CN101163724A - 具有控制的pH的包含低量含氟表面活性剂的含氟聚合物水分散体的制备方法 - Google Patents

具有控制的pH的包含低量含氟表面活性剂的含氟聚合物水分散体的制备方法 Download PDF

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Publication number
CN101163724A
CN101163724A CNA2006800112481A CN200680011248A CN101163724A CN 101163724 A CN101163724 A CN 101163724A CN A2006800112481 A CNA2006800112481 A CN A2006800112481A CN 200680011248 A CN200680011248 A CN 200680011248A CN 101163724 A CN101163724 A CN 101163724A
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CN
China
Prior art keywords
dispersion
fluoropolymer
exchange resin
water
fluorochemical surfactant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CNA2006800112481A
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English (en)
Chinese (zh)
Inventor
D·W·约翰逊
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EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of CN101163724A publication Critical patent/CN101163724A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/14—Treatment of polymer emulsions
    • C08F6/16—Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/04—Processes using organic exchangers
    • B01J41/05—Processes using organic exchangers in the strongly basic form
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F14/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F14/18—Monomers containing fluorine
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/06—Ethers; Acetals; Ketals; Ortho-esters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D127/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers
    • C09D127/02—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
    • C09D127/12—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
    • C09D127/18—Homopolymers or copolymers of tetrafluoroethene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2327/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers
    • C08J2327/02—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment
    • C08J2327/12—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Dispersion Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Paints Or Removers (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
CNA2006800112481A 2005-02-10 2006-02-10 具有控制的pH的包含低量含氟表面活性剂的含氟聚合物水分散体的制备方法 Pending CN101163724A (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US65160405P 2005-02-10 2005-02-10
US60/651,604 2005-02-10

Publications (1)

Publication Number Publication Date
CN101163724A true CN101163724A (zh) 2008-04-16

Family

ID=36569962

Family Applications (1)

Application Number Title Priority Date Filing Date
CNA2006800112481A Pending CN101163724A (zh) 2005-02-10 2006-02-10 具有控制的pH的包含低量含氟表面活性剂的含氟聚合物水分散体的制备方法

Country Status (5)

Country Link
US (1) US20060178472A1 (https=)
EP (1) EP1846462A1 (https=)
JP (1) JP2008530314A (https=)
CN (1) CN101163724A (https=)
WO (1) WO2006086795A1 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103443196A (zh) * 2011-03-31 2013-12-11 大金工业株式会社 含氟聚合物水性分散液

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008062653A1 (en) 2006-11-24 2008-05-29 Asahi Glass Company, Limited Method for producing aqueous fluorine-containing polymer dispersion with reduced fluorine-containing emulsifier content
WO2008132959A1 (ja) * 2007-04-13 2008-11-06 Asahi Glass Company, Limited 含フッ素カルボン酸化合物を用いた含フッ素ポリマーの製造方法
US20100036053A1 (en) * 2008-08-08 2010-02-11 E.I. Du Pont De Nemours And Company Aqueous Polymerization Process for the Manufacture of Fluoropolymer Comprising Repeating Units Arising from a Perfluoromonomer and a Monomer Having a Functional Group and a Polymerizable Carbon-Carbon Double Bond
US8058375B2 (en) * 2008-12-23 2011-11-15 E I. Du Pont De Nemours And Company Use of ethylene-tetrafluoroethylene carboxylic acids and salts as surfactants for aqueous emulsion polymerization of fluorinated monomer
US8329813B2 (en) * 2009-05-08 2012-12-11 E I Du Pont De Nemours And Company Thermal reduction of fluoroether carboxylic acids or salts from fluoropolymer dispersions
JP4858628B2 (ja) * 2010-05-25 2012-01-18 ユニマテック株式会社 含フッ素ポリマー水性分散液
CN103201300B (zh) * 2010-11-09 2016-11-09 纳幕尔杜邦公司 使用烃表面活性剂的含氟单体的含水聚合
JP2016023269A (ja) * 2014-07-23 2016-02-08 旭硝子株式会社 含フッ素樹脂水性分散液の製造方法
WO2019031617A1 (ja) 2017-08-10 2019-02-14 ダイキン工業株式会社 精製ポリテトラフルオロエチレン水性分散液の製造方法、改質ポリテトラフルオロエチレン粉末の製造方法、ポリテトラフルオロエチレン成形体の製造方法、及び、組成物
SG11202000862YA (en) 2017-08-10 2020-02-27 Daikin Ind Ltd Method for producing purified polytetrafluoroethylene aqueous dispersion liquid, method for producing modified polytetrafluoroethylene powder, method for producing polytetrafluoroethylene molded body, and composition
CN115536770A (zh) * 2022-06-11 2022-12-30 泰兴梅兰新材料有限公司 一种用于聚四氟乙烯分散聚合的预微乳液制备方法
JP7850324B1 (ja) 2025-07-14 2026-04-22 ユニマテック株式会社 フルオロポリマー水性分散液の製造方法、フルオロポリマーの製造方法、含フッ素乳化剤を含むフルオロポリマー水性分散液の含フッ素乳化剤濃度を低減する方法

Family Cites Families (18)

* Cited by examiner, † Cited by third party
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US2559752A (en) * 1951-03-06 1951-07-10 Du Pont Aqueous colloidal dispersions of polymers
US3037953A (en) * 1961-04-26 1962-06-05 Du Pont Concentration of aqueous colloidal dispersions of polytetrafluoroethylene
US3882153A (en) * 1969-09-12 1975-05-06 Kureha Chemical Ind Co Ltd Method for recovering fluorinated carboxylic acid
US3704272A (en) * 1970-09-15 1972-11-28 Du Pont Concentration of polytetrafluoroethylene aqueous dispersion
DE2903981A1 (de) * 1979-02-02 1980-08-07 Hoechst Ag Rueckgewinnung fluorierter emulgatorsaeuren aus basischen anionenaustauschern
JP3346090B2 (ja) * 1995-03-31 2002-11-18 ダイキン工業株式会社 ポリテトラフルオロエチレン水性分散液組成物及びその用途
DE19857111A1 (de) * 1998-12-11 2000-06-15 Dyneon Gmbh Wäßrige Dispersionen von Fluorpolymeren
DE19933696A1 (de) * 1999-07-17 2001-01-18 Dyneon Gmbh Verfahren zur Rückgewinnung fluorierter Emulgatoren aus wässrigen Phasen
US6720360B1 (en) * 2000-02-01 2004-04-13 3M Innovative Properties Company Ultra-clean fluoropolymers
US6720437B2 (en) * 2001-02-07 2004-04-13 E. I. Du Pont De Nemours And Company Fluorinated carboxylic acid recovery and reuse
US20030125421A1 (en) * 2001-08-03 2003-07-03 Hermann Bladel Aqueous dispersions of fluoropolymers
US7279522B2 (en) * 2001-09-05 2007-10-09 3M Innovative Properties Company Fluoropolymer dispersions containing no or little low molecular weight fluorinated surfactant
EP1364972B1 (en) * 2002-05-22 2006-08-30 3M Innovative Properties Company Process for reducing the amount of fluorinated surfactant in aqueous fluoropolymer dispersions
EP1441014A1 (en) * 2003-01-22 2004-07-28 3M Innovative Properties Company Aqueous fluoropolymer dispersion comprising a melt processible fluoropolymer and having a reduced amount of fluorinated surfactant
DE60301322T2 (de) * 2003-02-28 2006-06-08 3M Innovative Properties Co., St. Paul Fluoropolymerdispersion enthaltend kein oder wenig fluorhaltiges Netzmittel mit niedrigem Molekulargewicht
EP1533325B1 (en) * 2003-11-17 2011-10-19 3M Innovative Properties Company Aqueous dispersions of polytetrafluoroethylene having a low amount of fluorinated surfactant
US7619018B2 (en) * 2004-12-22 2009-11-17 E.I. Du Pont De Nemours And Company Process for removing fluorosurfactant from aqueous fluoropolymer dispersions and reducing scum formation
US7659329B2 (en) * 2004-12-22 2010-02-09 E. I. Du Pont De Nemours And Company Removing fluorosurfactant from aqueous fluoropolymer dispersions using monodisperse ion exchange resin

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103443196A (zh) * 2011-03-31 2013-12-11 大金工业株式会社 含氟聚合物水性分散液
US9080035B2 (en) 2011-03-31 2015-07-14 Daikin Industries, Ltd. Aqueous fluoropolymer dispersion
CN103443196B (zh) * 2011-03-31 2015-11-25 大金工业株式会社 含氟聚合物水性分散液

Also Published As

Publication number Publication date
WO2006086795A1 (en) 2006-08-17
JP2008530314A (ja) 2008-08-07
US20060178472A1 (en) 2006-08-10
EP1846462A1 (en) 2007-10-24

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Open date: 20080416