CN100557287C - A kind of production method of large caliber ultra-long rubber plastic composite hose for oil extraction - Google Patents
A kind of production method of large caliber ultra-long rubber plastic composite hose for oil extraction Download PDFInfo
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- CN100557287C CN100557287C CNB2008100113201A CN200810011320A CN100557287C CN 100557287 C CN100557287 C CN 100557287C CN B2008100113201 A CNB2008100113201 A CN B2008100113201A CN 200810011320 A CN200810011320 A CN 200810011320A CN 100557287 C CN100557287 C CN 100557287C
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Abstract
A kind of production method of large caliber ultra-long rubber plastic composite hose for oil extraction; belong to rubber and plastic flexible pipe forming field; it is little only to produce bore at present forming technique; the rubber plastic pipe that length is short; deficiency such as can not on the oil field, use; a kind of heavy caliber is disclosed; overlength; rubber and plastic composite pipe and production method thereof, this pipe are to be provided with cushioned layer, first successively at rubber and plastic alloy hose surface upper edge radial direction; second enhancement layer and rubber and plastic external protection; for increasing cohesion; each interlayer is provided with the rubber and plastic alloy glue bed of material, and the production method of this pipe comprises preparation rubber and plastic alloy sizing material, and centreless is extruded; manufacture cushioned layer; first; two enhancement layers and external protection vulcanize and suppress inspection step, products obtained therefrom bore 30~50mm; long 800m~2000m; high-strength; anti-corrosion; non-joint, energy paraffin removal wax control is suitable for the oil field and uses.
Description
Technical field
The invention belongs to the rubber plastic composite hose forming field, is the production method about large caliber ultra-long rubber plastic composite hose for oil extraction furtherly.
Background technique
At present, recovering the oil with petroleum pipeline all is metal tubes, by well depth metal tube one is connected together by movable joint successively, because metal tube is very heavy, wax easy to hang often needs maintenance, and labor intensity is big, influences the lifting service life of equipment.For overcoming the shortcoming on the prior art, people proposed to replace with the rubber and plastic flexible pipe, the production method of producing this nonmetallic pipe is at first to select materials, determine the finished product internal diameter, adopt corresponding core rod, wrap one deck light film glue on core rod, bag is established ply of paper one by one again, glue-line, sheet lead layer or plastic layer or water layer of cloth enter sulfurizing pot vulcanization, the cooling of sulfuration back, the demoulding, this traditional production method is only applicable to produce the rubber hose of the following length of 40m, can't produce large caliber ultra-long rubber plastic composite hose, and this tube-surface does not have reinforced layer and zone of heating, therefore, also do not satisfy the anti-technical requirements of hanging wax of oil field needs large caliber ultra-long far away.
Summary of the invention
At the deficiencies in the prior art part; the invention provides a kind of structural feature is heavy caliber, the overlength that is coated with zone of heating, first reinforced layer, second reinforced layer and rubber and plastic external protection on the rubber and plastic hose surface successively; compound; anti-wax deposition; pipe thickness is even; not damaged, the rubber plastic composite hose that tensile strength is big and the production method of this pipe thereof.
The technical solution adopted for the present invention to solve the technical problems is:
Rubber and plastic alloy hose surface upper edge radial direction is provided with zone of heating successively, first reinforced layer, and second reinforced layer and rubber and plastic external protection, each interlayer is equipped with the rubber and plastic alloy glue bed of material.
Zone of heating is a kind of silicone rubber plate, is provided with electric heating element in it, and this part is electrically-heated-wire or electric heating piece, and an end is electrically connected, and forms single-phase circuit or three-phase circuit and links to each other with power supply.
First reinforced layer and second reinforced layer are copper facing high tensile wire stratum reticulares, mesh wire diameter 0.35~0.6mm, open weave angle 40~70 degree.
Rubber plastic composite hose internal diameter 30mm to 50mm, pipe range 800~2000m.
The production method of this pipe comprises that following process step carries out:
1, preparation rubber and plastic alloy sizing material step, this step 1 is by basic use level, measures according to unit of mass, get: 5075 rubber and plastic alloys 100~110 of day local terminal father-in-law rubber Co., Ltd. product, ZnO zine oxide 5~5.5, SA stearic acid 1~1.5, PW paraffin 1~1.5, RD age resister 1~1.5, BLE age resister 3~4, white carbon 10~12, N330 carbon black 35~40, N550 carbon black 35~40, precipitated calcium carbonate 30~35, AS-88 tackiness agent 3~4, DOP dioctyl phthalate 10~12, solid coumarone 3~4, TMTD promoter 1.5~2, CZ promoter 2~3, S Cosan 0.5~1 is mixed, the 75 liters of pressurization banburies of packing into, carry out banburying 10~14min, treat that the banburying temperature reaches 120~140 ℃, binder removal is then put into the XK-560 mill and is cooled off slitting, filter with 40 * 60 order steel meshes, weighing is put into mill and is added sulphur, and cooling keeps flat, change extrusion step over to
2, adopt extruder, when the rubber and plastic alloy sizing material that step 1 is made waits to be warmed up to 90~120 ℃ of temperature, extrude the rubber and plastic alloy flexible pipe continuously, the cooling hub disk is on the sulfuration cylinder, spray into a small amount of French chalk that plays buffer action in the pipe, in vulcanizing chamber, carry out semi-cure, 140 ℃~160 ℃ of sulfurize temperatures, cure time 15~30min changes over to after the end and twines the zone of heating making step;
3, select the Manufactured silicone rubber plate that has electric heating element for use, produce zone of heating as take-up strap, the rubber and plastic alloy flexible pipe that elder generation makes step 2, fill the compression air, pressure is 0.3~0.5MPa, and coating a bed thickness again on tube outer surface is the rubber and plastic alloy glue bed of material of 0.3~0.8mm, and to this tube outer surface by 20~60 degree lift angles with take-up strap around solid on it, take-up strap end at the whole story is reserved connector lug, changes the reinforced layer making step after the end over to;
4, utilize wire knitting machine having on the rubber and plastic alloy flexible pipe outer surface of zone of heating, carry out the centreless braided steel wire, make reinforced layer, coating a bed thickness earlier on tube outer surface is the rubber and plastic alloy glue bed of material of 0.5~0.7mm, tube outer surface to present structural form weaves copper facing Strong Steel silk screen layer as first reinforced layer again, coating a bed thickness on this basis again is 0.3~0.8mm rubber and plastic alloy glue bed of material, braiding copper facing Strong Steel silk screen layer changes the external protection making step over to as second reinforced layer on tube outer surface again;
5, step 4 is made the rubber and plastic alloy hose surface with reinforced layer and made external protection, at first coating a layer thickness is the rubber and plastic alloy glue bed of material of 0.3~0.5mm, glue-line or plastic layer or water layer of cloth outside coating on extruder again;
6, step 5 is made the rubber and plastic alloy flexible pipe with external protection and vulcanized continuously, sulfurize temperature is 140~160 ℃, and cure time 50~70min finally obtains large caliber ultra-long rubber plastic composite hose for oil extraction, changes over to after the end and suppresses the quality inspection step;
7, the large caliber ultra-long rubber plastic composite hose for oil extraction that step 6 is finally made is suppressed 20~40Mpa and is stopped 10min, observe do not leak, indeformable, qualified packing warehouse-in.
The invention has the beneficial effects as follows: the product bore is big, overlength, and the rubber hose pipe thickness is even, not damaged, tensile strength is big, and method is simple, easily operation.
Description of drawings
Fig. 1 is the product sectional schematic diagram that the present invention makes;
Fig. 2 is an electric heating element structural representation among Fig. 1;
Among the figure: 1 rubber and plastic flexible pipe, 2 zones of heating, 3 first reinforced layers, 4 second reinforced layers, 5 rubber and plastic external protections, 6 silicone rubber plates, 7 electric heating elements.
Embodiment
Further advance to describe large caliber ultra-long rubber plastic composite hose for oil extraction and production method thereof with reference to accompanying drawing.
Example 1:
Rubber and plastic alloy hose surface upper edge radial direction is provided with zone of heating successively, first reinforced layer, and second reinforced layer and rubber and plastic external protection, each interlayer is equipped with the rubber and plastic alloy glue bed of material.Zone of heating is a kind of silicone rubber plate, is provided with electric heating element in it, and this part is electrically-heated-wire or electric heating piece, and an end is electrically connected, and forms single-phase circuit or three-phase circuit and links to each other with power supply.First enhancement layer and second enhancement layer are copper facing high tensile wire stratum reticulares, mesh wire diameter 0.35mm, open weave angle 40 degree.Rubber plastic composite hose internal diameter 30mm, pipe range 800m.The preparation method of this pipe may further comprise the steps:
1, preparation rubber and plastic alloy sizing material step, this step 1 is by basic use level, measures according to unit of mass, get: 5075 rubber and plastic alloys 100 of day local terminal father-in-law rubber Co., Ltd. product, ZnO zine oxide 5, SA stearic acid 1, PW paraffin 1, RD age resister 1, BLE age resister 3, white carbon 10, N330 carbon black 35, N550 carbon black 35, precipitated calcium carbonate 30, AS-88 tackiness agent 3, DOP dioctyl phthalate 10, coumarone (solid) 3, TMTD promoter 1.5, CZ promoter 2, S Cosan 0.5 is mixed, the 75 liters of pressurization banburies of packing into, carry out banburying 10min, treat that the banburying temperature reaches 120 ℃, binder removal is then put into the XK-560 mill and is cooled off slitting, filter with 40 * 60 order steel meshes, weighing is put into mill and is added sulphur, and cooling keeps flat, change extrusion step over to
2, adopt extruder, when the rubber and plastic alloy sizing material that step 1 is made waits to be warmed up to 90 ℃ of temperature, extrude the rubber and plastic alloy flexible pipe continuously, the cooling hub disk is on the sulfuration cylinder, spray into a small amount of French chalk that plays buffer action in the pipe, in vulcanizing chamber, carry out semi-cure, 140 ℃ of sulfurize temperatures, cure time 15min changes over to after the end and twines the zone of heating making step;
3, select the Manufactured silicone rubber plate that has electric heating element for use, produce zone of heating as take-up strap, the rubber and plastic alloy flexible pipe that elder generation makes step 2, fill the compression air, pressure is 0.3MPa, is the rubber and plastic alloy glue bed of material of 0.3mm to coating a bed thickness on the tube outer surface again, again in the case, to this tube-surface by 20 degree lift angles with take-up strap around solid on it, take-up strap end at the whole story is reserved connector lug, changes the reinforced layer making step after the end over to;
4, on having the rubber and plastic alloy hose surface of zone of heating, it utilizes wire knitting machine, it is carried out the centreless braided steel wire, make reinforced layer, earlier coating one bed thickness being gone up on its surface is the rubber and plastic alloy glue bed of material of 0.5mm, tube-surface to present structural form weaves copper facing Strong Steel silk screen layer as first reinforced layer again, coating a bed thickness on this basis again is the 0.3mm rubber and plastic alloy glue bed of material, braiding copper facing Strong Steel silk screen layer changes the external protection making step over to as second reinforced layer on its pipe table again;
5, step 4 is made the rubber and plastic alloy hose surface with reinforced layer and made external protection, at first coating a layer thickness is the rubber and plastic alloy glue bed of material of 0.3mm, glue-line or plastic layer or water layer of cloth outside coating on extruder again;
6, step 5 is made rubber and plastic alloy flexible pipe and vulcanized continuously with external protection, 140 ℃ of its sulfurize temperatures, cure time 50min finally obtains large caliber ultra-long rubber plastic composite hose for oil extraction, changes over to after the end to suppress the quality inspection step;
7, the large caliber ultra-long rubber plastic composite hose for oil extraction that step 6 is finally made is suppressed 20Mpa and is stopped 10min, observe do not leak, indeformable, qualified packing warehouse-in.
Example 2:
Rubber plastic composite hose surface composite layer structure is identical with example 1, and wherein zone of heating is a silicone rubber plate, is provided with electric heating piece in it, one end is electrically connected, and forms three-phase circuit and links to each other with power supply, and first enhancement layer, second enhancement layer are copper facing high tensile wire stratum reticulares, mesh wire diameter 0.4mm, open weave angle 60 degree.Rubber plastic composite hose internal diameter 40mm, pipe range 1500m.The preparation method of this pipe may further comprise the steps:
1, preparation rubber and plastic alloy sizing material step, this step 1 is by basic use level, according to the unit of mass metering, gets:
5075 rubber and plastic alloys 105 that day local terminal father-in-law rubber Co., Ltd. produces, ZnO zine oxide 5.2, SA stearic acid 1.2, PW paraffin 1.3, RD age resister 1.3, BLE age resister 3.5, white carbon 11, N330 carbon black 38, N550 carbon black 38, precipitated calcium carbonate 32, AS-88 tackiness agent 3.5, DOP dioctyl phthalate 11, coumarone (solid) 3.5, TMTD promoter 1.8, CZ promoter 2.5, S Cosan 0.8 is mixed, the 75 liters of pressurization banburies of packing into, carry out banburying 13min, treat that the banburying temperature reaches 130 ℃, binder removal, then put into the XK-560 mill and cool off bar down, filter with 40 * 60 order steel meshes, weighing is put into mill and is added sulphur, cooling keeps flat, and changes extrusion step over to;
2, adopt extruder, when the rubber and plastic alloy sizing material that step 1 is made waits to be warmed up to 100 ℃ of temperature, extrude the rubber and plastic alloy flexible pipe continuously, the cooling hub disk is on the sulfuration cylinder, spray into a small amount of French chalk that plays buffer action in the pipe, in vulcanizing chamber, carry out semi-cure, 150 ℃ of sulfurize temperatures, cure time 20min changes over to after the end and twines the zone of heating making step;
3, select the Manufactured silicone rubber plate that has electric heating element for use, produce zone of heating as take-up strap, the rubber and plastic alloy flexible pipe that elder generation makes step 2, fill the compression air, pressure is 0.4MPa, is the rubber and plastic alloy glue bed of material of 0.5mm to coating a bed thickness on the tube outer surface again, again in the case, to this tube-surface by 40 degree lift angles with take-up strap around solid on it, take-up strap end at the whole story is reserved connector lug, changes the reinforced layer making step after the end over to;
4, on having the rubber and plastic alloy hose surface of zone of heating, it utilizes wire knitting machine, it is carried out the centreless braided steel wire, make reinforced layer, earlier coating one bed thickness being gone up on its surface is the rubber and plastic alloy glue bed of material of 0.6mm, tube-surface to present structural form weaves copper facing Strong Steel silk screen layer as first reinforced layer again, coating a bed thickness on this basis again is the 0.5mm rubber and plastic alloy glue bed of material, braiding copper facing Strong Steel silk screen layer changes the external protection making step over to as second reinforced layer on its pipe table again;
5, step 4 is made the rubber and plastic alloy hose surface with reinforced layer and made external protection, at first coating a layer thickness is the rubber and plastic alloy glue bed of material of 0.4mm, glue-line or plastic layer or water layer of cloth outside coating on extruder again;
6, step 5 is made rubber and plastic alloy flexible pipe and vulcanized continuously with external protection, 150 ℃ of its sulfurize temperatures, cure time 60min finally obtains large caliber ultra-long rubber plastic composite hose for oil extraction, changes over to after the end to suppress the quality inspection step;
7, the large caliber ultra-long rubber plastic composite hose for oil extraction that step 6 is finally made is suppressed 30Mpa and is stopped 10min, observe do not leak, indeformable, qualified packing warehouse-in.
Example 3:
Rubber plastic composite hose surface composite layer structure is identical with example 1, and wherein zone of heating is a silicone rubber plate, is provided with electric heating wire in it, one end is electrically connected, and forms three-phase circuit and links to each other with power supply, and first enhancement layer, second enhancement layer are copper facing high tensile wire stratum reticulares, mesh wire diameter 0.6mm, open weave angle 70 degree.Rubber plastic composite hose internal diameter 50mm, pipe range 2000m.The preparation method of this pipe may further comprise the steps:
1, preparation rubber and plastic alloy sizing material, by basic use level,, get according to the unit of mass metering:
5075 rubber and plastic alloys 110 that day local terminal father-in-law rubber Co., Ltd. produces, ZnO zine oxide 5.5, SA stearic acid 1.5, PW paraffin 1.5, RD age resister 1.5, BLE age resister 4, white carbon 12, N330 carbon black 40, N550 carbon black 40, precipitated calcium carbonate 35, AS-88 tackiness agent 4, DOP dioctyl phthalate 12, coumarone (solid) 4, TMTD promoter 2, CZ promoter 3, S Cosan 1 is mixed, the 75 liters of pressurization banburies of packing into, carry out banburying 14min, treat that the banburying temperature reaches 140 ℃, binder removal, then put into the XK-560 mill and cool off bar down, filter with 40 * 60 order steel meshes, weighing is put into mill and is added sulphur, cooling keeps flat, and changes extrusion step over to;
2, adopt extruder, when the rubber and plastic alloy sizing material that step 1 is made waits to be warmed up to 120 ℃ of temperature, extrude the rubber and plastic alloy flexible pipe continuously, the cooling hub disk is on the sulfuration cylinder, spray into a small amount of French chalk that plays buffer action in the pipe, in vulcanizing chamber, carry out semi-cure, 160 ℃ of sulfurize temperatures, cure time 30min changes over to after the end and twines the zone of heating making step;
3, select the Manufactured silicone rubber plate that has electric heating element for use, produce zone of heating as take-up strap, the rubber and plastic alloy flexible pipe that elder generation makes step 2, fill the compression air, pressure is 0.5MPa, is the rubber and plastic alloy glue bed of material of 0.8mm to coating a bed thickness on the tube outer surface again, again in the case, to this tube-surface by 60 degree lift angles with take-up strap around solid on it, take-up strap end at the whole story is reserved connector lug, changes the reinforced layer making step after the end over to;
4, on having the rubber and plastic alloy hose surface of zone of heating, it utilizes wire knitting machine, it is carried out the centreless braided steel wire, make reinforced layer, earlier coating one bed thickness being gone up on its surface is the rubber and plastic alloy glue bed of material of 0.7mm, tube-surface to present structural form weaves copper facing Strong Steel silk screen layer as first reinforced layer again, coating a bed thickness on this basis again is the 0.8mm rubber and plastic alloy glue bed of material, braiding copper facing Strong Steel silk screen layer changes the external protection making step over to as second reinforced layer on its pipe table again;
5, step 4 is made the rubber and plastic alloy hose surface with reinforced layer and made external protection, at first coating a layer thickness is the rubber and plastic alloy glue bed of material of 0.5mm, glue-line or plastic layer or water layer of cloth outside coating on extruder again;
6, step 5 is made rubber and plastic alloy flexible pipe and vulcanized continuously with external protection, 160 ℃ of its sulfurize temperatures, cure time 70min finally obtains large caliber ultra-long rubber plastic composite hose for oil extraction, changes over to after the end to suppress the quality inspection step;
7, the large caliber ultra-long rubber plastic composite hose for oil extraction that step 6 is finally made is suppressed 40Mpa and is stopped 10min, observe do not leak, indeformable, qualified packing warehouse-in.
Claims (3)
1, a kind of production method of large caliber ultra-long rubber plastic composite hose for oil extraction is characterized in that comprising following process step:
Step 1, preparation rubber and plastic alloy sizing material is by basic use level, measures according to unit of mass, get: 5075 rubber and plastic alloys 100~110 of day local terminal father-in-law rubber Co., Ltd. product, ZnO zine oxide 5~5.5, SA stearic acid 1~1.5, PW paraffin 1~1.5, RD age resister 1~1.5, BLE age resister 3~4, white carbon 10~12, N330 carbon black 35~40, N550 carbon black 35~40, precipitated calcium carbonate 30~35, AS-88 tackiness agent 3~4, DOP dioctyl phthalate 10~12, solid coumarone 3~4, TMTD promoter 1.5~2, CZ promoter 2~3, S Cosan 0.5~1, be mixed, the 75 liters of pressurization banburies of packing into carry out banburying 10~14min, treat that the banburying temperature reaches 120~140 ℃, binder removal is then put into the XK-560 mill and is cooled off slitting, filters with 40 * 60 order steel meshes, weighing, put into mill and add sulphur, cooling keeps flat, and changes extrusion step over to;
Step 2, employing extruder, when the rubber and plastic alloy sizing material that step 1 is made waits to be warmed up to 90~120 ℃ of temperature, extrude the rubber and plastic alloy flexible pipe continuously, the cooling hub disk is on the sulfuration cylinder, spray into a small amount of French chalk that plays buffer action in the pipe, in vulcanizing chamber, carry out semi-cure, 140 ℃~160 ℃ of sulfurize temperatures, cure time 15~30min changes over to after the end and twines the zone of heating making step;
Step 3, select the Manufactured silicone rubber plate that has electric heating element for use, produce zone of heating as take-up strap, the rubber and plastic alloy flexible pipe that elder generation makes step 2, fill the compression air, pressure is 0.3~0.5MPa, and coating a bed thickness again on tube outer surface is the rubber and plastic alloy glue bed of material of 0.3~0.8mm, and to this tube outer surface by 20~60 degree lift angles with take-up strap around solid on it, take-up strap end at the whole story is reserved connector lug, changes the reinforced layer making step after the end over to;
Step 4, utilize wire knitting machine having on the rubber and plastic alloy flexible pipe outer surface of zone of heating, it is carried out the centreless braided steel wire, make reinforced layer, coating a bed thickness earlier on tube outer surface is the rubber and plastic alloy glue bed of material of 0.5~0.7mm, tube outer surface to present structural form weaves copper facing Strong Steel silk screen layer as first reinforced layer again, coating a bed thickness on this basis again is 0.3~0.8mm rubber and plastic alloy glue bed of material, braiding copper facing Strong Steel silk screen layer changes the external protection making step over to as second reinforced layer on tube outer surface again;
Step 5, step 4 is made the rubber and plastic alloy flexible pipe outer surface with reinforced layer make external protection, at first coating a layer thickness is the rubber and plastic alloy glue bed of material of 0.3~0.5mm, glue-line or plastic layer or water layer of cloth outside coating on extruder again;
Step 6, step 5 is made the rubber and plastic alloy flexible pipe with external protection vulcanize continuously, sulfurize temperature is 140~160 ℃, and cure time 50~70min finally obtains large caliber ultra-long rubber plastic composite hose for oil extraction, changes over to after the end to suppress the quality inspection step;
Step 7, with the large caliber ultra-long rubber plastic composite hose for oil extraction that step 6 is finally made, suppress 20~40Mpa and stop 10min, observe do not leak, indeformable, qualified packing warehouse-in.
2, the production method of large caliber ultra-long rubber plastic composite hose for oil extraction according to claim 1, it is characterized in that said first reinforced layer and second reinforced layer are copper facing high tensile wire stratum reticulares, mesh wire diameter 0.35~0.6mm, open weave angle 40~70 degree.
3, the production method of large caliber ultra-long rubber plastic composite hose for oil extraction according to claim 1 is characterized in that said rubber plastic composite hose internal diameter 30mm to 50mm, pipe range 800~2000m.
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