CN101125766A - Method for preparing ceramic glaze material by using granite waste material - Google Patents
Method for preparing ceramic glaze material by using granite waste material Download PDFInfo
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- CN101125766A CN101125766A CNA2007101484276A CN200710148427A CN101125766A CN 101125766 A CN101125766 A CN 101125766A CN A2007101484276 A CNA2007101484276 A CN A2007101484276A CN 200710148427 A CN200710148427 A CN 200710148427A CN 101125766 A CN101125766 A CN 101125766A
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- glaze
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- granite
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Abstract
The invention discloses a method for producing ceramic glaze with granite waste. The steps are that: granite waste is first crushed by a crusher, wet ball grinded, screened by a standard screen of 200 mesh to remove impurities, then produced into glaze slurry with concentration of 1.5-1.9g/ml. The glaze slurry is dotted on the surface of the rough-body, then the rough body is put into a bellow to be heated, dried or aired between the temperature 70 DEG C to 110 DEG C until the water content is less than 1 percent, roasted between the temperature of 1200-1350 DEG C, insulated for 0.5-3h, naturally cooled to room temperature and finally the glaze is obtained. The invention has low cost, strong adaptability to rough-body, wide temperature range of glaze roasting, excellent melting and stable performance, changes waste into valuables by applying granite waste as raw material and produces ceramic glaze that has no harmful substances such as lead, etc.
Description
Technical field
The present invention relates to the preparation method of ceramic glaze, particularly utilize the granite waste material to prepare the method for ceramic glaze.
Background technology
Stone material is a resources processing type industry, and resource is worked into finished product from the famine material, and the waste of half is arranged approximately.Granite is in exploitation and cutting processing process, and a large amount of fragments and cutting break flour are taken as waste material and abandon, and cause the wasting of resources.The at present domestic and international art pottery and the used glaze of terra-cotta all are to be processed for main raw material by multiple natural matter (as quartz, feldspar, Wingdale etc.).Because the mineral resources of glaze reduces day by day now, price improves day by day, has increased the cost of Production of Ceramics.Therefore, be that main raw material prepares glaze and can reduce trash discharge in the processing of stone process with the granite waste material, and new glaze source is provided.
Summary of the invention
Purpose of the present invention just provides a kind of with low cost, is the method for feedstock production ceramic glaze with the granite waste material.
The technical solution adopted in the present invention is: the granite waste material is carried out fragmentation with crusher earlier, granite waste material with fragmentation carries out wet ball grinding then, granite waste material behind the ball milling is crossed 200 mesh standard sieves and is sieved and remove impurity, be made into glaze slip then, concentration of glaze slip is controlled at 1.5～1.9g/ml; Glaze slip is granted billet surface, in bellows in 70 ℃～110 ℃ heat dryings or dry the back to its moisture less than 1%, at last it is burnt till between 1200 ℃～1350 ℃, be incubated after 0.5～3 hour, naturally cool to room temperature with stove, can make glaze.
The present invention is with low cost, is that raw material can be turned waste into wealth with the granite waste material, the not leaded toxic substance that waits of made ceramic glaze,, temperature of glaze firing wide ranges strong to base substrate adaptability, melt well, stable performance.
Embodiment
Embodiment 1:
Single black gabbride granite waste material (chemical ingredients such as table 1) is carried out fragmentation with crusher, black gabbride granite waste material with fragmentation carries out wet ball grinding then, black gabbride granite waste material behind the ball milling is crossed 200 mesh standard sieves and is sieved and remove impurity, be made into glaze slip then, the concentration of glaze slip is 1.65g/ml, is applied to ceramic body surface (chemical ingredients such as the table 2 of base substrate) in the brushing glazing mode.With sample in bellows in 80 ℃ of oven dry, in stove, slowly be heated to 1250 ℃ then, be incubated 1 hour after, being allowed to condition at lowers the temperature in the stove naturally is cooled to room temperature, can obtain wine-colored glaze.
The granitic chemical ingredients of table 1 black gabbride
| Composition | SiO 2 | TiO 2 | Al 2O 3 | Fe 2O 3 | FeO | MnO | MgO | CaO | Na 2O | K 2O | P 2O 5 |
| Content/% | 61.88 | 0.65 | 15.87 | 1.80 | 3.65 | 0.09 | 3.26 | 5.19 | 3.53 | 3.48 | 0.26 |
The chemical ingredients of table 2 base substrate
| Composition | SiO 2 | Al 2O 3 | Fe 2O 3 | MgO | CaO | Na 2O | K 2O |
| Content/% | 69.50 | 25.70 | 0.19 | 0.07 | 0.16 | 3.87 | 3.87 |
Embodiment 2:
The long class granite waste material of single flesh pink potassium (chemical ingredients such as table 3) is carried out fragmentation with crusher, the long class class of flesh pink potassium granite waste material with fragmentation carries out wet ball grinding then, the long class granite of flesh pink potassium behind ball milling waste material is crossed 200 mesh standard sieves and is sieved and remove impurity, be made into glaze slip then, the concentration of glaze slip is 1.65g/ml, is applied to ceramic body surface (chemical ingredients such as the table 2 of base substrate) in the brushing glazing mode.With sample in bellows in 80 ℃ of oven dry, in stove, slowly be heated to 1250 ℃ then, be incubated 1 hour after, being allowed to condition at lowers the temperature in the stove naturally is cooled to room temperature, can obtain ruddy glaze.
The granitic chemical ingredients of the long class of table 3 flesh pink potassium
| Composition | SiO 2 | TiO 2 | Al 2O 3 | Fe 2O 3 | FeO | MnO | MgO | CaO | Na 2O | K 2O | P 2O 5 |
| Content/% | 72.18 | 0.34 | 13.31 | 0.85 | 2.43 | 0.05 | 0.33 | 1.18 | 3.33 | 1.80 | 0.01 |
Embodiment 3:
Single canescence dioritoid granite waste material (chemical ingredients such as table 4) is carried out fragmentation with crusher, canescence dioritoid granite waste material with fragmentation carries out wet ball grinding then, canescence dioritoid granite waste material behind the ball milling is crossed 200 mesh standard sieves and is sieved and remove impurity, be made into glaze slip then, the concentration of glaze slip is 1.65g/ml, is applied to ceramic body surface (chemical ingredients such as the table 2 of base substrate) in the brushing glazing mode.With sample in bellows in 80 ℃ of oven dry, in stove, slowly be heated to 1250 ℃ then, be incubated 1 hour after, being allowed to condition at lowers the temperature in the stove naturally is cooled to room temperature, can obtain transparent glaze.
The granitic chemical ingredients of table 4 canescence dioritoid
| Composition | SiO 2 | TiO 2 | Al 2O 3 | Fe 2O 3 | FeO | MnO | MgO | CaO | Na 2O | K 2O | P 2O 5 |
| Content/% | 69.09 | 0.54 | 15.73 | 1.38 | 2.73 | 0.08 | 1.74 | 3.83 | 3.75 | 2.73 | 0.18 |
Embodiment 4:
With the long class granite of black gabbride granite, flesh pink potassium, canescence dioritoid granite waste material mixed by 1: 1: 1, carry out fragmentation with crusher, mixing granite waste material with fragmentation carries out wet ball grinding then, mixing granite waste material behind the ball milling is crossed 200 mesh standard sieves and is sieved and remove impurity, be made into glaze slip then, the concentration of glaze slip is 1.65g/ml, the ceramic glaze of making (chemical ingredients such as table 5) is applied to ceramic body surface (chemical ingredients such as the table 2 of base substrate) in the brushing glazing mode.With sample in bellows in 80 ℃ of oven dry, in stove, slowly be heated to 1300 ℃ then, be incubated 1 hour after, being allowed to condition at lowers the temperature in the stove naturally is cooled to room temperature, can obtain lurid glaze.
The chemical ingredients of table 5 ceramic glaze
| Composition | SiO 2 | TiO 2 | Al 2O 3 | Fe 2O 3 | FeO | MnO | MgO | CaO | Na 2O | K 2O | P 2O 5 |
| Content/% | 67.72 | 0.51 | 14.97 | 1.34 | 2.94 | 0.07 | 1.78 | 3.50 | 3.54 | 3.67 | 0.15 |
Embodiment 5:
Single black gabbride granite waste material (chemical ingredients such as table 1) is carried out fragmentation with crusher, black gabbride granite waste material with fragmentation carries out wet ball grinding then, black gabbride granite waste material behind the ball milling is crossed 200 mesh standard sieves and is sieved and remove impurity, be made into glaze slip then, the concentration of glaze slip is 1.65g/ml, with the brushing glazing mode be applied to through 1000 ℃ of unglazed terra-cotta billet surface (these terra-cotta be by red mud and clay by 3: 7 mixed and make chemical ingredients such as table 6).With sample in bellows in 80 ℃ of oven dry, in stove, slowly be heated to 1200 ℃ then, be incubated 1 hour after, being allowed to condition at lowers the temperature in the stove naturally is cooled to room temperature, can obtain wine-colored glaze.
The chemical ingredients of table 6 terra-cotta base substrate
| Composition | SiO 2 | TiO 2 | Al 2O 3 | Fe 2O 3 | MgO | CaO | Na 2O | K 2O |
| Content/% | 52.17 | 2.27 | 20.25 | 2.72 | 0.58 | 12.42 | 1.06 | 2.82 |
Claims (1)
1. method of utilizing the granite waste material to prepare ceramic glaze, it is characterized in that concrete steps are: the granite waste material is carried out fragmentation with crusher earlier, granite waste material with fragmentation carries out wet ball grinding then, granite waste material behind the ball milling is crossed 200 mesh standard sieves and is sieved and remove impurity, be made into glaze slip then, concentration of glaze slip is controlled at 1.5～1.9g/ml; Glaze slip is granted billet surface, in bellows in 70 ℃～110 ℃ heat dryings or dry the back to its moisture less than 1%, at last it is burnt till between 1200 ℃～1350 ℃, be incubated after 0.5～3 hour, naturally cool to room temperature with stove, can make glaze.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007101484276A CN101125766A (en) | 2007-08-27 | 2007-08-27 | Method for preparing ceramic glaze material by using granite waste material |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007101484276A CN101125766A (en) | 2007-08-27 | 2007-08-27 | Method for preparing ceramic glaze material by using granite waste material |
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| Publication Number | Publication Date |
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| CN101125766A true CN101125766A (en) | 2008-02-20 |
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| CNA2007101484276A Pending CN101125766A (en) | 2007-08-27 | 2007-08-27 | Method for preparing ceramic glaze material by using granite waste material |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102344280A (en) * | 2011-06-10 | 2012-02-08 | 广东省枫溪陶瓷工业研究所 | Method for producing ceramic article from granite waste |
| CN103332925A (en) * | 2013-06-14 | 2013-10-02 | 何晓洪 | Silicate raw material regenerated by utilizing waste slag powder of granite sedimentation tank, as well as production method and application thereof |
| CN103539486A (en) * | 2013-10-08 | 2014-01-29 | 大埔县高陂恒辉陶瓷工艺厂 | Ceramic flower leopard print glaze composite mineralizing agent and preparation method thereof |
| CN104058792A (en) * | 2014-07-08 | 2014-09-24 | 高太昇 | Volcanic vein rock transmutation glaze |
| CN104941774A (en) * | 2015-07-13 | 2015-09-30 | 黄顺昌 | Method for recovering and processing waste granite into ceramic tile raw material |
| CN106810071A (en) * | 2016-11-28 | 2017-06-09 | 佛山市尚好门窗有限责任公司 | A kind of glaze and preparation method thereof |
| CN106977102A (en) * | 2017-03-30 | 2017-07-25 | 南昌航空大学 | A kind of preparation method of modified granite waste stone dust crystalline glaze |
| CN106995315A (en) * | 2017-05-18 | 2017-08-01 | 东北大学 | A kind of preparation method of butter yellow bright glaze |
| CN110357430A (en) * | 2019-08-19 | 2019-10-22 | 东北大学 | Folded brilliant glaze of a kind of potassium feldspar-diopside and preparation method thereof and application method |
| CN113666638A (en) * | 2021-08-13 | 2021-11-19 | 龙泉南宋青瓷文化研究所 | Formula of porcelain glaze imitating Nansong official kiln and preparation method thereof |
-
2007
- 2007-08-27 CN CNA2007101484276A patent/CN101125766A/en active Pending
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102344280A (en) * | 2011-06-10 | 2012-02-08 | 广东省枫溪陶瓷工业研究所 | Method for producing ceramic article from granite waste |
| CN102344280B (en) * | 2011-06-10 | 2013-07-10 | 韩山师范学院 | Method for producing ceramic article from granite waste |
| CN103332925A (en) * | 2013-06-14 | 2013-10-02 | 何晓洪 | Silicate raw material regenerated by utilizing waste slag powder of granite sedimentation tank, as well as production method and application thereof |
| CN103332925B (en) * | 2013-06-14 | 2015-05-20 | 何晓洪 | Silicate raw material regenerated by utilizing waste slag powder of granite sedimentation tank, as well as production method and application thereof |
| CN103539486A (en) * | 2013-10-08 | 2014-01-29 | 大埔县高陂恒辉陶瓷工艺厂 | Ceramic flower leopard print glaze composite mineralizing agent and preparation method thereof |
| CN104058792A (en) * | 2014-07-08 | 2014-09-24 | 高太昇 | Volcanic vein rock transmutation glaze |
| CN104941774A (en) * | 2015-07-13 | 2015-09-30 | 黄顺昌 | Method for recovering and processing waste granite into ceramic tile raw material |
| CN106810071A (en) * | 2016-11-28 | 2017-06-09 | 佛山市尚好门窗有限责任公司 | A kind of glaze and preparation method thereof |
| CN106977102A (en) * | 2017-03-30 | 2017-07-25 | 南昌航空大学 | A kind of preparation method of modified granite waste stone dust crystalline glaze |
| CN106995315A (en) * | 2017-05-18 | 2017-08-01 | 东北大学 | A kind of preparation method of butter yellow bright glaze |
| CN110357430A (en) * | 2019-08-19 | 2019-10-22 | 东北大学 | Folded brilliant glaze of a kind of potassium feldspar-diopside and preparation method thereof and application method |
| CN113666638A (en) * | 2021-08-13 | 2021-11-19 | 龙泉南宋青瓷文化研究所 | Formula of porcelain glaze imitating Nansong official kiln and preparation method thereof |
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