CN101020860A - Anti-senility golden shaddock oil - Google Patents

Anti-senility golden shaddock oil Download PDF

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Publication number
CN101020860A
CN101020860A CN 200710051319 CN200710051319A CN101020860A CN 101020860 A CN101020860 A CN 101020860A CN 200710051319 CN200710051319 CN 200710051319 CN 200710051319 A CN200710051319 A CN 200710051319A CN 101020860 A CN101020860 A CN 101020860A
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China
Prior art keywords
oil
vitamin
golden shaddock
golden
shaddock
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CN 200710051319
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CN101020860B (en
Inventor
刘思强
刘彦
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Liu Siqiang
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Individual
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Publication of CN101020860B publication Critical patent/CN101020860B/en
Expired - Fee Related legal-status Critical Current
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  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Medicinal Preparation (AREA)

Abstract

The anti-senility golden shaddock oil is prepared with gold shaddock peel oil, tea seed oil, corn plumule oil, vitamin A, vitamin E, etc and through mixing, conditioning, filtering, curing and other technological steps. It has the functions of resisting senility, diminishing inflammation, sterilizing, activating skin, improving blood circulation, etc. It may be taken orally and applied externally to reach excellent health effects.

Description

Anti-senility golden shaddock oil
Technical field
The present invention relates to a kind of volatile oil and production method thereof, especially a kind of anti-senility golden shaddock oil.
Background technology
Shaddock has numerous species, as the close shaddock in Fujian, Zhejiang pomelo shaddock, U.S.'s grapefruit.But in these various shaddocks, the unique style of the shatian pomelo in Guangxi, in every autumn, shatian pomelo is ripe, and clinquant shatian pomelo makes us happy, so shatian pomelo also claims golden shaddock.Its epidermis golden yellow of shatian pomelo takes off from tree that to deposit its epidermis of some months harmless, and color and luster is golden always as new, thereby people prefer crying golden shaddock.The gold shaddock can be given a kind of sensation of having good luck of people.The gold shaddock does not make sanitas and handles and can deposit some months even 1 year and without putrefaction really is peculiar.Its oneself is fresh-keeping to be because golden shaddock epidermis has the protection of one deck volatile oil (cortex oil).The volatile oil of golden shaddock being extracted, through Compound Machining, become and be used for the healthy shielding of people, is our hope.Though the essential oil of Xiao Shouing also has multiplely on the market, comprises the essential oil that extracts with flower, plant or fruit,, do not find that also the product that useful shatian pomelo on the market (golden shaddock) carries out the essential oil deep processing sells through investigation.
Summary of the invention
The purpose of this invention is to provide a kind of is main raw material with natural golden shaddock (shaddock) extraction essential oil, and compound again other helps the phytochemicals of HUMAN HEALTH, product innovation---the anti-senility golden shaddock oil that VITAMIN is made.Its role is to: having the effect of antibiotic, anti aging effect, crease-resistant, anti-inflammatory, removing beverage, is the quality products of people's health and beauty.
The present invention is achieved in that
The pure natural golden shaddock oil of grapefruit abstract, molten tea-seed oil, Fructus Maydis oil, vitamin A, the E nutritional drugs of being assigned in is with in the oily liquid, and synergy is a kind of protective foods, health ﹠ beauty products.
1, main raw material:
1. golden shaddock oil.From golden shaddock (shaddock) epidermis, extract and form.
2. Camellia oil.
3. vitamin-E, vitamin A.
4. wetting Agent for Printing Inks.
5. Fructus Maydis oil.
6. antioxidant, sanitas.
2, proportioning raw materials of the present invention (calculating by weight):
Golden shaddock oil (purity 99.8%) 5~1 2 (weight parts)
Tea-seed oil 35~70 (weight part)
Fructus Maydis oil 20~30 (weight part)
Propylene glycol 1.5~2.5 (weight part)
Vitamin A 0.2~0.4 (weight part)
Vitamin-E 0.2~0.6 (weight part)
Antioxidant 0.01 (weight part)
Sanitas 0.1 (weight part)
3, the technological process of production
1. golden shaddock oil extracts flow process
Gold shaddock → cleaning → minute shell → get skin → fragmentation → distillation → separation → filtration → storage → detection → packing
2. complex process flow process
Tea-seed oil, propylene glycol are carried out matrix mix, 50 ℃ of preheatings add golden shaddock oil, Fructus Maydis oil and vitamin A, E, and antioxidant mixes, and conditioning adds sanitas again, filtration, cooling, slaking, finished product, packing.
4, production method
(1) raw material
Golden shaddock oil---golden shaddock especially Guangxi shatian pomelo is not addled indoor the depositing 1 year of normal temperature, and this mainly is because the essential oil of golden shaddock epidermis works.That the essential oil (also claiming volatile oil) of gold shaddock epidermis has is antibiotic, anti-inflammatory, anti-oxidant, aging-resistant manifest function, and this is that other fruit is incomparable.We extract golden shaddock oil as main function raw material of the present invention from shaddock ped, but high density has certain stimulation to skin, and use separately, and function is unilateral, must be composite.
Tea-seed oil---this is the more stable nondrying oil of a kind of performance, tangible skin moisten effect is arranged, and do not hinder skin, does not have pungency, with golden shaddock oil good mutual solubility is arranged, and is as matrix of the present invention, respond well with it.
Semen Maydis oil---be a kind of secondary solvent in the present invention, it can well dissolve vitamin A, E, again can and golden shaddock oil dissolve each other.It can form skim at skin surface again simultaneously, can make essential oil and VITAMIN rest on human epidermal more longways, makes drug effect more lasting, and it can also make skin salubrious, is well auxilliary solvent, skin-protecting agent among the present invention.
Propylene glycol---it act as a kind of wetting Agent for Printing Inks among the present invention, can keep the humidity and the pliability of skin.
Vitamin A---this is a kind of nutrient substance of anti-aging, anti-corneaization of Oil solvent, and the division and the growth of epidermis oil vacuole had tangible regulating effect, and compound with golden shaddock oil can avoid the weakness of its oxidisability, strengthened anti-aging function again.
Vitamin-E---the present invention adds vitamin-E, can promote microvascular blood circulation, strengthens the activity of skin, slows down the aging of skin.Can also prevent and treat pachylosis, macula makes the skin delicacy, and is flexible.Vitamin-E also is anti-aging reinforcing aids in the present invention.
Sanitas employing phenylformic acid among the present invention or propylparaben, ethyl p-hydroxybenzoate.
Antioxidant among the present invention adopts: tertiarybutylhydroquinone (TBHQ), itself and vitamin-E have synergistic function, can reach 3~5 years to the grease provide protection.
(2) production technique
The extraction of a, golden shaddock oil
Golden shaddock oil among the present invention adopts the water vapor rectificating method to extract.That is: after the chopping of golden shaddock (shaddock) skin, put into still pot, outer heating makes a pot interior temperature of charge rise to 85 ℃, under decompression state, water vapor is taken golden shaddock oil out of, after oily water separation, refrigerated separation is separated again after filtration again, and it is standby to extract the golden shaddock oil of concentration more than 99.5%.
100 kilograms of golden shaddock peds, can extract 99.5% essential oil is 0.45kg~0.55kg.
B, production preparation method
After vitamin A, the weighing of E difference, be dissolved in the Fructus Maydis oil of specified amount, standby.
Propylene glycol is dropped in the tea-seed oil, oil is preheated to 50 ℃, drop into golden shaddock oil, Fructus Maydis oil and vitamin A, E again, all raw materials mix in pot, and temperature of charge is risen to 70 ℃, and insulated and stirred stops heating after 10 minutes, again material is cooled to 40 ℃, add sanitas ethyl p-hydroxybenzoate or propylparaben, continue to stir cooling, to 30 ℃ of filtrations, pack.
In whole process for preparation, must controlled temperature, temperature is too high to cause the essential oil loss through volatilization easily, VITAMIN is decomposed destroy, if temperature is low excessively, increases the material denseness again, is unfavorable for that each collision of molecules is fused.Therefore should be strict temperature to be controlled at when the highest be 70 ℃ to whole process of production, and this temperature can sterilization, can not cause VITAMIN to decompose loss again.
In the production process, used container is generally stainless steel or glasswork, and pure to guarantee quality, finished product packing should not be used general Plastic Bottle with aluminium matter bottle formula coloured (brown and blue) glass for well.
Product quality of the present invention is yellow bright liquid, and good fluidity has good penetration.Golden shaddock oil is a volatility piece plate class essential oil faster, but owing to there is the matrix oil of a great deal of to exist and cooperate, has slowed down the evaporation rate of golden shaddock oil.Because the film-forming properties protection of Fructus Maydis oil is arranged, make golden shaddock oil improve the ability of downward infiltration again, help the absorption of skin product.In the process of golden shaddock oil infiltration downwards, vitamin A, E improve the microvascular vigor of skin also along with the activity that excites the skin oil vacuole together, improve the capillary blood vessel circulation.
Anti-aging golden shaddock oil is fit to people's external use, embrocates behind human epidermal, suitably massage, and allows skin that the sensation of heating is arranged, and effect is better.This is because of the skin adstante febre, and the expansion of epidermis pore helps medicine and nutraceutical infiltration, improves the transport capacity of blood.Also help the drainage of human body toxin.
Medicine in the golden shaddock oil in being coated with back and massage process, has the part medicine to come out, by the air admission human body except entering human body by respiratory tract by the skin absorption.Adopt vapor therapy, more can allow the medicine of product of the present invention breathe and enter inside of human body and absorb, improve the volume of blood flow circulation, improve the vigor of brain, got final product in 30 minutes with product 10ml champignon of the present invention by air medium.
Anti-senility golden shaddock oil product of the present invention can also be absorbed by the body by edible.All raw materials are food grade without exception among the present invention, meet national food sanitation standard requirement fully.This product is nontoxic to human body.Because this product is the oily matter that certain fragrance is arranged, can improve the mouthfeel delicious food by mixing cold tea, noodles served with soy sauce, sesame butter, etc. bar, mixing ground rice and be absorbed by the body, strengthen nutritive ingredient.This product also is the another bright spot of resisting the reducing human aging.
Through probationary certificate, product of the present invention all can allow the people dynamic no matter be to take orally or outer clothes, improves spirit, and the effect of desalinating color spot, removing wrinkle, delicate skin is arranged.This product is also having certain effect aspect the body shaping fat-reducing.This product chill of invigorating blood circulation in addition, the effect of anti-flu, this is a kind of product innovation that market outlook are arranged very much.
Embodiment
Embodiment 1
Produce golden shaddock oil
Fresh shaddock skin is cleaned for 200 kilograms, cut, grind to form the pericarp slurry again, divide two batches to drop into still kettle, stirring heating.Temperature is risen to 80 ℃, drive vacuum pump, carry out underpressure distillation, temperature is 80 ℃ in the insulation liquid material, under vacuum attraction, water vapor is brought the essential oil molecule into condensate port, separating opening, after the gas-liquid separation, liquid is separated, after the oily water separation, again the further separating and filtering of golden shaddock oil, get content and reach 99.8% natural proof gold shaddock oil 980 grams, be used for the adapted of following two examples.
Embodiment 2
With tea-seed oil 5000 grams, Fructus Maydis oil 1600 grams, propylene glycol 140 grams, drop into ingredients pot, be heated to 60 ℃ outward, add vitamin A 14 grams, vitamin-E 21 grams, stir after 15 minutes, add antioxidant tertiarybutylhydroquinone 0.7 gram again, after 5 minutes, temperature has risen to 70 ℃, promptly stop heating, be cooled to 50 ℃, add golden shaddock oil 400 grams, when temperature is reduced to 45 ℃, under agitation, add preservative benzoic acid 7 grams and stir after 10 minutes, filter, sampling detects PH, purity, color and luster, taste, proportion, the qualified material temperature is packaged as finished product in the time of 30 ℃, this is routine that finished product 7150 restrains.
Embodiment 3
With tea-seed oil 5800 grams, Fructus Maydis oil 800 grams, propylene glycol 160 grams drop into ingredients pot, be heated to 65 ℃, drop into oxygenant tertiarybutylhydroquinone 0.7 gram, stop heating, drop into vitamin A 28 grams, drop into vitamin-E 42 grams, after temperature reduced to 45 ℃, add golden shaddock oil 600 grams, add propylparaben 7 grams.Filtration is cooled to room temperature, and test package gets product 7400 grams.
More than two kinds of example products, the quality guaranteed period all can reach 3 years.

Claims (2)

1, a kind of anti-senility golden shaddock oil, it is characterized in that: the pure natural golden shaddock oil of grapefruit abstract, molten tea-seed oil, Fructus Maydis oil, vitamin A, the E nutritional drugs of being assigned in is with in the oily liquid, and through mixing, nurse one's health, filtering curing process, synergy is a kind of protective foods, health ﹠ beauty products.
2, anti-senility golden shaddock oil according to claim 1 is characterized in that various proportion of raw materials are:
Golden shaddock oil 5~12 weight parts
Tea-seed oil 35~70 weight parts
Fructus Maydis oil 20~30 weight parts
Propylene glycol 1.5~2.5 weight parts
Vitamin A 0.2~0.4 weight part
Vitamin-E 0.2~0.6 weight part
Antioxidant 0.01 weight part
Sanitas 0.1 weight part
Above-described golden shaddock oil purity is 99.8%.
CN2007100513197A 2007-01-16 2007-01-16 Anti-senility golden shaddock oil Expired - Fee Related CN101020860B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
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CN101020860A true CN101020860A (en) 2007-08-22
CN101020860B CN101020860B (en) 2011-01-05

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101787330A (en) * 2010-03-08 2010-07-28 丽江华利生物开发药业有限公司 Costusroot oil extraction method
CN107019653A (en) * 2017-03-21 2017-08-08 广州雅纯化妆品制造有限公司 A kind of anti-apolexis composition and preparation method thereof
CN107987969A (en) * 2017-11-28 2018-05-04 杨玉祥 A kind of method of fragrant citrus pericarp extraction essential oil
CN108841447A (en) * 2018-06-25 2018-11-20 大埔县通美实业有限公司 A kind of shaddock essential oil and preparation method thereof
CN109303734A (en) * 2018-12-13 2019-02-05 北京天奇益人健康科技有限公司 A kind of perfume Flos Nelumbinis extract and its preparing the application in cosmetics
CN110229718A (en) * 2018-05-04 2019-09-13 南京理工大学 A method of extracting essential oil from orange peel
CN113092405A (en) * 2021-04-08 2021-07-09 晨光生物科技集团股份有限公司 Method for rapidly predicting induction period of vegetable oil under normal temperature condition

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1134230A (en) * 1996-04-03 1996-10-30 临川市油酯化工厂 Nutrient intensified oil and its producing process
CN1530376A (en) * 2003-03-12 2004-09-22 中南大学 Extraction of eight products, such as pectine, naringin, etc.

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101787330A (en) * 2010-03-08 2010-07-28 丽江华利生物开发药业有限公司 Costusroot oil extraction method
CN101787330B (en) * 2010-03-08 2012-11-28 丽江华利生物开发药业有限公司 Costusroot oil extraction method
CN107019653A (en) * 2017-03-21 2017-08-08 广州雅纯化妆品制造有限公司 A kind of anti-apolexis composition and preparation method thereof
CN107987969A (en) * 2017-11-28 2018-05-04 杨玉祥 A kind of method of fragrant citrus pericarp extraction essential oil
CN110229718A (en) * 2018-05-04 2019-09-13 南京理工大学 A method of extracting essential oil from orange peel
CN108841447A (en) * 2018-06-25 2018-11-20 大埔县通美实业有限公司 A kind of shaddock essential oil and preparation method thereof
CN109303734A (en) * 2018-12-13 2019-02-05 北京天奇益人健康科技有限公司 A kind of perfume Flos Nelumbinis extract and its preparing the application in cosmetics
CN113092405A (en) * 2021-04-08 2021-07-09 晨光生物科技集团股份有限公司 Method for rapidly predicting induction period of vegetable oil under normal temperature condition
CN113092405B (en) * 2021-04-08 2023-06-16 晨光生物科技集团股份有限公司 Method for rapidly pre-judging induction period of vegetable oil under normal temperature condition

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Owner name: GUANGXI NANNING JINYOU INDUSTRY CO., LTD.

Free format text: FORMER OWNER: LIU SIQIANG

Effective date: 20110922

C41 Transfer of patent application or patent right or utility model
COR Change of bibliographic data

Free format text: CORRECT: ADDRESS; FROM: 530022 NANNING, GUANGXI ZHUANG AUTONOMOUS REGION TO: 530219 NANNING, GUANGXI ZHUANG AUTONOMOUS REGION

TR01 Transfer of patent right

Effective date of registration: 20110922

Address after: 530219 the Guangxi Zhuang Autonomous Region Nanning City Jinxiang Sha Tin Zone Road No. 97

Patentee after: Guangxi Nanning pomelo Industry Co. Ltd.

Address before: 530022, the Guangxi Zhuang Autonomous Region Nanning garden, Hunan West Road, one mile pharmacy administration dormitory

Patentee before: Liu Siqiang

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20151023

Address after: 530022, the Guangxi Zhuang Autonomous Region Nanning garden, Hunan West Road, one mile pharmacy administration dormitory

Patentee after: Liu Siqiang

Address before: 530219 the Guangxi Zhuang Autonomous Region Nanning City Jinxiang Sha Tin Zone Road No. 97

Patentee before: Guangxi Nanning pomelo Industry Co. Ltd.

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20110105

Termination date: 20190116

CF01 Termination of patent right due to non-payment of annual fee