CN102940310B - A kind of method of adjustment based on each component in the Cigarette design of N-nitrosamine burst size - Google Patents

A kind of method of adjustment based on each component in the Cigarette design of N-nitrosamine burst size Download PDF

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CN102940310B
CN102940310B CN201210534586.0A CN201210534586A CN102940310B CN 102940310 B CN102940310 B CN 102940310B CN 201210534586 A CN201210534586 A CN 201210534586A CN 102940310 B CN102940310 B CN 102940310B
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cigarette
nitrosamine
air permeability
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discharge
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CN102940310A (en
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孔浩辉
吴君章
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China Tobacco Guangdong Industrial Co Ltd
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Abstract

The invention provides the method for adjustment of each Cigarette design parameter in a kind of Cigarette design based on N-nitrosamine burst size, said method comprising the steps of: the step 1) determining the discharge index of flue gas N-nitrosamine; 2) the N-nitrosamine discharge relational model based on cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop, expanded cut stem ginseng proportioning is set up; 3) select relevant parameter according to N-nitrosamine discharge relational model, obtain the step of N-nitrosamine discharge model value, described parameter comprises cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop and expanded cut stem ginseng proportioning, obtains the N-nitrosamine discharge model value corresponding to above-mentioned parameter; 4) make comparisons according to sample value and discharge index, if described model value is not more than discharge index, adopts corresponding parameter to carry out Cigarette design, otherwise repeat step 3).Relevance reasonable adjusting component between the parameters that only need count on according to N-nitrosamine discharge relational model, just can be good at reaching lowering harm and decreasing coking effect.

Description

A kind of method of adjustment based on each component in the Cigarette design of N-nitrosamine burst size
Technical field
The present invention relates to Cigarette design field, particularly relate to the method for adjustment of each Cigarette design parameter in a kind of Cigarette design based on N-nitrosamine burst size.
Background technology
How reduce the harmful substance in cigarette smoke by effective means, improve cigarette quality, be the inside and outside common topic be concerned about of industry, be also main task and the focus of industry tackling of key scientific and technical problems always, this be also simultaneously I to cross in cigarette evolution must in the face of and the focal issue that solves.Each tobacco research institution is devoted to the research of this work always and achieves gratifying achievement, but still has achievement greatly to can not get application, reason be more the complexity of flue gas system and people to cigarette special suck requirement.
In existing research field, technical staff reviews 189 sections of open source literatures to people such as Paschke in cigarette, contains the influence research of 300 multiple additives to cigarette smoke character.They find different additive and add the impact of concentration on smoke components there are differences.In most cases, after some additive adds with its maximum addition in commercial cigarettes or excess (one addition is all ppm level), some smoke components has and increases or reduce.
But the design of cigarette also can exist and there is very large impact to the discharge of flue gas, therefore, science differentiates that the Cigarette design index such as cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop, expanded cut stem ginseng proportioning is to the influence degree of flue gas composition burst size amount exactly, to judgement lowering harm and decreasing coking additive effect, improve cigarette product quality safety and have important practical significance.
About Cigarette design indexs such as additive amount, air permeance for cigarette paper, filter stick pressure drops in cigarette paper on the impact of flue gas composition burst size amount, report in existing many research in the past, and have researcher to attempt setting up the regression equation between the adjustment of Cigarette design index parameter and flue gas composition burst size.But major part research is mainly limited to the effect that single index adjustment changes flue gas conventional constituents (tar, nicotine, N-nitrosamine), only have small part to research and analyse Cigarette design parameter mainly contains pest burst size impact on flue gas 7 kinds, or the synergistic effect of research multi objective.But it is all obtain by comparing with the simple, intuitive contrasting cigarette that the conspicuousness of current many correlative studys is inferred, can not by additive amount, air permeance for cigarette paper, filter stick pressure drop in cigarette paper, the Cigarette design index changes such as expanded cut stem ginseng proportioning are distinguished the fluctuation that impact and the experimental error of Chemical Components in Cigarette Smoke are brought, and have impact on the accurate judgement of additive lowering harm and decreasing coking effect.And up to now, about the research of multi objective synergistic action effect, there is repugnance in the conclusion that the analysis of its indivedual index action effect is but studied with other, therefore additive amount, air permeance for cigarette paper, filter stick pressure drop in cigarette paper is differentiated according to analysis result, the Cigarette design indexs such as expanded cut stem ginseng proportioning are to the unfeasible way of cigarette smoke components influence degree, and then serious have influence on Cigarette design, make the design of cigarette cannot well reach lowering harm and decreasing coking effect.
Summary of the invention
Goal of the invention of the present invention is the defect overcoming prior art, there is provided a kind of in production cigarette process, effectively can control the N-nitrosamine discharge capacity in flue gas, improve the method for adjustment based on each component in the Cigarette design of N-nitrosamine burst size of Cigarette design efficiency.
In order to realize above-mentioned goal of the invention, the invention provides:
A method of adjustment for each Cigarette design parameter in Cigarette design based on N-nitrosamine burst size, said method comprising the steps of:
1) step of the discharge index of flue gas N-nitrosamine is determined;
2) the N-nitrosamine discharge relational model based on cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop, expanded cut stem ginseng proportioning is set up;
3) select relevant parameter according to N-nitrosamine discharge relational model, obtain the step of N-nitrosamine discharge model value, described parameter comprises cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop and expanded cut stem ginseng proportioning, obtains the N-nitrosamine discharge model value corresponding to above-mentioned parameter;
4) make comparisons according to sample value and discharge index, if described model value is not more than discharge index, adopts corresponding parameter to carry out Cigarette design, otherwise repeat step 3) after adjusting each Cigarette design parameter.
Further, in the Cigarette design based on N-nitrosamine burst size, each component adjustment method, when determining tipping paper air permeability, can adopt the discharge relational model of new N-nitrosamine for improving forecasting accuracy.
Further, when not distinguishing tipping paper air permeability, described N-nitrosamine discharge relational model is: C=6.574 – 106.56 × b1-0.0059 × b3+0.0012 × b5, wherein C is the discharge capacity of N-nitrosamine, b1 is cigarette paper additive consumption, b3 is tipping paper air permeability, the pressure drop of b5 filter stick.Tipping paper air permeability has the greatest impact to flue gas N-nitrosamine burst size.
Further, when tipping paper air permeability is 150CU, the discharge relational model of described N-nitrosamine is: C=8.1771 – 82.5 × b1-0.0293 × b2 – 4.3600 × b6(formula 2), wherein C is the discharge capacity of N-nitrosamine, b1 is cigarette paper additive consumption, b2 is air permeance for cigarette paper, and b6 is expanded cut stem ginseng proportioning.When tipping paper air permeability is 150CU, air permeance for cigarette paper has the greatest impact to flue gas N-nitrosamine burst size, and the impact of cigarette paper additive consumption and expanded cut stem ginseng proportioning is relatively little, and the impact of forming paper air permeability and filter stick pressure drop is relatively little.
Further, when tipping paper air permeability is 300CU, the discharge relational model of described N-nitrosamine is: C=-2.7300+0.1403 × b2+0.0035 × b5(formula 3), wherein C is the discharge capacity of N-nitrosamine, b2 is air permeance for cigarette paper, and b5 is filter stick pressure drop.When tipping paper air permeability is 300CU, air permeance for cigarette paper has the greatest impact to flue gas N-nitrosamine burst size, and the impact of the addition of citrate, forming paper air permeability and expanded cut stem ginseng proportioning is relatively little.
Further, when tipping paper air permeability is 450CU, the discharge relational model of described N-nitrosamine is: C=9.3160-0.0626 × b2-(4.98 × 10 -5) × b4 – 8.6666 × b6(formula 4), wherein C is the discharge capacity of N-nitrosamine, and b2 is air permeance for cigarette paper, and b4 is forming paper air permeability, and b6 is expanded cut stem ginseng proportioning.When tipping paper air permeability is 450CU, air permeance for cigarette paper has the greatest impact to flue gas N-nitrosamine burst size, and the addition of citrate, the impact of filter stick pressure drop are relatively little.
Further, when repeating step 3) in step 4), also comprise according to N-nitrosamine discharge relational model obtain cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop and expanded cut stem ginseng proportioning respectively with the relevance of N-nitrosamine burst size, and regulate the step of described parameter according to this relevance.
Further, control method for described parameter is: the parameter of relevance to current use according to parameters and N-nitrosamine burst size regulates, first determine tipping paper air permeability, then increase according to the Cigarette design parameter of each correspondence under different tipping paper air permeability and the relevance formula of N-nitrosamine burst size or reduce the value of parameters.
Further, by improving citrate consumption, improving tipping paper air permeability, improve forming paper air permeability, reduce filter stick pressure drop and improving expanded cut stem ginseng proportioning, the reduction of N-nitrosamine burst size is realized.And according to the situation of tipping paper air permeability, adjustment air permeance for cigarette paper: when tipping paper air permeability is 150CU or 450CU, improves the reduction that air permeance for cigarette paper realizes N-nitrosamine discharge capacity; Being 300CU at tipping paper air permeability is, reduces the reduction that air permeance for cigarette paper realizes N-nitrosamine burst size.
Further, control method for described parameter is, when tipping paper air permeability is 150CU, the control method for described parameter is following: improve air permeance for cigarette paper, improve cigarette paper additive consumption or improve one or more combination adjusting method in expanded cut stem ginseng proportioning.。
Further, the control method for described parameter is, when tipping paper air permeability is 300CU, reduces air permeance for cigarette paper, and/or reduces filter stick pressure drop.
Further, control method for described parameter is, when tipping paper air permeability is 450CU, the control method for described parameter is following: improve air permeance for cigarette paper, improve forming paper air permeability, to improve in expanded cut stem ginseng proportioning one or more combination adjusting method.
Further, in Cigarette design, each component on the size that N-nitrosamine burst size affects is: tipping paper air permeability > air permeance for cigarette paper > filter stick pressure drop > cigarette paper additive consumption > forming paper air permeability > expand swollen silk ginseng proportioning.
Compared with prior art, the invention has the advantages that:
Technical scheme of the present invention is by the production process of cigarette, adopt the N-nitrosamine discharge relational model based on cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop, expanded cut stem ginseng proportioning, fundamentally control the discharge capacity of N-nitrosamine in cigarette, and without the need to improving existing process equipment and material, relevance reasonable adjusting component between the parameters that only need count on according to N-nitrosamine discharge relational model, just can be good at reaching lowering harm and decreasing coking effect.
Accompanying drawing explanation
Fig. 1 is method flow diagram of the present invention.
Detailed description of the invention
Below in conjunction with specific embodiment, the invention will be further described.
As shown in Figure 1, a kind of method of adjustment based on each component in the Cigarette design of N-nitrosamine burst size provided by the invention, said method comprising the steps of:
1) step of the discharge index of flue gas N-nitrosamine is determined;
2) the N-nitrosamine discharge relational model based on cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop, expanded cut stem ginseng proportioning is set up;
3) select relevant parameter according to N-nitrosamine discharge relational model, obtain the step of N-nitrosamine discharge model value, described parameter comprises cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop and expanded cut stem ginseng proportioning, obtains the N-nitrosamine discharge model value corresponding to above-mentioned parameter;
4) make comparisons according to sample value and discharge index, if described model value is not more than discharge index, adopts corresponding parameter to carry out Cigarette design, otherwise repeat step 3) after adjusting each Cigarette design parameter.
Wherein, when repeating step 3) in step 4), also comprise according to N-nitrosamine discharge relational model obtain cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop and expanded cut stem ginseng proportioning respectively with the relevance of N-nitrosamine burst size, and regulate the deal of each parameter described according to this relevance, until described model value is not more than discharge index.
Wherein, in above-mentioned for the control method of described parameter be: the parameter of relevance to current use according to parameters and N-nitrosamine burst size regulates, first determine tipping paper air permeability, then increase according to the Cigarette design parameter of each correspondence under different tipping paper air permeability and the relevance formula of N-nitrosamine burst size or reduce the value of parameters.
Embodiment 1
The statistics of data all in the present invention is all adopt from the domestic transformation standard of ISO 4387 with detecting, adopt prepare according to different materials design parameter demand, single-tobacco-typed cigarette cigarette product is laboratory sample.
The measurement standard of sample is: ISO regime scheme is according to GB/T 19609(ISO 4387 domestic transformation standard) regulation set: pumping volume, 35mL; Suction frequencies, 60s/ mouth; Artificially do not close filter stick air penetrability.
The detection of cigarette physical index, performs according to GB/T 22838.The mensuration of N-nitrosamine in flue gas gas phase, performs according to GB/T 23228-2008.
The flue gas inspection result of described N-nitrosamine discharge relational model by carrying out under joining proportioning situation multiple cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop, expanded cut stem, right employing to multiple stepwise regression, and then obtains above-mentioned several parameter and affects size statistical model to flue gas N-nitrosamine burst size.
The parameter of each cigarette sample is as following table.
The parameter (adopting identical tobacco raw material) of table 1 cigarette laboratory sample
Sample number into spectrum Additive (citrate) consumption in cigarette paper Air permeance for cigarette paper (CU) Tipping paper air permeability (CU) Forming paper air permeability (CU) Filter stick pressure drop Expanded cut stem ginseng is joined
1 0.7% 30 150 12000 800Pa 10%
2 0.7% 60 150 12000 800Pa 10%
5 0.5% 40 150 12000 800Pa 10%
6 0.7% 40 150 12000 800Pa 10%
7 0.9% 40 150 12000 800Pa 10%
8 0.7% 40 300 12000 800Pa 10%
9 0.7% 40 450 12000 800Pa 10%
10 0.7% 40 150 6000 800Pa 10%
11 0.7% 40 150 20000 800Pa 10%
12 0.7% 40 150 32000 800Pa 10%
13 0.7% 40 150 12000 700Pa 10%
14 0.7% 40 150 12000 900Pa 10%
17 0.7% 40 150 12000 800Pa 5%
18 0.7% 40 150 12000 800Pa 15%
19 0.7% 60 450 32000 700Pa 5%
20 0.7% 60 450 20000 700Pa 5%
21 0.7% 60 450 6000 900Pa 15%
22 0.9% 60 450 6000 700Pa 15%
23 0.7% 30 300 20000 900Pa 5%
24 0.7% 30 300 6000 700Pa 15%
25 0.9% 30 300 6000 900Pa 5%
Wherein the 6th standard of behaviour cigarette sample and design parameter thereof.
Carry out multiple stepwise regression for above-mentioned data, cigarette material design parameter affects Analyzing on Size as table 2 to flue gas N-nitrosamine burst size:
The each cigarette material design parameter of table 2 affects the analysis of size on NNN burst size
Influence factor Standardized regression factor Standard error P value Conspicuousness
Cigarette paper additive consumption b1 -106.56 149.32 0.4851 Certain correlation
Air permeance for cigarette paper b2 -0.0041 0.0148 0.7861 Uncorrelated
Tipping paper air permeability b3 -0.0059 0.001 2.75E-05 Significantly
Forming paper air permeability b4 -6.56E-06 1.83E-05 0.7243 Uncorrelated
Filter stick pressure drop b5 0.0012 0.0019 0.4412 Certain correlation
Swollen stem ginseng proportioning b6 -0.7207 3.9374 0.8571 Uncorrelated
Thus the regression equation (getting P<0.5) of NNN burst size under each cigarette material design parameter can be obtained
C = 6.574 – 106.56 × b1 - 0.0059 × b3 + 0.0012 × b5
Analytical table and above regression equation can be known: 1. cigarette tipping paper air permeability paper (b3) having the greatest impact to flue gas NNN burst size, and its multiple stepwise regression gained P value is less than 0.0001, less than the one thousandth of other each factor P value.And b3 is larger, in flue gas, the burst size of NNN is lower; This variation tendency is identical with the situation of phenol with carbon monoxide.2. cigarette paper additive consumption (b1) and filter stick pressure drop (b5) have certain influence to index C, show as that b1 is larger, b5 is less, then C value is lower.
And apply the prediction that this regression equation carries out flue gas NNN burst size, and it predicts the outcome and to compare with gained detected value under ISO pattern, and relative deviation is on average 8.0% lower than 10%(), predict the outcome comparatively accurate.But what sample segment (having 6 samples) predicted the outcome departs from more than 10%(relative deviation), wherein predicting the outcome of 2 samples is departed from more than 20%, therefore has the space of improving further.For this reason, need that it carries out classification analysis to the peculiar N-nitrosamine of tobacco equally.And can intuitively carry out simple to the various components in cigarette simply according to above-mentioned testing result and reasonably regulate, thus realize in process of production according to productive target design cigarette.
Embodiment 2
As tipping paper air permeability (b3)=150CU
Through multiple stepwise regression, cigarette material design parameter to the analysis of Influential Factors of flue gas NNN burst size as table 3:
The analysis of Influential Factors (ISO pattern, b3=150CU) of table 3 NNN burst size
Influence factor Standardized regression factor Standard error P value Conspicuousness
Cigarette paper additive consumption b1 -82.5 139.36 0.4702 Certain correlation
Air permeance for cigarette paper b2 -0.0293 0.0178 0.1376 More remarkable
Tipping paper air permeability b3 - - - Significantly
Forming paper air permeability b4 -6.75E-06 1.95E-05 0.7395 Weak dependence
Filter stick pressure drop b5 0.0014 0.0029 0.6381 Weak dependence
Swollen stem ginseng proportioning b6 -4.3600 5.5744 0.4566 Certain correlation
During according to b3=150CU, the regression equation (getting P<0.5) of NNN burst size
C = 8.1771 – 82.5 × b1 - 0.0293 × b2 – 4.3600 × b6
Analytical table 3 and above regression equation can be known: 1. as tipping paper air permeability lower (b3=150CU), air permeance for cigarette paper (b2) having the greatest impact to C, b2 larger C value is lower.2. cigarette paper additive consumption (b1) also has certain influence to C value, and b1 larger then C value is lower.3. other pipe tobacco ginseng dosage (b6) also has certain influence to C value, and b6 larger then C value is lower.Can intuitively carry out simple to the various components in cigarette simply according to above-mentioned testing result and reasonably regulate, thus realize in process of production according to productive target design cigarette.
Embodiment 3
As tipping paper air permeability (b3)=300CU
Through multiple stepwise regression, cigarette material design parameter to the analysis of Influential Factors of flue gas NNN burst size as table 4:
The analysis of Influential Factors (ISO pattern, b3=300CU) of table 4 NNN burst size
Influence factor Standardized regression factor Standard error P value Conspicuousness
Cigarette paper additive consumption b1 51 Inf NaN Uncorrelated
Air permeance for cigarette paper b2 0.1403 0.0085 0.0383 Significantly
Tipping paper air permeability b3 - - - Significantly
Forming paper air permeability b4 -7.29E-06 Inf NaN Uncorrelated
Filter stick pressure drop b5 0.0035 4.42E-04 0.0807 Significantly
Swollen stem ginseng proportioning b6 0 Inf NaN Uncorrelated
During according to b3=300CU, the regression equation (getting P<0.5) of NNN burst size
C = -2.7300 + 0.1403 × b2 + 0.0035 × b5
Analytical table 4 and above regression equation (formula 3) can be known: 1. when tipping paper air permeability is medium (b3=300CU), and air permeance for cigarette paper is more remarkable on the impact of NNN burst size, but contrary with the effect under low tipping paper air permeability, and b2 less C value is lower.2. filter stick pressure drop (b5) also has impact impact to C, and b5 less then C value is lower.Can intuitively carry out simple to the various components in cigarette simply according to above-mentioned testing result and reasonably regulate, thus realize in process of production according to productive target design cigarette.
Embodiment 4
As tipping paper air permeability (b3)=450CU
Through multiple stepwise regression, the relevance of cigarette material design parameter and NNN burst size, namely parameters to the analysis of Influential Factors of flue gas NNN burst size as table 5:
The analysis of Influential Factors (ISO pattern, b3=450CU) of table 5 NNN burst size
Influence factor Standardized regression factor Standard error P value Conspicuousness
Cigarette paper additive consumption b1 51 Inf NaN Uncorrelated
Air permeance for cigarette paper b2 -0.0626 0.0044 0.0444 Significantly
Tipping paper air permeability b3 - - - Significantly
Forming paper air permeability b4 -4.98E-05 8.50E-06 0.1076 More remarkable
Filter stick pressure drop b5 -5.10E-04 Inf NaN Uncorrelated
Swollen stem ginseng proportioning b6 -8.6666 1.8467 0.1337 More remarkable
During according to b3=450CU, the regression equation (getting P<0.5) of NNN burst size
C = 9.3160 - 0.0626 × b2 - (4.98×10-5) × b4 – 8.6666 × b6
Analytical table 5 and above regression equation (formula 4) can be known: 1. when tipping paper air permeability is higher time (b3=450CU), air permeance for cigarette paper (b2) on the impact of NNN burst size, b2 larger C value lower (similar to the situation of low air permeance for cigarette paper).2. now, forming paper air permeability (b4) impact on C value manifests and comparatively remarkable, and b4 larger then C value is less.3. the impact of other pipe tobacco ginseng dosage (b6) becomes large again, and b6 larger then C value is less.Can intuitively carry out simple to the various components in cigarette simply according to above-mentioned testing result and reasonably regulate, thus realize in process of production according to productive target design cigarette.
Embodiment 5
To comparing according to its predicted value of cigarette designed by the present invention and actual value
The interpretation of result that cigarette material design parameter is predicted flue gas nuisance burst size is applied under table 6 ISO suction mode
Apply each regression equation predicting the outcome by cigarette material coaptation flue gas composition burst size, with ISO suction mode lower to obtain the deviation detecting data less, show that this regression equation predicts the outcome ideal, comparatively accurate to the correlation analysis of cigarette material factor: the relative deviation mean value of NNK index is 2.6% lower than 3%(), relative standard deviation values except one group of data is except 14.35%, and the relative standard deviation values of other data is all less than 8%.
Each cigarette material parameter is as follows on the impact of tobacco-specific nitrosamine burst size in flue gas: 1. increase citrate addition (b1) in cigarette paper material, effectively can reduce flue gas NNN burst size, but only under low tipping paper air permeability (b3=150CU) condition its effect just comparatively remarkable.2. air permeance for cigarette paper (b2) has considerable influence to flue gas NNN burst size (C), but different for the effect under ISO pattern, different tipping paper air permeability (b3) condition.3. improve tipping paper air permeability design load (b3), can effectively reduce C value.4., only as tipping paper air permeability high (b3=450CU), improving forming paper air permeability (b4) just has comparatively positive effect to the reduction of C value.5. reduce filter stick pressure drop (b5) to be conducive to reducing NNN burst size, and effect is particularly evident as air permeance for cigarette paper b3=300CU.6. improve other pipe tobacco ginseng dosage (b6), also can reduce AC value, but only effect is just obviously as low or high air permeance for cigarette paper (b3=150CU or 450CU).
Therefore, the design of low NNN burst size cigarette is: 1. increase cigarette paper material citrate consumption (b1), the design load of air permeance for cigarette paper (b2), tipping paper air permeability (b3), forming paper air permeability (b4) is improved under height breathes freely tipping paper condition, and reduce filter stick pressure drop, under low or high ventilative tipping paper condition, improve other pipe tobacco ginseng dosage (b6), be all conducive to reducing carbon monoxide in flue gas burst size.2. under ISO pattern, the relevance size of different materials parameter and flue gas nuisance burst size is, b3 (+) > b2 (+) > b5 (-) > b1 (+) > b4 (+, b3=450CU) > b6 (+, b3=150CU or 450CU).

Claims (5)

1. a method of adjustment for each Cigarette design parameter in the Cigarette design based on N-nitrosamine burst size, is characterized in that, said method comprising the steps of:
1) discharge index of flue gas N-nitrosamine is determined;
2) the N-nitrosamine discharge relational model based on cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop, expanded cut stem mixed ratio is set up;
3) select relevant parameter according to N-nitrosamine discharge relational model, obtain the step of N-nitrosamine discharge model value, described parameter comprises cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop and expanded cut stem mixed ratio;
4) make comparisons according to model value and discharge index, if described model value is not more than discharge index, adopt corresponding parameter to adjust the cigarette paper additive consumption in Cigarette design, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop and expanded cut stem mixed ratio, otherwise repeat step 3) after adjusting each Cigarette design parameter;
The measurement standard of each Cigarette design parameter is: ISO regime scheme sets according to the regulation of GB/T 19609;
When not distinguishing tipping paper air permeability, described N-nitrosamine discharge relational model is: C=6.574 – 106.56 × b1-0.0059 × b3+0.0012 × b5, wherein C is the discharge capacity of N-nitrosamine, b1 is cigarette paper additive consumption, b3 is tipping paper air permeability, the pressure drop of b5 filter stick;
When tipping paper air permeability is 150CU, the discharge relational model of described N-nitrosamine is: C=8.1771 – 82.5 × b1-0.0293 × b2 – 4.3600 × b6, wherein C is the discharge capacity of N-nitrosamine, b1 is cigarette paper additive consumption, b2 is air permeance for cigarette paper, and b6 is expanded cut stem mixed ratio;
When tipping paper air permeability is 300CU, the discharge relational model of described N-nitrosamine is: C=-2.7300+0.1403 × b2+0.0035 × b5, and wherein C is the discharge capacity of N-nitrosamine, and b2 is air permeance for cigarette paper, and b5 is filter stick pressure drop;
When tipping paper air permeability is 450CU, the discharge relational model of described N-nitrosamine is: C=9.3160-0.0626 × b2-(4.98 × 10 -5) × b4 – 8.6666 × b6, wherein C is the discharge capacity of N-nitrosamine, and b2 is air permeance for cigarette paper, and b4 is forming paper air permeability, and b6 is expanded cut stem mixed ratio;
Parameters on the size that N-nitrosamine burst size affects is: tipping paper air permeability > air permeance for cigarette paper > filter stick pressure drop > cigarette paper additive consumption > forming paper air permeability > expands swollen silk mixed ratio;
When repeating step 3) in step 4), also comprise according to N-nitrosamine discharge relational model obtain cigarette paper additive consumption, air permeance for cigarette paper, tipping paper air permeability, forming paper air permeability, filter stick pressure drop and expanded cut stem mixed ratio respectively with the relevance of N-nitrosamine burst size, and regulate the step of described parameter according to this relevance.
2. the method for adjustment of each Cigarette design parameter in the Cigarette design based on N-nitrosamine burst size according to claim 1, it is characterized in that, control method for described parameter is: the parameter of relevance to current use according to parameters and N-nitrosamine burst size regulates, first determine tipping paper air permeability, then increase according to the Cigarette design parameter of each correspondence under different tipping paper air permeability and the relevance formula of N-nitrosamine burst size or reduce the value of parameters.
3. the method for adjustment based on parameters in the Cigarette design of N-nitrosamine burst size according to claim 1, it is characterized in that, when tipping paper air permeability is 150CU, the control method for described parameter is following: improve air permeance for cigarette paper, improve cigarette paper additive consumption or to improve in expanded cut stem mixed ratio one or more combination adjusting method.
4. the method for adjustment based on parameters in the Cigarette design of N-nitrosamine burst size according to claim 1, it is characterized in that, control method for described parameter is, when tipping paper air permeability is 300CU, reduces air permeance for cigarette paper and/or reduces filter stick pressure drop.
5. the method for adjustment based on parameters in the Cigarette design of N-nitrosamine burst size according to claim 1, it is characterized in that, when tipping paper air permeability is 450CU, the control method for described parameter is following: improve air permeance for cigarette paper, improve forming paper air permeability, to improve in expanded cut stem mixed ratio one or more combination adjusting method.
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