CN101073674B - Production of deodorant - Google Patents
Production of deodorant Download PDFInfo
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- CN101073674B CN101073674B CN2007100696499A CN200710069649A CN101073674B CN 101073674 B CN101073674 B CN 101073674B CN 2007100696499 A CN2007100696499 A CN 2007100696499A CN 200710069649 A CN200710069649 A CN 200710069649A CN 101073674 B CN101073674 B CN 101073674B
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Abstract
The invention is concerned with a peoduce method for deodorizer. Take Chinese traditional medicine with certain weight ratio, cut, crush, dip with organic solution, distill and refine to ferment in closed condition as semi finished articles to get Chinese traditional medicine finished product. Dispose chitosan with deacetylation, when the deacetylating of chitosan is over 70 percent, react methylation process to get the chitosan production with 0.1 to 10 percent of concentration. Add water, Chinese traditional medicine finished product and chitosan production into enameled reactor or stainless steel reactor with stirring plasm, add 0.1 to 5 shares of metal salt, stir for 1 to 3 hours to get the deodorizer. It has reasonable component, nice effect to deodorization and safe for environment.
Description
Technical field
The present invention relates to a kind of preparation method of deodorizer, this deodorizer is particularly suitable for using in trade effluent, sanitary sewage disposal, also can satisfy the needs of the deodorization use occasion in routine work, the life simultaneously.
Background technology
Along with the progress of society, the scale of industry and sanitary sewage disposal enlarges rapidly, and how is the stink that the waste water of sewage treatment plant and mud send handled? this exercise question places on the agenda.Simultaneously, house refuse is stacked ground, lavatory, animal farm, the place of butchering the serious abnormal smells from the patient pollution of generations such as booty of factory, hospital also needs high-efficiency deodorant.And existing deodorizer mostly uses chemical agent, itself environment is had pollution, and odor removal efficient is not high yet.
Summary of the invention
It is reasonable that technical problem to be solved by this invention provides a kind of prescription, the preparation method of the deodorizer of good deodorization effect, safety and environmental protection.
The present invention solves the problems of the technologies described above the preparation method that the technical scheme that is adopted is this deodorizer, and processing step is:
A, with the raw material of Chinese crude drug in proportion weight feed intake, shear, pulverize, carry out processed with operations such as organic solvent soak, extracts, makes with extra care, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content obtains the Chinese crude drug finished product between 1-20%, with the peak that goes out of high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content;
B, the chitosan raw material is carried out deacetylated processing, the deacetylation that makes chitosan is greater than 70%, and the reprocessing that methylates, be mixed with the aqueous solution of 0.1%-10% concentration then, obtain the chitosan finished product, packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material;
C, in the enamel or rust steel reactor of band stirring arm, the pure water that adds the 30-90 weight portion, add 5-30 weight portion Chinese crude drug finished product and 0.1-10 weight portion chitosan finished product then, add slaine again, slaine is that ferrous sulfate, copper sulfate, zinc sulfate, manganese sulfate, manganese chloride, Borax, potassium permanganate etc. are intermediary a kind of, several or whole, the parts by weight of slaine are 0.1～5, and stirring and processing is one to three hour in reactor, obtains deodorant products.
The raw material of Chinese crude drug of the present invention is the leaf of Radix Scutellariae, Cortex Phellodendri, Rhizoma Coptidis, Rhizoma Acori Graminei, Rhizoma Atractylodis, Chinese mugwort and stem, Folium Isatidis, Radix Arnebiae (Radix Lithospermi), Radix Gentianae, wherein, the parts by weight of leaf of Chinese mugwort and stem, Folium Isatidis, Radix Arnebiae (Radix Lithospermi), Radix Gentianae are 0.5-6, the parts by weight of Rhizoma Acori Graminei, Rhizoma Atractylodis, Radix Scutellariae are 0.5-4, if i.e.: Rhizoma Coptidis portion, the usage ratio of leaf of Chinese mugwort and stem, Folium Isatidis, Radix Arnebiae (Radix Lithospermi), Radix Gentianae can be brought up to 2 to 6 parts, and the usage ratio of leaf of Chinese mugwort and stem, Folium Isatidis, Radix Arnebiae (Radix Lithospermi), Radix Gentianae can be brought up to 2 to 4 parts.If i.e.: Rhizoma Coptidis portion, the usage ratio of leaf of Chinese mugwort and stem, Folium Isatidis, Radix Arnebiae (Radix Lithospermi), Radix Gentianae can be brought up to 6 parts, and the usage ratio of leaf of Chinese mugwort and stem, Folium Isatidis, Radix Arnebiae (Radix Lithospermi), Radix Gentianae can be brought up to 4 parts.
Organic solvent of the present invention is methanol, ethanol, acetone and petroleum ether.
The present invention compares with prior art and has the following advantages and effect: Chinese herbal medicine of the present invention, contain abundant plant glycoside, glycoside unit, biological alkali, polysaccharose substance in the extract of these Chinese medicines, has stronger, broad-spectrum kill bacteria ability, and can keep the long time, the derivant of chitosan also has sterilizing ability.The another kind of material that the present invention adopts is the inorganic chemistry article of using always, for example: ferrous sulfate, copper sulfate, zinc sulfate, magnesium sulfate, Borax, potassium permanganate etc., these materials are common chemical materials in the sewage disposal, they have stronger, broad-spectrum and smelly material to carry out the ability of chemical reaction, produce deodorizing effect.It is raw material that the present invention adopts the Chinese crude drug of mass efficient, utilizes the sterilizing ability of Chinese medicine to realize deodorizing effect.It is a kind of production method of the deodorizer that is different from international popular of uniqueness.The present invention has adopted the hybrid technology of the method that biological extraction technology and chemical substance mixed technology combine; Technology of the present invention had both considered because the putrid abnormal smells from the patient of article that the effect of antibacterial produces, and consider that also the deodorization of the stink that chemical pollutant that sewage, mud and dirt carry sends is used, so the deodorant effect is more remarkable.
Description of drawings
Fig. 1 is a process chart of the present invention.
The specific embodiment
The present invention is described in further detail below in conjunction with embodiment, and following examples are explanation of the invention and the present invention is not limited to following examples.
Embodiment 1:
Get leaf and the stem of 1.5 kilograms of Chinese mugworts, 2.5 kilogram Folium Isatidis, 4.8 kilogram Radix Arnebiae (Radix Lithospermi), 6 kilograms of Radix Gentianaes, 2.2 kilogram Rhizoma Acori Graminei, 3.6 kilogram Rhizoma Atractylodis, 2.4 kilogram Radix Scutellariae, 0.5 kilogram Cortex Phellodendri, 4 kilograms of Rhizoma Coptidis, shear, pulverize, soak with methanol, extract, operation such as refining, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content is between 1-20%, obtain the Chinese crude drug finished product, the peak that goes out with the high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content.
Chitosan is carried out deacetylated processing; the deacetylation that makes chitosan is greater than 70%; and the reprocessing that methylates; be mixed with the aqueous solution of 0.1%-10% concentration then; obtain the chitosan finished product; packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material.
In the enamel or rust steel reactor of band stirring arm, the pure water that adds 30 kilograms, add 5 kilograms of Chinese crude drug finished products and 0.2 kilogram of chitosan finished product then, the slaine that adds 4 kilograms again, slaine is the mixture of ferrous sulfate, copper sulfate, zinc sulfate, the part by weight of each component is 1: 1: 1, and stirring and processing is one to three hour in reactor, obtains deodorant products.Inject pail pack then.
Embodiment 2:
Get leaf and the stem of 0.8 kilogram of Chinese mugwort, 5.4 kilogram Folium Isatidis, 3.8 kilogram Radix Arnebiae (Radix Lithospermi), 3.2 kilogram Radix Gentianae, 0.5 kilogram Rhizoma Acori Graminei, 3 kilograms of Rhizoma Atractylodis, 2 kilograms of Radix Scutellariaes, 3 kilograms of Cortex Phellodendris, 2.5 kilogram Rhizoma Coptidis, shear, pulverize, use soak with ethanol, extract, operation such as refining, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content is between 1-20%, obtain the Chinese crude drug finished product, the peak that goes out with the high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content.
Chitosan is carried out deacetylated processing; the deacetylation that makes chitosan is greater than 70%; and the reprocessing that methylates; be mixed with the aqueous solution of 0.1%-10% concentration then; obtain the chitosan finished product; packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material.
In the enamel or rust steel reactor of band stirring arm, the pure water that adds 40 kilograms, add 10 kilograms of Chinese crude drug finished products and 4 kilograms of chitosan finished products then, the slaine that adds 4.8 kilograms again, slaine is the mixture of manganese sulfate, manganese chloride, Borax, the part by weight of each component is 1: 1: 1, and stirring and processing is one to three hour in reactor, obtains deodorant products.Inject pail pack then.
Embodiment 3:
Get leaf and the stem of 6 kilograms of Chinese mugworts, 0.8 kilogram Folium Isatidis, 3.2 kilogram Radix Arnebiae (Radix Lithospermi), 4 kilograms of Radix Gentianaes, 1.5 kilogram Rhizoma Acori Graminei, 2.8 kilogram Rhizoma Atractylodis, 4 kilograms of Radix Scutellariaes, 3.2 kilogram Cortex Phellodendri, 3.4 kilogram Rhizoma Coptidis, shear, pulverize, soak with acetone, extract, operation such as refining, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content is between 1-20%, obtain the Chinese crude drug finished product, the peak that goes out with the high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content.
Chitosan is carried out deacetylated processing; the deacetylation that makes chitosan is greater than 70%; and the reprocessing that methylates; be mixed with the aqueous solution of 0.1%-10% concentration then; obtain the chitosan finished product; packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material.
In the enamel or rust steel reactor of band stirring arm, the pure water that adds 80 kilograms, add 12 kilograms of Chinese crude drug finished products and 3 kilograms of chitosan finished products then, the slaine that adds 3.7 kilograms again, slaine is the mixture of manganese sulfate, manganese chloride, Borax, potassium permanganate, the part by weight of each component is 1: 1: 1: 1, and stirring and processing is one to three hour in reactor, obtains deodorant products.Inject pail pack then.
Embodiment 4:
Get leaf and the stem of 2.4 kilograms of Chinese mugworts, 0.5 kilogram Folium Isatidis, 5.6 kilogram Radix Arnebiae (Radix Lithospermi), 2.8 kilogram Radix Gentianae, 0.8 kilogram Rhizoma Acori Graminei, 3.2 kilogram Rhizoma Atractylodis, 3.2 kilogram Radix Scutellariae, 4 kilograms of Cortex Phellodendris, 1.2 kilogram Rhizoma Coptidis, shear, pulverize, soak with petroleum ether, extract, operation such as refining, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content is between 1-20%, obtain the Chinese crude drug finished product, the peak that goes out with the high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content.
Chitosan is carried out deacetylated processing; the deacetylation that makes chitosan is greater than 70%; and the reprocessing that methylates; be mixed with the aqueous solution of 0.1%-10% concentration then; obtain the chitosan finished product; packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material.
In the enamel or rust steel reactor of band stirring arm, the pure water that adds 60 kilograms, add 25 kilograms of Chinese crude drug finished products and 0.1 kilogram of chitosan finished product then, the slaine that adds 3.2 kilograms again, slaine is the mixture of ferrous sulfate, copper sulfate, zinc sulfate, manganese sulfate, the part by weight of each component is 1: 1: 1: 1, and stirring and processing is one to three hour in reactor, obtains deodorant products.Inject pail pack then.
Embodiment 5:
Get leaf and the stem of 5.8 kilograms of Chinese mugworts, 3.2 kilogram Folium Isatidis, 1.5 kilogram Radix Arnebiae (Radix Lithospermi), 5.7 kilogram Radix Gentianae, 3.8 kilogram Rhizoma Acori Graminei, 4 kilograms of Rhizoma Atractylodis, 0.5 kilogram Radix Scutellariae, 3 kilograms of Cortex Phellodendris, 0.5 kilogram Rhizoma Coptidis, shear, pulverize, soak with methanol, extract, operation such as refining, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content is between 1-20%, obtain the Chinese crude drug finished product, the peak that goes out with the high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content.
Chitosan is carried out deacetylated processing; the deacetylation that makes chitosan is greater than 70%; and the reprocessing that methylates; be mixed with the aqueous solution of 0.1%-10% concentration then; obtain the chitosan finished product; packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material.
In the enamel or rust steel reactor of band stirring arm, the pure water that adds 70 kilograms, add 30 kilograms of Chinese crude drug finished products and 2 kilograms of chitosan finished products then, the slaine that adds 5 kilograms again, slaine is the mixture of ferrous sulfate, copper sulfate, zinc sulfate, the part by weight of each component is 1: 1: 1, and stirring and processing is one to three hour in reactor, obtains deodorant products.Inject pail pack then.
Embodiment 6:
Get leaf and the stem of 0.5 kilogram of Chinese mugwort, 4.5 kilogram Folium Isatidis, 6 kilograms of Radix Arnebiae (Radix Lithospermi)s, 2.5 kilogram Radix Gentianae, 4 kilograms of Rhizoma Acori Graminei, 0.5 kilogram Rhizoma Atractylodis, 2.8 kilogram Radix Scutellariae, 2.1 kilogram Cortex Phellodendri, 0.7 kilogram Rhizoma Coptidis, shear, pulverize, use soak with ethanol, extract, operation such as refining, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content is between 1-20%, obtain the Chinese crude drug finished product, the peak that goes out with the high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content.
Chitosan is carried out deacetylated processing; the deacetylation that makes chitosan is greater than 70%; and the reprocessing that methylates; be mixed with the aqueous solution of 0.1%-10% concentration then; obtain the chitosan finished product; packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material.
In the enamel or rust steel reactor of band stirring arm, the pure water that adds 50 kilograms, add 20 kilograms of Chinese crude drug finished products and 6 kilograms of chitosan finished products then, the slaine that adds 2.5 kilograms again, slaine is the mixture of manganese sulfate, manganese chloride, Borax, the part by weight of each component is 1: 1: 1, and stirring and processing is one to three hour in reactor, obtains deodorant products.Inject pail pack then.
Embodiment 7:
Get leaf and the stem of 3.8 kilograms of Chinese mugworts, 4.8 kilogram Folium Isatidis, 2.4 kilogram Radix Arnebiae (Radix Lithospermi), 5 kilograms of Radix Gentianaes, 3 kilograms of Rhizoma Acori Graminei, 0.7 kilogram Rhizoma Atractylodis, 3.7 kilogram Radix Scutellariae, 1.5 kilogram Cortex Phellodendri, 1.7 kilogram Rhizoma Coptidis, shear, pulverize, soak with acetone, extract, operation such as refining, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content is between 1-20%, obtain the Chinese crude drug finished product, the peak that goes out with the high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content.
Chitosan is carried out deacetylated processing; the deacetylation that makes chitosan is greater than 70%; and the reprocessing that methylates; be mixed with the aqueous solution of 0.1%-10% concentration then; obtain the chitosan finished product; packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material.
In the enamel or rust steel reactor of band stirring arm, the pure water that adds 90 kilograms, add 28 kilograms of Chinese crude drug finished products and 9 kilograms of chitosan finished products then, the slaine that adds 0.1 kilogram again, slaine is the mixture of manganese sulfate, manganese chloride, Borax, potassium permanganate, the part by weight of each component is 1: 1: 1: 1, and stirring and processing is one to three hour in reactor, obtains deodorant products.Inject pail pack then.
Embodiment 8:
Get leaf and the stem of 4.8 kilograms of Chinese mugworts, 1.7 kilogram Folium Isatidis, 0.5 kilogram Radix Arnebiae (Radix Lithospermi), 4.2 kilogram Radix Gentianae, 3.4 kilogram Rhizoma Acori Graminei, 1 kilogram of Rhizoma Atractylodis, 3.9 kilogram Radix Scutellariae, 1 kilogram of Cortex Phellodendri, 2.2 kilogram Rhizoma Coptidis, shear, pulverize, soak with petroleum ether, extract, operation such as refining, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content is between 1-20%, obtain the Chinese crude drug finished product, the peak that goes out with the high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content.
Chitosan is carried out deacetylated processing; the deacetylation that makes chitosan is greater than 70%; and the reprocessing that methylates; be mixed with the aqueous solution of 0.1%-10% concentration then; obtain the chitosan finished product; packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material.
In the enamel or rust steel reactor of band stirring arm, the pure water that adds 55 kilograms, add 18 kilograms of Chinese crude drug finished products and 5 kilograms of chitosan finished products then, the slaine that adds 1 kilogram again, slaine is the mixture of ferrous sulfate, copper sulfate, zinc sulfate, manganese sulfate, the part by weight of each component is 1: 1: 1: 1, and stirring and processing is one to three hour in reactor, obtains deodorant products.Inject pail pack then.
Embodiment 9:
Get leaf and the stem of 3 kilograms of Chinese mugworts, 6 kilograms of Folium Isatidiss, 3.8 kilogram Radix Arnebiae (Radix Lithospermi), 2 kilograms of Radix Gentianaes, 2.6 kilogram Rhizoma Acori Graminei, 2.2 kilogram Rhizoma Atractylodis, 1.5 kilogram Radix Scutellariae, 2.8 kilogram Cortex Phellodendri, 3 kilograms of Rhizoma Coptidis, shear, pulverize, use soak with ethanol, extract, operation such as refining, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content is between 1-20%, obtain the Chinese crude drug finished product, the peak that goes out with the high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content.
Chitosan is carried out deacetylated processing; the deacetylation that makes chitosan is greater than 70%; and the reprocessing that methylates; be mixed with the aqueous solution of 0.1%-10% concentration then; obtain the chitosan finished product; packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material.
In the enamel or rust steel reactor of band stirring arm, the pure water that adds 65 kilograms, add 15 kilograms of Chinese crude drug finished products and 8 kilograms of chitosan finished products then, the slaine that adds 0.3 kilogram again, slaine is the mixture of manganese sulfate, manganese chloride, Borax, the part by weight of each component is 1: 1: 1, and stirring and processing is one to three hour in reactor, obtains deodorant products.Inject pail pack then.
Embodiment 10:
Get leaf and the stem of 5.2 kilograms of Chinese mugworts, 2 kilograms of Folium Isatidiss, 4.2 kilogram Radix Arnebiae (Radix Lithospermi), 0.5 kilogram Radix Gentianae, 1 kilogram of Rhizoma Acori Graminei, 2.5 kilogram Rhizoma Atractylodis, 1 kilogram of Radix Scutellariae, 3.6 kilogram Cortex Phellodendri, 3.8 kilogram Rhizoma Coptidis, shear, pulverize, soak with acetone, extract, operation such as refining, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content is between 1-20%, obtain the Chinese crude drug finished product, the peak that goes out with the high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content.
Chitosan is carried out deacetylated processing; the deacetylation that makes chitosan is greater than 70%; and the reprocessing that methylates; be mixed with the aqueous solution of 0.1%-10% concentration then; obtain the chitosan finished product; packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material.
In the enamel or rust steel reactor of band stirring arm, the pure water that adds 75 kilograms, add 8 kilograms of Chinese crude drug finished products and 10 kilograms of chitosan finished products then, the slaine that adds 0.8 kilogram again, slaine is the mixture of manganese sulfate, manganese chloride, Borax, potassium permanganate, the part by weight of each component is 1: 1: 1: 1, and stirring and processing is one to three hour in reactor, obtains deodorant products.Inject pail pack then.
Example 1
Use in sewage treatment plant, method is:
Deodorizer is placed the sealing storage tank, and pressurization.Be connected to the sudden and violent gas of sewage pond with pipeline.On the one hand with deodorizer by the consumption that calculates regularly, quantitatively join in the cesspool, deodorizer spray above cesspool with spray pattern cause a mist layer on the other hand, isolation sewage contacts with air, the generation excellent deodorization effect.
Example 2
Deodorizer is directly sprayed at place where the garage is piled up widely, repeatedly with spray pattern, produce excellent deodorization effect.
Example 3
Deodorizer directly is sprayed onto in the footwear that stink with spray pattern, and in 3-5 divided bell, the stink in the footwear was eliminated greatly.
Claims (1)
1. the preparation method of a deodorizer, it is characterized in that: processing step is:
A, with the raw material of Chinese crude drug in proportion weight feed intake, shear, pulverize, carry out processed with operations such as organic solvent soak, extracts, makes with extra care, seal fermentation up for safekeeping as semi-finished product are airtight then, ferment to the individual event content of effective between 0.001%-10%, total content obtains the Chinese crude drug finished product between 1-20%, with the peak that goes out of high-performance liquid chromatogram determination active substance, calculate the content that peak area draws the individual event material that of individual event material, calculate the gross area and draw total content;
B, the chitosan raw material is carried out deacetylated processing, the deacetylation that makes chitosan is greater than 70%, and the reprocessing that methylates, be mixed with the aqueous solution of 0.1%-10% concentration then, obtain the chitosan finished product, packing is sealed up for safekeeping stand-by, and the peak that goes out with the high-performance liquid chromatogram determination active substance calculates the content that peak area can draw material;
C, in the enamel or rust steel reactor of band stirring arm, the pure water that adds the 30-90 weight portion, add 5-30 weight portion Chinese crude drug finished product and 0.1-10 weight portion chitosan finished product then, add slaine again, slaine is that ferrous sulfate, copper sulfate, zinc sulfate, manganese sulfate, manganese chloride, Borax, potassium permanganate etc. are intermediary a kind of, several or whole, the parts by weight of slaine are 0.1～5, and stirring and processing is one to three hour in reactor, obtains deodorant products;
The raw material of above-described Chinese crude drug is the leaf of Radix Scutellariae, Cortex Phellodendri, Rhizoma Coptidis, Rhizoma Acori Graminei, Rhizoma Atractylodis, Chinese mugwort and stem, Folium Isatidis, Radix Arnebiae (Radix Lithospermi), Radix Gentianae, wherein, the parts by weight of leaf of Chinese mugwort and stem, Folium Isatidis, Radix Arnebiae (Radix Lithospermi), Radix Gentianae are 0.5-6, and the parts by weight of Rhizoma Acori Graminei, Rhizoma Atractylodis, Radix Scutellariae, Cortex Phellodendri, Rhizoma Coptidis are 0.5-4;
Above-described organic solvent is methanol, ethanol, acetone and petroleum ether.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007100696499A CN101073674B (en) | 2007-06-22 | 2007-06-22 | Production of deodorant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007100696499A CN101073674B (en) | 2007-06-22 | 2007-06-22 | Production of deodorant |
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| Publication Number | Publication Date |
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| CN101073674A CN101073674A (en) | 2007-11-21 |
| CN101073674B true CN101073674B (en) | 2010-12-29 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2007100696499A Expired - Fee Related CN101073674B (en) | 2007-06-22 | 2007-06-22 | Production of deodorant |
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| CN1044903A (en) * | 1990-03-15 | 1990-08-29 | 缪予 | Deodorizing shoe powder |
| CN1032733C (en) * | 1993-10-09 | 1996-09-11 | 王刚生 | Foot-odor removing spray agent |
| CN1280173A (en) * | 2000-07-05 | 2001-01-17 | 何仙良 | Name and formula of deodorizing toilet soap and its producing method |
-
2007
- 2007-06-22 CN CN2007100696499A patent/CN101073674B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1044903A (en) * | 1990-03-15 | 1990-08-29 | 缪予 | Deodorizing shoe powder |
| CN1032733C (en) * | 1993-10-09 | 1996-09-11 | 王刚生 | Foot-odor removing spray agent |
| CN1280173A (en) * | 2000-07-05 | 2001-01-17 | 何仙良 | Name and formula of deodorizing toilet soap and its producing method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101073674A (en) | 2007-11-21 |
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