CN101033189A - 从葡萄糖酸δ-内酯结晶后母液中制备葡萄糖酸钙的方法 - Google Patents
从葡萄糖酸δ-内酯结晶后母液中制备葡萄糖酸钙的方法 Download PDFInfo
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- CN101033189A CN101033189A CN 200710021440 CN200710021440A CN101033189A CN 101033189 A CN101033189 A CN 101033189A CN 200710021440 CN200710021440 CN 200710021440 CN 200710021440 A CN200710021440 A CN 200710021440A CN 101033189 A CN101033189 A CN 101033189A
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- calglucon
- lactone
- gluconic acid
- crystallization
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Abstract
Description
加热时间(min) | 50 | 60 | 70 | 80 | 90 | 100 | 110 | 120 | 130 | 140 |
葡萄糖酸钙结晶量(g) | 1.08 | 1.12 | 1.30 | 1.44 | 1.85 | 2.04 | 2.23 | 2.40 | 2.36 | 2.44 |
管号 | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 | 11 | 12 | 13 |
20%葡萄糖酸钙(ml)水(ml)无水乙醇(ml)总体积(ml)葡萄糖钙浓度(%)乙醇浓度(%) | 98.41.62098 | 98.21.82099 | 98.02.020910 | 97.82.220911 | 97.62.420912 | 97.42.620913 | 97.22.820914 | 97.03.020915 | 96.83.220916 | 96.63.420917 | 96.43.620918 | 96.23.820919 | 96.04.020920 |
结晶的葡萄糖酸钙重(g) | 0.88 | 1.23 | 1.30 | 1.55 | 1.65 | 1.67 | 1.68 | 1.67 | 1.70 | 1.72 | 1.68 | 1.71 | 1.70 |
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CNB2007100214405A CN100564345C (zh) | 2007-04-02 | 2007-04-02 | 从葡萄糖酸δ-内酯结晶后母液中制备葡萄糖酸钙的方法 |
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CNB2007100214405A CN100564345C (zh) | 2007-04-02 | 2007-04-02 | 从葡萄糖酸δ-内酯结晶后母液中制备葡萄糖酸钙的方法 |
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CN101033189A true CN101033189A (zh) | 2007-09-12 |
CN100564345C CN100564345C (zh) | 2009-12-02 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102190578A (zh) * | 2011-03-09 | 2011-09-21 | 石允生 | 以葡萄糖磷酸盐为原料制备次磷酸(盐)和葡萄糖酸(盐)的方法 |
CN103910620A (zh) * | 2014-04-22 | 2014-07-09 | 郑州大学 | 葡萄糖酸亚锡的制备方法 |
CN111635304A (zh) * | 2020-06-28 | 2020-09-08 | 江西新赣江药业股份有限公司 | 一种葡萄糖酸亚铁的制备方法 |
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2007
- 2007-04-02 CN CNB2007100214405A patent/CN100564345C/zh not_active Expired - Fee Related
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102190578A (zh) * | 2011-03-09 | 2011-09-21 | 石允生 | 以葡萄糖磷酸盐为原料制备次磷酸(盐)和葡萄糖酸(盐)的方法 |
CN102190578B (zh) * | 2011-03-09 | 2013-06-26 | 石允生 | 以葡萄糖磷酸盐为原料制备次磷酸(盐)和葡萄糖酸(盐)的方法 |
CN103910620A (zh) * | 2014-04-22 | 2014-07-09 | 郑州大学 | 葡萄糖酸亚锡的制备方法 |
CN103910620B (zh) * | 2014-04-22 | 2015-09-09 | 郑州大学 | 葡萄糖酸亚锡的制备方法 |
CN111635304A (zh) * | 2020-06-28 | 2020-09-08 | 江西新赣江药业股份有限公司 | 一种葡萄糖酸亚铁的制备方法 |
CN111635304B (zh) * | 2020-06-28 | 2023-04-07 | 江西新赣江药业股份有限公司 | 一种葡萄糖酸亚铁的制备方法 |
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Assignee: ANHUI JINZHAI QIAOKANG PHARMACEUTICAL Co.,Ltd. Assignor: Jinzhai Shanshui edible medicinal fungus development Co.,Ltd. Contract record no.: 2012340000135 Denomination of invention: Method of preparing calcium gluconate from mother liquid after gluconate delta-lactone crystallization Granted publication date: 20091202 License type: Exclusive License Open date: 20070912 Record date: 20120418 |
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