CN101199689B - Grape chrysanthemum capsule and preparing method thereof - Google Patents
Grape chrysanthemum capsule and preparing method thereof Download PDFInfo
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- CN101199689B CN101199689B CN2007103020933A CN200710302093A CN101199689B CN 101199689 B CN101199689 B CN 101199689B CN 2007103020933 A CN2007103020933 A CN 2007103020933A CN 200710302093 A CN200710302093 A CN 200710302093A CN 101199689 B CN101199689 B CN 101199689B
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- vitis viniferae
- extracting solution
- semen vitis
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- powder
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Abstract
The invention discloses a grape-and-chrysanthemum capsule and the preparation method. The grape-and-chrysanthemum capsule contains chrysanthemum concrete powder with the weight percentage between 18 percent and 95 percent and grape pip extractive with the weight percentage between 82 percent and 5 percent. Chrysanthemum and grape pips are respectively prepared into extractives and then the extractives are mixed and prepared into capsules. The invention has the functions of oxidation resistance and regulating blood fat and is applicable for middle-aged people and senior citizens, achieving the purposes of delaying senility, reducing blood fat and improving cardiovascular efficiency.
Description
Technical field
The present invention relates to the Chinese medicine health care product field, especially, relate to a kind of grape chrysanthemum capsule (or soft capsule) and preparation method thereof.
Background technology
Along with being showing improvement or progress day by day and developing of society, people's work pressure is also along with increasing the weight of, and the food of research antioxidation (slow down aging) is extremely rising; People very pay attention to the health care of self, hope life lengthening.
Flos Chrysanthemi is the dry capitulum of feverfew chrysanthemum (Chrysanthemum morifollium Ramat.).Existing research shows: Flos Chrysanthemi extract has good antioxidation.
Fructus Vitis viniferae is famous fruit, belongs to Vitaceae Vitis (Vitis L.) plant.Semen Vitis viniferae is its mature fruit seed, the leftover bits and pieces of wine-making industry often.Experiment shows, contains multiple materials such as procyanidin, flavonoid, unsaturated fatty acid, multivitamin and trace element in the Semen Vitis viniferae extract, not only has good antioxidation, and can improve cardiovascular function.
Many to Semen Vitis viniferae and Flos Chrysanthemi extract and chemical research at present, but be that the health food of combination does not also have with them at present.Main cause is the not enough system of research, also has many difficulties simultaneously on preparation and the production technology.
Summary of the invention
The objective of the invention is to the deficiency to prior art, a kind of grape chrysanthemum capsule and preparation method thereof is provided, product has antioxidation or effect for reducing blood fat.
The objective of the invention is to realize through following technical scheme: a kind of grape chrysanthemum capsule, it is that 18%～95% chrysanthemum concrete powder and 82～5% Semen Vitis viniferae extract are formed by percentage by weight.
Further, said Semen Vitis viniferae extract is made up of the grease and the Semen Vitis viniferae extract powder of Semen Vitis viniferae extraction.
A kind of method for preparing of grape chrysanthemum capsule may further comprise the steps,
(1) be equipped with the chrysanthemum concrete powder: Flos Chrysanthemi adds 70%～80% ethanol of 6 times of amounts, and reflux, extract, 2 hours is filtered, the high speed centrifugation time extracting solution of winning; Residue adds 5 times of amount 70%～80% ethanol, and reflux, extract, 1.5 hours is filtered, and high speed centrifugation gets extracting solution for the second time; Merge extracted twice liquid, the relative density that the extracting solution after merging is evaporated to concentrated solution is 1.10～1.15, and spray drying gets the chrysanthemum concrete powder;
(2) preparation Semen Vitis viniferae extract: Semen Vitis viniferae is ground into coarse powder, through supercritical extraction, the grease of Semen Vitis viniferae extraction, will be through the Semen Vitis viniferae powder after the extraction,, filter the high speed centrifugation inferior extracting solution of winning with the ethanol extraction of 5 times of amounts 70%～80% 2 hours; Residue adds 4 times of amount 70～80 ethanol, extracts 1.5 hours, filters, and high speed centrifugation gets extracting solution for the second time; Residue adds 4 times of amount 70～80 ethanol, extracts 1 hour, filters, and high speed centrifugation gets extracting solution for the third time; Merge three times extracting solution, the relative density that the extracting solution after merging is evaporated to concentrated solution is 1.10～1.15, and spray drying gets the Semen Vitis viniferae extract powder;
(3) with 18%～95% Flos Chrysanthemi extract and 82～5% the abundant mix homogeneously of Semen Vitis viniferae extract;
(4) process capsule.
The present invention has following technique effect: antioxidation, blood lipid regulation effect; Be applicable to mid-aged population, reach slow down aging, blood fat reducing, improve the purpose of cardiovascular function.
The specific embodiment
Specify specific embodiment of the present invention below.
Embodiment 1
Get Flos Chrysanthemi 5000 gram, add 70% ethanol of 6 times of amounts, reflux, extract, 2 hours is filtered; Win time extracting solution of high speed centrifugation, residue adds 5 times of amount 70% ethanol, reflux, extract, 1.5 hours; Filter, high speed centrifugation gets extracting solution for the second time, merges extracted twice liquid; The relative density that extracting solution after merging is evaporated to concentrated solution is 1.10～1.15, and spray drying gets chrysanthemum concrete powder 800 grams; Get Semen Vitis viniferae 20000 grams, be ground into coarse powder (crossing 40 orders),, get oily extract 2800 grams through supercritical extraction, subsequent use; Will be through the Semen Vitis viniferae powder after the extraction,, filter the high speed centrifugation inferior extracting solution of winning with 5 times of amount ethanol extractions of 70% 2 hours; Residue adds 4 times of amount 70% ethanol, extracts 1.5 hours, filters, and high speed centrifugation gets extracting solution for the second time; Residue adds 4 times of amount 70% ethanol, extracts 1 hour, filters, and high speed centrifugation gets extracting solution for the third time; Merge three times extracting solution, with the extracting solution concentrating under reduced pressure after merging, thickening temperature is less than 70 ℃; The relative density that is concentrated into concentrated solution is 1.10～1.15, and spray drying gets extract powder 700 grams.Among this embodiment, Semen Vitis viniferae extract is made up of the grease and the Semen Vitis viniferae extract powder of Semen Vitis viniferae extraction.With the grease and the abundant mix homogeneously of Semen Vitis viniferae extract powder of chrysanthemum concrete powder, Semen Vitis viniferae extraction, behind the homogenizer homogenizing, process the consistent mixture of color and luster again.Mixture is pressed into soft capsule.Get soft capsule.
Embodiment 2
Get Flos Chrysanthemi 20000 gram, add 70% ethanol of 6 times of amounts, reflux, extract, 2 hours is filtered; Win time extracting solution of high speed centrifugation, residue adds 5 times of amount 70% ethanol, reflux, extract, 1.5 hours; Filter, high speed centrifugation gets extracting solution for the second time, merges extracted twice liquid; The relative density that extracting solution after merging is evaporated to concentrated solution is 1.10～1.15, and spray drying gets extract powder 3200 grams; Get Semen Vitis viniferae 5000 grams, be ground into coarse powder (crossing 40 orders),, get oily extract 700 grams (abandoning) through supercritical extraction; Will be through the Semen Vitis viniferae powder after the extraction,, filter the high speed centrifugation inferior extracting solution of winning with 5 times of amount ethanol extractions of 70% 2 hours; Residue adds 4 times of amount 70% ethanol, extracts 1.5 hours, filters, and high speed centrifugation gets extracting solution for the second time; Residue adds 4 times of amount 70% ethanol, extracts 1 hour, filters, and high speed centrifugation gets extracting solution for the third time; Merge three times extracting solution, with the extracting solution concentrating under reduced pressure after merging, thickening temperature is less than 70 ℃; The relative density that is concentrated into concentrated solution is 1.10～1.15, and spray drying gets extract powder 175 grams.Among this embodiment, Semen Vitis viniferae extract is the Semen Vitis viniferae extract powder.With chrysanthemum concrete powder and the abundant mix homogeneously of Semen Vitis viniferae extract powder, mixture is carried out capsule fill, get capsule.
Embodiment 3
Get Flos Chrysanthemi 10000 gram, add 70% ethanol of 6 times of amounts, reflux, extract, 2 hours is filtered; Win time extracting solution of high speed centrifugation, residue adds 5 times of amount 70% ethanol, reflux, extract, 1.5 hours; Filter, high speed centrifugation gets extracting solution for the second time, merges extracted twice liquid; The relative density that extracting solution after merging is evaporated to concentrated solution is 1.10～1.15, and spray drying gets extract powder 1600 grams; Get Semen Vitis viniferae 10000 grams, be ground into coarse powder (crossing 40 orders),, get oily extract 1400 grams (abandoning) through supercritical extraction; Will be through the Semen Vitis viniferae powder after the extraction,, filter the high speed centrifugation inferior extracting solution of winning with 5 times of amount ethanol extractions of 70% 2 hours; Residue adds 4 times of amount 70% ethanol, extracts 1.5 hours, filters, and high speed centrifugation gets extracting solution for the second time; Residue adds 4 times of amount 70% ethanol, extracts 1 hour, filters, and high speed centrifugation gets extracting solution for the third time; Merge three times extracting solution, with the extracting solution concentrating under reduced pressure after merging, thickening temperature is less than 70 ℃; The relative density that is concentrated into concentrated solution is 1.10～1.15, and spray drying gets extract powder 350 grams.Among this embodiment, Semen Vitis viniferae extract is the Semen Vitis viniferae extract powder.With chrysanthemum concrete powder and the abundant mix homogeneously of Semen Vitis viniferae extract powder, mixture is carried out capsule fill, get capsule.
The foregoing description is used for the present invention that explains, rather than limits the invention, and in the protection domain of spirit of the present invention and claim, any modification and change to the present invention makes all fall into protection scope of the present invention.
Claims (1)
1. the method for preparing of a grape chrysanthemum capsule is characterized in that, may further comprise the steps,
(1) preparation chrysanthemum concrete powder: Flos Chrysanthemi adds 70%～80% ethanol of 6 times of amounts, and reflux, extract, 2 hours is filtered, the high speed centrifugation time extracting solution of winning; Residue adds 5 times of amount 70%～80% ethanol, and reflux, extract, 1.5 hours is filtered, and high speed centrifugation gets extracting solution for the second time; Merge extracted twice liquid, the relative density that the extracting solution after merging is evaporated to concentrated solution is 1.10～1.15, and spray drying gets the chrysanthemum concrete powder;
(2) preparation Semen Vitis viniferae extract: Semen Vitis viniferae is ground into coarse powder, through supercritical extraction, the grease of Semen Vitis viniferae extraction, will be through the Semen Vitis viniferae powder after the extraction,, filter the high speed centrifugation inferior extracting solution of winning with the ethanol extraction of 5 times of amounts 70%～80% 2 hours; Residue adds 4 times of amount 70%～80% ethanol, extracts 1.5 hours, filters, and high speed centrifugation gets extracting solution for the second time; Residue adds 4 times of amount 70%～80% ethanol, extracts 1 hour, filters, and high speed centrifugation gets extracting solution for the third time; Merge three times extracting solution, the relative density that the extracting solution after merging is evaporated to concentrated solution is 1.10～1.15, and spray drying gets the Semen Vitis viniferae extract powder;
(3) with 18%～95% chrysanthemum concrete powder and 82%～5% the abundant mix homogeneously of Semen Vitis viniferae extract, said Semen Vitis viniferae extract is the grease of Semen Vitis viniferae extraction and the mixture of Semen Vitis viniferae extract powder;
(4) process capsule.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007103020933A CN101199689B (en) | 2007-12-24 | 2007-12-24 | Grape chrysanthemum capsule and preparing method thereof |
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| CN2007103020933A CN101199689B (en) | 2007-12-24 | 2007-12-24 | Grape chrysanthemum capsule and preparing method thereof |
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| Publication Number | Publication Date |
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| CN101199689A CN101199689A (en) | 2008-06-18 |
| CN101199689B true CN101199689B (en) | 2012-04-18 |
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| CN2007103020933A Expired - Fee Related CN101199689B (en) | 2007-12-24 | 2007-12-24 | Grape chrysanthemum capsule and preparing method thereof |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104161909A (en) * | 2014-09-09 | 2014-11-26 | 遵义陆圣康源科技开发有限责任公司 | Pharmaceutical composition for removing chloasma |
| CN108619906B (en) * | 2018-05-31 | 2021-04-06 | 杭州康嘻环保科技有限公司 | Environment-friendly deodorant for decoration and preparation method thereof |
| CN109224029A (en) * | 2018-09-30 | 2019-01-18 | 泓博元生命科技（深圳）有限公司 | Blood-fat reducing composition, preparation containing NMN and the preparation method and application thereof |
| CN109200243A (en) * | 2018-09-30 | 2019-01-15 | 泓博元生命科技（深圳）有限公司 | A kind of blood-fat reducing composition, preparation and the preparation method and application thereof |
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| CN1241623A (en) * | 1999-08-18 | 2000-01-19 | 孙传经 | Supercritical carbon dioxide extraction process of grape seed oil and cyanine oligomer |
| CN1463743A (en) * | 2002-06-29 | 2003-12-31 | 王勇智 | Capsule possessing antisenescent and spot dispelling effect and method for making the same |
| CN1582755A (en) * | 2004-06-02 | 2005-02-23 | 中国农业大学 | Nutrient food for face skin nourishment |
| CN1615753A (en) * | 2003-11-10 | 2005-05-18 | 刘会生 | Beauty dietetic health nutritive powder |
| CN1850140A (en) * | 2006-02-22 | 2006-10-25 | 天津大学 | Method for preparing chrysanthemum formula granules |
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2007
- 2007-12-24 CN CN2007103020933A patent/CN101199689B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1241623A (en) * | 1999-08-18 | 2000-01-19 | 孙传经 | Supercritical carbon dioxide extraction process of grape seed oil and cyanine oligomer |
| CN1463743A (en) * | 2002-06-29 | 2003-12-31 | 王勇智 | Capsule possessing antisenescent and spot dispelling effect and method for making the same |
| CN1615753A (en) * | 2003-11-10 | 2005-05-18 | 刘会生 | Beauty dietetic health nutritive powder |
| CN1582755A (en) * | 2004-06-02 | 2005-02-23 | 中国农业大学 | Nutrient food for face skin nourishment |
| CN1850140A (en) * | 2006-02-22 | 2006-10-25 | 天津大学 | Method for preparing chrysanthemum formula granules |
Non-Patent Citations (2)
| Title |
|---|
| 隋晓春等.一种抗辐射危害和缓解视疲劳保健食品的研制.食品与药品9 11A.2007,9(11A),19-21. |
| 隋晓春等.一种抗辐射危害和缓解视疲劳保健食品的研制.食品与药品9 11A.2007,9(11A),19-21. * |
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