CN100566695C - The shampoo composite that contains ozone factors - Google Patents
The shampoo composite that contains ozone factors Download PDFInfo
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- CN100566695C CN100566695C CNB200710135782XA CN200710135782A CN100566695C CN 100566695 C CN100566695 C CN 100566695C CN B200710135782X A CNB200710135782X A CN B200710135782XA CN 200710135782 A CN200710135782 A CN 200710135782A CN 100566695 C CN100566695 C CN 100566695C
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Abstract
The invention discloses a kind of shampoo composite that contains ozone factors, comprise ozone factors and be applicable to acceptable carrier component in the cosmetic of hair, wherein ozone factors accounts for the 0.01%-20% of composition total weight.Shampoo composite of the present invention can deep enoughly moisten and the maintenance skin of head, strengthens the hair conditioning effect, keeps scalp health.The present invention also provides the hair washing method of using the shampoo composite that contains ozone factors to realize scalp care, uses this method can make that hair is plentiful, abundant, elasticity, pitch-black and glossy.
Description
Technical field
The present invention relates to hair shampoo compositions.The invention still further relates to and use shampoo composite of the present invention to realize the hair washing method of scalp care.
Background technology
Healthy scalp is the pillar of hair healthy.The variety of issue that hair occurs, for example dandruff, alopecia, early white etc., all the health status with the head skin has relation.Existing shampoo is to behaviors such as Rinsing that hair carried out, hair cares, all just remedy in fact formula to give hair moist, smooth the hair scale sheet, allow hair not can because of dryly be entangled with, bifurcated or fracture.Want really to solve the problem of impaired hair, allow newborn hair healthy, tough, just must be from scalp maintenance assistant.
Though prior art discloses the multiple shampoo that contains surfactant and rinse additive, disclose a kind of shampoo composite that anti-dandruff efficacy and opsonic action are provided as Chinese patent ZL00809131.5, contained the surfactant of weight about 5% to about 50% in the said composition; Account for the non-volatile conditioner of composition weight about 0.01% to about 10%; Account for the anti-dandruff granule of composition weight about 0.1% to about 4%; Account for the cation melon that derivant of composition weight about 0.02% to about 5%; And water.This patent compositions plays significantly anti-dandruff and conditioning effect, yet is the surface at hair, can not go deep into the scalp maintenance, is not the road that effects a permanent cure.
Studies show that since 20 years old, human body percutaneous partial pressure of oxygen just began to reduce, the percutaneous partial pressure of oxygen reduces the mass exchange that causes between blood plasma and the extracellular fluid to be taken place slowly.Because blood capillary diffusion capacity deficiency, thereby make subcutaneous tissue can only obtain seldom even can not obtain nutrition fully.In this case, if the oxygen continued absence, skin is will be gradually old and feeble and become unhealthy.If show the head skin, will occur shaving one's head, scalp problems such as the dandruff, hair are greasy.
Ozone factors is a known substance, it is a kind of small inclusion enclave that is wrapped in high-load oxygen, with the contact skin process in the depths that can penetrate to the skin, slowly release PFD (artificial blood oxygen carrier raw material), PFD discharges oxygen in skin, PFD then in human body metabolism excrete, oxygen participates in body internal respiration chain reaction, produces the main energy source ATP of cell, improves the Skin Cell vigor, enhance metabolism, accelerate blood circulation.
Though prior art discloses the multiple shampoo that contains surfactant and rinse additive, do not see to disclose or advise in shampoo composite, using ozone factors that the relevant application of ozone factors in shampoo composite do not appear in the newspapers yet.
Summary of the invention
The inventor finds, on the basis of conventional shampoo composite component, add ozone factors and form new shampoo composite, not only can strengthen the opsonic action effect, and deep enough maintenance skin of head of energy and hair, keep scalp health, and then make that hair is plentiful, abundant, elasticity, pitch-black and glossy.
One of the object of the invention provides a kind of new shampoo composite that contains ozone factors, not only can strengthen the hair conditioning effect, and deep enough maintenance skin of head of energy and hair, keeps scalp health.
Another purpose of the present invention provides uses shampoo composite of the present invention to realize the hair washing method of scalp care.
Shampoo composite of the present invention comprises ozone factors and is applicable to acceptable carrier component in the cosmetic of hair.Wherein ozone factors accounts for the 0.01%-20% of composition total weight by weight percentage, preferred 0.05%-10.0%, more preferably 0.2%-8.0%, further preferred 0.5%-5.0%, 2.0%-5.0% most preferably.
The acceptable carrier component comprises surfactant, conditioner, cationic polymer, suspending agent and water in the described cosmetic that is applicable to hair.
Preferred shampoo composite of the present invention, it comprises each component of following percentage by weight:
A), the surfactant of 6%-40%;
B), the ozone factors of 0.05%-10%;
C), the conditioner of 0.05%-10%;
D), the cationic polymer of 0.02%-4.0%;
E), the suspending agent of 0.01%-10.0%; With
F), water;
In addition, shampoo composite of the present invention can also comprise other optional member, comprises that antistatic additive, antioxidant, foam booster, viscosity modifier, thickening agent, PH regulator, antiseptic, pigment, organic solvent or diluent, pearling agent, spice, aliphatic alcohol etc. are known or is effective to additional optional components among hair nursing or the personal care product.
To describe the various compositions of shampoo composite of the present invention below, and also describe various selection compositions and the preferred composition that is applicable in the specific embodiments of the present invention in addition and made concrete qualification.Except as otherwise noted, all percentage ratio and ratio be all with the total weight gained percentage by weight of shampoo composite of the present invention, and described composition is all with the cubage of active ingredient.
A. ozone factors
Normally used ozone factors is an emulsion liquid, can Cerasome Oxygen trade name be buied by Fu Bo company.In the shampoo composite of the present invention, ozone factors accounts for the 0.01%-20% of shampoo composite weight, preferred 0.05%-10.0%, more preferably 0.2%-8.0%, further preferred 0.5%-5.0%, most preferably 2.0%-5.0%.
Ozone factors is a kind of small inclusion enclave that is wrapped in high-load oxygen, and it mainly is made up of following several materials:
1.PerFluorodecalin (PFD), artificial blood oxygen carrier raw material is the most critical composition of artificial blood, can dissolve the pure oxygen (47 milliliters of oxygen of 100 milliliters of PFD solubilized) of high level.
2. oxygen is dissolved among the PFD.
3. natural Jojoba oil disperses PFD, and itself also has skin care effect.
4.Glycosphingolipids the vegetative nerve amide as outer wrap film, forms inclusion enclave, itself also has skin care effect.
Ozone factors is as the active ingredient of shampoo composite of the present invention, and its mechanism to skin of head is as follows:
1. in penetrating to the skin, its nominal particle size can guarantee its depths that can penetrate to the skin;
2. slowly release PFD, PFD discharges oxygen in skin;
3.PFD metabolism goes out external in human body;
4. oxygen participates in body internal respiration chain reaction in skin, produces the main energy source ATP of cell, improves the Skin Cell vigor.
Test shows that ozone factors can improve oxygen concentration in the skin really.Under the assistance of ozone factors conventional carrier component in shampoo composite, not only the oxygen that it provided can quicken the skin of head blood circulation, enhance metabolism, and the natural Jojoba oil that it comprised and vegetative nerve amide can also more careful maintenance head skin, keeps scalp health.
B. surfactant
Contain one or more cosmetics in the shampoo composite of the present invention and go up the cleaning surfactant that acceptable and suitable part is used for hair, surface active agent composition comprises anionic detersive surfactant, zwitterionic surfactant, perhaps their combination; The preferred anionic detersive surfactant.
The 5%-50% (w/w) of surfactant comprise shampoo composite weight described herein, preferred 6%-40% (w/w), more preferably 8%-35% (w/w), further preferred 10%-30% (w/w), most preferably 12%-25% (w/w).
It is following at least a to be applicable to that surfactant in the shampoo composite described herein is selected from: ammonium lauryl sulfate, cocoyl ammonium sulfate, lauryl potassium sulfate, the cocoyl potassium sulfate, sodium lauryl sulfate, cocoyl sodium sulfate, lauryl sulfate monoethanolamine, cocoyl sulphuric acid monoethanolamine, lauryl sulfate diethanolamine, lauryl polyethenoxy ether sodium sulfate, the laureth potassium sulfate, sodium laureth sulfate, laureth sulphuric acid monoethanolamine, laureth sulphuric acid triethanolamine, the N-disodium octadecyl sulfosuccinate; Lauryl disodium sulfosuccinate, sodium lauryl sarcosinate, cocoyl sodium sarcosinate, cocos nucifera oil acyl aminopropyl betanin, lauryl dimethyl betanin, coco dimethyl third sulfobetaines, cocos nucifera oil both sexes carboxyl Glycine sodium, C14-16 sodium olefin sulfonate, lauryl amine oxide, cocamidopropyl amine propyl group amine oxide, alkyl-glucoside.
The preferred ammonium lauryl sulfate of above-mentioned surfactant, laureth sulphuric acid triethanolamine, lauryl polyethenoxy ether sodium sulfate, lauryl sulfate monoethanolamine, cocos nucifera oil acyl aminopropyl betanin, lauryl amine oxide, lauryl disodium sulfosuccinate, most preferably lauryl polyethenoxy ether sodium sulfate, ammonium lauryl sulfate, cocamido propyl betaine.
C. conditioner
Conditioner content accounts for the 0.01%-20.0% (w/w) of shampoo composite weight in the compositions of the present invention, preferred 0.05%-10.0% (w/w), more preferably 0.1%-5.0% (w/w), most preferably 0.2%-4.0% (w/w).Conditioner of the present invention is when being coated on hair, and is non-stimulated, nontoxic or harmless, and can with other component compatibility in the shampoo composite, routine use and condition of storage under chemical property stablize.
Be applicable to that the conditioner in the shampoo composite of the present invention is generally those conditioners or organic conditioning oil of polysiloxanes.The polysiloxanes conditioner can be at least a in polysiloxane oil, cationic silicone, silicone gums, high refractive index polysiloxanes and the polyorganosiloxane resin; Organic conditioning oil can be selected from least a in hydrocarbon ils, polyolefin, the fatty acid ester, as paraffin oils, mineral oil, isostearic acid isopropyl ester, maleic acid Semen Ricini grease, olive oil, Semen Armeniacae Amarum wet goods.These conditioners can use separately, also can compositely use.
A kind of or its combination in the preferred polysiloxanes of above-mentioned conditioner, the maleic acid Semen Ricini grease.Polysiloxanes is those nonvolatile polysiloxanes conditioners preferably.Here " non-volatile " be meant under environmental condition, has very little or do not have the polysiloxanes material of obvious vapour pressure.The viscosity that the polysiloxanes conditioner records under 25 ℃ is 20-5, and 000,000 centistoke is preferably 2,000-4,000,000 centistoke, more preferably 200,000-3,000,000 centistoke, more preferably 500,000-2,000,000 centistoke most preferably is 100,000-1,500,000 centistokes.
The part that comprises the preparation method that polysiloxane fluid, sizing material and resin and polysiloxanes are discussed about the background knowledge of polysiloxanes can be with reference to Encyclopaedia of Polymer Science andEngineering (polymer science and engineering encyclopedia) (the 15th volume, second edition, the 204-308 page or leaf, John Wiley ﹠amp; Sons, Incorporated, 1989).
D. cationic polymer
Shampoo composite of the present invention comprises at least a cationic polymer that is applicable on hair or the skin, these cationic polymers should be compatible on chemical property and physical property with the solvent of shampoo composite, and the stability of infringement product within reason, attractive in appearance or performance.Above-mentioned cationic polymer is preferably water miscible.
Cationic polymer of the present invention accounts for the 0.01%-10.0% (w/w) of shampoo composite gross weight, preferred 0.02%-4.0% (w/w), more preferably 0.05%-3.0% (w/w), most preferably 0.1%-1.0% (w/w).
Be applicable to that cationic polymer of the present invention is selected from least a in following: cation guar gum, polyquaternary ammonium salt-2, polyquaternary ammonium salt-4, polyquaternary ammonium salt-7, polyquaternary ammonium salt-10, polyquaternary ammonium salt-11, Salcare SC60 (ciba company), Salcare SC96 (ciba company).Preferred cationic guar gum, polyquaternary ammonium salt-4, polyquaternary ammonium salt-7, polyquaternary ammonium salt-10.Polyquaternary ammonium salt-10 most preferably.
The mean molecule quantity that is applicable to cationic conditioning polymer of the present invention is 5,000-10, and 000,000, preferred 100,000-2,000,000, more preferably 200,000-1,500,000, more more preferably 250,000-850,000, most preferably 350,000-500,000.Under the pH value that the shampoo composite expection is used, recording polymer cation charge density is that about 0.1meq/g is to about 7meq/g, preferred about 0.2meq/g is to about 5meq/g, more preferably from about 0.5meq/g is to about 2meq/g, more preferably from about 0.6meq/g is to about 1meq/g again, and most preferably from about 0.6meq/g is to about 0.8meq/g.PH value when shampoo composite expection is used is generally about 3 to about 9, is preferably about 4 to about 7.Can use Kjeldahl method (American Pharmacopeia-test chemical-＜461〉N2 method-method II) to determine the cationic charge density of cationic polymer, those skilled in the art can know that charge density changes with pH value and amino isoelectric point, IP.
E. suspending agent
Shampoo composite of the present invention comprises at least a suspending agent that is applicable on hair or the skin, can play water-insoluble dispersive material is suspended in the shampoo composite, these suspending agents should be compatible on physics and chemical property with the basis of compositions, and should excessively not damage the stability of product, attractive in appearance or performance.Above-mentioned suspending agent accounts for shampoo composite gross weight 0.005%-20.0% (w/w), preferred 0.01%-10.0% (w/w), more preferably 0.1%-8.0% (w/w).
Being useful in suspending agent in the shampoo composite of the present invention is selected from following at least a: (with Carbopol SF-1 is trade name for HANSHENGJIAO, acrylate copolymer, buy from NOVEON company), hydroxypropyl cellulose, hydroxypropyl guar gum, polyvinyl pyrrolidone and maleic anhydride-methyl ethylene ether copolymer, preferred HANSHENGJIAO, acrylate copolymer.
F. water
In the shampoo composite of the present invention, except the above composition and other optional auxiliary element, water is supplemented to requirement.
It is following known or be effective at least a among hair nursing or the personal care product to be applicable to that shampoo composite of the present invention can also comprise: antistatic additive, antioxidant, foam booster, viscosity modifier, thickening agent, PH regulator (for example sodium citrate, citric acid, succinic acid, phosphoric acid, sodium hydroxide and sodium carbonate), antiseptic, pigment, organic solvent or diluent, pearling agent, spice, aliphatic alcohol etc.
Above-mentioned antistatic additive can be water-insoluble cationic surfactant, and accounting for composition weight usually is 0.1%-5.0%.Such antistatic additive is answered the serviceability and the final benefit of interference shampoo composite within reason, and especially, antistatic additive is the interference table surface-active agent not.The indefiniteness instantiation of suitable antistatic additive is a quaternary ammonium salt-80.
Described foam booster comprises cocos nucifera oil acyl monoethanolamine, cocos nucifera oil acyl diethanolamine and their mixture.
Described viscosity modifier and thickening agent are used for shampoo composite of the present invention with effective dose ground, regulate suitable overall viscosity, and making overall viscosity is 4,000mPa.s to 13,000mPa.s.The concrete non-limiting example of this viscosity modifier and thickening agent comprises: sodium chloride, ammonium chloride and their mixture.
The present invention adds ozone factors and forms new shampoo composite on the basis of conventional shampoo composite component, each component not only can be goed deep into maintenance skin of head and hair through the new shampoo composite of the proportioning of science, keep scalp health, and can strengthen the opsonic action effect, make that hair is plentiful, abundant, elasticity, pitch-black and glossy.
Shampoo composite of the present invention can by any known or other effectively be applicable to technology preparation of shampoo composite, the method that prepare shampoo composite of the present invention comprises conventional preparation and hybrid technology, specifically preparation method is referring to embodiment.
Shampoo composite of the present invention uses with the usual manner of cleaning and conditioning hair or skin.The compositions that is used to clean and nurse one's health the effective dose of scalp is coated on the hair and the scalp of moistening in advance (normally water), then compositions is rinsed.The effective dose scope is generally about 1 gram to about 50 grams, and preferred about 1 gram is to about 20 grams.Be applied to generally include on the hair compositions is rubbed and smeared in hair and on the scalp, thereby make compositions contact with scalp with hair.
1), water is the hair moistening the invention provides a kind of method of nursing scalp, comprise following step:; 2), the invention described above shampoo composite (2-20 gram) with effective dose is administered on hair and the scalp; 3), water rinsing shampoo composite from the hair.These steps can repeat many times as required, to reach cleaning, conditioning and anti-dandruff efficacy.
The specific embodiment
Following examples can make those skilled in the art more comprehensively understand the present invention, but limit the present invention never in any form.Because without departing from the spirit and scope of the present invention, can carry out many conversion to the present invention.In these embodiments, unless stated otherwise, all concentration all is percentage by weight.Used term " small amount of matter " refers to those optional materials, as antiseptic, viscosity modifier, PH regulator, spice, pigment etc.
Preparation embodiment
It is as follows to prepare the method for shampoo composite (seeing Table 1) in embodiment (I, III, V, VII) and the Comparative Examples (II, IV, VI, VIII) suitably: will about 1/3 join in the blending tank that strap clamp overlaps to whole lauryl polyethenoxy ether sodium sulfate (25%wt solution), under slowly stirring, be heated to about 70 ℃ to 80 ℃, then add cocos nucifera oil acyl monoethanolamine, spermol, glycol distearate, salt (for example ammonium chloride), pH regulator agent (for example citric acid) (if using these materials), these materials are dissolved fully.Polyquaternary ammonium salt-10 is pre-dispersed in the water, obtains about 0.1% to about 10% aqueous solution, with this dispersion liquid and aforesaid mixture mix homogeneously.Cooling gained mixture is collected these mixture in the finished product jar, under agitation adds remaining lauryl polyethenoxy ether sodium sulfate and remaining ingredient, continues to stir, and guarantees to obtain uniform mixture.After adding all components, can add viscosity modifier and pH regulator agent as required, regulate product viscosity and pH value to suitable degree.Randomly can add low amounts of water at last supplies.
The composition of the various shampoo composites of table 1.
Effect embodiment
Effect evaluation method for embodiment is: the shampoo composite of preparation embodiment (I, III, V, VII) and Comparative Examples (II, IV, VI, VIII) is done the contrast test, promptly prepare example I and Comparative Example II and do the contrast test, preparation EXAMPLE III and Comparative Examples I V do the contrast test, preparation EXAMPLE V and Comparative Examples VI do the contrast test, preparation example VII A and Comparative Examples VIII do the contrast test, issue test crowd (each 50 people) contrast respectively and use.
According to identical method hair washing, every kind of shampoo used for two weeks when the tester used the shampoo sample.The people of half uses a kind of shampoo wherein earlier, second half people uses another kind of shampoo earlier, for example, when I and II contrast test sample, 25 people are at the last fortnight I shampoo on probation, two weeks of back are tried out II shampoo, and 25 people are at the last fortnight II shampoo on probation in addition, and two weeks of back are tried out I shampoo.The tester according to oneself feel mark.Standards of grading adopt 7 fens systems, and 1 minute the poorest, and 7 minutes best, and mark is high more good more.
The various shampoo composite results of use of table 2. are estimated
Claims (12)
1. shampoo composite, acceptable carrier component in the cosmetic that it is characterized in that containing ozone factors and being applicable to hair, described ozone factors mainly is made up of PerFluorodecalin, oxygen, natural Jojoba oil, Glycosphingolipids, and described ozone factors accounts for the 0.01%-20% of composition total weight by weight percentage.
2. according to the shampoo composite of claim 1, it is characterized in that ozone factors accounts for the 0.05%-10% of composition total weight by weight percentage.
3. according to the shampoo composite of claim 1 or 2, it comprises each component of following percentage by weight:
A) surfactant of 6%-40%;
B) ozone factors of 0.05%-10%;
C) conditioner of 0.05%-10%;
D) cationic polymer of 0.02%-4.0%;
E) suspending agent of 0.01%-10.0%; With
F) water.
4,, it is characterized in that ozone factors accounts for the 2.0%-5.0% of composition total weight by weight percentage according to the shampoo composite of claim 3.
5,, it is characterized in that described surfactant is anionic detersive surfactant or zwitterionic surfactant or the combination of the two according to the shampoo composite of claim 3.
6,, it is characterized in that described conditioner is at least a in polysiloxane oil, silicone gums and the polyorganosiloxane resin according to the shampoo composite of claim 3.
7,, it is characterized in that described conditioner is at least a in cationic silicone and the high refractive index polysiloxanes according to the shampoo composite of claim 3.
8,, it is characterized in that described cationic polymer is at least a in cation guar gum, polyquaternary ammonium salt-4, polyquaternary ammonium salt-7, the polyquaternary ammonium salt-10 according to the shampoo composite of claim 3.
9,, it is characterized in that described suspending agent is at least a in HANSHENGJIAO, acrylate copolymer, hydroxypropyl cellulose, hydroxypropyl guar gum, polyvinyl pyrrolidone and maleic anhydride-methyl ethylene ether copolymer according to the shampoo composite of claim 3.
10,, it is characterized in that also containing and comprise at least a in antistatic additive, antioxidant, foam booster, viscosity modifier, thickening agent, PH regulator, antiseptic, pigment, organic solvent or diluent, pearling agent, the spice according to the shampoo composite of claim 3.
11,, it is characterized in that also comprising aliphatic alcohol according to the shampoo composite of claim 3.
12, a kind of method of nursing scalp, it may further comprise the steps:
1), uses the water-wet hair;
2), on hair, use effective use amount as each described shampoo composite of claim 1-9, in hair and on the scalp, rub and smear; With
3), with the described shampoo composite on the water rinse hair.
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| CNB200710135782XA CN100566695C (en) | 2007-08-16 | 2007-08-16 | The shampoo composite that contains ozone factors |
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| CNB200710135782XA CN100566695C (en) | 2007-08-16 | 2007-08-16 | The shampoo composite that contains ozone factors |
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| CN100566695C true CN100566695C (en) | 2009-12-09 |
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