetting acrylic resin, and mute light powder is an aerosil, and described solvent is by acetone, pimelinketone, butyl glycol ether, and ethyl acetate and diacetone alcohol are formed, and it counts 1.5: 1: 3 by weight: 1.5: 1.
Form according to above-mentioned prescription, described strain indicating lacquer adopts following method preparation:
(1) in having the container of agitator, add thermosetting acrylic resin, dispersion agent, mute light powder, anti-settling agent, flow agent and mixed solvent stir evenly.
(2) add pigment in the slurries that make, grind to disperse with shredder, it is even to add remaining stirring solvent, filters and promptly gets the strain indicating lacquer finished product.
The strain indicating lacquer lines that embodiments of the invention make is bigger, but the lines nature, stereoeffect is good, and crackle is even; The crackle effect is attractive in appearance.
Embodiment 4
A kind of strain indicating lacquer that embodiments of the invention provide, it comprises following component by weight: thermosetting acrylic resin A-371 is 24, pigment 13, dispersion agent 1.4, anti-settling agent 0.76, flow agent 0.36, mute light powder 8, solvent 30, solidifying agent is an amount of.
Described resin is a thermosetting acrylic resin, and mute light powder is an aerosil, and described solvent is by acetone, pimelinketone, butyl glycol ether, and ethyl acetate and diacetone alcohol are formed, and it counts 1.5: 1.5: 3 by weight: 1.5: 1.
Form according to above-mentioned prescription, described strain indicating lacquer adopts following method preparation:
(1) in having the container of agitator, add thermosetting acrylic resin, dispersion agent, mute light powder, anti-settling agent, flow agent and mixed solvent stir evenly.
(2) add pigment in the slurries that make, grind to disperse with shredder, it is even to add remaining stirring solvent, filters and promptly gets the strain indicating lacquer finished product.
The strain indicating lacquer lacquer painting that embodiments of the invention make is level and smooth, even, and the crackle lines is smaller.
Embodiment 5
A kind of strain indicating lacquer that embodiments of the invention provide, it comprises following component by weight: thermosetting acrylic resin A-371 is 11, pigment 5, dispersion agent 1.5, mute light powder 5, solvent 33, solidifying agent is an amount of.
Described resin is a thermosetting acrylic resin, and mute light powder is an aerosil, and described solvent is by acetone, pimelinketone, butyl glycol ether, and ethyl acetate and diacetone alcohol are formed, and it counts 1.5: 1.5: 2 by weight: 1.5: 1.
Form according to above-mentioned prescription, described strain indicating lacquer adopts following method preparation:
(1) in having the container of agitator, add thermosetting acrylic resin, dispersion agent, mute light powder and mixed solvent stir evenly.
(2) add pigment in the slurries that make, grind to disperse with shredder, it is even to add remaining stirring solvent, filters and promptly gets the strain indicating lacquer finished product.
The strain indicating lacquer lines nature that embodiments of the invention make, stereoeffect is good, and crackle is even; The crackle effect is attractive in appearance.
Embodiment 6
A kind of strain indicating lacquer that embodiments of the invention provide, it comprises following component by weight: thermosetting acrylic resin A-371 is 40, pigment 10, dispersion agent 1.4, anti-settling agent 0.76, flow agent 0.36, softening agent 0.73, mute light powder 20, solvent 33, solidifying agent is an amount of.
Described resin is a thermosetting acrylic resin, and mute light powder is an aerosil, and described solvent is by acetone, pimelinketone, butyl glycol ether, and ethyl acetate and diacetone alcohol are formed, and it counts 1.5: 1.5: 2 by weight: 1.5: 1.
The preparation method of embodiments of the invention is identical with embodiment 1, and the strain indicating lacquer crackle is even, and lines is better, but lacquer painting has slight floating powder, fades.
Embodiment 7
A kind of strain indicating lacquer that embodiments of the invention provide, it comprises following component by weight: thermosetting acrylic resin A-371 is 24, pigment 13, dispersion agent 10, anti-settling agent 5, flow agent 6, softening agent 5, mute light powder 8, solvent 30, solidifying agent is an amount of.
Described resin is a thermosetting acrylic resin, and mute light powder is an aerosil, and described solvent is by acetone, pimelinketone, butyl glycol ether, and ethyl acetate and diacetone alcohol are formed, and it counts 1.5: 1.5: 3 by weight: 1.5: 1.
The strain indicating lacquer lacquer painting that embodiments of the invention make is level and smooth, even, and the crackle lines is finer and closely woven.
Embodiment 8
Embodiments of the invention provide a kind of spraying method of strain indicating lacquer, make strain indicating lacquer according to the prescription of embodiment 1-3, and spraying method may further comprise the steps:
(1) spraying crackle priming paint;
(2) strain indicating lacquer is mixed with an amount of solidifying agent, be adjusted to certain viscosity, stir evenly with thinner;
(3) mixture with (2) step sprays on the crackle priming paint, and surface drying 6 minutes was dried 15 minutes under 60 ℃ of conditions then;
The described solidifying agent of the embodiment of the invention is the isocyanates solidifying agent.
Embodiment 9
Embodiments of the invention provide a kind of spraying method of strain indicating lacquer, make strain indicating lacquer according to the prescription of embodiment 4-7, and spraying method may further comprise the steps:
(1) spraying crackle priming paint;
(2) strain indicating lacquer is mixed with an amount of solidifying agent, be adjusted to certain viscosity, stir evenly with thinner;
(3) mixture with (2) step sprays on the crackle priming paint, and surface drying 8 minutes was dried 25 minutes under 80 ℃ of conditions then;
The described solidifying agent of the embodiment of the invention is the isocyanates solidifying agent.
The spraying method of the strain indicating lacquer that the above embodiment of the present invention 8 and 9 provides is to spray priming paint earlier, make it supporting with strain indicating lacquer, in spraying process, utilize strain indicating lacquer self solid content height, solvent evaporates is fast, cracks the temperature head of lacquer surface and bottom, relies on the tension force effect of paint film, on crackle priming paint, ftracture, priming paint and strain indicating lacquer color distinction are big more, and the strain indicating lacquer stereoeffect of formation is good more, and ornamental aesthetic feeling is obvious more.
Claims (11)
1. strain indicating lacquer comprises following component by weight:
Thermosetting acrylic resin 11-40
Mute light powder 4-20
Auxiliary material 0.5-26
Mixed solvent 2.7-33
Pigment 5-20.
2. strain indicating lacquer according to claim 1 is characterized in that: described strain indicating lacquer comprises following component by weight:
Thermosetting acrylic resin 15-30
Mute light powder 5-10
Auxiliary material 1-10
Mixed solvent 2.7-33
Pigment 5-15.
3. strain indicating lacquer according to claim 1 and 2 is characterized in that: the solid content of described thermosetting acrylic resin is 40-60%.
4. strain indicating lacquer according to claim 3 is characterized in that: described mute light powder is an aerosil, and itself and thermosetting acrylic resin solid content weight ratio are: 1: 0.5-6.
5. strain indicating lacquer according to claim 1 is characterized in that: described auxiliary material comprises one or more compositions in the anti-settling agent of the softening agent of flow agent, 0.1-6 of dispersion agent, the 0.1-5 of 0.1-10 and 0.1-5 by weight.
6. strain indicating lacquer according to claim 3, it is characterized in that: described mixed solvent is the mixed solvent that ketone, ethers, ester class and alcohols are formed, and ketone: ethers: ester class: the weight ratio of alcohols is (15-30): (10-20): (20-40): (15-30).
7. strain indicating lacquer according to claim 6 is characterized in that: described ketone is one or more compositions of acetone, butanone, methyl iso-butyl ketone (MIBK), ring ethyl ketone or pimelinketone; Described ethers is one or more compositions of butyl glycol ether, ethylene glycol ethyl ether; One or more compositions that described ester class is ethyl acetate, butylacetate, ethylene glycol ether acetate or 2-Butoxyethyl acetate; Described alcohols is one or more compositions of diacetone alcohol, Virahol, butanols or isopropylcarbinol.
8. strain indicating lacquer according to claim 7, it is characterized in that: described mixed solvent is acetone, pimelinketone, butyl glycol ether, the mixed solvent that ethyl acetate and diacetone alcohol are formed, acetone, pimelinketone, butyl glycol ether, ethyl acetate and diacetone alcohol count 1.5 by weight: (1-1.5): (2-3): 1.5: 1.
9. the preparation method of a strain indicating lacquer, it is characterized in that: this method is the auxiliary material mixing with the heat cured acrylic resin of 11-40 weight part and 0.5-26 weight part, make in the mixed solvent that is dispersed in the 2.7-33 weight part, fully mix the pigment of back adding 5-20 weight part, continue to mix, grind, be uniformly dispersed.
10. the spraying method of a strain indicating lacquer is characterized in that: comprise the following steps:
(1) spraying crackle priming paint;
(2) strain indicating lacquer is mixed with an amount of solidifying agent, be adjusted to certain viscosity, stir evenly with thinner;
(3) mixture with (2) step sprays on the crackle priming paint, surface drying 6-8 minute, dries 15-25 minute under 60-80 ℃ of left and right sides condition then;
11. the spraying method of strain indicating lacquer according to claim 10 is characterized in that: described solidifying agent is the isocyanates solidifying agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200610063702XA CN101210129B (en) | 2006-12-30 | 2006-12-30 | Crackle lacquer, preparing method thereof and spraying method for the same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200610063702XA CN101210129B (en) | 2006-12-30 | 2006-12-30 | Crackle lacquer, preparing method thereof and spraying method for the same |
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| Publication Number | Publication Date |
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| CN101210129A true CN101210129A (en) | 2008-07-02 |
| CN101210129B CN101210129B (en) | 2011-04-06 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN200610063702XA Expired - Fee Related CN101210129B (en) | 2006-12-30 | 2006-12-30 | Crackle lacquer, preparing method thereof and spraying method for the same |
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| CN109280445A (en) * | 2018-09-29 | 2019-01-29 | 佛山齐安建筑科技有限公司 | A kind of preparation method of the fire-retardant crackle paint of high rigidity |
| CN110105862A (en) * | 2019-06-11 | 2019-08-09 | 浙江伟星实业发展股份有限公司 | A kind of spray painting major ingredient and rain and dew paint for button |
| CN111391191A (en) * | 2020-04-22 | 2020-07-10 | 利高工艺品（厦门）有限公司 | Production method of crack product |
| CN111992469A (en) * | 2020-08-25 | 2020-11-27 | 苏州欧普照明有限公司 | Three-dimensional pattern coating, preparation method thereof, lamp fitting and lamp |
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