CN100569934C - Calcium fruit dry red wine complete processing - Google Patents
Calcium fruit dry red wine complete processing Download PDFInfo
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- CN100569934C CN100569934C CNB2006100470159A CN200610047015A CN100569934C CN 100569934 C CN100569934 C CN 100569934C CN B2006100470159 A CNB2006100470159 A CN B2006100470159A CN 200610047015 A CN200610047015 A CN 200610047015A CN 100569934 C CN100569934 C CN 100569934C
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Abstract
The invention discloses a kind of fruit wine drink, particularly relate to and utilize calcium fruit dry red wine complete processing that polygalacturonase is degraded, chitosan is clarified, membrane separation technique is brewageed a kind of new liquor-making raw material and products thereof.It is by calcium fruit, polygalacturonase, H
2SO
3, white sugar, yeast, Preparation of Chitosan form.This calcium fruit dry red wine has color and luster and is orange, and is as clear as crystal, nutritious, unique flavor, and colours of wine and interior quality are good, and liquor quality stability does not produce sedimentary characteristics after the bottling.
Description
Technical field
The present invention relates to a kind of fruit wine drink, particularly relate to and utilize calcium fruit dry red wine complete processing that polygalacturonase is degraded, chitosan is clarified, membrane separation technique is brewageed a kind of new liquor-making raw material and products thereof.
Background technology
Calcium really is a kind of fruit of very suitable processing, can process fruit juice, preserved fruit, jelly, fruit wine, and its local flavor is very unique, and the content of calcium, iron is high, is a kind of new high nutrition of fruit processing industry, the raw material of high health care.
Contain nutritive substances such as abundant sugar, protein, mineral element, VITAMIN and amino acid in the calcium fruits, especially the content of calcium and iron is very high, the content of calcium can reach 60mg/100g in the fresh fruit, and the amount that iron contains reaches 1.5mg/100g (apple is respectively 9mg/100g and 0.24mg/100g).
Contain 17 seed amino acids in the fruit of calcium fruit, total amount reaches 338.3-451.7mg/100g, and wherein the necessary aminoacids content of children growth is up to 102.7-126.6mg/100g, especially Methionin, Xie Ansuan, leucine and isoleucine content are higher, are children and old man's health fruit.Total sugar content is 5.20% in the calcium fruit, reducing sugar 3.38%, organic acid 1.31%, Vc content 6.17 milligrams/100 grams.
Processing really is confined to preserved fruit, dried fruit more and plants benevolence and utilize the aspect to calcium at present, thereby the health fruit of this high nutrition of calcium fruit can not be utilized fully.Therefore, utilize new technology to brewage the calcium fruit dry red wine, be the deep processing of calcium fruit a kind of newly by way of.
Summary of the invention
The present invention provides a kind of calcium fruit dry red wine product of brewageing in order to address the above problem, its color and luster is orange, and is as clear as crystal, nutritious, unique flavor, and colours of wine and interior quality are good, and liquor quality stability does not produce throw out after the bottling.
Another technical problem to be solved by this invention provides a kind of complete processing of calcium fruit dry red wine.
The present invention is on the basis to the traditional fermentation process modification, and depolymerized pectin makes the fermented liquid clarification when utilizing polygalacturonase to improve crushing juice rate; After ageing finishes, use chitosan to improve colours of wine and interior quality as finings; Use the tubular fibre membrane sepn to remove trickle suspended matter and assorted bacterium in the wine, make the wine body more stable in storage.This product has and the similar taste of ice-wine, is orange, and is as clear as crystal, sparkling and crystal-clear pleasing.
Another technical problem to be solved by this invention provides the complete processing of calcium fruit dry red wine.
Be achieved in that in order to solve the problems of the technologies described above the present invention
A kind of calcium fruit dry red wine complete processing, it is to be made by following preparation technology: get the calcium fruits, after the fruit fragmentation, the polygalacturonase that in pulp, adds the 0.1-0.2 ‰ of pulp weight, behind the dissolving mixing, the hot dipping degraded is 1-3 hour under 50-60 ℃ of temperature, the back pulp is pressed extracting juice to degrading, the fruit juice that squeezes is filtered, get clear juice, in clear juice, add the H of 1-2ml/L, 60-80ppm
2SO
3Solution left standstill 1-3 hour, adjusted the fruit juice pol, yeast after adding is adjusted in adjusted fruit juice after the activation of fruit juice weight 1-2 ‰ carries out fermenting and aging to fruit juice under 14-22 ℃ of temperature, the ageing time is 1-3, in traditional aging process wine is carried out clarifying treatment, smart filtering bacterium both got.
Described clarifying treatment is to use chitosan as finings, and the chitosan add-on is the 0.05-0.15 ‰ of fermented juice weight.
Described adjustment pol is: add white sugar in fruit juice, the fruit juice pol is transferred to 22-24%.
Described interpolation yeast is: the syrup that with yeast concentration is 1-3%, 35-40 ℃ earlier soaked 15-20 minute, wherein syrup and zymic mass ratio are 8-12: 1, reduce to then about 25 ℃ and activate 80-100 minute, the zymic addition is for adjusting 1.5 ‰ of back fruit juice weight.
The described polygalacturonase that adds in pulp is 0.12 ‰ of a broken back pulp, and the hot dipping degraded is 2 hours under 55 ℃ of temperature.
Described to the degraded after pulp squeeze separation, gained fruit juice filters with diatomite filter.
Described smart filtering bacterium is: adopt the filtration sterilization of tubular fibre Membrane filtering machine, the tubular fibre fenestra is 0.2-0.5 μ m, and the filter operating pressure is 0.2MPa.
A kind of calcium fruit dry red wine product, it is by calcium fruit, polygalacturonase, H
2SO
3, white sugar, yeast, Preparation of Chitosan form, wherein the addition of polygalacturonase is the 0.1-0.2 ‰ of broken back pulp; H
2SO
3The concentration of solution is 60-80ppm, adds H in clear juice
2SO
3The addition of solution is 1-2ml/L; The additive capacity of white sugar is for to transfer to 22-24% with the fruit juice pol; The zymic addition is for adjusting the 1-2 ‰ of back fruit juice weight; The add-on of chitosan is the 0.05-0.15 ‰ of fermented juice weight.
Above-mentioned its physical and chemical index of calcium fruit dry red wine product is as follows:
| Title | Physical and chemical index |
| Alcoholic strength | 13(％) |
| Pol | 4(g/L) |
| Acidity | 0.56(％) |
| Tannin content | 0.0951(％) |
Advantage of the present invention and effect:
1, calcium really is a kind of fruit of very suitable processing, can process fruit wine, preserved fruit, preserved fruit etc.Sophistication really is processed into dry red wine with calcium, both complied with current people drink turn to brewage, the trend of low, health promoting wine, also can promote plant production development.
2, the raw material calcium fruit of the present invention's employing has rich nutrient contents, and wherein the content of solubility calcium reaches 60mg/100g, and iron level reaches 1.5mg/100g.In addition, contain 17 seed amino acids in the fruit, total amount reaches 338.3-451.7mg/100g.As the dry red wine of raw material brew, nutritious, unique flavor, local flavor and ice-wine are close.
3, the present invention adopts chitosan as finings, and not only clarifying effect is good, and has improved colours of wine and interior quality.
4, the present invention uses the tubular fibre Membrane filtering machine to carry out filtration sterilization, can remove suspended substance and assorted bacterium in the wine, and can make vinosity more stable, does not produce throw out after the bottling.
5, the calcium fruit dry red wine of the present patent application people development has kept the nutrition of calcium fruit.Its color and luster is orange, pure taste, unique flavor.Its main physical and chemical index is as follows: alcoholic strength 12%, pol 4g/L, acidity 0.56%, tannin content 0.0951%.
Further specify beneficial effect of the present invention below in conjunction with testing data:
Above-mentioned its physical and chemical index of calcium fruit dry red wine product is as follows:
| Title | Physical and chemical index |
| Alcoholic strength | 13(％) |
| Pol | 4(g/L) |
| Acidity | 0.56(％) |
| Tannin content | 0.0951(％) |
Calcium fruit dry red wine nutritive ingredient is as follows:
| Title | Physical and chemical index (mg/100g) |
| Protein | 580 |
| Carbohydrate | 160 |
| Calcium | 52 |
| Iron | 1.0 |
| Zinc | 0.06 |
| Magnesium | 0.15 |
| Selenium | 0.01 |
Below in conjunction with embodiment, the present invention is described in further details.
Embodiment
Embodiment one:
Raw material: calcium fruit, polygalacturonase, H
2SO
3, white sugar, yeast, chitosan.
Preparation technology: sophisticated fresh calcium is really extractd carpopodium, branches and leaves, and reject disease and pest, variable color, go bad etc. do not conform to ciruela, cleans up and control water in flowing water, the Oranoleptic indicator: blue or green red grain≤5%, fruit≤5% that rots, inclusion≤3%;
After the fruit fragmentation, in pulp, add the polygalacturonase of pulp weight 0.12 ‰, fully dissolve mixing after, the hot dipping degraded is 2 hours under 55 ℃ of temperature, then the back pulp of degrading is pressed extracting juice, the fruit juice that squeezes is passed through the diatomite filter coarse filtration, get clear juice;
The H that in above-mentioned clear juice, adds 1.5ml/L, 60ppm
2SO
3Solution left standstill 1 hour;
Adjust the fruit juice pol, to adding H
2SO
3Sugaring in the fruit juice behind the solution, used sugar is sucrose, general crystallization white sugar with 98%-99.5%, it is 22.1% more suitable that the fruit juice sugar degree is reached with concentration meter, addition means is for dissolving white sugar earlier in part fruit juice, join then in all the other fruit juice, stirring and evenly mixing makes sugar be distributed in the fruit juice uniformly;
Yeast in adjusted fruit juice after the activation of adding fruit juice weight 1.5 ‰, adding yeast is: the syrup that with yeast concentration is 2%, 35 ℃ earlier soaked 15 minutes, wherein syrup and zymic mass ratio are 8: 1, reduce to then about 25 ℃ and activate 80 minutes, under 15 ℃ of temperature, fruit juice is fermented then, sooner or later use the pol in the concentration meter measurement fermented liquid every day, Primary Fermentation finishes when pol is lower than 2g/L, stop fermentation, make yeast and suspended substance rapid subsidence thereof, leave standstill to separate after 5 days and remove wine mud continuation secondary fermentation;
The fermented liquid Intake Quantity is 95% of a container during secondary fermentation, and temperature is controlled at 20 ℃, and the fermentation bung sealing is installed, and observes every day, when the tranquil secondary fermentation end of liquid level, sealing ageing after diatomite filter filters;
In order to clarify former wine, separate during the fruit wine ageing, prevent that impurity such as wine pin from bring peculiar smell will carry out pouring for former wine and handling with the container bottom throw out.Pouring is for the first time taked open, contacts in a large number with air to impel wine liquid, and the oxidation that helps former wine is removing carbon dioxide gas side by side; Pouring was for the second time carried out in winter; Pouring for the third time is before in May, second; The 4th pouring was 1 year autumn.Whether want the running check wine holding container to fill in the traditional aging process, then should add fullly immediately as discontented, the used wine of freshening the drink, with the former wine in time or the different year wine of same kind, the ageing temperature is controlled at 15 ℃ if should be same quality, same kind, the ageing time is 1 year;
In traditional aging process, wine is carried out clarifying treatment, use chitosan as finings, the chitosan add-on is 0.1 ‰ of a fermented juice weight, defecation method is: the fruit wine of earlier chitosan that will add being put into 10 times of quality soaked 12 hours, pour into then in the container of wine of ageing, mix, after leaving standstill 7 days, adopt the siphon method with precipitate and separate on wine liquid and container bottom and the wall, by the tubular fibre Membrane filtering machine fruit wine is carried out the essence filter at last, the tubular fibre fenestra is 0.4 μ m, and the filter operating pressure is 0.2MPa.
Embodiment two:
Raw material: calcium fruit, polygalacturonase, H
2SO
3, white sugar, yeast, chitosan.
Get the fresh calcium fruit in sophisticated clean back, after the fragmentation of calcium fruits, the polygalacturonase that in pulp, adds broken back pulp weight 0.1 ‰, fully behind the dissolving mixing, the hot dipping degraded is 3 hours under 50 ℃ of temperature, then the back pulp of degrading is pressed extracting juice, the fruit juice that squeezes is passed through filter, get clear juice;
The H that in above-mentioned clear juice, adds 1ml/L, 70ppm
2SO
3Solution left standstill 3 hours;
Adjust the fruit juice pol: to adding H
2SO
3Sugaring in the fruit juice behind the solution transfers to 22% with the fruit juice pol;
Yeast in the fruit juice after adjusting pol after the activation of adding fruit juice weight 1 ‰, adding yeast is: the syrup that with yeast concentration is 3%, 38 ℃ earlier soaked 15 minutes, wherein syrup and zymic mass ratio are 12: 1, reduce to then about 25 ℃ and activate 100 minutes, under 15 ℃ of temperature, fruit juice is fermented then, sooner or later use the pol in the concentration meter measurement fermented liquid every day, Primary Fermentation finishes when pol is lower than 2g/L, stop fermentation, make yeast and suspended substance rapid subsidence thereof, leave standstill to separate after 5 days and remove wine mud continuation secondary fermentation;
The fermented liquid Intake Quantity is 95% of a container during secondary fermentation, and temperature is controlled at 20 ℃, and the fermentation bung sealing is installed, and observes every day, when the tranquil secondary fermentation end of liquid level, and sealing ageing after diatomite filter filters, the ageing time is 1 year;
In traditional aging process, wine is carried out clarifying treatment, use chitosan as finings, the chitosan add-on is 0.15 ‰ of a fermented juice weight, defecation method is: the fruit wine of earlier chitosan that will add being put into 10 times of quality soaked 13 hours, pour into then in the container of wine of ageing, mix, after leaving standstill 5 days, adopt the siphon method with precipitate and separate on wine liquid and container bottom and the wall, by the tubular fibre Membrane filtering machine fruit wine is carried out the essence filter at last, the tubular fibre fenestra is 0.5 μ m, and the filter operating pressure is 0.2MPa.
Embodiment three:
Raw material: calcium fruit, polygalacturonase, H
2SO
3, white sugar, yeast, chitosan.
Get the fresh calcium fruit in sophisticated clean back, after the fragmentation of calcium fruits, the polygalacturonase that in pulp, adds broken back pulp weight 0.2 ‰, fully behind the dissolving mixing, the hot dipping degraded is 1 hour under 60 ℃ of temperature, then the back pulp of degrading is pressed extracting juice, the fruit juice that squeezes is passed through filter, get clear juice;
The H that in above-mentioned clear juice, adds 2ml/L, 80ppm
2SO
3Solution left standstill 1 hour;
Adjust the fruit juice pol: to adding H
2SO
3Sugaring in the fruit juice behind the solution transfers to 24% with the fruit juice pol;
Yeast in the fruit juice after adjusting pol after the activation of adding fruit juice weight 1.5 ‰, adding yeast is: the syrup that with yeast concentration is 3%, 38 ℃ earlier soaked 18 minutes, wherein syrup and zymic mass ratio are 11: 1, reduce to then about 25 ℃ and activate 90 minutes, under 15 ℃ of temperature, fruit juice is fermented then, sooner or later use the pol in the concentration meter measurement fermented liquid every day, Primary Fermentation finishes when pol is lower than 2g/L, stop fermentation, make yeast and suspended substance rapid subsidence thereof, leave standstill to separate after 5 days and remove wine mud continuation secondary fermentation;
The fermented liquid Intake Quantity is 95% of a container during secondary fermentation, and temperature is controlled at 22 ℃, and the fermentation bung sealing is installed, and observes every day, when the tranquil secondary fermentation end of liquid level, and sealing ageing after diatomite filter filters, the ageing time is 2 years;
In traditional aging process, wine is carried out clarifying treatment, use chitosan as finings, the chitosan add-on is 0.15 ‰ of a fermented juice weight, defecation method is: the fruit wine of earlier chitosan that will add being put into 10 times of quality soaked 13 hours, pour into then in the container of wine of ageing, mix, after leaving standstill 5 days, adopt the siphon method with precipitate and separate on wine liquid and container bottom and the wall, by the tubular fibre Membrane filtering machine fruit wine is carried out the essence filter at last, the tubular fibre fenestra is 0.3 μ m, and the filter operating pressure is 0.2MPa.
Embodiment four:
Raw material: calcium fruit, polygalacturonase, H
2SO
3, white sugar, yeast, chitosan.
Preparation technology: sophisticated fresh calcium is really extractd carpopodium, branches and leaves, and reject disease and pest, variable color, go bad etc. do not conform to ciruela, cleans up and control water in flowing water, the Oranoleptic indicator: blue or green red grain≤5%, fruit≤5% that rots, inclusion≤3%;
After the fruit fragmentation, in pulp, add the polygalacturonase of pulp weight 0.15 ‰, fully dissolve mixing after, the hot dipping degraded is 1.5 hours under 53 ℃ of temperature, then the back pulp of degrading is pressed extracting juice, the fruit juice that squeezes is passed through the diatomite filter coarse filtration, get clear juice;
The H that in above-mentioned clear juice, adds 1.8ml/L, 65ppm
2SO
3Solution left standstill 2.2 hours;
Adjust the fruit juice pol, to adding H
2SO
3Sugaring in the fruit juice behind the solution, used sugar is sucrose, general crystallization white sugar with 98%-99.5%, it is 22.5% more suitable that the fruit juice sugar degree is reached with concentration meter, addition means is for dissolving white sugar earlier in part fruit juice, join then in all the other fruit juice, stirring and evenly mixing makes sugar be distributed in the fruit juice uniformly;
Yeast in adjusted fruit juice after the activation of adding fruit juice weight 1.3 ‰, adding yeast is: the syrup that with yeast concentration is 2%, 36 ℃ earlier soaked 17 minutes, wherein syrup and zymic mass ratio are 10: 1, reduce to then about 25 ℃ and activate 90 minutes, under 16 ℃ of temperature, fruit juice is fermented then, sooner or later use the pol in the concentration meter measurement fermented liquid every day, Primary Fermentation finishes when pol is lower than 2g/L, stop fermentation, make yeast and suspended substance rapid subsidence thereof, leave standstill to separate after 6 days and remove wine mud continuation secondary fermentation;
The fermented liquid Intake Quantity is 95% of a container during secondary fermentation, and temperature is controlled at 22 ℃, and the fermentation bung sealing is installed, and observes every day, when the tranquil secondary fermentation end of liquid level, sealing ageing after diatomite filter filters;
In order to clarify former wine, separate during the fruit wine ageing, prevent that impurity such as wine pin from bring peculiar smell will carry out pouring for former wine and handling with the container bottom throw out.Pouring is for the first time taked open, contacts in a large number with air to impel wine liquid, and the oxidation that helps former wine is removing carbon dioxide gas side by side; Pouring was for the second time carried out in winter; Pouring for the third time is before in May, second; The 4th pouring was 1 year autumn.Whether want the running check wine holding container to fill in the traditional aging process, then should add fullly immediately as discontented, the used wine of freshening the drink, with the former wine in time or the different year wine of same kind, the ageing temperature is controlled at 15 ℃ if should be same quality, same kind, the ageing time is 1 year;
In traditional aging process, wine is carried out clarifying treatment, use chitosan as finings, the chitosan add-on is 0.09 ‰ of a fermented juice weight, defecation method is: the fruit wine of earlier chitosan that will add being put into 10 times of quality soaked 12 hours, pour into then in the container of wine of ageing, mix, after leaving standstill 7 days, adopt the siphon method with precipitate and separate on wine liquid and container bottom and the wall, by the tubular fibre Membrane filtering machine fruit wine is carried out the essence filter at last, the tubular fibre fenestra is 0.2 μ m, and the filter operating pressure is 0.2MPa.
Claims (6)
1, a kind of calcium fruit dry red wine complete processing, it is characterized in that getting the calcium fruits, after the fruit fragmentation, the polygalacturonase that in pulp, adds the 0.1-0.2 ‰ of pulp weight, behind the dissolving mixing, the hot dipping degraded is 1-3 hour under 50-60 ℃ of temperature, the back pulp is pressed extracting juice to degrading, the fruit juice that squeezes is filtered, get clear juice, in every liter of clear juice, add the 1-2ml sulfurous acid solution, the concentration of added sulfurous acid solution is 60-80ppm, left standstill 1-3 hour, and adjusted the fruit juice pol, the yeast after adding is adjusted in adjusted fruit juice after the activation of fruit juice weight 1-2 ‰, under 14-22 ℃ of temperature, fruit juice is fermented, the ageing time is 1-3, in traditional aging process wine is carried out clarifying treatment, and smart filtering bacterium had both got product.
2, calcium fruit dry red wine complete processing according to claim 1 is characterized in that described clarifying treatment is to use chitosan as finings, and the chitosan add-on is the 0.05-0.15 ‰ of the weight of fermented juice.
3, calcium fruit dry red wine complete processing according to claim 1 is characterized in that described adjustment pol is: add white sugar in fruit juice, the fruit juice pol is transferred to 22-24%.
4, calcium fruit dry red wine complete processing according to claim 1 is characterized in that the described polygalacturonase that adds is 0.12 ‰ of broken back pulp in pulp, the hot dipping degraded is 2 hours under 55 ℃ of temperature.
5, calcium fruit dry red wine complete processing according to claim 1, it is characterized in that described to the degraded after pulp squeeze separation, gained fruit juice filters with diatomite filter.
6, calcium fruit dry red wine complete processing according to claim 1 is characterized in that described smart filtering bacterium is: adopt the filtration sterilization of tubular fibre Membrane filtering machine, the tubular fibre fenestra is 0.2-0.5 μ m, and the filter operating pressure is 0.2MPa.
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|---|---|---|---|
| CNB2006100470159A CN100569934C (en) | 2006-06-23 | 2006-06-23 | Calcium fruit dry red wine complete processing |
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| CN100569934C true CN100569934C (en) | 2009-12-16 |
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Cited By (1)
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| CN109234096A (en) * | 2018-11-12 | 2019-01-18 | 宁夏西夏王葡萄酒业有限公司 | A kind of Europe Lee grape wine and preparation method thereof |
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| CN101812392A (en) * | 2010-05-06 | 2010-08-25 | 天津蕾傲生物科技有限公司 | Preparation method of calcic fruit ice wine |
| CN103892266A (en) * | 2014-03-18 | 2014-07-02 | 李柏松 | Calcium-supplementing and bone-strengthening shrimp wine and preparation method thereof |
| CN103952256B (en) * | 2014-04-30 | 2015-10-21 | 北京市农林科学院 | A kind of Europe Lee's blueberry wine and preparation method thereof |
| CN104130901B (en) * | 2014-08-06 | 2016-08-24 | 河北科技大学 | Prunus humilis jujube wine and brewing method thereof |
| CN107699410A (en) * | 2017-12-06 | 2018-02-16 | 甘肃农业大学 | A kind of preparation method of calcium fruit modulation wine |
| CN111304041A (en) * | 2020-04-28 | 2020-06-19 | 辽宁省果树科学研究所 | Preparation method of dried apricot white spirit and brandy |
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| 欧李果酒的初步研究. 朱华.酿酒科技，第4期. 2004 |
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| CN109234096A (en) * | 2018-11-12 | 2019-01-18 | 宁夏西夏王葡萄酒业有限公司 | A kind of Europe Lee grape wine and preparation method thereof |
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