Determine the method for cigarette filter tip paper permeating degree
Technical field
The present invention relates to determine in a kind of tobacco business the method for cigarette filter tip paper permeating degree.
Background technology
In recent years, along with the growing interest of society to " smoking is with healthy " problem, people are more and more higher to the requirement that cigarette product is sucked security, country has also put into effect corresponding measure emission of harmful substances quantity such as the tar of cigarette, nicotine, CO has been proposed strict restriction, and meaning from now on will be more and more stricter to the restriction of tobacco product.
Filter tip ventilation dilution technology is a kind of important means of cigarette lowering harm and decreasing coking, and it can make, and most harmful substances are effectively reduced in the cigarette smoke, and is particularly particularly evident for the higher gas phase composition of diffusion coefficient (as CO, NH3, HCN) effect.Because cigarette new national standard " GB 5606-2005 cigarette " proposes clear and definite control requirement to the discharging of CO in smoke of cigarettes, will be applied on a large scale as the filter tip ventilation dilution technology that reduces the effective measures of CO.
The action principle of cigarette filter ventilation dilution can be divided into the following aspects: (1) when suction air thus passage directly enter main flume, change the stream condition of filter segment, reach the purpose of dilution flue gas; (2) ventilation dilution changes the fired state of cigarette, and the air velocity of the burning awl of flowing through is reduced, and burning awl oxygen-supplying amount reduces composition and the quantity that has changed product; (3) ventilate to causing burning around the awl and to enter the air-flow velocity that cigarette props up and reduce, having changed the thermograde of pyrolysis distillation zone, burning awl back; (4) flue gas aerosol leaves the red-hot district cigarette of flowing through and props up low-temperature space, and it continues to be subjected to the influence that filter tip ventilates, and supposes that the flue gas total amount of every mouthful of suction is constant, and the flue gas flow rate and the degree of ventilation of air vent Upstream section reduce pro rata.The flue gas flow rate reduction causes the cigarette paper pressure drop to reduce, and causes by cigarette paper to enter the air minimizing that cigarette props up.The more important thing is that the time lengthening that flue gas stops makes more low-molecular-weight gas such as CO diffusion smoke prop up, so ventilation dilution all changes condensation, filtration, diffusion, the diluting effect of cigarette low-temperature space to some extent in cigarette props up.
In a word, the variation that the filter tip ventilation dilution brings whole cigarette is not only the dilution flue gas, it be many-sided, be very complicated, therefore to seek out a stable product quality, the filter tip dilution rate of cigarette accurately controlled be very important.
At present, the filter tip dilution rate of cigarette generally is to be (the cigarette plug paper air permeability is constant) that the hole drilling ventilation degree of yew paper is controlled by tipping paper used on it, be subjected to simultaneously the influence of nozzle rod sucting resistance and factors such as length, air permeance for cigarette paper and pipe tobacco characteristic again, be the yew paper and the cigarette plug paper of same air permeability, for different cigarette, dilution rate also is discrepant, also there is not a kind of comparatively easy passing method that cigarette filter tip paper permeating degree is carried out accurate method for measuring to this, so that its dilution rate is controlled.
Summary of the invention
Purpose of the present invention is exactly to solve present cigarette filter dilution rate to be difficult for the accurately problem of control, provides a kind of simple and easy to do, can determine the method for cigarette filter tip tipping paper air permeability comparatively accurately.
For achieving the above object, the present invention has adopted following technical scheme: a kind of method of definite cigarette filter tip paper permeating degree, its step be,
A, tipping paper and filter tip are selected and preparation, and wherein tipping paper air permeability minimum of a value is 50-80CU, and its maximum should be less than 1/20 of forming paper air permeability; To the tipping paper punching, the air permeability coefficient of variation is all less than 5%; Be processed into the mouth rod with high porosity plug wrap paper;
B, above-mentioned perforated tipping paper and high saturating forming nozzle rod are processed into cigarette;
C, select at least 50 cigarette and carry out the test of total dilution rate and filter tip dilution rate, count its mean value and the coefficient of variation;
D, experimental data is carried out finishing analysis, set up change curve and equation of linear regression that the tipping paper air permeability influences cigarette ventilation dilution rate: Y=-7X respectively
2* 10
-5+ 0.1198X+2.5522
Wherein, X-tipping paper air permeability; Y-mouth rod dilution rate.
Change curve and regression equation that e, application experiment are set up are carried out the selection and the design of cigarette filter tip paper permeating degree conversely according to the needs of cigarette Design of ventilation.
Described tipping paper is a yew paper.
Described step a is: (1) punch in advance selection of filter tip tipping paper air permeability: according to the enterprise product situation, select the filter tip tipping paper of the different air permeabilities of 5-10 kind to experimentize; Its air permeability minimum of a value is 60CU; The maximum of tipping paper air permeability is no more than 1/20 of forming paper air permeability, between the maximum and minimum of a value of every kind of filter tip tipping paper, selects the tipping paper of 4-9 air permeability value by the equispaced;
(2) punch the in advance control of filter tip tipping paper air permeability stability: select the punch device of stable performance to punch, and to the punching sample carry out the air permeability test verification, reject greater than 5% sample for the air permeability coefficient of variation, the coefficient of variation that guarantees all samples air permeability is below 5%;
(3) selection of filter tip high porosity plug wrap paper: according to the enterprise product situation, select for use 1-2 kind high porosity plug wrap paper to experimentize, in order to guarantee experimental precision, the coefficient of variation of air permeability is controlled at below 5%.
(4) control of the mouth rod that is processed into high porosity plug wrap paper: select the equipment of stable performance, use selected forming paper and carry out the processing of mouth rod, and carry out test verification, guarantee that finally the circumference of filter rod meets design load ± 0.1mm, resistance to suction meets design load ± 15mmH
2O, hardness meet the requirement of design load ± 1.5%, and all the other indexs are by normal requirement.
Among the described step b, (1) cigarette machine of selection stable performance, the mouth rod and specific cigarette shreds and the auxiliary material that are processed into above-mentioned pre-perforated tipping paper with high porosity plug wrap paper, under other process conditions of cigarette and the parameter condition identical with normal product, only change filter tip tipping paper and filter rod, be processed into cigarette sample respectively;
(2) all cigarette samples are selected, finally will meet weight is standard value ± 0.01g, and the sealing resistance to suction is standard value ± 5mmH
2O, cigarette Zhi Yuanzhou are the requirement of experiment of standard value ± 0.1mm.
In the described steps d, use the result of cigarette sample dilution rate test result and filter tip tipping paper, the test of high porosity plug wrap paper air permeability,, carry out the linear regression analysis of tipping paper air permeability and cigarette ventilation dilution rate at each mouth rod high porosity plug wrap paper; Setting up the tipping paper air permeability respectively influences the change curve and the linear regression equation of cigarette ventilation dilution rate; At last, utilize statistics to carry out remarkable type analysis to change curve and linear regression equation, reach the level of highly significant at curve, it and equation of linear regression formula can be applicable to the cigarette design.
The present invention is by the experimental analysis to different tipping paper air permeabilities, having set up the tipping paper air permeability influences change curve and the linear regression equation of cigarette ventilation dilution rate, can not only obtain the air permeability of tipping paper comparatively accurately by this equation, also can use it for the design of cigarette, to be met the cigarette of requirement.
The invention has the beneficial effects as follows that method is easy, the result is accurate, has improved the cigarette accuracy of design.
Description of drawings
Fig. 1 is the change curve schematic diagram.
The specific embodiment
The invention will be further described below in conjunction with accompanying drawing and embodiment.
Embodiment one:
A, tipping paper and filter tip are selected and preparation:
(1) punch the in advance selection of filter tip tipping paper air permeability:, generally select the filter tip tipping paper of 5-10 kind air permeability to experimentize according to the enterprise product situation; If because tipping paper air permeability too little (less than 50CU), its air permeability coefficient of variation is bigger, less stable is so the air permeability minimum of a value is 50CU; The maximum of tipping paper air permeability generally is subjected to the influence of cigarette plug paper, generally is no more than 1/20 of forming paper air permeability, between maximum and minimum of a value, selects other 4 air permeability values by the equispaced.
(2) punch the in advance control of filter tip tipping paper air permeability stability: select the punch device of stable performance to punch, and to the punching sample carry out the air permeability test verification, reject greater than 5% sample for the air permeability coefficient of variation, the coefficient of variation that finally guarantees all samples air permeability is below 5%.
(3) selection of filter tip high porosity plug wrap paper: according to the enterprise product situation, generally select for use 1-2 kind high porosity plug wrap paper to experimentize, in order to guarantee experimental precision, the coefficient of variation of air permeability is controlled at below 5% equally.
(4) control of high saturating forming nozzle rod; Select the equipment of stable performance, use selected forming paper and carry out the processing of mouth rod, and carry out test verification, finally guarantee filter rod
CircumferenceMeet design load ± 0.1mm,
Resistance to suctionMeet design load ± 15mmH
2O,
HardnessMeet the requirement (all the other indexs are by normal requirement) of design load ± 1.5%.
B, above-mentioned perforated tipping paper and high saturating forming nozzle rod are processed into cigarette:
(1) cigarette machine of selection stable performance, use above-mentioned pre-perforated tipping paper and high saturating forming nozzle rod and specific cigarette shreds and auxiliary material, under other process conditions of cigarette and the parameter condition identical, (guarantee that the pipe tobacco loading of cigarette and circumference, hardness, resistance to suction etc. are constant substantially) with normal product, only change filter tip tipping paper and filter rod, be processed into cigarette sample respectively.
(2) all cigarette samples are selected, finally will meet weight is standard value ± 0.01g, and the sealing resistance to suction is standard value ± 5mmH
2O, cigarette Zhi Yuanzhou are the requirement of experiment of standard value ± 0.1mm.
C, all samples after selecting is carried out the test of the total dilution rate of cigarette and filter tip dilution rate, requiring each cigarette sample test quantity minimum is 50, counts the mean value and the coefficient of variation at last.
The result of d, application cigarette sample dilution rate test result and filter tip tipping paper, the test of high porosity plug wrap paper air permeability at each mouth rod high porosity plug wrap paper, carries out the linear regression analysis of tipping paper air permeability and cigarette ventilation dilution rate; Setting up the tipping paper air permeability respectively influences the change curve and the linear regression equation of cigarette ventilation dilution rate; At last, change curve and linear regression equation are carried out remarkable type analysis, as coefficient of determination R
2When above, represent promptly that curve reaches the level of highly significant greater than 0.95, change curve and linear regression equation just can be applied to the cigarette design like this.
E, equational application:
Change curve and regression equation that application experiment is set up can be carried out the selection and the design of cigarette filter tip paper permeating degree conversely according to the needs of cigarette Design of ventilation.
For example: we draw by experiment about when the mouth rod uses the 10000CU high porosity plug wrap paper, about the linear regression curve of tipping paper air permeability and cigarette ventilation dilution rate and equation as shown in Figure 1, for the high porosity plug wrap paper of 10000CU, the rule that yew paper air permeability influences the total dilution rate of cigarette meets following linear regression equation:
Y=-7X
2* 10
-5+ 0.1198X+2.5522 (X-tipping paper air permeability; Y-mouth rod dilution rate)
Conspicuousness coefficient: R
2=0.9971 (highly significant) be if we want to design the filter tip dilution rate is 40% cigarette, Y=40 brought into formula can easily calculate filter tip tipping paper air permeability and be: X=412CU.Can improve our cigarette accuracy of design so greatly.
Embodiment two:
In the present embodiment, the air permeability minimum of a value is 60CU among the step a (1), and the air permeability value is got 7, and all the other contents are identical with embodiment one.
Embodiment three:
In the present embodiment, the air permeability minimum of a value is 80CU among the step a (1), and the air permeability value is got 9, and all the other contents are identical with embodiment one.