CN100999705A - Donkey-hide gelatin polypeptide and production process thereof - Google Patents
Donkey-hide gelatin polypeptide and production process thereof Download PDFInfo
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- CN100999705A CN100999705A CN 200710066613 CN200710066613A CN100999705A CN 100999705 A CN100999705 A CN 100999705A CN 200710066613 CN200710066613 CN 200710066613 CN 200710066613 A CN200710066613 A CN 200710066613A CN 100999705 A CN100999705 A CN 100999705A
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Abstract
The present invention relates to health drink, and is especially donkey-hide gelatin polypeptide wine with easy-to-absorb nutritious components and the health functions of replenishing blood, beautifying, promoting tissue repair and strengthening immunity and its production process. Through biological enzymolysis, donkey-hide gelatin is degraded into peptide and amino acids with higher solubility in wine. The production process of the donkey-hide gelatin polypeptide wine includes the steps of freezing donkey-hide gelatin, crushing, enzymolyzing with papain to form donkey-hide gelatin polypeptide, extracting date, seabuckthorn and wolfberry fruit to obtain extracted liquid, blending, cold storing, precipitating, filtering, packing and sterilizing to obtain donkey-hide gelatin polypeptide wine. The process is suitable for industrial production.
Description
Technical field
The present invention is a kind of health promoting beverage, especially for people's physical efficiency rapid absorption nutritive substance, has the donkey-hide gelatin polypeptide and the production method thereof of the effect of improving the health of enriching blood, improve looks, promote tissue repair, raise immunity.
Background technology
Donkey-hide gelatin is traditional famous and precious invigorant, the enriching yin of enriching blood, moisturizes hemostatic function, is used for that sallow, the dizzy palpitaition of the deficiency of blood, flesh impotence are unable, dysphoria and insomnia, stirring-up of pathogenic wind in the interior resulting from deficiency, xeropulmonary cough, labor are coughed diseases such as spitting of blood, the hematuria of spitting blood, the uterine bleeding of having blood in stool, vaginal bleeding during pregnancy.Traditional instructions of taking of donkey-hide gelatin is with being equipped with rock sugar after the wine molten again through repeatedly taking after the boiling, because of the commodity donkey-hide gelatin becomes bulk very hard, must take long to could be by molten, and need to eat through boiling repeatedly, existing in the market composite donkey-hide gelatin wine product, its production technique is that first water becomes the donkey-hide gelatin slurry to the donkey-hide gelatin molten, again with the grain wine preparation of Chinese medicine extract and 65 °, contain donkey-hide gelatin 0.6-1.5g in per hundred milliliters of wine, the donkey-hide gelatin dose that pharmacopeia is recommended is 3-6g every day, calculate by the maximum concentration of this donkey-hide gelatin wine donkey-hide gelatin and will take 200 milliliters every day and also only can reach the minimum quantity of recommending to take, the main crowd who takes donkey-hide gelatin is the women, and most of women do not have hobby to wine.Taking 200 ml ethanol degree and be 65 ° donkey-hide gelatin wine undertakes to do what is apparently beyond one's ability.Donkey-hide gelatin in the donkey-hide gelatin wine exists with the macromole form of its collagen protein at present, must just can be absorbed after the decomposition through the intestines and stomach enzyme, and utilization ratio is subjected to the influence of biont difference bigger.And the solubleness of donkey-hide gelatin in high wine is limited, separates out easily to produce precipitation, thereby can't improve the concentration of donkey-hide gelatin in wine.
Donkey-hide gelatin is tortured by donkey hide and is formed, its main component is a collagen protein, previous theory thinks that protein enters digestive tube, after resolving into amino acid, GI proteolytic enzyme effect just is absorbed, modern biological metabolism is discovered, human panning protein after gastral plurality of enzymes effect unlike thinking in the past, only absorb with amino acid whose form, more be directly to absorb with the form of hanging down peptide, and the speed that absorbs is faster than the amino acid of same composition, wherein some low peptide can not only provide the human body required nutritive substance that grows, and the important physical function is arranged.
Donkey-hide gelatin belongs to protein substance, mainly form by the macromole of collagen protein, utilize the principle of biological enzymolysis, under appropriate condition, it can be degraded to peptide and amino acid, peptide and the amino acid solubleness in wine is more much bigger than donkey-hide gelatin, can improve the solubleness of donkey-hide gelatin in wine like this, can increase the donkey-hide gelatin ratio in prescription, can directly be absorbed by body because of peptide and amino acid again, can improve the absorption by human body utilization ratio.
Summary of the invention
The objective of the invention is donkey-hide gelatin (collagen protein) is transformed into the peptide and the amino acid of solubility after the proteolytic enzyme effect, increase the solubleness of donkey-hide gelatin in wine, improve the concentration of donkey-hide gelatin in wine, reduce the dose of wine, and the alcoholic strength in the donkey-hide gelatin polypeptide is low, mouthfeel is fragrant and sweet pure and mild good to eat, peptide and amino acid easily are absorbed and used, with traditional donkey-hide gelatin and yellow rice wine, the instructions of taking of rock sugar compatibility is organic, combine dexterously, and have and enrich blood, beauty treatment, promote tissue repair, the effect that many-sides such as raise immunity improve the health, make and be easy to carry the donkey-hide gelatin instant.The polypeptides with donkey hide gelatin wine producing process is simple, can realize suitability for industrialized production, can be welcome by ladies.
The present invention utilizes the principle of biological enzymolysis, under appropriate condition, donkey-hide gelatin is degraded to peptide and amino acid, peptide and the amino acid solubleness in wine is more much bigger than the solubleness of donkey-hide gelatin, can improve the solubleness of donkey-hide gelatin in wine like this, in prescription, increase the donkey-hide gelatin ratio, can directly be absorbed by body because of peptide and amino acid again, can improve the absorption by human body utilization ratio.
The present invention utilizes papoid, and donkey-hide gelatin is hydrolyzed into polypeptide and amino acid, and is formulated with rock sugar or brown sugar and red date, wolfberry fruit, sea-buckthorn extracting solution and shao-hsing rice wine again.Method is: it is freezing that donkey-hide gelatin is put freezer, and through pulverizing, enzymolysis, make polypeptides with donkey hide gelatin liquid, red date, wolfberry fruit, sea-buckthorn are extracted respectively and make extracting solution, mix with rock sugar or brown sugar, yellow rice wine again and blend, through cold storage, precipitation, filter, can, sterilization makes donkey-hide gelatin polypeptide.
Donkey-hide gelatin of the present invention (collagen protein) is transformed into the peptide and the amino acid of solubility after the proteolytic enzyme effect, be increased in the solubleness in the wine, and peptide and amino acid easily are absorbed and used.
Donkey-hide gelatin is through freezing and pulverizing, and with making polypeptides with donkey hide gelatin liquid behind the papain enzymolysis, polypeptides with donkey hide gelatin liquid main component is polypeptide, oxyproline, amino acid, and peptide and amino acid can directly be absorbed by human body, and can improve the absorption by human body utilization ratio.Donkey-hide gelatin polypeptide is the wine base with the yellow rice wine, and alcoholic strength is 8～15 degree, and mouthfeel is fragrant and sweet pure and mild good to eat.
Donkey-hide gelatin polypeptide of the present invention is made in following ratio proportioning:
Donkey-hide gelatin 10-20kg, rock sugar 12-30kg, shao-hsing rice wine 200-400kg, water 40-100kg.
The production method of donkey-hide gelatin polypeptide; carry out block donkey-hide gelatin freezing; be ground into fine particle or powder; powder is dissolved in water; add papain enzymolysis; temperature is controlled at 50 ℃～60 ℃, 10～16 hours time, the polypeptides with donkey hide gelatin liquid that obtains; again rock sugar is added water-solubleization; add in the yellow rice wine with polypeptides with donkey hide gelatin liquid, add 12～16kg donkey-hide gelatin enzymolysis solution in every 300kg yellow rice wine, 15～30kg rock sugar; the wine liquid that obtains is at 4～10 ℃ of deepfreezes; filter, can, sterilization makes the finished product donkey-hide gelatin polypeptide.
The concrete production method of donkey-hide gelatin polypeptide of the present invention comprises the steps:
The donkey-hide gelatin raw material of step 1, finished product all is block, will pulverize earlier for accelerating molten, earlier donkey-hide gelatin is put into freezer a couple of days, to increase brittleness, takes out and pulverizes immediately.
Step 2, with the donkey-hide gelatin powder 12-16kg after smashing, adding water 40-60kg slowly heats in jacketed kettle, and constantly stir, treat to add when temperature is reduced to 55 ℃ after the whole moltens of donkey-hide gelatin papoid 20g, and 50 ℃-60 ℃ of holding temperatures, constantly stir, in time replenish evaporated water, add papoid 20g after 6 hours again, continued enzymolysis 6-10 hour, after enzymolysis finishes, heat up and concentrate quantitatively to 60 liters, put into stainless steel cask Mi Gai and put into freezer, skim surperficial grease (, can save this step) after 24 hours and make polypeptides with donkey hide gelatin liquid as big production donkey-hide gelatin raw material fixed point production from now on because of adding soya-bean oil in the donkey-hide gelatin course of processing.
Step 3, with above-mentioned polypeptides with donkey hide gelatin liquid 60L, add the 15-30kg rock sugar and mix and blend with 300L shao-hsing rice wine (alcoholic strength is 15-18 °), stir in 4 ℃ of-10 ℃ of cold storages of low temperature, then the wine liquid after the cold storage is filtered, can, sterilization, sterilising conditions is (82-85 ℃ of 20-30 ').
Donkey-hide gelatin polypeptide of the present invention and production method thereof, utilize the effect of proteolytic enzyme, donkey-hide gelatin is decomposed into peptide and amino acid, cooperate with rock sugar, yellow rice wine again, kept the traditional habit of the edible compatibility of donkey-hide gelatin dexterously, the donkey-hide gelatin polypeptide of making, solved the problem of donkey-hide gelatin inconvenient eating, polypeptides with donkey hide gelatin content is 4.3% after measured, and hydroxyproline content 388mg/100ml takes 100ml every day and can reach the taking dose that donkey-hide gelatin is recommended.Donkey-hide gelatin polypeptide has solved the problems of dissolution of donkey-hide gelatin in wine, has improved the concentration of donkey-hide gelatin in wine, can reduce the dose of wine, and the alcoholic strength in the donkey-hide gelatin polypeptide has only about the 8-15 degree, and mouthfeel is fragrant and sweet pure and mild good to eat, can be drunk by most of Mies.Donkey-hide gelatin polypeptide have enrich blood, improve looks, promote tissue repair, raise immunity, etc. the multi-faceted effect that improves the health, and production technique is simple, is suitable for suitability for industrialized production.
Description of drawings
Fig. 1 is the production technique schema.
Embodiment
Embodiment 1
Donkey-hide gelatin polypeptide of the present invention is made in following ratio proportioning:
Donkey-hide gelatin 12-16kg, water 40-60kg, rock sugar 15-30kg, Shaoxing rice wine 300kg,
The production method of donkey-hide gelatin polypeptide; carry out block donkey-hide gelatin freezing; be ground into fine particle or powder; powder is dissolved in water; add papain enzymolysis; temperature is controlled at 50 ℃～60 ℃, 10～16 hours time, the polypeptides with donkey hide gelatin liquid that obtains; again rock sugar is added water-solubleization; add in the yellow rice wine with polypeptides with donkey hide gelatin liquid, add 12～16kg donkey-hide gelatin enzymolysis solution in every 300kg yellow rice wine, 15～30kg rock sugar; the wine liquid that obtains is at 4～10 ℃ of deepfreezes; after filtration, can, sterilization makes the finished product donkey-hide gelatin polypeptide.
Concrete production method comprises the steps:
1) block donkey-hide gelatin is carried out freezing, be ground into fine particle or powder;
2) the donkey-hide gelatin powder that obtains is dissolved in water, and adds papain enzymolysis, and temperature is at 50-60 ℃, time 10-16 hour;
3) rock sugar is added water-solubleization;
4) the polypeptides with donkey hide gelatin liquid, the rock sugar liquid that obtain join in the yellow rice wine, in every 300kg yellow rice wine, add 12-16kg donkey-hide gelatin enzymolysis solution 15-30kg rock sugar.
5) the wine liquid that obtains is at 4-10 ℃ of deepfreeze;
6) the wine liquid that obtains carries out Plate Filtration, removes insoluble flocculation material.
7) obtain wine liquid and carry out can.
8) to the bottled wine after the can sterilize (82-85 ℃, 20-30 ')
9) obtain the finished product donkey-hide gelatin polypeptide.
Embodiment 2
Donkey-hide gelatin polypeptide of the present invention is made in following ratio proportioning:
Donkey-hide gelatin 12-20kg, water 40-100kg, brown sugar 15-30kg, red date 15-30kg, shao-hsing rice wine 200-400kg.
The production method of donkey-hide gelatin polypeptide is carried out block donkey-hide gelatin freezing, is ground into fine particle or powder, and powder is dissolved in water, and adds papain enzymolysis, and temperature is controlled at 50 ℃～60 ℃, 10～16 hours time, the polypeptides with donkey hide gelatin liquid that obtains; Brown sugar adds water-solubleization, boils, filters; Red date broken enzymolysis, extraction, filtration, concentrate, make jujube extract; Last three kinds prepare liquid and yellow rice wine and are mixed together and blend, add 15kg donkey-hide gelatin enzymolysis solution in every 350kg yellow rice wine, 20kg brown sugar, jujube extract 20kg.The wine liquid that obtains filters at 4～10 ℃ of deepfreezes, can, and sterilization makes the finished product donkey-hide gelatin polypeptide.
Concrete production method comprises the steps:
1) block donkey-hide gelatin is carried out freezing, be ground into fine particle or powder;
2) the donkey-hide gelatin powder that obtains is dissolved in water, and adds papain enzymolysis, and temperature is at 50-60 ℃, time 10-16 hour; Obtain polypeptides with donkey hide gelatin liquid.
3) red date is cleaned broken polygalacturonase, the cellulase degradation filtering and concentrating of adding, make jujube extract.
4) brown sugar adds water boil and dissolves, filters, and makes red sugar.
5) red sugar, jujube extract, polypeptides with donkey hide gelatin liquid are mixed with yellow rice wine blend.
6) the wine liquid that obtains is at 4-10 ℃ of deepfreeze;
7) the wine liquid that obtains carries out Plate Filtration, removes insoluble flocculation material.
8) obtain wine liquid and carry out can.
9) to the bottled wine after the can sterilize (82-85 ℃, 20-30 ')
10) obtain the finished product donkey-hide gelatin polypeptide.
Embodiment 3
Donkey-hide gelatin polypeptide of the present invention is made in following ratio proportioning:
Donkey-hide gelatin 10-20kg, water 40-100kg, sea-buckthorn 12-30kg, red date 15-25kg, shao-hsing rice wine 200-400kg.
The production method of donkey-hide gelatin polypeptide is carried out block donkey-hide gelatin freezing, is ground into fine particle or powder, and powder is dissolved in water, and adds papain enzymolysis, and temperature is controlled at 50 ℃～60 ℃, 10～16 hours time, the polypeptides with donkey hide gelatin liquid that obtains; Sea-buckthorn adds water boil kept 1 hour, filtered, and got filtrate, and slag is extracting in water 1 hour again, crosses leaching filtrate, united extraction liquid, and thickening filtration makes the sea-buckthorn extracting solution; Red date broken enzymolysis, extraction, filtration, concentrate, make jujube extract; Last three kinds prepare liquid and yellow rice wine and are mixed together and blend, add 18kg donkey-hide gelatin enzymolysis solution in every 350kg yellow rice wine, 15kg sea-buckthorn extracting solution, jujube extract 25kg.The wine liquid that obtains filters at 4～10 ℃ of deepfreezes, can, and sterilization makes the finished product donkey-hide gelatin polypeptide.
Concrete production method comprises the steps:
1) block donkey-hide gelatin is carried out freezing, be ground into fine particle or powder;
2) the donkey-hide gelatin powder that obtains is dissolved in water, and adds papain enzymolysis, and temperature is at 50-60 ℃,
Time 10-16 hour; The polypeptides with donkey hide gelatin liquid that obtains.
3) red date is cleaned broken polygalacturonase, the cellulase degradation filtering and concentrating of adding, make jujube extract.
4) sea-buckthorn adds the water boil extraction, filters, and concentrates and makes the sea-buckthorn extracting solution.
5) sea-buckthorn extracting solution, jujube extract, polypeptides with donkey hide gelatin liquid are mixed with yellow rice wine blend.
6) the wine liquid that obtains is at 4-10 ℃ of deepfreeze;
7) the wine liquid that obtains carries out Plate Filtration, removes insoluble flocculation material.
8) obtain wine liquid and carry out can.
9) to the bottled wine after the can sterilize (82-85 ℃, 20-30 ')
10) obtain the finished product donkey-hide gelatin polypeptide.
Claims (7)
1, a kind of donkey-hide gelatin polypeptide is characterized in that donkey-hide gelatin polypeptide, makes by following prescription:
Donkey-hide gelatin 10-20kg, water 40-100kg, rock sugar 15-30kg, yellow rice wine 200-400kg.
2, a kind of production method of donkey-hide gelatin polypeptide; it is characterized in that carrying out block donkey-hide gelatin freezing; be ground into fine particle or powder; heating for dissolving then; add papain enzymolysis; temperature is controlled at 50 ℃～60 ℃, 10～16 hours time, the polypeptides with donkey hide gelatin liquid that obtains; again rock sugar is added water-solubleization; add in the yellow rice wine with polypeptides with donkey hide gelatin liquid, add 12～16kg donkey-hide gelatin enzymolysis solution in every 300kg yellow rice wine, 15～30kg rock sugar; the wine liquid that obtains is at 4～10 ℃ of deepfreezes; filter, can, sterilization makes the finished product donkey-hide gelatin polypeptide.
3, the production method of donkey-hide gelatin polypeptide according to claim 2 is characterized in that donkey-hide gelatin through freezing and pulverizing, with making polypeptides with donkey hide gelatin liquid behind the papain enzymolysis.
4, the production method of donkey-hide gelatin polypeptide according to claim 3 is characterized in that polypeptides with donkey hide gelatin liquid main component is polypeptide, oxyproline, amino acid.
5, the production method of donkey-hide gelatin polypeptide according to claim 4 is characterized in that polypeptide and amino acid can directly be absorbed by body, and can improve the absorption by human body utilization ratio.
6, donkey-hide gelatin polypeptide according to claim 1 is characterized in that the alcoholic strength in the donkey-hide gelatin wine is 8～15 degree.
7, the production method of donkey-hide gelatin polypeptide according to claim 2 is characterized in that the concrete steps of producing are as follows:
1) block donkey-hide gelatin is carried out freezing, be ground into fine particle or powder;
2) the donkey-hide gelatin powder that obtains is dissolved in water, and adds papain enzymolysis, and temperature is at 50-60 ℃, time 10-16 hour;
3) rock sugar is added water-solubleization;
4) the polypeptides with donkey hide gelatin liquid, the rock sugar liquid that obtain join in the yellow rice wine, in every 300kg yellow rice wine, add 12-16kg donkey-hide gelatin enzymolysis solution 15-30kg rock sugar;
5) the wine liquid that obtains is at 4-10 ℃ of deepfreeze;
6) the wine liquid that obtains carries out Plate Filtration, removes insoluble flocculation material;
7) obtain wine liquid and carry out can;
8) to the bottled wine after the can sterilize (82-85 ℃, 20-30 ');
9) obtain the finished product donkey-hide gelatin polypeptide.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN 200710066613 CN100582214C (en) | 2007-01-05 | 2007-01-05 | Donkey-hide gelatin polypeptide wine and production process thereof |
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| CN 200710066613 CN100582214C (en) | 2007-01-05 | 2007-01-05 | Donkey-hide gelatin polypeptide wine and production process thereof |
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| CN100999705A true CN100999705A (en) | 2007-07-18 |
| CN100582214C CN100582214C (en) | 2010-01-20 |
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| CN102389071A (en) * | 2011-11-10 | 2012-03-28 | 河南辅仁堂制药有限公司 | Donkey-hide gelatin raw powder and its preparation method |
| CN102443509A (en) * | 2010-10-06 | 2012-05-09 | 山东即墨妙府老酒有限公司 | Production method for donkey-hide gelatin wine |
| CN102499376A (en) * | 2011-12-29 | 2012-06-20 | 山东东阿阿胶股份有限公司 | Active small-molecule donkey-hide gelatin mixture and preparation method and application thereof |
| CN103173339A (en) * | 2013-04-22 | 2013-06-26 | 潘惠标 | Donkey-hide gelatin rice wine and preparation method thereof |
| CN103666940A (en) * | 2012-09-06 | 2014-03-26 | 张金荣 | Process for preparing purple sweet potato liquor with biological enzymolysis method |
| CN104130920A (en) * | 2014-07-29 | 2014-11-05 | 安徽陈瑶湖黄酒有限公司 | Method for preparing flavored fruit juice yellow rice wine |
| CN108315177A (en) * | 2018-03-19 | 2018-07-24 | 王海臣 | A kind of medicine-food two-purpose hides careless Tibetan medicine assembled alcoholic drinks and preparation method thereof |
| CN112608809A (en) * | 2020-12-21 | 2021-04-06 | 山东鲁润阿胶药业有限公司 | Donkey-hide gelatin health-care medicinal liquor and preparation process thereof |
| CN113197302A (en) * | 2021-06-01 | 2021-08-03 | 山西振东五和健康科技股份有限公司 | Anti-oxidation and anti-aging instant drinking powder and preparation method thereof |
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| CN100335607C (en) * | 2003-09-08 | 2007-09-05 | 山东东阿酒厂（有限责任公司） | Donkey-hid gelatin wine and production process thereof |
| CN1290574C (en) * | 2004-06-07 | 2006-12-20 | 成都市药友科技发展有限公司 | Injection of donkey hide gelatin and its preparation |
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- 2007-01-05 CN CN 200710066613 patent/CN100582214C/en not_active Expired - Fee Related
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| CN102443509A (en) * | 2010-10-06 | 2012-05-09 | 山东即墨妙府老酒有限公司 | Production method for donkey-hide gelatin wine |
| CN102389071A (en) * | 2011-11-10 | 2012-03-28 | 河南辅仁堂制药有限公司 | Donkey-hide gelatin raw powder and its preparation method |
| CN102389071B (en) * | 2011-11-10 | 2013-03-20 | 河南辅仁堂制药有限公司 | Donkey-hide gelatin raw powder and its preparation method |
| CN102499376A (en) * | 2011-12-29 | 2012-06-20 | 山东东阿阿胶股份有限公司 | Active small-molecule donkey-hide gelatin mixture and preparation method and application thereof |
| CN102499376B (en) * | 2011-12-29 | 2014-08-27 | 山东东阿阿胶股份有限公司 | Active small-molecule donkey-hide gelatin mixture and preparation method and application thereof |
| CN103666940A (en) * | 2012-09-06 | 2014-03-26 | 张金荣 | Process for preparing purple sweet potato liquor with biological enzymolysis method |
| CN103173339B (en) * | 2013-04-22 | 2013-12-11 | 潘惠标 | Donkey-hide gelatin rice wine and preparation method thereof |
| CN103173339A (en) * | 2013-04-22 | 2013-06-26 | 潘惠标 | Donkey-hide gelatin rice wine and preparation method thereof |
| CN104130920A (en) * | 2014-07-29 | 2014-11-05 | 安徽陈瑶湖黄酒有限公司 | Method for preparing flavored fruit juice yellow rice wine |
| CN104130920B (en) * | 2014-07-29 | 2016-01-20 | 安徽陈瑶湖黄酒有限公司 | A kind of making method of local flavor brewing yellow wine with juice |
| CN108315177A (en) * | 2018-03-19 | 2018-07-24 | 王海臣 | A kind of medicine-food two-purpose hides careless Tibetan medicine assembled alcoholic drinks and preparation method thereof |
| CN112608809A (en) * | 2020-12-21 | 2021-04-06 | 山东鲁润阿胶药业有限公司 | Donkey-hide gelatin health-care medicinal liquor and preparation process thereof |
| CN113197302A (en) * | 2021-06-01 | 2021-08-03 | 山西振东五和健康科技股份有限公司 | Anti-oxidation and anti-aging instant drinking powder and preparation method thereof |
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