CN101070501A - Energy-saving environment-protective fuel-oil compounding agent - Google Patents
Energy-saving environment-protective fuel-oil compounding agent Download PDFInfo
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- CN101070501A CN101070501A CNA200610078672XA CN200610078672A CN101070501A CN 101070501 A CN101070501 A CN 101070501A CN A200610078672X A CNA200610078672X A CN A200610078672XA CN 200610078672 A CN200610078672 A CN 200610078672A CN 101070501 A CN101070501 A CN 101070501A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L10/00—Use of additives to fuels or fires for particular purposes
- C10L10/02—Use of additives to fuels or fires for particular purposes for reducing smoke development
Abstract
This invention has publicized one kind of energy conservation environmental protection fuel oil recombined, its characteristic is that it is comprised by the following component and the content quality percentage preparation: The pure dispersing agent 13-25%, anti-detonator 5-15%, combustion antismoke agent 5-20%, certain number modifying addition 0-35%, anti-oxygen polymerization retarded 0.3-3%, metal passivator 0-5%, deicing medicinal preparation 2-10%, lubrication antiwar additive 8-20%, antiseptic 0.2-4%, against preignition medicinal preparation 0-3%, emulsion breaker 0.01-0.5%, defoamer 0.01-0.5%, the remainder is the organic solvent. When this invention energy conservation environmental protection fuel oil recombined, use, by oil emulsion compared to 2000:1 the proportion joins in the bunker oil, saves gas and oil 8%-30%, and the short time stops Canada, fuel oil Shan Haobing rises not obviously. Simultaneously also has both the obvious clear coal to remove dirty stuff, anti-rubs the rust prevention, to reduce CO, HC, SO2, NOX and the mist and dust pollution and the noise, protects the atmospheric environment, lengthens service life and so on internal combustion engine effects. But widely uses in power generator equipment and so on vehicle, ship, mechanical internal combustion engine and oil-fired boiler, kiln stove.
Description
Technical field the invention belongs to the oil fuel composite additive of petrochemical industry, relates to specifically a kind ofly be applicable to that with unleaded, methyl alcohol, ethanol petrol, light, heavy gas oil or heavy oil be the energy-saving environment-protective fuel-oil compounding agent of fuel.
The background technology mankind consume in development social economy, enjoyment material and spiritual civilization
Nearly half petroleum resources on the earth, also severe contamination ecotope, just threatening the healthy survival and development of controlling oneself.China of particularly vast 1,300,000,000 populations, along with national economy increases for many years fast, car, ship etc. with oily power machine every year with about 12% speed increase.Only nearly 2.5 hundred million tons in oil is just consumed in the whole nation in 2005, and wherein half is gasoline and diesel oil, and 1/3rd oil is by import.Not only make country pay a large amount of foreign exchanges and interior subsides, also strengthened production, operation, life cost pressure to numerous enterprises, cause and with oily individual because energy shortage and fuel oil appreciate.The incomplete combustion of great amount of fuel oil also makes urban air pollution be on the rise, and the health that is endangering people is with long-lived.As resolutely not taking effective energy-saving and environmental protection measure, certainly will aggravate the anxiety and the Ecological environment worsening of Nonrenewable resources.For this reason, central authorities have made the brilliant policies of decisive and fundamental importance of building a conservation-minded society, and State Environmental Protection Administration has also proposed more strict Europe II, Europe III automobile exhaust emission standard requirement.
At present, the exploitation and the application of fuel oil additive both at home and abroad, just towards by one-pack type to compound, by the trend development of attaching most importance to and attaching most importance to the fuel-saving environmental protection type with peace and quiet type.Wherein truly have quite some brand product fuel-economizings, environment protecting remarkable, and produced good economy, society and environmental benefit.But also there is some deficiency unavoidably, such as: prescription lacks performance balance, and machinery is had corrosion phenomenon; Sulphur, phosphorus composition exceed standard, and make the catalyst failure in the vehicle exhaust three wastes transfer equipment; Excessive use polymerizable alkenyl hydro carbons detergent-dispersant additive has increased the generation of settling in the combustion chamber again when disperseing greasy filth; Strong polarity of excessive use and semi-polarity solvent cause the swelling of sealing material to lose efficacy; Really the composition of energy boosting of octane rating and cetane value is low excessively, and product anti-knocking property that make and oil-saving effect are outstanding; The smoke suppressor of containing metal composition and ignition dope consumption are excessive, use of a specified duration to cause cylinder inner wall and piston ring scuffing, the ash settling that grades to increase; The poor efficiency carrier is too much in the product, has squeezed out the space of effective constituent, has increased idle cost, and terminal user's fuel-economizing is not saved money, and input-output ratio is very little, promotes not open.
Summary of the invention the purpose of this invention is to provide a kind of fuel-economizing, saves money, clear charcoal scale removal, wear-resistant antirust, reduce obnoxious flavour and smoke contamination and noise, protection atmospheric environment, prolong the energy-saving environment-protective fuel-oil compounding agent in work-ing life such as oil engine, to overcome the deficiencies in the prior art.
For realizing purpose of the present invention, energy-saving environment-protective fuel-oil compounding agent of the present invention, the technical scheme of taking is:
Fuel-oil compounding agent of the present invention is prepared from by following component and content mass percent: detergent-dispersant additive 13-25%, octane promoter 5-15%, combustion-supporting smoke suppressor 5-20%, cetane number improver 0-35%, antioxygen stopper 0.3-3%, metal passivator 0-5%, anti-icer 2-10%, lubrication anti-wear agent 8-20%, sanitas 0.2-4%, anti-pre-ignition agent 0-3%, emulsion splitter 0.01-0.5%, defoamer 0.01-0.5%, surplus is an organic solvent.
Described detergent-dispersant additive is N methyl-2-pyrrolidone, phosphoamide, mono alkenyl succimide, diene base succimide, polyene-based succimide, polymer allyl butyrate imide, the mixture of any mass ratio of two or more in the said components.
Described octane promoter is dimethyl cyclopentadiene tricarbonyl manganese, ferrocene, methylcarbonate, monomethylaniline, the mixture of any mass ratio of one or more in the said components.
Described combustion-supporting smoke suppressor is barium alkylsulfonate, isocaprylic acid barium, magnesium naphthenate, the mixture of any mass ratio of one or more in the said components.
Described cetane number improver is isoamyl nitrate, oxalic acid isobutyl ester, the mixture of any mass ratio of one or both in the said components.
Described antioxygen stopper is diformazan salicyl propylene diamine, 4-methyl 2,6 di-tertiary butyl methyl phenol, with the mixture of 1: 2～3 mass ratioes.
Described metal passivator is N, N ' two salicylidenes, 1,2 propyl diamine and benzotriazole, and one or both in the component are with 0～1: the mixture of 1.5～3 mass ratioes.
Described anti-icer is alkylphenol polyoxyethylene, alkyl ethyl imidazol(e) quinoline, the mixture of any mass ratio of one or both in the component.
Described lubrication anti-wear agent is poly-alpha-olefin synthetic oil, whiteruss, the mixture of any mass ratio of one or both in the component.
Described anticorrosive agent is C
12Alkenyl succinic acid.
Described anti-pre-ignition agent is a kind of in cycloalkyl boric acid ester, the Tritolyl Phosphate.
Described emulsion splitter is epoxy second, propane block polyether.
Described defoamer is acrylate and ether copolymer.
Described organic solvent is methyl ethyl diketone, N,N-DIMETHYLACETAMIDE, dimethylbenzene, kerosene, two or more mixtures with any mass ratio in the said components.
Energy-saving environment-protective fuel-oil compounding agent its preparation method of the present invention is for to be dissolved in the bigger raw material of hydrophilic and oleophilic value (HLB) in the strong ketones solvent of polarity; Raw material that the hydrophilic and oleophilic value is less and nonpolar raw material are dissolved in the more weak benzene of polarity, the wet goods solvent, be stirred to complete molten transparent, no post precipitation and combine under 40 ℃ ± 5 ℃ conditions, and adding breakdown of emulsion, defoamer are mixed well, and filtration, can are promptly.
Energy-saving environment-protective fuel-oil compounding agent of the present invention has following characteristics:
Removed the carrier that gasoline, diesel oil, solvent wet goods do not play too big effect in the prescription, changed the starting material that have two or more demand characteristicss concurrently and serve as carrier;
A, the smoke elimination that has reduced the containing metal ash, ignition dope dosage are to keep the prime the fuel system cleaning;
B, reduced the dosage of intensive polar solvent, replaced tensio-active agent, alleviated swelling sealing material;
C, increase the component of boosting of octane rating and cetane value, more adapted to low vapour, the label of diesel oil and the use of high compression ratio vehicle;
D, other protective raw materials are just given a hint, and are just enough, to reduce unnecessary cost, make the user really accomplish not only fuel-economizing but also save money.
Be described in detail preparation method of the present invention and processing step below:
1, in little tempering tank, under the normal temperature antioxygen stopper, metal passivator are dissolved in methyl ethyl diketone and/or the dimethyl formamide, make A liquid.
2, in big blending kettle, add dimethylbenzene and/or kerosene and lubrication anti-wear agent, heat 40 ℃ ± 5 ℃, add octane promoter, clear powder, combustion-supporting smoke suppressor, anti-icer, anticorrosive agent while stirring, make B liquid.
3, A liquid is added B liquid, after mixing well, add cetane number improver, anti-pre-ignition agent, emulsion splitter and defoamer, transfer to complete molten transparently, filter can and promptly get energy-saving environment-protective fuel-oil compounding agent of the present invention.
Energy-saving environment-protective fuel-oil compounding agent of the present invention adds in the oil fuel with the ratio of finish than 2000: 1 during use, can produce the oil-saving effect that fuel-economizing 8%-30% does not wait, and the short period of time stop adding, the fuel oil unit consumption there is no obvious rising.Also have concurrently simultaneously significantly clear charcoal scale removal, wear-resistant antirust, reduce CO, HC, SO
2, NO
xWith smoke contamination and noise, protection atmospheric environment, the effect that prolongs work-ing lifes such as oil engine.Can be widely used in car, ship, mechanical internal combustion engine and motive power machine equipments such as oil-firing boiler, kiln.Press rate of economizing gasoline average 10% and calculate, also can save 1,200 ten thousand tons of fuel oils every year, be worth 60,000,000,000 yuans, and can make the big contaminated vapor degree in city reduce more than 1/3rd.
Embodiment is operated by following processing step:
1, in little tempering tank, under the normal temperature antioxygen stopper, metal passivator are dissolved in methyl ethyl diketone and/or the dimethyl formamide, make A liquid.
2, in big blending kettle, add dimethylbenzene and/or kerosene and lubrication anti-wear agent, heat 40 ℃ ± 5 ℃, add octane promoter, clear powder, combustion-supporting smoke suppressor, anti-icer, anticorrosive agent while stirring, make B liquid.
3, A liquid is added B liquid, after mixing well, add cetane number improver, anti-pre-ignition agent, emulsion splitter and defoamer, transfer to complete molten transparently, filter can and promptly get energy-saving environment-protective fuel-oil compounding agent of the present invention.
Following table: exemplified 4 embodiment
| Component and content (%) | Material name | Mass percent | |||
| Example 1 | Example 2 | Example 3 | Example 4 | ||
| Clear powder (13～25) | (1) phosphoamide | 2.6 | - | 2.5 | - |
| (2) N-Methyl pyrrolidone | 2.4 | 3.2 | 2.0 | 2.0 | |
| (3) mono alkenyl succimide | 6.0 | - | 4.0 | - | |
| (4) diene base succimide | - | 8.0 | - | - | |
| (5) polyene-based succimide | - | - | - | 6.9 | |
| (6) polymer allyl butyrate imide | 4.0 | 6.0 | 6.0 | 5.0 | |
| Octane promoter (5～15) | (7) dimethyl cyclopentadiene tricarbonyl manganese | 6.0 | - | 8.0 | - |
| (8) ferrocene | 4.0 | 2.8 | 2.7 | 5.0 | |
| (9) methylcarbonate | 4.0 | - | - | - | |
| (10) monomethylaniline | - | - | 4.0 | - | |
| Combustion-supporting smoke suppressor (5～20) | (11) barium alkylsulfonate | 2.0 | 4.0 | 3.0 | 3.0 |
| (12) isooctoate of rare earth metal | 2.0 | 4.0 | 3.0 | 5 | |
| (13) magnesium naphthenate | 3.0 | 5.0 | 2.0 | - | |
| Cetane number improver (0～35) | (14) isoamyl nitrate | - | 24 | - | - |
| (15) oxalic acid isobutyl ester | - | - | - | 25 | |
| Antioxygen stopper (0.3～3) | (16) 4-methyl 2,6 di-tertiary butyl methyl phenol | 0.2 | 0.4 | 0.3 | 0.4 |
| (17) diformazan salicyl propylene diamine | 0.1 | 0.2 | 0.10 | 0.2 | |
| Metal passivator (0～5) | (18) N, N ' two salicylidenes 1,2 propyl diamine | 0.3 | 0.4 | 0.4 | - |
| (19) benzotriazole | 0.6 | 1.2 | 0.8 | 1.5 | |
| Anti-icer (2～10) | (20) alkyl ethyl imidazol(e) woods | - | 2.0 | - | 1.0 |
| (21) alkylphenol polyoxyethylene | 2.0 | - | 2.5 | 1.0 | |
| Lubrication anti-wear agent (8～20) | (22 poly-alpha-olefin synthetic oils | 15 | - | - | 7.5 |
| (23) whiteruss | - | 15 | 14 | 7.5 | |
| Sanitas (0.2～4) | (24) C12 alkenyl succinic acid | 1.1 | 1.6 | 0.6 | 0.8 |
| Anti-pre-ignition agent (0～3) | (25) Tritolyl Phosphate | 2.6 | - | - | - |
| (26) cycloalkyl boric acid ester | - | 3.0 | 3.0 | ||
| Emulsion splitter | (27) epoxy second, propane block polyether | 0.05 | 0.1 | 0.05 | 0.1 |
| Defoamer | (28) acrylate and ether copolymer | 0.05 | 0.1 | 0.05 | 0.1 |
| Organic solvent adds to 100% | (29) N,N-DIMETHYLACETAMIDE | 4.0 | 3.0 | 3.0 | - |
| (30) methyl ethyl diketone | 3.0 | 4.0 | 4.0 | 5 | |
| (31) dimethylbenzene | 20 | - | 22 | 10 | |
| (32) kerosene | 15 | 15 | 12 | 10 | |
Trial effect: example 1 gained energy-saving environment-protective fuel-oil compounding agent of the present invention can be used for gasoline car, example 2 gained energy-saving environment-protective fuel-oil compounding agent of the present invention can be used for diesel vehicle, and detect through Shandong Province's energy utilization monitoring center: rate of economizing gasoline is respectively 14.3% and 17.82%.Through many vehicle in use pavement tests, after 1000 kilometers of operations, rate of economizing gasoline does not all wait between 8%-30%, and dynamic property obviously strengthens, and exhaust gas smoke and noise are all very little.
Claims (14)
1, a kind of energy-saving environment-protective fuel-oil compounding agent, it is characterized in that being prepared from by following component and content mass percent: detergent-dispersant additive 13-25%, octane promoter 5-15%, combustion-supporting smoke suppressor 5-20%, cetane number improver 0-35%, antioxygen stopper 0.3-3%, metal passivator 0-5%, anti-icer 2-10%, lubrication anti-wear agent 8-20%, sanitas 0.2-4%, anti-pre-ignition agent 0-3%, emulsion splitter 0.01-0.5%, defoamer 0.01-0.5%, surplus is an organic solvent.
2, according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1, it is characterized in that described detergent-dispersant additive is N methyl-2-pyrrolidone, phosphoamide, mono alkenyl succimide, diene base succimide, polyene-based succimide, polymer allyl butyrate imide, the mixture of any mass ratio of two or more in the said components.
3,, it is characterized in that described octane promoter is dimethyl cyclopentadiene tricarbonyl manganese, ferrocene, methylcarbonate, monomethylaniline, the mixture of any mass ratio of one or more in the said components according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1.
4,, it is characterized in that described combustion-supporting smoke suppressor is barium alkylsulfonate, isocaprylic acid barium, magnesium naphthenate, the mixture of any mass ratio of one or more in the said components according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1.
5,, it is characterized in that described cetane number improver is isoamyl nitrate, oxalic acid isobutyl ester, the mixture of any mass ratio of one or both in the said components according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1.
6,, it is characterized in that described antioxygen stopper is diformazan salicyl propylene diamine, 4-methyl 2,6 di-tertiary butyl methyl phenol, with the mixture of 1: 2～3 mass ratioes according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1.
7, according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1, it is characterized in that described metal passivator is N, N ' two salicylidenes, 1,2 propyl diamine and benzotriazole, one or both in the component are with 0～1: the mixture of 1.5～3 mass ratioes.
8,, it is characterized in that described anti-icer is alkylphenol polyoxyethylene, alkyl ethyl imidazol(e) quinoline, the mixture of any mass ratio of one or both in the component according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1.
9,, it is characterized in that described lubrication anti-wear agent is poly-alpha-olefin synthetic oil, whiteruss, the mixture of any mass ratio of one or both in the component according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1.
10,, it is characterized in that described anticorrosive agent is C according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1
12Alkenyl succinic acid.
11,, it is characterized in that described anti-pre-ignition agent is a kind of in cycloalkyl boric acid ester, the Tritolyl Phosphate according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1.
12,, it is characterized in that described emulsion splitter is epoxy second, propane block polyether according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1.
13,, it is characterized in that described defoamer is acrylate and ether copolymer according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1.
14,, it is characterized in that described organic solvent is methyl ethyl diketone, N,N-DIMETHYLACETAMIDE, dimethylbenzene, kerosene, two or more mixtures in the said components with any mass ratio according to the said energy-saving environment-protective fuel-oil compounding agent of claim 1.
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