CN1836592A - Method for determining cigarette filter tip paper permeating degree - Google Patents
Method for determining cigarette filter tip paper permeating degree Download PDFInfo
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- CN1836592A CN1836592A CN 200610043848 CN200610043848A CN1836592A CN 1836592 A CN1836592 A CN 1836592A CN 200610043848 CN200610043848 CN 200610043848 CN 200610043848 A CN200610043848 A CN 200610043848A CN 1836592 A CN1836592 A CN 1836592A
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Abstract
The process of determining the permeability of cigarette filter tip paper can solve the problem of precisely controlling the dilution rate of filter tip and determine the permeability precisely. The process includes the following steps: A. sorting and making filter tip paper and filter tip; B. processing cigarette with the perforated filter tip paper and high permeability formed filter tip; C. measuring the total dilution rates and filter tip dilution rates of at least 50 cigarettes and calculating the average value and the variation coefficient; D. analyzing the measured data to establish the variation curve of cigarette ventilation dilution rate vs filer tip paper permeability and linear regression equation Y=-7X<SUP>2</SUP>*10<SUP>-5</SUP>+0.1227X+2.11, where X is permeability of tip paper and Y is dilution rate of filter tip; and E. applying the established variation curve and linear regression equation in selection and design of the permeability of cigarette filter tip paper.
Description
Technical field
The present invention relates to determine in a kind of tobacco business the method for cigarette filter tip paper permeating degree.
Background technology
In recent years, along with the growing interest of society to " smoking is with healthy " problem, people are more and more higher to the requirement that cigarette product is sucked security, country has also put into effect corresponding measure emission of harmful substances quantity such as the tar of cigarette, nicotine, CO has been proposed strict restriction, and meaning from now on will be more and more stricter to the restriction of tobacco product.
Filter tip ventilation dilution technology is a kind of important means of cigarette lowering harm and decreasing coking, and it can make, and most harmful substances are effectively reduced in the cigarette smoke, and is particularly particularly evident for the higher gas phase composition of diffusion coefficient (as CO, NH3, HCN) effect.Because cigarette new national standard " GB 5606-2005 cigarette " proposes clear and definite control requirement to the discharging of CO in smoke of cigarettes, will be applied on a large scale as the filter tip ventilation dilution technology that reduces the effective measures of CO.
The action principle of cigarette filter ventilation dilution can be divided into the following aspects: (1) when suction air thus passage directly enter main flume, change the stream condition of filter segment, reach the purpose of dilution flue gas; (2) ventilation dilution changes the fired state of cigarette, and the air velocity of the burning awl of flowing through is reduced, and burning awl oxygen-supplying amount reduces composition and the quantity that has changed product; (3) ventilate to causing burning around the awl and to enter the air-flow velocity that cigarette props up and reduce, having changed the thermograde of pyrolysis distillation zone, burning awl back; (4) flue gas aerosol leaves the red-hot district cigarette of flowing through and props up low-temperature space, and it continues to be subjected to the influence that filter tip ventilates, and supposes that the flue gas total amount of every mouthful of suction is constant, and the flue gas flow rate and the degree of ventilation of air vent Upstream section reduce pro rata.The flue gas flow rate reduction causes the cigarette paper pressure drop to reduce, and causes by cigarette paper to enter the air minimizing that cigarette props up.The more important thing is that the time lengthening that flue gas stops makes more low-molecular-weight gas such as CO diffusion smoke prop up, so ventilation dilution all changes condensation, filtration, diffusion, the diluting effect of cigarette low-temperature space to some extent in cigarette props up.
In a word, the variation that the filter tip ventilation dilution brings whole cigarette is not only the dilution flue gas, it be many-sided, be very complicated, therefore to seek out a stable product quality, the filter tip dilution rate of cigarette accurately controlled be very important.
At present, the filter tip dilution rate of cigarette generally is to be (the cigarette plug paper air permeability is constant) that the hole drilling ventilation degree of yew paper is controlled by tipping paper used on it, be subjected to simultaneously the influence of nozzle rod sucting resistance and factors such as length, air permeance for cigarette paper and pipe tobacco characteristic again, be the yew paper and the cigarette plug paper of same air permeability, for different cigarette, dilution rate also is discrepant, also there is not a kind of comparatively easy passing method that cigarette filter tip paper permeating degree is carried out accurate method for measuring to this, so that its dilution rate is controlled.
Summary of the invention
Purpose of the present invention is exactly to solve present cigarette filter dilution rate to be difficult for the accurately problem of control, provides a kind of simple and easy to do, can determine the method for cigarette filter tip tipping paper air permeability comparatively accurately.
For achieving the above object, the present invention has adopted following technical scheme: a kind of method of definite cigarette filter tip paper permeating degree, its step be,
A, tipping paper and filter tip are selected and preparation, and wherein tipping paper air permeability minimum of a value is 50-80CU, and its maximum should be less than 1/20 of forming paper air permeability; To the tipping paper punching, the air permeability coefficient of variation is all less than 5%; Be processed into the mouth rod with high porosity plug wrap paper;
B, above-mentioned perforated tipping paper and high saturating forming nozzle rod are processed into cigarette;
C, select at least 50 cigarette and carry out the test of total dilution rate and filter tip dilution rate, count its mean value and the coefficient of variation;
D, experimental data is carried out finishing analysis, set up change curve and equation of linear regression that the tipping paper air permeability influences cigarette ventilation dilution rate: Y=-7X respectively
2* 10
-5+ 0.1198X+2.5522
Wherein, X-tipping paper air permeability; Y-mouth rod dilution rate.
Change curve and regression equation that e, application experiment are set up are carried out the selection and the design of cigarette filter tip paper permeating degree conversely according to the needs of cigarette Design of ventilation.
Described tipping paper is a yew paper.
Described step a is: (1) punch in advance selection of filter tip tipping paper air permeability: according to the enterprise product situation, select the filter tip tipping paper of 5-10 kind air permeability to experimentize; Its air permeability minimum of a value is 60CU; The maximum of tipping paper air permeability is no more than 1/20 of forming paper air permeability, between maximum and minimum of a value, selects other 49 air permeability values by the equispaced;
(2) punch the in advance control of filter tip tipping paper air permeability stability: select the punch device of stable performance to punch, and to the punching sample carry out the air permeability test verification, reject greater than 5% sample for the air permeability coefficient of variation, the coefficient of variation that guarantees all samples air permeability is below 5%;
(3) selection of filter tip high porosity plug wrap paper: according to the enterprise product situation, select for use 1-2 kind high porosity plug wrap paper to experimentize, in order to guarantee experimental precision, the coefficient of variation of air permeability is controlled at below 5%.
(4) control of high saturating forming nozzle rod: select the equipment of stable performance, use selected forming paper and carry out the processing of mouth rod, and carry out test verification, guarantee that finally the circumference of filter rod meets design load ± 0.1mm, resistance to suction meets design load ± 15mmH
2O, hardness meet the requirement of design load ± 1.5%, and all the other indexs are by normal requirement.
Among the described step b, (1) cigarette machine of selection stable performance, with above-mentioned pre-perforated tipping paper and high saturating forming nozzle rod and specific cigarette shreds and auxiliary material, under other process conditions of cigarette and the parameter condition identical with normal product, only change filter tip tipping paper and filter rod, be processed into cigarette sample respectively.
(2) all cigarette samples are selected, finally will meet weight is standard value ± 0.01g, and the sealing resistance to suction is standard value ± 5mmH
2O, cigarette Zhi Yuanzhou are the requirement of experiment of standard value ± 0.1mm.
In the described steps d, use the result of cigarette sample dilution rate test result and filter tip tipping paper, the test of high porosity plug wrap paper air permeability,, carry out the linear regression analysis of tipping paper air permeability and cigarette ventilation dilution rate at each mouth rod high porosity plug wrap paper; Setting up the tipping paper air permeability respectively influences the change curve and the linear regression equation of cigarette ventilation dilution rate; At last, utilize statistics to carry out remarkable type analysis to change curve and linear regression equation, reach the level of highly significant at curve, it and equation of linear regression formula can be applicable to the cigarette design.
The present invention is by the experimental analysis to different tipping paper air permeabilities, having set up the tipping paper air permeability influences change curve and the linear regression equation of cigarette ventilation dilution rate, can not only obtain the air permeability of tipping paper comparatively accurately by this equation, also can use it for the design of cigarette, to be met the cigarette of requirement.
The invention has the beneficial effects as follows that method is easy, the result is accurate, has improved the cigarette accuracy of design.
Description of drawings
Fig. 1 is the change curve schematic diagram.
The specific embodiment
The invention will be further described below in conjunction with accompanying drawing and embodiment.
Embodiment one:
A, tipping paper and filter tip are selected and preparation:
(1) punch the in advance selection of filter tip tipping paper air permeability:, generally select the filter tip tipping paper of 5-10 kind air permeability to experimentize according to the enterprise product situation; If because tipping paper air permeability too little (less than 50CU), its air permeability coefficient of variation is bigger, less stable is so the air permeability minimum of a value is 50CU; The maximum of tipping paper air permeability generally is subjected to the influence of cigarette plug paper, generally is no more than 1/20 of forming paper air permeability, between maximum and minimum of a value, selects other 4 air permeability values by the equispaced.
(2) punch the in advance control of filter tip tipping paper air permeability stability: select the punch device of stable performance to punch, and to the punching sample carry out the air permeability test verification, reject greater than 5% sample for the air permeability coefficient of variation, the coefficient of variation that finally guarantees all samples air permeability is below 5%.
(3) selection of filter tip high porosity plug wrap paper: according to the enterprise product situation, generally select for use 1-2 kind high porosity plug wrap paper to experimentize, in order to guarantee experimental precision, the coefficient of variation of air permeability is controlled at below 5% equally.
(4) control of high saturating forming nozzle rod: select the equipment of stable performance, use selected forming paper and carry out the processing of mouth rod, and carry out test verification, guarantee that finally the circumference of filter rod meets design load ± 0.1mm, resistance to suction meets design load ± 15mmH
2O, hardness meet the requirement (all the other indexs are by normal requirement) of design load ± 1.5%.
B, above-mentioned perforated tipping paper and high saturating forming nozzle rod are processed into cigarette:
(1) cigarette machine of selection stable performance, use above-mentioned pre-perforated tipping paper and high saturating forming nozzle rod and specific cigarette shreds and auxiliary material, under other process conditions of cigarette and the parameter condition identical, (guarantee that the pipe tobacco loading of cigarette and circumference, hardness, resistance to suction etc. are constant substantially) with normal product, only change filter tip tipping paper and filter rod, be processed into cigarette sample respectively.
(2) all cigarette samples are selected, finally will meet weight is standard value ± 0.01g, and the sealing resistance to suction is standard value ± 5mmH
2O, cigarette Zhi Yuanzhou are the requirement of experiment of standard value ± 0.1mm.
C, all samples after selecting is carried out the test of the total dilution rate of cigarette and filter tip dilution rate, requiring each cigarette sample test quantity minimum is 50, counts the mean value and the coefficient of variation at last.
The result of d, application cigarette sample dilution rate test result and filter tip tipping paper, the test of high porosity plug wrap paper air permeability at each mouth rod high porosity plug wrap paper, carries out the linear regression analysis of tipping paper air permeability and cigarette ventilation dilution rate; Setting up the tipping paper air permeability respectively influences the change curve and the linear regression equation of cigarette ventilation dilution rate; At last, change curve and linear regression equation are carried out remarkable type analysis, as coefficient of determination R
2When above, represent promptly that curve reaches the level of highly significant greater than 0.95, change curve and linear regression equation just can be applied to the cigarette design like this.
E, equational application:
Change curve and regression equation that application experiment is set up can be carried out the selection and the design of cigarette filter tip paper permeating degree conversely according to the needs of cigarette Design of ventilation.
For example: we draw by experiment about when the mouth rod uses the 10000CU high porosity plug wrap paper, about the linear regression curve of tipping paper air permeability and cigarette ventilation dilution rate and equation as shown in Figure 1, for the high porosity plug wrap paper of 10000CU, the rule that yew paper air permeability influences the total dilution rate of cigarette meets following linear regression equation:
Y=-7X
2* 10
-5+ 0.1198X+2.5522 (X-tipping paper air permeability; Y-mouth rod dilution rate)
Conspicuousness coefficient: R
2=0.9971 (highly significant) be if we want to design the filter tip dilution rate is 40% cigarette, Y=40 brought into formula can easily calculate filter tip tipping paper air permeability and be: X=412CU.Can improve our cigarette accuracy of design so greatly.
Embodiment two:
In the present embodiment, the air permeability minimum of a value is 60CU among the step a (1), and the air permeability value is got 7, and all the other contents are identical with embodiment one.
Embodiment three:
In the present embodiment, the air permeability minimum of a value is 80CU among the step a (1), and the air permeability value is got 9, and all the other contents are identical with embodiment one.
Claims (5)
1, a kind of method of definite cigarette filter tip paper permeating degree is characterized in that: its step is,
A, tipping paper and filter tip are selected and preparation, and wherein tipping paper air permeability minimum of a value is 50-80CU, and its maximum should be less than 1/20 of forming paper air permeability; To the tipping paper punching, the air permeability coefficient of variation is all less than 5%; Be processed into the mouth rod with high porosity plug wrap paper;
B, above-mentioned perforated tipping paper and high saturating forming nozzle rod are processed into cigarette;
C, select at least 50 cigarette and carry out the test of total dilution rate and filter tip dilution rate, count its mean value and the coefficient of variation;
D, experimental data is carried out finishing analysis, set up change curve and equation of linear regression that the tipping paper air permeability influences cigarette ventilation dilution rate: Y=-7X respectively
2* 10
-5+ 0.1198X+2.5522
Wherein, X-tipping paper air permeability; Y-mouth rod dilution rate.
Change curve and regression equation that e, application experiment are set up are carried out the selection and the design of cigarette filter tip paper permeating degree conversely according to the needs of cigarette Design of ventilation.
2, the method for definite cigarette filter tip paper permeating degree according to claim 1 is characterized in that: described tipping paper is a yew paper.
3, the method for definite cigarette filter tip paper permeating degree according to claim 1 is characterized in that: described step a is:
(1) punch the in advance selection of filter tip tipping paper air permeability:, select the filter tip tipping paper of 5-10 kind air permeability to experimentize according to the enterprise product situation; Its air permeability minimum of a value is 60CU; The maximum of tipping paper air permeability is no more than 1/20 of forming paper air permeability, between maximum and minimum of a value, selects other 4-9 air permeability values by the equispaced;
(2) punch the in advance control of filter tip tipping paper air permeability stability: select the punch device of stable performance to punch, and to the punching sample carry out the air permeability test verification, reject greater than 5% sample for the air permeability coefficient of variation, the coefficient of variation that guarantees all samples air permeability is below 5%;
(3) selection of filter tip high porosity plug wrap paper: according to the enterprise product situation, select for use 1-2 kind high porosity plug wrap paper to experimentize, in order to guarantee experimental precision, the coefficient of variation of air permeability is controlled at below 5%.
(4) control of high saturating forming nozzle rod: the equipment of selecting stable performance, use selected forming paper and carry out the processing of mouth rod, and carry out test verification, the final circumference that guarantees filter rod meets design load ± 0.1mm, resistance to suction and meets the requirement that design load ± 15mmH2O, hardness meet design load ± 1.5%, and all the other indexs are by normal requirement.
4, the method for definite cigarette filter tip paper permeating degree according to claim 1 is characterized in that: among the described step b,
(1) cigarette machine of selection stable performance, with above-mentioned pre-perforated tipping paper and high saturating forming nozzle rod and specific cigarette shreds and auxiliary material, under other process conditions of cigarette and the parameter condition identical with normal product, only change filter tip tipping paper and filter rod, be processed into cigarette sample respectively.
(2) all cigarette samples are selected, finally will meet weight is standard value ± 0.01g, and the sealing resistance to suction is standard value ± 5mmH2O, and cigarette Zhi Yuanzhou is the requirement of experiment of standard value ± 0.1mm.
5, the method for definite cigarette filter tip paper permeating degree according to claim 1, it is characterized in that: in the described steps d, use the result of cigarette sample dilution rate test result and filter tip tipping paper, the test of high porosity plug wrap paper air permeability, at each mouth rod high porosity plug wrap paper, carry out the linear regression analysis of tipping paper air permeability and cigarette ventilation dilution rate; Setting up the tipping paper air permeability respectively influences the change curve and the linear regression equation of cigarette ventilation dilution rate; At last, utilize statistics to carry out remarkable type analysis to change curve and linear regression equation, reach the level of highly significant at curve, it and equation of linear regression formula can be applicable to the cigarette design.
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| GB2047513A (en) * | 1979-04-21 | 1980-12-03 | Molins Ltd | Cigarette ventilation control |
| CA2244453A1 (en) * | 1998-07-31 | 2000-01-31 | Marcel Champagne | Tubular band assembly process |
| CN2545843Y (en) * | 2002-05-24 | 2003-04-23 | 牡丹江恒丰纸业股份有限公司 | High-Permeability forming paper for cigarette filtering holder |
| CN2623038Y (en) * | 2003-04-04 | 2004-07-07 | 红河卷烟厂 | Drilling forming package paper for cigarette filter rod |
| CN1718122A (en) * | 2005-04-14 | 2006-01-11 | 曾立 | Paper for enclosing filter-tip of cigarette having porous and groove structure |
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| CN103005702A (en) * | 2012-12-12 | 2013-04-03 | 广东中烟工业有限责任公司 | Design method of less harmful cigarette based on harm index under deep smoking |
| CN103005703A (en) * | 2012-12-12 | 2013-04-03 | 广东中烟工业有限责任公司 | Cigarette designing method based on smoke perniciousness index |
| CN103005702B (en) * | 2012-12-12 | 2015-03-18 | 广东中烟工业有限责任公司 | Design method of less harmful cigarette based on harm index under deep smoking |
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| CN105021512A (en) * | 2015-07-28 | 2015-11-04 | 昆明理工大学 | Tipping paper air permeability detection method based on least squares |
| CN105300868A (en) * | 2015-11-24 | 2016-02-03 | 昆明理工大学 | Detection method for air permeability of perforated tipping paper used in tobacco industry |
| CN108260850A (en) * | 2016-12-30 | 2018-07-10 | 贵州中烟工业有限责任公司 | A kind of method of the adhesive-free area area of determining rolling up and connecting machine |
| CN108260850B (en) * | 2016-12-30 | 2022-05-03 | 贵州中烟工业有限责任公司 | Method for determining glue-free area of cigarette making and plug assembling machine |
| CN107173847A (en) * | 2017-05-10 | 2017-09-19 | 浙江中烟工业有限责任公司 | A kind of cigarette degree of ventilation control system and its control method |
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| CN108535167A (en) * | 2018-06-12 | 2018-09-14 | 河南中烟工业有限责任公司 | A kind of method and system promoting cigarette making machine air permeability |
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