CN107496967A - A kind of Vehicular air freshener and preparation method thereof - Google Patents
A kind of Vehicular air freshener and preparation method thereof Download PDFInfo
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- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A—HUMAN NECESSITIES
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- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
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- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/72—Organic compounds not provided for in groups B01D53/48 - B01D53/70, e.g. hydrocarbons
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
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- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
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- A61L2209/21—Use of chemical compounds for treating air or the like
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- A—HUMAN NECESSITIES
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- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/22—Treatment by sorption, e.g. absorption, adsorption, chemisorption, scrubbing, wet cleaning
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- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
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Abstract
The invention belongs to technical field of air purification, more particularly to a kind of Vehicular air freshener, including following raw material to be prepared：Rattletop, dark plum, Desmodium styracifolium, extract, Rosa Damascana, zinc sulfate, the rilanit specials of PEG 60, triethanolamine；Vehicular air freshener prepared by the present invention, there is good degradation of formaldehyde and settle PM2.5 effect.In addition, Vehicular air freshener prepared by the present invention belongs to actual nontoxic to the LD50 of passing through mouth ＞ 6500mg/kgbw of Kunming mouse.
Description
Technical field
The invention belongs to technical field of air purification, more particularly to a kind of Vehicular air freshener and preparation method thereof.
Background technology
With expanding economy, the living standard of people improves constantly, and automobile has come into average family, to the daily of people
Life brings unprecedented convenience, but consequently also exacerbates air pollution degree, and many drivers like windowing to travel, still
The poor health to people of air quality brings potential safety hazard along driving.So many Vehicular air fresheners
Arise at the historic moment.
Current market sales of Vehicular air freshener species is a lot, but is essentially all by compositions such as ether, essence
Composition, these materials in atmosphere after chemical breakdown caused by some compositions of gas inherently air pollutants, this is in fact
It is the pollution level for exacerbating air, it is long-term use of that generation pessimal stimulation is known from experience to people.This air freshener does not decompose
Pernicious gas, reaching the purpose of fresh air, its effect is to cover peculiar smell by distributing fragrance, rather than with being led in air
The gas of peculiar smell is caused to react, the simply smell by obscuring people carrys out " desalination " peculiar smell.In addition, interior space is smaller, air is clear
The harmful substance contained in new agent can cause people to produce the symptoms such as sacred disease, mucous membrane discomfort.
The content of the invention
The present invention is in order to solve the above technical problems, provide a kind of Vehicular air freshener and preparation method thereof, specifically
It is achieved through the following technical solutions.
A kind of Vehicular air freshener, include the raw material of following mass parts：Rattletop 20-60 parts, dark plum 10-50 parts, wide gold
Money grass 20-40 parts, extract 10-30 parts, Rosa Damascana 1-20 parts, zinc sulfate 1-15 parts, PEG-60 rilanit special 1-10 parts,
Triethanolamine 1-10 parts.
Further, described Vehicular air freshener, the raw material of following mass parts is included：Rattletop 43-47 parts, dark plum 25-
31 parts, Desmodium styracifolium 25-30 parts, extract 8-12 parts, Rosa Damascana 7-13 parts, zinc sulfate 2-6 parts, PEG-60 rilanit specials
3-5 parts, triethanolamine 3-5 parts.
Further, described extract, it is prepared by the raw material of following mass parts：Fresh leaf of bamboo 30-35 parts, fresh mountain
Aster 20-23 parts, fresh hill grass 17-19 parts.
Further, described extract includes following preparation process：
1) it is passed through hot blast and handles the fresh leaf of bamboo, fresh mountain aster, fresh hill grass, obtains material 1；
2) material 1 is irradiated with ultraviolet, obtains material 2；
3) material 2 carries out oscillation treatment, obtains material 3；
4) 170-180 DEG C of steam treatment 20-25min is passed through in material 3, obtains material 4；
5) material 4 crushes, and adds the ethanol of 1-2 times of powder quality, 45-50 DEG C of immersion 2-3h, filters, filtrate carries out decompression steaming
Evaporate recovery ethanol, obtain residual solution, residual solution it is dry medicinal extract 1；
6) the ethyl acetate dissolving medicinal extract 1 of 2 times of mass of medicinal extract 1, filtering, the activity of 1/15 times of filtrate quality of addition are added
Charcoal, filter, filtrate decompression is distilled to recover ethyl acetate, both obtains extract；
Further, described hot blast processing, the temperature of hot blast is 35-37 DEG C, and the water content for controlling raw material is 80-82%.
Further, described ultraviolet irradiation, ultraviolet wavelength 390-400nm, irradiation time 1-1.2h.
Further, described oscillation treatment, it is that 20-30min is vibrated under 70-80r/min frequency, suspends 10-
30-35min is vibrated under 13min, 150-180r/min frequency.
Further, described Vehicular air freshener, including following preparation method：
1) rattletop, dark plum, Desmodium styracifolium mixing, crushing, replace unicellular bacterium solution with vacation and mix, it is 60- that water content, which is made,
63% compound, ferment 1-2 days at 33-35 DEG C, obtain fermentation material, add the clear water of 1 times of fermentation material quality, decoct 2-2.5h,
Filtering, filtrate add pH=8.5-8.8 sodium hydroxide solution precipitation 10-20min, filtering, filter residue and drying, obtain solid 1；
2) extract, Rosa Damascana, PEG-60 rilanit specials, triethanolamine mix, and stirring and dissolving at 40-45 DEG C, obtain
Mixed liquor 1；
3) solid 1, zinc sulfate mixing, add the deionized water of 1 times of mass of solid 1, stirring and dissolving, obtain mixed liquor 2；
3) mixed liquor 1, mixed liquor 2 are stirred 60-70min at 3700-3900r/min, 35-37 DEG C, obtain stoste, add
The deionized water mixing of 100-105 times of stoste volume, adds spray bottle, 700-710KPa is pressurized in bottle, both.
The beneficial effects of the present invention are：The Vehicular air freshener prepared according to the present invention, there is degraded first well
The effect of aldehyde and the effect for settling PM2.5.In addition, its pair also has corresponding effect of settling with benzene, for TVOC (general volatiles
Organic matter) also there is corresponding absorption degradation effect.
Acute toxicity testing shows that the Vehicular air freshener prepared with the present invention is oral with 6500mg/kgbw dosage
After gavage, poisoning symptom is had no within interior 14 day observation period, gross anatomy is done after off-test to experimental animal and also has no obvious
It is abnormal.Result of the test shows, the LD50 of passing through mouth ＞ 6500mg/ of Vehicular air freshener prepared by the present invention to Kunming mouse
Kgbw, belong to actual nontoxic.
Embodiment
The embodiment of the present invention is described in further detail below, but the invention is not limited in these realities
Mode is applied, any improvement or replacement on the present embodiment essence spirit, it is claimed to still fall within the claims in the present invention
Scope.
Embodiment 1
A kind of Vehicular air freshener, including following raw material：Rattletop 43kg, dark plum 25kg, Desmodium styracifolium 25kg, extract
8kg, Rosa Damascana 7kg, zinc sulfate 2kg, PEG-60 rilanit special 3kg, triethanolamine 3kg.
Described extract, it is prepared by the raw material of following mass parts：Fresh leaf of bamboo 30kg, fresh mountain aster 20kg,
Fresh hill grass 17kg.
Described extract includes following preparation process：
1) it is passed through hot blast and handles the fresh leaf of bamboo, fresh mountain aster, fresh hill grass, obtains material 1；
2) material 1 is irradiated with ultraviolet, obtains material 2；
3) material 2 carries out oscillation treatment, obtains material 3；
4) 170 DEG C of steam treatment 20min are passed through in material 3, obtain material 4；
5) material 4 crushes, and adds the ethanol of 1 times of powder quality, 45 DEG C of immersion 2h, filters, filtrate carries out vacuum distillation recovery
Ethanol, obtains residual solution, residual solution it is dry medicinal extract 1；
6) the ethyl acetate dissolving medicinal extract 1 of 2 times of mass of medicinal extract 1, filtering, the activity of 1/15 times of filtrate quality of addition are added
Charcoal, filter, filtrate decompression is distilled to recover ethyl acetate, both obtains extract；
Described hot blast processing, the temperature of hot blast is 35 DEG C, and the water content for controlling raw material is 80%.
Described ultraviolet irradiation, ultraviolet wavelength 390nm, irradiation time 1h.
Described oscillation treatment, it is that 20min is vibrated under 70r/min frequency, suspends 10min, 150r/min frequency
Lower vibration 30min.
Described Vehicular air freshener, including following preparation method：
1) rattletop, dark plum mixing, Desmodium styracifolium crush, and replacing unicellular bacterium solution with vacation mixes, and water content is made as 60%
Compound, ferment 1 day at 33 DEG C, obtain fermentation material, add the clear water of 1 times of fermentation material quality, decoct 2-2.5h, filtering, filtrate
PH=8.5-8.8 sodium hydroxide solution precipitation 10-20min is added, filtering, filter residue and drying, obtains solid 1；
2) extract, Rosa Damascana, PEG-60 rilanit specials, triethanolamine mix, and stirring and dissolving at 40-45 DEG C, obtain
Mixed liquor 1；
3) solid 1, zinc sulfate mixing, add the deionized water of 1 times of mass of solid 1, stirring and dissolving, obtain mixed liquor 2；
3) mixed liquor 1, mixed liquor 2 are stirred 60-70min at 3700-3900r/min, 35-37 DEG C, obtain stoste, add
The deionized water mixing of 100-105 times of stoste volume, adds spray bottle, 700-710KPa is pressurized in bottle, both.
Embodiment 2
A kind of Vehicular air freshener, including following raw material：Rattletop 43kg, dark plum 25kg, Desmodium styracifolium 25kg, extract
8kg, Rosa Damascana 7kg, zinc sulfate 2kg, PEG-60 rilanit special 3kg, triethanolamine 3kg.
Described extract, it is prepared by the raw material of following mass parts：Fresh leaf of bamboo 30kg, fresh mountain aster 20kg,
Fresh hill grass 17kg.
Described extract includes following preparation process：
1) material 1 is irradiated with ultraviolet, obtains material 1；
2) material 2 carries out oscillation treatment, obtains material 2；
3) 170 DEG C of steam treatment 20min are passed through in material 3, obtain material 3；
4) material 3 crushes, and adds the ethanol of 1 times of powder quality, 45 DEG C of immersion 2h, filters, filtrate carries out vacuum distillation recovery
Ethanol, obtains residual solution, residual solution it is dry medicinal extract 1；
5) the ethyl acetate dissolving medicinal extract 1 of 2 times of mass of medicinal extract 1, filtering, the activity of 1/15 times of filtrate quality of addition are added
Charcoal, filter, filtrate decompression is distilled to recover ethyl acetate, both obtains extract；
Described ultraviolet irradiation, ultraviolet wavelength 390nm, irradiation time 1h.
Described oscillation treatment, it is that 20min is vibrated under 70r/min frequency, suspends 10min, 150r/min frequency
Lower vibration 30min.
Described Vehicular air freshener, including following preparation method：
1) rattletop, dark plum, Desmodium styracifolium mixing, crushing, replace unicellular bacterium solution with vacation and mix, water content is made as 60%
Compound, ferment 1 day at 33 DEG C, obtain fermentation material, add the clear water of 1 times of fermentation material quality, decoct 2-2.5h, filtering, filtrate
PH=8.5-8.8 sodium hydroxide solution precipitation 10-20min is added, filtering, filter residue and drying, obtains solid 1；
2) extract, Rosa Damascana, PEG-60 rilanit specials, triethanolamine mix, and stirring and dissolving at 40-45 DEG C, obtain
Mixed liquor 1；
3) solid 1, zinc sulfate mixing, add the deionized water of 1 times of mass of solid 1, stirring and dissolving, obtain mixed liquor 2；
3) mixed liquor 1, mixed liquor 2 are stirred 60-70min at 3700-3900r/min, 35-37 DEG C, obtain stoste, add
The deionized water mixing of 100-105 times of stoste volume, adds spray bottle, 700-710KPa is pressurized in bottle, both.
Embodiment 3
A kind of Vehicular air freshener, including following raw material：Rattletop 43kg, dark plum 25kg, Desmodium styracifolium 25kg, extract
8kg, Rosa Damascana 7kg, zinc sulfate 2kg, PEG-60 rilanit special 3kg, triethanolamine 3kg.
Described extract, it is prepared by the raw material of following mass parts：Fresh leaf of bamboo 30kg, fresh mountain aster 20kg,
Fresh hill grass 17kg.
Described extract includes following preparation process：
1) it is passed through hot blast and handles the fresh leaf of bamboo, fresh mountain aster, fresh hill grass, obtains material 1；
2) 170 DEG C of steam treatment 20min are passed through in material 1, obtain material 2；
3) material 2 crushes, and adds the ethanol of 1 times of powder quality, 45 DEG C of immersion 2h, filters, filtrate carries out vacuum distillation recovery
Ethanol, obtains residual solution, residual solution it is dry medicinal extract 1；
4) the ethyl acetate dissolving medicinal extract 1 of 2 times of mass of medicinal extract 1, filtering, the activity of 1/15 times of filtrate quality of addition are added
Charcoal, filter, filtrate decompression is distilled to recover ethyl acetate, both obtains extract；
Described hot blast processing, the temperature of hot blast is 35 DEG C, and the water content for controlling raw material is 80%.
Described Vehicular air freshener, including following preparation method：
1) rattletop, dark plum, Desmodium styracifolium mixing, crushing, replace unicellular bacterium solution with vacation and mix, water content is made as 60%
Compound, ferment 1 day at 33 DEG C, obtain fermentation material, add the clear water of 1 times of fermentation material quality, decoct 2-2.5h, filtering, filtrate
PH=8.5-8.8 sodium hydroxide solution precipitation 10-20min is added, filtering, filter residue and drying, obtains solid 1；
2) extract, Rosa Damascana, PEG-60 rilanit specials, triethanolamine mix, and stirring and dissolving at 40-45 DEG C, obtain
Mixed liquor 1；
3) solid 1, zinc sulfate mixing, add the deionized water of 1 times of mass of solid 1, stirring and dissolving, obtain mixed liquor 2；
3) mixed liquor 1, mixed liquor 2 are stirred 60-70min at 3700-3900r/min, 35-37 DEG C, obtain stoste, add
The deionized water mixing of 100-105 times of stoste volume, adds spray bottle, 700-710KPa is pressurized in bottle, both.
Embodiment 4
A kind of Vehicular air freshener, including following raw material：Rattletop 43kg, dark plum 25kg, Desmodium styracifolium 25kg, extract
8kg, Rosa Damascana 7kg, zinc sulfate 2kg, PEG-60 rilanit special 3kg, triethanolamine 3kg.
Described extract, it is prepared by the raw material of following mass parts：Fresh leaf of bamboo 30kg, fresh mountain aster 20kg,
Fresh hill grass 17kg.
Described extract includes following preparation process：
1) it is passed through hot blast and handles the fresh leaf of bamboo, fresh mountain aster, fresh hill grass, obtains material 1；
2) material 1 is irradiated with ultraviolet, obtains material 2；
3) material 2 carries out oscillation treatment, obtains material 3；
4) 170 DEG C of steam treatment 20min are passed through in material 3, obtain material 4；
5) material 4 crushes, and adds the ethanol of 1 times of powder quality, 45 DEG C of immersion 2h, filters, filtrate carries out vacuum distillation recovery
Ethanol, obtains residual solution, residual solution it is dry medicinal extract 1；
6) the ethyl acetate dissolving medicinal extract 1 of 2 times of mass of medicinal extract 1, filtering, the activity of 1/15 times of filtrate quality of addition are added
Charcoal, filter, filtrate decompression is distilled to recover ethyl acetate, both obtains extract；
Described hot blast processing, the temperature of hot blast is 35 DEG C, and the water content for controlling raw material is 80%.
Described ultraviolet irradiation, ultraviolet wavelength 390nm, irradiation time 1h.
Described oscillation treatment, it is that 20min is vibrated under 70r/min frequency, suspends 10min, 150r/min frequency
Lower vibration 30min.
Described Vehicular air freshener, including following preparation method：
1) rattletop, dark plum, Desmodium styracifolium mixing, crushing, add the clear water of 1 times of mixed-powder quality, decoct 2-2.5h, mistake
Filter, filtrate add pH=8.5-8.8 sodium hydroxide solution precipitation 10-20min, filtering, filter residue and drying, obtain solid 1；
2) extract, Rosa Damascana, PEG-60 rilanit specials, triethanolamine mix, and stirring and dissolving at 40-45 DEG C, obtain
Mixed liquor 1；
3) solid 1, zinc sulfate mixing, add the deionized water of 1 times of mass of solid 1, stirring and dissolving, obtain mixed liquor 2；
3) mixed liquor 1, mixed liquor 2 are stirred 60-70min at 3700-3900r/min, 35-37 DEG C, obtain stoste, add
The deionized water mixing of 100-105 times of stoste volume, adds spray bottle, 700-710KPa is pressurized in bottle, both.
Embodiment 5
A kind of Vehicular air freshener, including following raw material：Rattletop 43kg, dark plum 25kg, Desmodium styracifolium 25kg, extract
8kg, Rosa Damascana 7kg, zinc sulfate 2kg, PEG-60 rilanit special 3kg, triethanolamine 3kg.
Described extract, it is prepared by the raw material of following mass parts：Fresh leaf of bamboo 30kg, fresh mountain aster 20kg,
Fresh hill grass 17kg.
Described extract includes following preparation process：
1) the fresh leaf of bamboo, fresh mountain aster, the grass mixing of fresh hill, are passed through 170 DEG C of steam treatment 20min, obtain material 1；
2) material 1 crushes, and adds the ethanol of 1 times of powder quality, 45 DEG C of immersion 2h, filters, filtrate carries out vacuum distillation recovery
Ethanol, obtains residual solution, residual solution it is dry medicinal extract 1；
3) the ethyl acetate dissolving medicinal extract 1 of 2 times of mass of medicinal extract 1, filtering, the activity of 1/15 times of filtrate quality of addition are added
Charcoal, filter, filtrate decompression is distilled to recover ethyl acetate, both obtains extract；
Described hot blast processing, the temperature of hot blast is 35 DEG C, and the water content for controlling raw material is 80%.
Described Vehicular air freshener, including following preparation method：
1) rattletop, dark plum, Desmodium styracifolium mixing, crushing, add the clear water of 1 times of mixed-powder quality, decoct 2-2.5h, mistake
Filter, filtrate add pH=8.5-8.8 sodium hydroxide solution precipitation 10-20min, filtering, filter residue and drying, obtain solid 1；
2) extract, Rosa Damascana, PEG-60 rilanit specials, triethanolamine mix, and stirring and dissolving at 40-45 DEG C, obtain
Mixed liquor 1；
3) solid 1, zinc sulfate mixing, add the deionized water of 1 times of mass of solid 1, stirring and dissolving, obtain mixed liquor 2；
3) mixed liquor 1, mixed liquor 2 are stirred 60-70min at 3700-3900r/min, 35-37 DEG C, obtain stoste, add
The deionized water mixing of 100-105 times of stoste volume, adds spray bottle, 700-710KPa is pressurized in bottle, both.
Experimental example
1st, air freshener effect is tested and assessed
The air freshener prepared according to embodiment 1 and the method for embodiment 5 is the He of experimental group 1, according to application number CN
201710367017.4《Solid air freshener for vehicle》The Vehicular air freshener of preparation as a control group, tests 3 groups of air
The effect of freshener.With reference to GB/T18883-2002《Indoor Air Quality standards》Three identical rooms are detected, tied
Fruit is as shown in table 1.
As known from Table 1, according to embodiment 1 prepare Vehicular air freshener, have the function that good degradation of formaldehyde with
Settle PM2.5 effect.In addition, its pair also has corresponding effect of settling with benzene, for TVOC (total volatile organism)
With corresponding absorption degradation effect.Embodiment 5 compared with Example 1, due to when preparing Vehicular air freshener, for carrying
The preparation of thing is taken, its raw material did not enter hot blast processing, ultraviolet irradiation, oscillation treatment, for rattletop, dark plum, Desmodium styracifolium only
It is simply to be handled, not by fermentation process, so that its effect of the air freshener of preparation is poor, not as implementing
Example 1.
The Vehicular air freshener experimental result (mg/m of table 13)
2nd, acute poisons mouth experiment:From SPF levels Kunming mouse 18, body weight 18-22g, male and female half and half, divide equally
3 groups, for using once test method(s) to greatest extent, poisoning dosage 6500mg/kgbw, passed through by 0.2ml/10gbw during experiment
Mouth gavage tested material.Experimental animal fasting 16h before gavage, free water, normal diet is given after continuing fasting 2h after gavage, even
Continuous observation 14 days, the poisoning manifestations and death condition of recording laboratory animal, and everywhere dead animal enters to dead animal and observation period
Row gross anatomy.
As a result show, 3 experimental groups, after the oral gavage of 6500mg/kgbw dosage, had no within interior 14 day observation period
Poisoning symptom, gross anatomy is done to experimental animal after off-test and also shown no obvious abnormalities.Result of the test shows prepared by the present invention
Vehicular air freshener to the LD50 of passing through mouth ＞ 6500mg/kgbw of Kunming mouse, belong to actual nontoxic.
Claims (8)
1. a kind of Vehicular air freshener, it is characterised in that include the raw material of following mass parts：Rattletop 20-60 parts, dark plum 10-
50 parts, Desmodium styracifolium 20-40 parts, extract 10-30 parts, Rosa Damascana 1-20 parts, zinc sulfate 1-15 parts, PEG-60 hydrogenated castors
Oily 1-10 parts, triethanolamine 1-10 parts.
2. Vehicular air freshener as claimed in claim 1, it is characterised in that include the raw material of following mass parts：Rattletop 43-
47 parts, dark plum 25-31 parts, Desmodium styracifolium 25-30 parts, extract 8-12 parts, Rosa Damascana 7-13 parts, zinc sulfate 2-6 parts, PEG-
60 rilanit special 3-5 parts, triethanolamine 3-5 parts.
3. Vehicular air freshener as claimed in claim 1, it is characterised in that described extract, by following mass parts
Raw material is prepared：Fresh leaf of bamboo 30-35 parts, fresh mountain aster 20-23 parts, fresh hill grass 17-19 parts.
4. Vehicular air freshener as claimed in claim 3, it is characterised in that described extract includes following prepare and walked
Suddenly：
1) it is passed through hot blast and handles the fresh leaf of bamboo, fresh mountain aster, fresh hill grass, obtains material 1；
2) material 1 is irradiated with ultraviolet, obtains material 2；
3) material 2 carries out oscillation treatment, obtains material 3；
4) 170-180 DEG C of steam treatment 20-25min is passed through in material 3, obtains material 4；
5) material 4 crushes, and adds the ethanol of 1-2 times of powder quality, 45-50 DEG C of immersion 2-3h, filters, filtrate is evaporated under reduced pressure back
Receive ethanol, obtain residual solution, residual solution it is dry medicinal extract 1；
6) the ethyl acetate dissolving medicinal extract 1 of 2 times of mass of medicinal extract 1 is added, filtering, the activated carbon of 1/15 times of filtrate quality is added, takes out
Filter, filtrate decompression are distilled to recover ethyl acetate, both obtain extract.
5. Vehicular air freshener as claimed in claim 4, it is characterised in that described hot blast processing, the temperature of hot blast are
35-37 DEG C, the water content for controlling raw material is 80-82%.
6. Vehicular air freshener as claimed in claim 4, it is characterised in that described ultraviolet irradiation, ultraviolet wavelength
For 390-400nm, irradiation time 1-1.2h.
7. Vehicular air freshener as claimed in claim 4, it is characterised in that described oscillation treatment, be in 70-80r/
20-30min is vibrated under min frequency, suspends 10-13min, vibrates 30-35min under 150-180r/min frequency.
8. Vehicular air freshener as claimed in claim 1, it is characterised in that including following preparation process：
1) rattletop, dark plum, the mixing of wide money, crushing, replace unicellular bacterium solution with vacation and mix, it is 60-63%'s that water content, which is made,
Compound, ferment 1-2 days at 33-35 DEG C, obtain fermentation material, add the clear water of 1 times of fermentation material quality, decoct 2-2.5h, filter, filter
Liquid adds pH=8.5-8.8 sodium hydroxide solution precipitation 10-20min, filtering, filter residue and drying, obtains solid 1；
2) extract, Rosa Damascana, PEG-60 rilanit specials, triethanolamine mix, and stirring and dissolving at 40-45 DEG C, must mix
Liquid 1；
3) solid 1, zinc sulfate mixing, add the deionized water of 1 times of mass of solid 1, stirring and dissolving, obtain mixed liquor 2；
3) mixed liquor 1, mixed liquor 2 are stirred 60-70min at 3700-3900r/min, 35-37 DEG C, obtain stoste, add 100-
The deionized water mixing of 105 times of stoste volumes, adds spray bottle, 700-710KPa is pressurized in bottle, both.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113368290A (en) * | 2021-07-15 | 2021-09-10 | 湖北瑞晟生物有限责任公司 | Rose fragrance fumigant |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN86106630A (en) * | 1986-09-23 | 1988-04-06 | 那福延 | Broad-spectrum hygienic deodorant |
| CN101073674A (en) * | 2007-06-22 | 2007-11-21 | 俞祖勋 | Production of deodoriferant |
| CN103463952A (en) * | 2013-09-05 | 2013-12-25 | 杨振生 | Antibacterial formaldehyde scavenger used in automobile |
| CN103690986A (en) * | 2013-12-23 | 2014-04-02 | 青岛安信医疗器械有限公司 | Plant air purifier |
| CN104174056A (en) * | 2014-08-29 | 2014-12-03 | 成都顺发消洗科技有限公司 | Formaldehyde-removal traditional Chinese medicine solid air refresher |
| CN105688244A (en) * | 2014-11-26 | 2016-06-22 | 上海新舒环环保科技有限公司 | Production method of novel air odor remover |
| CN105770945A (en) * | 2016-03-24 | 2016-07-20 | 大连晟景科技有限公司 | Formaldehyde-removing and deodorizing ferment smell-cleaning agent and preparation method and application thereof |
| CN105833324A (en) * | 2016-05-30 | 2016-08-10 | 杭州筑净环境科技有限公司 | Method for preparing pure plant extract deodorant |
| CN106075517A (en) * | 2016-05-31 | 2016-11-09 | 刘贤伦 | Except formaldehyde, eliminate the unusual smell air purifying preparation and preparation method thereof |
| CN106983884A (en) * | 2017-03-18 | 2017-07-28 | 长沙协浩吉生物工程有限公司 | A kind of compound method of indoor ferment air freshener |
-
2017
- 2017-09-25 CN CN201710876596.5A patent/CN107496967A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN86106630A (en) * | 1986-09-23 | 1988-04-06 | 那福延 | Broad-spectrum hygienic deodorant |
| CN101073674A (en) * | 2007-06-22 | 2007-11-21 | 俞祖勋 | Production of deodoriferant |
| CN103463952A (en) * | 2013-09-05 | 2013-12-25 | 杨振生 | Antibacterial formaldehyde scavenger used in automobile |
| CN103690986A (en) * | 2013-12-23 | 2014-04-02 | 青岛安信医疗器械有限公司 | Plant air purifier |
| CN104174056A (en) * | 2014-08-29 | 2014-12-03 | 成都顺发消洗科技有限公司 | Formaldehyde-removal traditional Chinese medicine solid air refresher |
| CN105688244A (en) * | 2014-11-26 | 2016-06-22 | 上海新舒环环保科技有限公司 | Production method of novel air odor remover |
| CN105770945A (en) * | 2016-03-24 | 2016-07-20 | 大连晟景科技有限公司 | Formaldehyde-removing and deodorizing ferment smell-cleaning agent and preparation method and application thereof |
| CN105833324A (en) * | 2016-05-30 | 2016-08-10 | 杭州筑净环境科技有限公司 | Method for preparing pure plant extract deodorant |
| CN106075517A (en) * | 2016-05-31 | 2016-11-09 | 刘贤伦 | Except formaldehyde, eliminate the unusual smell air purifying preparation and preparation method thereof |
| CN106983884A (en) * | 2017-03-18 | 2017-07-28 | 长沙协浩吉生物工程有限公司 | A kind of compound method of indoor ferment air freshener |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113368290A (en) * | 2021-07-15 | 2021-09-10 | 湖北瑞晟生物有限责任公司 | Rose fragrance fumigant |
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