CN101092249B - 一种采用红外烧结炉制备三氧化钼纳米结构及其薄膜的方法 - Google Patents
一种采用红外烧结炉制备三氧化钼纳米结构及其薄膜的方法 Download PDFInfo
- Publication number
- CN101092249B CN101092249B CN2007100277368A CN200710027736A CN101092249B CN 101092249 B CN101092249 B CN 101092249B CN 2007100277368 A CN2007100277368 A CN 2007100277368A CN 200710027736 A CN200710027736 A CN 200710027736A CN 101092249 B CN101092249 B CN 101092249B
- Authority
- CN
- China
- Prior art keywords
- molybdenum trioxide
- molybdenum
- substrate
- trioxide nano
- sintering furnace
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- JKQOBWVOAYFWKG-UHFFFAOYSA-N molybdenum trioxide Chemical compound O=[Mo](=O)=O JKQOBWVOAYFWKG-UHFFFAOYSA-N 0.000 title claims abstract description 106
- 239000002086 nanomaterial Substances 0.000 title claims abstract description 22
- 238000000034 method Methods 0.000 title claims abstract description 21
- 238000005245 sintering Methods 0.000 title claims abstract description 20
- 239000010409 thin film Substances 0.000 title abstract 4
- 239000000758 substrate Substances 0.000 claims abstract description 54
- 238000001704 evaporation Methods 0.000 claims abstract description 18
- 230000008020 evaporation Effects 0.000 claims abstract description 17
- 239000011521 glass Substances 0.000 claims description 43
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 21
- 239000002120 nanofilm Substances 0.000 claims description 15
- 229910052750 molybdenum Inorganic materials 0.000 claims description 12
- 239000011733 molybdenum Substances 0.000 claims description 12
- 239000002135 nanosheet Substances 0.000 claims description 11
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 4
- 238000004506 ultrasonic cleaning Methods 0.000 claims description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 3
- 229910052710 silicon Inorganic materials 0.000 claims description 3
- 239000010703 silicon Substances 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 abstract description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract description 2
- 229910052760 oxygen Inorganic materials 0.000 abstract description 2
- 239000001301 oxygen Substances 0.000 abstract description 2
- 238000000151 deposition Methods 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 description 12
- 239000000463 material Substances 0.000 description 11
- 238000002173 high-resolution transmission electron microscopy Methods 0.000 description 10
- 239000002073 nanorod Substances 0.000 description 10
- 238000001237 Raman spectrum Methods 0.000 description 7
- 238000002441 X-ray diffraction Methods 0.000 description 7
- 239000010453 quartz Substances 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- 238000001228 spectrum Methods 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 5
- 238000001069 Raman spectroscopy Methods 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 230000005540 biological transmission Effects 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 238000002003 electron diffraction Methods 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 239000002127 nanobelt Substances 0.000 description 3
- 238000004098 selected area electron diffraction Methods 0.000 description 3
- 239000012528 membrane Substances 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 230000000007 visual effect Effects 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910016001 MoSe Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000000862 absorption spectrum Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000005518 electrochemistry Effects 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000005078 molybdenum compound Substances 0.000 description 1
- 150000002752 molybdenum compounds Chemical class 0.000 description 1
- 229910000476 molybdenum oxide Inorganic materials 0.000 description 1
- 239000002070 nanowire Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- PQQKPALAQIIWST-UHFFFAOYSA-N oxomolybdenum Chemical compound [Mo]=O PQQKPALAQIIWST-UHFFFAOYSA-N 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
Images
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
- Physical Vapour Deposition (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2007100277368A CN101092249B (zh) | 2007-04-27 | 2007-04-27 | 一种采用红外烧结炉制备三氧化钼纳米结构及其薄膜的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2007100277368A CN101092249B (zh) | 2007-04-27 | 2007-04-27 | 一种采用红外烧结炉制备三氧化钼纳米结构及其薄膜的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101092249A CN101092249A (zh) | 2007-12-26 |
CN101092249B true CN101092249B (zh) | 2010-12-08 |
Family
ID=38990719
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2007100277368A Active CN101092249B (zh) | 2007-04-27 | 2007-04-27 | 一种采用红外烧结炉制备三氧化钼纳米结构及其薄膜的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN101092249B (zh) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102153142B (zh) * | 2011-04-25 | 2012-11-07 | 郑州大学 | 一种三氧化钼纳米片及其制备方法 |
CN102351249B (zh) * | 2011-07-21 | 2013-08-28 | 华南理工大学 | 一种纳米结构三氧化钼的制备方法 |
CN102603005B (zh) * | 2012-03-07 | 2013-12-04 | 洛阳开拓者投资管理有限公司 | 一种制备纳米三氧化钼的方法 |
CN103288138B (zh) * | 2013-05-15 | 2014-11-26 | 中国地质大学(武汉) | 一种刺球状光致变色MoO3薄膜的制备方法 |
CN104003446B (zh) * | 2014-05-29 | 2015-06-17 | 中国计量科学研究院 | 一种高纯三氧化钼的制备方法 |
CN104909407B (zh) * | 2015-06-08 | 2016-09-14 | 湖北大学 | 一种氧化钼纳米纤维纸及其制备方法 |
CN106517332B (zh) * | 2016-10-26 | 2018-06-29 | 湖北大学 | 含有Pd量子点修饰的氧化钼纳米纤维纸制备方法 |
US10669498B1 (en) | 2017-06-12 | 2020-06-02 | U.S.A. as Represented by the Administrator of the National Aeronautics and S pace Administration | MOS2- or WS2-filled hollow ZnS hexagonal nanotubes as core-shell structured solid lubricants and lubricant modifiers for space mechanisms |
CN108996549B (zh) * | 2018-10-10 | 2021-06-15 | 金堆城钼业光明(山东)股份有限公司 | 一种MoO3片组装的网络结构纳米材料及其制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5223234A (en) * | 1988-12-22 | 1993-06-29 | Kloeckner-Humboldt-Deutz Ag | Method for producing molybdenum trioxide (MOO3) from raw materials that contain MOS2 |
JP2004203720A (ja) * | 2002-12-26 | 2004-07-22 | National Institute For Materials Science | 三酸化モリブデンナノベルトとその製造方法 |
KR100700348B1 (ko) * | 2005-09-30 | 2007-03-29 | (주)권풍 | 탈황 폐촉매로부터 산화몰리브덴을 회수하는 방법 및 그장치 |
-
2007
- 2007-04-27 CN CN2007100277368A patent/CN101092249B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5223234A (en) * | 1988-12-22 | 1993-06-29 | Kloeckner-Humboldt-Deutz Ag | Method for producing molybdenum trioxide (MOO3) from raw materials that contain MOS2 |
JP2004203720A (ja) * | 2002-12-26 | 2004-07-22 | National Institute For Materials Science | 三酸化モリブデンナノベルトとその製造方法 |
KR100700348B1 (ko) * | 2005-09-30 | 2007-03-29 | (주)권풍 | 탈황 폐촉매로부터 산화몰리브덴을 회수하는 방법 및 그장치 |
Also Published As
Publication number | Publication date |
---|---|
CN101092249A (zh) | 2007-12-26 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101092249B (zh) | 一种采用红外烧结炉制备三氧化钼纳米结构及其薄膜的方法 | |
Bai et al. | Synthesis of ZnO nanorods and its application in NO2 sensors | |
Chen et al. | Zinc gallium oxide—a review from synthesis to applications | |
Hung et al. | Low-temperature solution approach toward highly aligned ZnO nanotip arrays | |
Wu et al. | Tetragonal tungsten oxide nanobelts synthesized by chemical vapor deposition | |
Chalapathi et al. | Investigations on Cu3SnS4 thin films prepared by spray pyrolysis | |
Zeng et al. | Fabrication of Mg-doped ZnO nanofibers with high purities and tailored band gaps | |
Filippo et al. | Single crystalline β-Ga2O3 nanowires synthesized by thermal oxidation of GaSe layer | |
Li et al. | Controllable low-temperature chemical vapor deposition growth and morphology dependent field emission Property of SnO2 nanocone arrays with different morphologies | |
Gutierrez et al. | Interfacial phase modulation-induced structural distortion, band gap reduction, and nonlinear optical activity in tin-incorporated Ga2O3 | |
Babu et al. | Synthesis and electrochromic properties of nanocrystalline WO3 thin films | |
CN102351249B (zh) | 一种纳米结构三氧化钼的制备方法 | |
Kulkarni et al. | Synthesis and characterization of uniform spherical shape nanoparticles of indium oxide | |
Petrović et al. | Hydrothermal processing of electrospun fibers in the synthesis of 1D ZnO nanoparticles | |
Tharsika et al. | Catalyst free single-step fabrication of SnO2/ZnO core–shell nanostructures | |
WO2005062785A2 (en) | Solution-phase synthesis of metal oxide nanostructures | |
López-Mena et al. | ZnO thin films prepared at low annealing temperatures, from a novel, simple sol–gel precursor solution | |
Kuo et al. | Synthesis of nanocrystalline lithium niobate powders via a fast chemical route | |
Diallo et al. | Effect of substrate temperature on the structure and the metal insulator transition in pulsed laser deposed V0 2\films on soda lime glass | |
Gouma et al. | Novel synthesis of hexagonal WO 3 nanostructures | |
Su et al. | Self-catalytic formation and characterization of Zn2SnO4 nanowires | |
Xie et al. | Controllable synthesis of SnO2 nanowires and nanobelts by Ga catalysts | |
Duraia et al. | Synthesis, characterization and photoluminescence of tin oxide nanoribbons and nanowires | |
CN109336180B (zh) | 一种超长氧化钼纳米带生长方法 | |
Vila et al. | Thermal growth, structural and optical characterization of hierarchical Bi2O3-MoO3 nanostructures |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C53 | Correction of patent for invention or patent application | ||
CB03 | Change of inventor or designer information |
Inventor after: Xu Ningsheng Inventor after: Ban Dongmei Inventor after: Deng Shaozhi Inventor after: Chen Jun Inventor after: She Juncong Inventor before: Xu Ningsheng Inventor before: Ban Dongmei Inventor before: Deng Shaozhi Inventor before: Chen Jun Inventor before: Yu Juncong |
|
COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: XU NINGSHENG BAN DONGMEI DENG SHAOZHI CHEN JUN YU JUNCONG TO: XU NINGSHENGBAN DONGMEI DENG SHAOZHI CHEN JUN SHE JUNCONG |