CN101006849B - Durian extract, preparing process and application thereof - Google Patents

Durian extract, preparing process and application thereof Download PDF

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Publication number
CN101006849B
CN101006849B CN200710003365A CN200710003365A CN101006849B CN 101006849 B CN101006849 B CN 101006849B CN 200710003365 A CN200710003365 A CN 200710003365A CN 200710003365 A CN200710003365 A CN 200710003365A CN 101006849 B CN101006849 B CN 101006849B
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extract
durian
paste
food
durian extract
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CN101006849A (en
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孙步祥
汤凌志
王智慧
唐丽娟
刘健雄
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GUILIN LAIYIN BIOTECHNOLOGY CO Ltd
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GUILIN LAIYIN BIOTECHNOLOGY CO Ltd
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  • Coloring Foods And Improving Nutritive Qualities (AREA)
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Abstract

The invention discloses paste or pulverescent Durio zibethinus extract and its preparation method. The Durio zibethinus extract is prepared by extracting Durio zibethinus flesh with water or lower alcohol such as methanol, ethanol, propanol, isopropanol or butanol; filtering; concentrating to give paste; or further spray-drying to give powder. The obtained paste is yellowish with Baume degree of 25-30 and has special flavor; and the powder is yellow brown, has special flavor, and contains the Durio zibethinus extract more than 80 wt% and protein more than 9.5 wt%. It can be used for preparinghealth food and food, especially fruit juice and baked food.

Description

A kind of durian extract and preparation method thereof and application
Technical field
The present invention relates to a kind of durian extract and preparation method thereof, the invention still further relates to durian extract at health food, field of food, particularly at fruit juice, bake and bank up with earth Application in Food.
Background technology
Durian is the fruit of Bombacaceae aiphyllium durian (Durio zibethinus L.), originates from the torrid areas.Leaf is dense, the blade ellipse, and the top is point; Cyme, pattern is yellowish; Fruit is tied on trunk and branch, ovalize, and pericarp is solid, and close living triangle stings firmly, is yellow or yellow green, each really heavy 1.2--3 kilogram.Durian is the good fruit of high-quality that is renown far and wide, and mature sarcocarp is yellowish, the stickiness succulence, and soft flavor is sweet, and tasting has old cheese and onion flavor.Durian tanginess, special, it is incomparable to smell cacosmia, but the delicious flavour of tasting, aromatic good to eat, sweet as honey is sliding like fat.
Durian contains rich in protein and lipid, contains protein 2.6%, fat 3.4%, and carbohydrate 27.9% also contains vitamin A, C and calcium, potassium, zinc several mineral materials.Calcium, potassium, the zinc content at the pulp of durian and the position that links to each other are high especially, body there is the effect of well taking a tonic or nourishing food to build up one's health, be good fruit type source of nutrition, human body is had the effect of strong help and yin-nourishing and essence-replenishing, the people of frigidity disease or flag is had effect preferably.The special odor of durian has appetizing, promotes the effect of appetite that dietary fiber wherein can also promote enterocinesia, therefore is described as " king in the fruit ".
Though durian is good, and is hot in nature, once can not eat more, because of its abundant nutrition, when can't absorbing fully, stomach can get angry.Though durian is rich in cellulose, it is the meeting imbibition in stomach, too much eats and can block enteron aisle on the contrary, causes constipation; Durian heat content and sugar are higher, and therefore fat personage should eat less, and the glycosuria patient more should not take food; It also contains higher potassium, and ephrosis and heart patient should eat less.
Through patent retrieval, also not having at present to find with the durian is the correlative study report that raw material extracts durian extract.
Summary of the invention
The present invention relates to a kind of durian extract and preparation method thereof, simultaneously, the invention still further relates to durian extract at health food, field of food, particularly at fruit juice, bake and bank up with earth Application in Food.
Durian extract of the present invention is a paste or Powdered, and the durian extract of paste is faint yellow, has the distinctive fragrance of durian, about 25~30 Baume degrees; Pulverous durian extract is a yellowish-brown, has the distinctive fragrance of durian, and wherein the durian extract weight content is more than 80%, and protein content is more than 9.5%.
The durian extract content height that the inventive method is produced, avoided the loss of active component, when keeping durian abundant nutrition composition, removed the high heat of durian, high sugar simultaneously, simultaneously, simplified production technology, shortened the production cycle.
For addressing the above problem, the present invention adopts following technical scheme:
The present invention extracts the method for durian extract from durian, a kind of is to be raw material with durian pulp, extracts, concentrates through extracting solvent, obtains the method for paste durian extract; Perhaps, the paste durian that obtains passes through spray-drying again, obtains the method for Powdered durian extract.
Seed is peeled off, gone to the inventive method with durian earlier before extraction, get durian pulp and extract.
The described extracting method of the inventive method is extracted for heating.
Extracting solvent described in the inventive method is water or low-carbon alcohols.Described low-carbon alcohols is methyl alcohol, ethanol, propyl alcohol, isopropyl alcohol or butanols, and the weight concentration of described low-carbon alcohols is 1%~95%.
Heating in the described extracting method of the inventive method is extracted, extraction time is a key that influences yield and content, and general extraction time is 1~3 time, according to test, take all factors into consideration the utilization rate of extraction equipment usage space and the working substance content of finished product, extraction time is preferably 2 times; The solvent consumption is 5~10 times, and temperature is 40~100 ℃, and extraction time is solvent boiling back 1~3 hour.
Of the present invention temperature is controlled at below 60 ℃ with needing to reclaim the low-carbon alcohols processing behind the low-carbon alcohols extraction durian, and vacuum degree control is more than 0.06Mpa, and the soup and the raw material weight ratio that reclaim low-carbon alcohols should be controlled between 1: 2~5.
Soup after durian extract of the present invention or the recovery low-carbon alcohols, after filtration, it is concentrated then that (vacuum concentrates, temperature is controlled at below 60 degrees centigrade, vacuum 0.06-0.1MPa), be concentrated into about 25~30 Baume degrees, promptly be concentrated into the 1/5-1/3 of original extracting liquid volume, obtain the durian extract of paste.
The durian extract of paste of the present invention passes through spray-drying (160~200 ℃ of intake air temperatures, 80~110 ℃ of air outlet temperature) again, gets Powdered durian extract.
The Powdered durian extract content height that the inventive method is produced, its weight content is more than 80%, has avoided the loss of active component.
Another object of the present invention is to provide the paste that obtains by the bright preparation method of we or pulverous durian extract at health food, field of food, particularly at fruit juice, bake and bank up with earth Application in Food.
The specific embodiment
Embodiment 1
1) pre-treatment: seed is peeled off, gone to durian, get durian pulp and extract.
2) extract: place 8 times of amount deionized waters to extract 2 times durian pulp in 60 ℃, stir frequently in the leaching process, be heated to the boiling back and kept temperature 2 hours, collect and extract feed liquid for the first time, extract the deionized water that adds 5 times of amounts more for the second time, ebuillition of heated insulation 2 hours is collected and is extracted feed liquid for the second time.
3) filter: extract is passed through centrifuge centrifugal filtration.
4) concentrate: it is concentrated to reduce pressure in the extract importing inspissator after will filtering, and temperature is controlled at below 60 degrees centigrade, and vacuum degree control is concentrated into about 25~30 Baume degrees more than 0.06MPa, obtains the durian extract of paste.
Embodiment 2
1) pre-treatment: seed is peeled off, gone to durian, get durian pulp and extract.
2) extract: place 8 times of amount deionized waters to extract 2 times durian pulp in 60 ℃, stir frequently in the leaching process, be heated to the boiling back and kept temperature 2 hours, collect and extract feed liquid for the first time, extract the deionized water that adds 5 times of amounts more for the second time, ebuillition of heated insulation 2 hours is collected and is extracted feed liquid for the second time.
3) filter: extract is passed through centrifuge centrifugal filtration.
4) concentrate: it is concentrated to reduce pressure in the extract importing inspissator after will filtering, and temperature is controlled at below 60 degrees centigrade, and vacuum degree control is concentrated into about 25~30 Baume degrees more than 0.06MPa, obtains the durian extract of paste.
5) spray-drying: the durian extract of paste passes through spray-drying again, 160~200 ℃ of intake air temperatures, and 80~110 ℃ of air outlet temperature get Powdered durian extract.
Embodiment 3
1) pre-treatment: seed is peeled off, gone to durian, get durian pulp and extract.
2) extract: place 10 times of amount 50% ethanol to extract 2 times durian pulp in 60 ℃, stir frequently in the leaching process, be heated to the boiling back and kept temperature 1 hour, collect and extract feed liquid for the first time, extract 50% ethanol that adds 8 times of amounts more for the second time, ebuillition of heated insulation 1 hour is collected and is extracted feed liquid for the second time.
3) reclaim ethanol: will reclaim Ethanol Treatment behind the durian extract, temperature is controlled at below 60 ℃, and vacuum degree control is more than 0.06Mpa, and the soup and the raw material weight ratio that reclaim ethanol should be controlled between 1: 5.]
3) filter: the extract that will reclaim behind the ethanol passes through centrifuge centrifugal filtration.
4) concentrate: it is concentrated to reduce pressure in the extract importing inspissator after will filtering, and temperature is controlled at below 60 degrees centigrade, and vacuum degree control is concentrated into about 25~30 Baume degrees more than 0.06MPa, obtains the durian extract of paste.
5) spray-drying: the durian extract of paste passes through spray-drying again, 160~200 ℃ of intake air temperatures, and 80~110 ℃ of air outlet temperature get Powdered durian extract.
Embodiment 4
1) pre-treatment: seed is peeled off, gone to durian, get durian pulp and extract.
2) extract: place 8 times of amount 60% methyl alcohol to extract 2 times durian pulp in 60 ℃, stir frequently in the leaching process, be heated to the boiling back and kept temperature 1 hour, collect and extract feed liquid for the first time, extract 60% methyl alcohol that adds 5 times of amounts more for the second time, ebuillition of heated insulation 1 hour is collected and is extracted feed liquid for the second time.
3) reclaim methyl alcohol: handle reclaiming methyl alcohol behind the durian extract, temperature is controlled at below 60 ℃, and vacuum degree control is more than 0.06Mpa, and the soup and the raw material weight ratio that reclaim methyl alcohol should be controlled between 1: 4.
4) filter: the extract that will reclaim behind the methyl alcohol passes through centrifuge centrifugal filtration.
5) concentrate: it is concentrated to reduce pressure in the extract importing inspissator after will filtering, and temperature is controlled at below 60 degrees centigrade, and vacuum degree control is concentrated into about 25~30 Baume degrees more than 0.06MPa, obtains the durian extract of paste.
6) spray-drying: the durian extract of paste passes through spray-drying again, 160~200 ℃ of intake air temperatures, and 80~110 ℃ of air outlet temperature get Powdered durian extract.Embodiment 5
1) pre-treatment: seed is peeled off, gone to durian, get durian pulp and extract.
2) extract: place 8 times of amount 70% propyl alcohol to extract 2 times durian pulp in 70 ℃, stir frequently in the leaching process, be heated to the boiling back and kept temperature 1.5 hours, collect and extract feed liquid for the first time, extract 70% propyl alcohol that adds 5 times of amounts more for the second time, ebuillition of heated insulation 1.5 hours is collected and is extracted feed liquid for the second time.
3) reclaim propyl alcohol: handle reclaiming propyl alcohol behind the durian extract, temperature is controlled at below 60 ℃, and vacuum degree control is more than 0.06Mpa, and the soup and the raw material weight ratio that reclaim propyl alcohol should be controlled between 1: 4.
4) filter: the extract that will reclaim behind the propyl alcohol passes through centrifuge centrifugal filtration.
5) concentrate: it is concentrated to reduce pressure in the extract importing inspissator after will filtering, and temperature is controlled at below 60 degrees centigrade, and vacuum degree control is concentrated into about 25~30 Baume degrees more than 0.06MPa, obtains the durian extract of paste.
6) spray-drying: the durian extract of paste passes through spray-drying again, 160~200 ℃ of intake air temperatures, and 80~110 ℃ of air outlet temperature get Powdered durian extract.
Embodiment 6
The blended fruit juice prescription of durian flavor:
Durian extract (paste) 1580kg
Durian extract (Powdered) 728kg
Lichee pulp 208kg
Longan pulp 208kg
Sodium Benzoate 5kg
Embodiment 7
Durian flavor butter jam biscuit prescription:
Superior wheat flour 5.2kg
Butter 2.5kg
Sugar 2.5kg
Egg 2.3kg
Water 1.3kg
Vanilla water 0.1kg
Durian extract (Powdered) 0.1kg

Claims (4)

1. the preparation method of a durian extract, it is characterized in that: with durian pulp is raw material, extracts, filters, concentrates through water or low-carbon alcohols, obtains the paste durian extract.
2. the preparation method of durian extract according to claim 1, it is characterized in that: described low-carbon alcohols is methyl alcohol, ethanol, propyl alcohol, isopropyl alcohol or butanols, the weight concentration of low-carbon alcohols is 1%~95%.
3. the application of the resulting durian extract of preparation method as claimed in claim 1 or 2, it is characterized in that: described durian extract is applied in the field of food.
4. as the application of durian extract as described in the claim 3, it is characterized in that: described durian extract is applied to fruit juice or bakes and banks up with earth in the food.
CN200710003365A 2007-02-06 2007-02-06 Durian extract, preparing process and application thereof Active CN101006849B (en)

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Application Number Priority Date Filing Date Title
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CN101006849B true CN101006849B (en) 2010-05-19

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Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NZ549739A (en) 2006-09-07 2009-01-31 Biovittoria Ltd Sweetening compositions and processes for preparing them
CN103040056A (en) * 2013-01-04 2013-04-17 张建国 Durian fruit juice beverage
CN105918727A (en) * 2016-05-09 2016-09-07 张辉和 Durian and grape fruit juice beverage and preparation method thereof
US11576412B2 (en) 2016-10-24 2023-02-14 Guilin Gfs Monk Fruit Corporation Extracts from fruits of the Cucurbitaceae family, and methods of preparing thereof
CN109757700B (en) * 2019-03-13 2022-07-08 山东天博食品配料有限公司 Durian-flavor essence and preparation method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
梁杰珍.脱水榴莲的启示.广西日 报.2005,第006版. *
阳君.南果水果之王-榴莲.中国果菜 2000年第1期.2000,(2000年第1期),25.
阳君.南果水果之王-榴莲.中国果菜 2000年第1期.2000,(2000年第1期),25. *

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Address after: No. 19 Renmin South Road, Lingui District, Guilin City, Guangxi Zhuang Autonomous Region, 541100

Patentee after: GUILIN LAYN NATURAL INGREDIENTS Corp.

Address before: 541100 Yangtang Industrial Park, Lingui Town, Lingui County, Guilin City, Guangxi Zhuang Autonomous Region

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