CN106810071A - A kind of glaze and preparation method thereof - Google Patents
A kind of glaze and preparation method thereof Download PDFInfo
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- CN106810071A CN106810071A CN201611058892.6A CN201611058892A CN106810071A CN 106810071 A CN106810071 A CN 106810071A CN 201611058892 A CN201611058892 A CN 201611058892A CN 106810071 A CN106810071 A CN 106810071A
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- China
- Prior art keywords
- glaze
- parts
- granite
- raw material
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Aftertreatments Of Artificial And Natural Stones (AREA)
Abstract
The present invention provides a kind of glaze and preparation method thereof, and the method mainly has granite, calcium silicates, potassium feldspar, ferric phosphate using raw material.The granite that the present invention is used is mainly leftover pieces discarded during exploitation, is utilized granite waste material by the present invention, is fabricated to marzacotto.Use simultaneously, with the particle diameter of particle size analyzer glaze, glossiness, microhardness to glaze, heat impact strength are tested, can show that the glaze of present invention preparation meets industry use requirement.
Description
Technical field
The present invention relates to a kind of field of inorganic nonmetallic material, and in particular to a kind of glaze and preparation method thereof.
Technical background
Granite is a kind of distribution most one of most abundant rock of wide, resource.With the development of modern architecture industry, to granite
Demand is also increased sharply, and traditional mode of production is generally used in China's rock material resource exploitation, and production technique falls behind, equipment
It is simple and crude to cause that producing capacity is low, lumber recovery is low (lumber recovery of the waste material exploitation having only has 10% ~ 20%), not only pollute ring
Border, and cause the serious waste of resource.
It by various natural materials (quartz, feldspar, lime stone etc.) is primary raw material that glaze used both at home and abroad is all at present
Process.Because the mineral resources of present glaze is increasingly reduced, price is increasingly improved, and increased the cost of production.The present invention is utilized
It is primary raw material with granite building material waste material, is subject to calcium silicates, potassium feldspar, ferric phosphate and prepares glaze, economizes on resources, and reduce life
Cost is produced, meets the sustainable development of today's society promotion.
The content of the invention
The purpose of the present invention is directed to above-mentioned problem, there is provided a kind of glaze and preparation method thereof, uses moyite waste material
For primary raw material prepares glaze, economize on resources, and reduce production cost.
To achieve the above object, the technical scheme taken：
A kind of glaze, it is characterised in that the raw material comprising following weight portion：
Granite：70 ~ 80 parts；Calcium silicates：20 ~ 30 parts；Potassium feldspar：10 ~ 20 parts；Ferric phosphate：3 ~ 5 parts.
Preferably, a kind of described glaze, it is characterised in that the raw material comprising following weight portion：
Granite：75 ~ 80 parts；Calcium silicates：20 ~ 25 parts；Potassium feldspar：10 ~ 15 parts；Ferric phosphate：3 ~ 4 parts.
Preferably, a kind of described low temperature, it is characterised in that the raw material comprising following weight portion：
Granite：80 parts；Calcium silicates：20 parts；Potassium feldspar：10 parts；Ferric phosphate：3 parts.
Preferably, described a kind of glaze, it is characterised in that described granite is the exploitation waste material of moyite.
Preferably, described a kind of glaze, it is characterised in that in described moyite main mine material for quartz,
Potassium feldspar, albite.
Preferably, described a kind of glaze, it is characterised in that including following preparation process:
(1) granite is cleaned and is less than 1mm with crusher in crushing to particle diameter；
(2) raw material is weighed by weight, wet ball grinding 20h is carried out, and is expected：Ball：Water=1：2：1；
(3) ball milling disposed slurry crosses 120 mesh sieves, except iron, obtains glaze slurry；
(4) after base substrate being immersed into glaze slurry, drying, sintering.
Beneficial effect
The beneficial effects of the present invention are：The granite for using is mainly leftover pieces discarded during exploitation, will flower by the present invention
Hilllock rock waste material is utilized, and is fabricated to marzacotto.Use simultaneously, with the particle diameter of particle size analyzer glaze, to the light of glaze
Damp degree, microhardness are tested, and can show that the glaze of present invention preparation meets industry use requirement.
Specific embodiment
In order to the object, technical solutions and advantages of the present invention are better described, the present invention is done below in conjunction with specific embodiment
Further illustrate.
Embodiment 1
A kind of glaze, it is characterised in that the raw material comprising following weight portion：
Granite：80 parts；Calcium silicates：20 parts；Potassium feldspar：10 parts；Ferric phosphate：3 parts.
Described a kind of glaze, it is characterised in that including following preparation process:
(1) granite is cleaned and is less than 1mm with crusher in crushing to particle diameter；
(2) raw material is weighed by weight, wet ball grinding 20h is carried out, and is expected：Ball：Water=1：2：1；
(3) ball milling disposed slurry crosses 120 mesh sieves, except iron, obtains glaze slurry；
(4) after base substrate being immersed into glaze slurry, drying, sintering.
Embodiment 2
A kind of glaze, it is characterised in that the raw material comprising following weight portion：
Granite：75 parts；Calcium silicates：15 parts；Potassium feldspar：15 parts；Ferric phosphate：4 parts.
Described a kind of glaze, it is characterised in that including following preparation process:
(1) granite is cleaned and is less than 1mm with crusher in crushing to particle diameter；
(2) raw material is weighed by weight, wet ball grinding 20h is carried out, and is expected：Ball：Water=1：2：1；
(3) ball milling disposed slurry crosses 120 mesh sieves, except iron, obtains glaze slurry；
(4) after base substrate being immersed into glaze slurry, drying, sintering.
Embodiment 3
A kind of glaze, it is characterised in that the raw material comprising following weight portion：
Granite：70 parts；Calcium silicates：15 parts；Potassium feldspar：10 parts；Ferric phosphate：3 parts.
Described a kind of glaze, it is characterised in that including following preparation process:
(1) granite is cleaned and is less than 1mm with crusher in crushing to particle diameter；
(2) raw material is weighed by weight, wet ball grinding 20h is carried out, and is expected：Ball：Water=1：2：1；
(3) ball milling disposed slurry crosses 120 mesh sieves, except iron, obtains glaze slurry；
(4) after base substrate being immersed into glaze slurry, drying, sintering.
Comparative example
The present embodiment is daily using market purchase, and its glaze paint is analyzed, and the glaze provided with the present invention is contrasted.
Embodiment 4
The present embodiment is characterized to the glaze prepared by embodiment 1 ~ 3 and comparative example.
Wherein, particle diameter is measured using Particle Size Analyzer, is characterized using D50；
Finish is tested glaze paint glossiness using the Photoelectric Brightness Meters of WYG 1；
Microhardness is tested the microhardness of glaze paint using EM3000A type Vickers hardness microscopes；
Heat impact strength is tested using standard GB/T/T2581-1993.
By table as can be seen that glaze provided by the present invention, glaze particle diameter composition between D50=10.34 ~ 11.11, burn
Into temperature at 1300 DEG C, the glaze to base substrate strong adaptability, stable performance can be obtained；Its flat appearance is smooth, and glossiness exists
89% ~ 90%, microhardness (HV) is in 598.2 ~ 622.1MPa；Heat impact strength test meet standard GB/T/
T2581-1993 test meets.
Finally it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than the present invention is protected
The limitation of scope, although being elaborated to the present invention with reference to preferred embodiment, one of ordinary skill in the art should manage
Solution, can modify or equivalent, without deviating from the essence and model of technical solution of the present invention to technical scheme
Enclose.
Claims (6)
1. a kind of glaze, it is characterised in that the raw material comprising following weight portion：
Granite：70 ~ 80 parts；Calcium silicates：20 ~ 30 parts；Potassium feldspar：10 ~ 20 parts；Ferric phosphate：3 ~ 5 parts.
2. a kind of glaze according to claim 1, it is characterised in that the raw material comprising following weight portion：
Granite：75 ~ 80 parts；Calcium silicates：20 ~ 25 parts；Potassium feldspar：10 ~ 15 parts；Ferric phosphate：3 ~ 4 parts.
3. a kind of glaze according to claim 1, it is characterised in that the raw material comprising following weight portion：
Granite：80 parts；Calcium silicates：20 parts；Potassium feldspar：10 parts；Ferric phosphate：3 parts.
4. a kind of glaze according to claim 1, it is characterised in that described granite gives up for the exploitation of moyite
Material.
5. a kind of glaze according to claim 4, it is characterised in that main mine material is stone in described moyite
English, potassium feldspar, albite.
6. a kind of preparation method of glaze, it is characterised in that comprise the following steps：
(1) granite is cleaned and is less than 1mm with crusher in crushing to particle diameter；
(2) raw material is weighed by weight, wet ball grinding 20h is carried out, and is expected：Ball：Water=1：2：1；
(3) ball milling disposed slurry crosses 120 mesh sieves, except iron, obtains glaze slurry；
(4) after base substrate being immersed into glaze slurry, drying, sintering.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611058892.6A CN106810071A (en) | 2016-11-28 | 2016-11-28 | A kind of glaze and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611058892.6A CN106810071A (en) | 2016-11-28 | 2016-11-28 | A kind of glaze and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106810071A true CN106810071A (en) | 2017-06-09 |
Family
ID=59106204
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611058892.6A Withdrawn CN106810071A (en) | 2016-11-28 | 2016-11-28 | A kind of glaze and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN106810071A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109502979A (en) * | 2019-01-10 | 2019-03-22 | 长沙铜官窑广华鑫陶艺有限公司 | A kind of ceramic glaze and the method using the glaze |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5795884A (en) * | 1980-12-08 | 1982-06-14 | Satoshi Suzumura | Granite baking method |
| CN101125766A (en) * | 2007-08-27 | 2008-02-20 | 桂林工学院 | Method for preparing ceramic glaze material by using granite waste material |
| CN103396166A (en) * | 2013-08-05 | 2013-11-20 | 桂林理工大学 | Method for preparing zinc metasilicate crystal glaze by taking granite as parent glaze raw material |
-
2016
- 2016-11-28 CN CN201611058892.6A patent/CN106810071A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5795884A (en) * | 1980-12-08 | 1982-06-14 | Satoshi Suzumura | Granite baking method |
| CN101125766A (en) * | 2007-08-27 | 2008-02-20 | 桂林工学院 | Method for preparing ceramic glaze material by using granite waste material |
| CN103396166A (en) * | 2013-08-05 | 2013-11-20 | 桂林理工大学 | Method for preparing zinc metasilicate crystal glaze by taking granite as parent glaze raw material |
Non-Patent Citations (3)
| Title |
|---|
| 蒋述兴等: "利用钾长花岗岩石材废料制备陶瓷釉料", 《桂林工学院学报》 * |
| 蔡飞虎等: "《陶瓷墙地砖生产技术》", 31 July 2011, 武汉理工大学出版社 * |
| 裴秀娟等: "《陶瓷墙地砖工厂技术员手册》", 30 June 2004, 化学工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109502979A (en) * | 2019-01-10 | 2019-03-22 | 长沙铜官窑广华鑫陶艺有限公司 | A kind of ceramic glaze and the method using the glaze |
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Application publication date: 20170609 |