CN101191138B - Method for producing gellan gum finished product from gellan gum fermentation liquor - Google Patents
Method for producing gellan gum finished product from gellan gum fermentation liquor Download PDFInfo
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- CN101191138B CN101191138B CN2006101188437A CN200610118843A CN101191138B CN 101191138 B CN101191138 B CN 101191138B CN 2006101188437 A CN2006101188437 A CN 2006101188437A CN 200610118843 A CN200610118843 A CN 200610118843A CN 101191138 B CN101191138 B CN 101191138B
- Authority
- CN
- China
- Prior art keywords
- liquid
- obtains
- gelling gum
- gum
- flocculation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 229920002148 Gellan gum Polymers 0.000 title claims abstract description 77
- 239000000216 gellan gum Substances 0.000 title claims abstract description 77
- 235000010492 gellan gum Nutrition 0.000 title claims abstract description 77
- 238000000855 fermentation Methods 0.000 title claims abstract description 29
- 230000004151 fermentation Effects 0.000 title claims abstract description 29
- 238000004519 manufacturing process Methods 0.000 title abstract description 6
- 238000000034 method Methods 0.000 claims abstract description 142
- 230000018044 dehydration Effects 0.000 claims abstract description 26
- 238000006297 dehydration reaction Methods 0.000 claims abstract description 26
- 238000005352 clarification Methods 0.000 claims abstract description 16
- 239000000049 pigment Substances 0.000 claims abstract description 13
- 238000004090 dissolution Methods 0.000 claims abstract description 9
- 239000007788 liquid Substances 0.000 claims description 210
- 239000000047 product Substances 0.000 claims description 72
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 68
- 238000005189 flocculation Methods 0.000 claims description 53
- 230000016615 flocculation Effects 0.000 claims description 53
- 239000012043 crude product Substances 0.000 claims description 32
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 28
- 238000001914 filtration Methods 0.000 claims description 27
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 23
- 238000009736 wetting Methods 0.000 claims description 20
- 239000002585 base Substances 0.000 claims description 18
- 239000006185 dispersion Substances 0.000 claims description 18
- 238000000926 separation method Methods 0.000 claims description 16
- 150000003839 salts Chemical class 0.000 claims description 15
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 14
- 230000001476 alcoholic effect Effects 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 10
- 229910052783 alkali metal Inorganic materials 0.000 claims description 9
- -1 alkali metal salts Chemical class 0.000 claims description 9
- 238000001704 evaporation Methods 0.000 claims description 9
- 239000003292 glue Substances 0.000 claims description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 8
- 238000010612 desalination reaction Methods 0.000 claims description 8
- 230000008020 evaporation Effects 0.000 claims description 8
- 238000001556 precipitation Methods 0.000 claims description 8
- 238000010298 pulverizing process Methods 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 238000011085 pressure filtration Methods 0.000 claims description 7
- 239000012716 precipitator Substances 0.000 claims description 6
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 5
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 5
- 239000004411 aluminium Substances 0.000 claims description 5
- 229910052782 aluminium Inorganic materials 0.000 claims description 5
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 5
- 229910052791 calcium Inorganic materials 0.000 claims description 5
- 239000011575 calcium Substances 0.000 claims description 5
- 230000003311 flocculating effect Effects 0.000 claims description 5
- 229910052749 magnesium Inorganic materials 0.000 claims description 5
- 239000011777 magnesium Substances 0.000 claims description 5
- 229910052751 metal Inorganic materials 0.000 claims description 5
- 239000002184 metal Substances 0.000 claims description 5
- 150000004703 alkoxides Chemical class 0.000 claims description 4
- 238000005345 coagulation Methods 0.000 claims description 4
- 230000001105 regulatory effect Effects 0.000 claims description 4
- 235000017550 sodium carbonate Nutrition 0.000 claims description 4
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 4
- 238000003828 vacuum filtration Methods 0.000 claims description 4
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 3
- 229910052788 barium Inorganic materials 0.000 claims description 3
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims description 3
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 3
- 235000015320 potassium carbonate Nutrition 0.000 claims description 3
- 229910052725 zinc Inorganic materials 0.000 claims description 3
- 239000011701 zinc Substances 0.000 claims description 3
- 125000002252 acyl group Chemical group 0.000 abstract description 19
- 229910021645 metal ion Inorganic materials 0.000 abstract description 4
- 238000009833 condensation Methods 0.000 abstract 3
- 230000005494 condensation Effects 0.000 abstract 3
- 230000036571 hydration Effects 0.000 abstract 1
- 238000006703 hydration reaction Methods 0.000 abstract 1
- 238000003756 stirring Methods 0.000 description 16
- 239000012141 concentrate Substances 0.000 description 8
- 238000005516 engineering process Methods 0.000 description 8
- 150000004676 glycans Chemical class 0.000 description 8
- 239000012535 impurity Substances 0.000 description 8
- 229920001282 polysaccharide Polymers 0.000 description 8
- 239000005017 polysaccharide Substances 0.000 description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 7
- 239000000706 filtrate Substances 0.000 description 7
- 230000001580 bacterial effect Effects 0.000 description 6
- 238000007599 discharging Methods 0.000 description 6
- 239000004744 fabric Substances 0.000 description 6
- 238000001471 micro-filtration Methods 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000012528 membrane Substances 0.000 description 4
- 238000005374 membrane filtration Methods 0.000 description 4
- 239000003960 organic solvent Substances 0.000 description 4
- 238000000746 purification Methods 0.000 description 4
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 3
- 150000001768 cations Chemical class 0.000 description 3
- 239000002932 luster Substances 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 230000001954 sterilising effect Effects 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- FRXSZNDVFUDTIR-UHFFFAOYSA-N 6-methoxy-1,2,3,4-tetrahydroquinoline Chemical compound N1CCCC2=CC(OC)=CC=C21 FRXSZNDVFUDTIR-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 230000002070 germicidal effect Effects 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 238000001291 vacuum drying Methods 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 235000019890 Amylum Nutrition 0.000 description 1
- 125000002353 D-glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 1
- 241001113556 Elodea Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 235000019733 Fish meal Nutrition 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241000237502 Ostreidae Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241000589516 Pseudomonas Species 0.000 description 1
- 229920000297 Rayon Polymers 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 241000790234 Sphingomonas elodea Species 0.000 description 1
- 108700016252 Staphylococcus aureus chemotaxis inhibitory Proteins 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- DPDMMXDBJGCCQC-UHFFFAOYSA-N [Na].[Cl] Chemical group [Na].[Cl] DPDMMXDBJGCCQC-UHFFFAOYSA-N 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229940041514 candida albicans extract Drugs 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000003381 deacetylation reaction Methods 0.000 description 1
- 230000013872 defecation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000012262 fermentative production Methods 0.000 description 1
- 239000004467 fishmeal Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 239000000413 hydrolysate Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 150000001455 metallic ions Chemical class 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 238000000643 oven drying Methods 0.000 description 1
- 235000020636 oyster Nutrition 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 239000012138 yeast extract Substances 0.000 description 1
Landscapes
- Jellies, Jams, And Syrups (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN2006101188437A CN101191138B (en) | 2006-11-28 | 2006-11-28 | Method for producing gellan gum finished product from gellan gum fermentation liquor |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN2006101188437A CN101191138B (en) | 2006-11-28 | 2006-11-28 | Method for producing gellan gum finished product from gellan gum fermentation liquor |
Publications (2)
Publication Number | Publication Date |
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CN101191138A CN101191138A (en) | 2008-06-04 |
CN101191138B true CN101191138B (en) | 2010-10-27 |
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CN2006101188437A Expired - Fee Related CN101191138B (en) | 2006-11-28 | 2006-11-28 | Method for producing gellan gum finished product from gellan gum fermentation liquor |
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CN (1) | CN101191138B (en) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101824095B (en) * | 2009-05-31 | 2012-10-10 | 上海众伟生化有限公司 | Transparent high acyl gellan gum and production method thereof |
CN101585886B (en) * | 2009-06-03 | 2012-10-03 | 浙江帝斯曼中肯生物科技有限公司 | Post-extracting method of high acyl gellan gum |
WO2011003269A1 (en) * | 2009-07-09 | 2011-01-13 | 浙江帝斯曼中肯生物科技有限公司 | Method for post-extracting low acyl gellan gum |
CN101597341B (en) * | 2009-07-09 | 2011-10-26 | 浙江帝斯曼中肯生物科技有限公司 | Method for post extraction of low-acyl gellan gum with high solubility |
CN101724090B (en) * | 2009-12-01 | 2011-10-26 | 淄博中轩生化有限公司 | Method for refining Gellan gum |
CN101885783A (en) * | 2010-07-09 | 2010-11-17 | 尹洪波 | Preparation method of transparent gellan gum finished product |
CN102391384A (en) * | 2011-09-30 | 2012-03-28 | 郸城财鑫糖业有限责任公司 | Production process for high acyl gellan gum |
CN103113488B (en) * | 2013-02-22 | 2015-12-23 | 天茁(上海)生物科技有限公司 | The extracting method of the low acyl transparent type gelling gum of a kind of easy dispersion and dissolving |
CN103145870A (en) * | 2013-03-27 | 2013-06-12 | 天茁(上海)生物科技有限公司 | Extraction method of gellan gum for meat product |
EP3421605A1 (en) * | 2017-06-29 | 2019-01-02 | DSM IP Assets B.V. | Process for producing gellan comprising feeding a nitrogen source during fermentation |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1351172A (en) * | 2000-10-26 | 2002-05-29 | 上海众伟生化有限公司 | Process for preparing microbial polyose jelly |
CN1635133A (en) * | 2004-11-19 | 2005-07-06 | 张禹 | Gellan gum post-extraction method |
CN1687437A (en) * | 2005-03-25 | 2005-10-26 | 张禹 | Method of high post extraction of acyl Gellan |
-
2006
- 2006-11-28 CN CN2006101188437A patent/CN101191138B/en not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1351172A (en) * | 2000-10-26 | 2002-05-29 | 上海众伟生化有限公司 | Process for preparing microbial polyose jelly |
CN1635133A (en) * | 2004-11-19 | 2005-07-06 | 张禹 | Gellan gum post-extraction method |
CN1687437A (en) * | 2005-03-25 | 2005-10-26 | 张禹 | Method of high post extraction of acyl Gellan |
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Publication number | Publication date |
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CN101191138A (en) | 2008-06-04 |
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