CN100421574C - Purple common perilla seed feedstuff additive and preparation method thereof - Google Patents
Purple common perilla seed feedstuff additive and preparation method thereof Download PDFInfo
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- CN100421574C CN100421574C CNB2006100541258A CN200610054125A CN100421574C CN 100421574 C CN100421574 C CN 100421574C CN B2006100541258 A CNB2006100541258 A CN B2006100541258A CN 200610054125 A CN200610054125 A CN 200610054125A CN 100421574 C CN100421574 C CN 100421574C
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Abstract
The present invention provides a perilla seed extractive feed additive having the advantages of no poison or harmless, good effect, long storage life and high activity and a preparation method thereof. The feed additive is prepared from 10 to 90 portions by weight of perilla seed oil, 2 to 20 portions by weight of auxiliary agent and 1 to 80 portions by weight of filling agent, wherein the auxiliary agent is the mixture of linoleic acid, or oleic acid, or oleic acid and linoleic acid; and the feed additive is prepared by activation, stabilization and pulverization. The feed additive has the efficacy for increasing the quality of livestock and disease resistance, fowl and fish products, promoting the growth of livestock, fowls and aquatic animals, and enhancing the immunity.
Description
Technical field
The present invention relates to a kind of feed addictive, particularly a kind of purple common perilla seed feedstuff additive and preparation method thereof.
Background technology
Along with improving constantly of people's living standard, also more and more higher to the requirement of each side such as the security of feeds such as poultry, fowl, fish, trophism, become a global problem.In recent years, " rabid ox disease ", “ bioxin " reach " clenbuterol hydrochloride " poisoning and constantly take place; the antibiotic in the daily feed makes bacterium and the virus of harm poultry, fowl, fish develop immunity to drugs or morph; its consumption is increasing thereupon; the result that it accumulates in animal body, makes human beings'health be subjected to serious harm.Chinese scholars generally believes in recent years: developing nontoxic natural bioactivity substance and replace chemosynthesis product to make feed addictive, is the safest, valid approach.Contain compositions such as natural activity composition saponin, alkaloid, flavonoids, polysaccharide in the Chinese herbal medicine and unique effects person is arranged, attracted numerous scholars to be engaged in the research of this respect, developed some efficient, safe feedstuff additive products.But relate to polyunsaturated fatty acid seldom as the research of animal feed additive aspect.The eugenic element of going up sea blue merit bio tech ltd and the winning development in science and technology in Chongqing City Co., Ltd joint research and development is to be that raw material adds zein or soybean protein or wheat bran again and makes with purple perilla, wheat embryo, evening primrose mixed extract, growth result to poultry, fowl, fish is better, but this product is because added zein or soybean protein, the product storage life is short, mouldy easily, the raw materials for production cost is also higher.
Summary of the invention
The high activity purple common perilla seed feedstuff additive that the purpose of this invention is to provide a kind of nontoxic, harmless, better effects if, long shelf-life the present invention also aims to provide the preparation method of this feed addictive.
Concrete technical scheme is as follows:
A kind of purple common perilla seed feedstuff additive is characterized in that by following method preparation:
(1) gets Purple Perilla Seed Oil 10～90 by weight, auxiliary agent 2～20, filler 1～80; Wherein said Purple Perilla Seed Oil is an extract of taking supercritical CO 2 extraction purple perilla seed; Described auxiliary agent is linoleic acid or oleic acid or oleic acid and linoleic mixture;
(2) activation mixes according to the prescription consumption Purple Perilla Seed Oil and auxiliary agent and filler in Conicaldoublewormmixer, changes in K-enamel reaction still again, 38～84 ℃ of temperature, activates 0.5～36 hour under the condition of pressure maintenance 76～96kpa;
(3) stabilisation changes in the stabilisation device, with 36～58 ℃, carries out stabilization processes under 101～103kpa condition 2～46 hours;
(4) can pack after taking-up is pulverized and dispatch from the factory.
Wherein the described filler of step (1) is a kind of in zeolite powder or diatomite or the white carbon.
It is primary raw material that the present invention chooses natural Chinese herbal medicines purple perilla seed, takes the prior art supercritical CO
2Extraction purple common perilla seed Purple Perilla Seed Oil; Adjuvant used is linoleic acid or oleic acid or both mixtures, and when selecting both mixtures for use, mixed proportion does not have specific (special) requirements yet, as long as both total amount shared ratios in prescription are 2～20 parts.Used filler such as zeolite powder, diatomite, white carbon all can have been bought on market, and on procedure of processing, used equipment is the conventional equipment of the sector, no specific (special) requirements.
The main active ingredient of purple common perilla seed Purple Perilla Seed Oil is alpha-linolenic acid and linoleic acid, purple perilla seed, zeolite powder, diatomite, white carbon etc. are that the Ministry of Public Health defends method prison and sends out in [2005] No. 51 file attachment 1 a kind of among 87 kinds of article of " be food be again the article list of medicine " lining, so that purple perilla has is clearing heat and detoxicating, sterilization is antibiotic, the dispersing swelling and dissipating binds effect need not add other antibiotic again, has nourishing and strengthening vital again, nourishing blood and tranquilization, the effect of tonifying liver kidney tonifying, also have disease preventing and treating and function of health care, its function is varied.Contain perilla herb oil 35～50% in the purple common perilla seed, wherein the content of alpha-linolenic acid is up to 50%～70%; Also contain oleic acid, linoleic acid simultaneously, the latter can be transformed into gamma-Linolenic acid at animal body.Alpha-linolenic acid has following main effect:
(1) alpha-linolenic acid is to constitute all biomembranous important compositions in the livestock and poultry body, can increase the permeability of cell membrane, regulates the flowability of cell membrane lipid; Poultry, in the fowl body under the effect of corresponding enzyme, deriving becomes PGE3, EPA and the DHA with important physiologically active, these derivatives all optionally infiltrate some vitals of beasts, birds and aquatic products animal, as cell, musculature, cerebral cortex, retina, testis and sperm, and be one of ultimate constituent of monoethanolamine phosphatide and lipid sphyngomyelin (cell and neuron).
(2) alpha-linolenic acid is the signal transmitter substance of some genes in poultry, the fowl body, is the derivant of some gene.The countless physiological and biochemical procedures that these chemical messengers start or control volume is interior.These processes comprise the growth and the differentiation that promote poultry, fowl cells in vivo, improve blood circulation, blood pool, adjusting blood pressure, improve cholesterol metabolic, fundamentally regulate the fat metabolic balance.
(3) alpha-linolenic acid can strengthen skin elasticity, improve figure and features and hair outward appearance.
(4) alpha-linolenic acid can be included leucocyte in, can change the leucocyte flowability, increases immune response ability and ability disease-resistant, anti-inflammatory response.
(5) alpha-linolenic acid can promote the absorption of beasts, birds and aquatic products animal to vitamin A, D, E, K, helps the health of livestock and poultry, growth fast.
(6) alpha-linolenic acid can suppress the activity of lipese, reduces accumulating of animal body fat, improves lean meat percentage.
(7) alpha-linolenic acid has no side effect.And in certain dosage range, can strengthen the drug effect of the some drugs that is used in the livestock and poultry fish, alleviate its side effect.
Be rich in alpha-linolenic acid and linoleic acid in the purple common perilla seed, its Physiology and biochemistry mechanism such as Figure of description in body, from the physiological and biochemical procedure of accompanying drawing linolenic and linoleic as can be seen, it is different with general aliphatic acid, to animal a certain amount of alpha-linolenic acid and linoleic purple common perilla seed of being rich in of feeding, not only can replenish the required portion of energy of body, can also improve simultaneously some enzyme and the Physiology and biochemistry effect relevant with ω-6PUFA with ω-3, make linked groups's function of body more sound, reach good growth poised state.
Gained derivative products DHA, PG E
2, PG E
3, PG E
1, all optionally infiltrate some vitals of poultry, fowl aquatic products thing, as cell, musculature, cerebral cortex, retina, testis and sperm, and be one of ultimate constituent of monoethanolamine phosphatide and lipid sphyngomyelin (cell and neuron).
Supercritical CO
2In the fluid purple common perilla seed Purple Perilla Seed Oil, because its main active one-tenth alpha-linolenic acid and linoleic existence, it is to the effect of animal, be far above in providing certain quantity of energy to animal, key is a series of Johnson ﹠ Johnson reason active material that its metabolic conversion forms, can regulate the many biochemical functions in the animal body, influence the whole life process of animal, and use supercritical CO
2The purple common perilla seed of fluid extraction is that the various active components in the purple perilla seed are more fully extracted, and this just makes product can fully intactly show the peculiar effect of China's Chinese medicine legacy purple perilla seed.Particularly importantly prescription of the present invention can obtain optimum efficiency with the product that the relative amount of alpha-linolenic acid, linoleic acid, oleic acid in the purple common perilla seed controls to after it is transformed; And, obtained high activity again by activation processing and stabilization processes.Owing to do not contain protein component in the raw material, just prolonged the shelf-life yet.
The invention has the beneficial effects as follows the quality that improves poultry, fowl, fishery-ies product, be used to feed pigs that lean meat percentage improves more than 10%, yellowish pink good.Be used for feeding fish, dirty body is than reducing more than 20%, and the fish body fat reduces more than 30%.After being processed into delicatessen the trend that returns poultry, fowl, the original local flavor of fish is arranged, considerably beyond other feed addictive person that feeds.This is the exclusive effect of purple common perilla seed feedstuff additive.Purple common perilla seed promotes each growth phase that is grown in pig of poultry, fowl, aquatic livestock all to have and promotes the growth effect preferably that daily gain improves more than 7.0% than control group; Be used for poultry, daily gain improves about 8%, is used for fish, and the daily gain comparison is according to improving about 20%.Purple common perilla seed reduces the material consumption of poultry, fowl, aquatic livestock, and purple common perilla seed feed poultry, fowl, fish can be improved food conversion ratio, the feedstuff-meat ratio that feeds pigs reduces about 6%, raise the poultry feedstuff-meat ratio and reduce about 7%, egg fowl laying rate improves about 5%, and egg size improves more than 5%.Improve the figure and features livestock and poultry and feed after the purple common perilla seed, tangible change can appear in its build appearance.Can see on one's body that pig whole body body is solid plentiful, bodily form compactness, the fur light is ruddy, back of the body ditch is broad, bilateral meat ditch was high-visible between waist was striden, and rear quarters muscle protrudes, and overall appearance more meets the requirement of lean meat pig, can significantly improve the selling price of pork pig, effectively strengthen the competitiveness in the market sale.Be used for broiler, it is closely glossy mainly to show as feather, and comb is scarlet, and is strong, is subjected to consumer's welcome.Build up health, the result of study that improves units such as resistance against diseases Zhejiang Academy of Agricultural Science, Agricultural University Of Anhui shows, gives after the pig feeding purple common perilla seed T lymphocyte content in its blood and LS transformation index and erythrocytic C
3B acceptor rosette rate and immune compound rosette rate have improved 6～84%, thereby can strengthen the immunologic function of pig greatly, improve resistance against diseases.The Chinese Academy of Agricultural Sciences's feed is tested and is shown the purple common perilla seed of feeding can obtain and the feed same effect of aureomycin, and the former is absolute harmless.Owing to do not contain protein ingredient in the raw materials for production, so storage life prolongs greatly.For further specifying the reliable effect of the present invention, done following experiment by feed research institute of the Chinese Academy of Agricultural Sciences:
This test has carried out ingesting the varying level purple common perilla seed feedstuff additive to the growth of hybridized prussian carp and the influence of fish body composition.Test is filtered in the aquarium at cocycle flowing water temperature control and is carried out, and the specification of aquarium is 60 44 45.Test divides 4 feed groups and 1 control group, control group (foundation bait, abbreviation A group), feed ingredient B group (basestocks+100mg.kg feed of the present invention), C group (basestocks+300mg.kg feed of the present invention), D group (basestocks+500mg.kg feed of the present invention), E organize (basestocks+800mg.kg feed of the present invention), put hybridized prussian carp 15 tails in a suitable place to breed for every group, the time was 8 weeks.Result of the test shows: C organizes not only fish body weight gains (99.5%) maximum, and feed coefficient minimum (2.35), demonstration is than the clear superiority of control group growth, from the biochemical component analysis, the dirty body of C group is than little, and muscle protein content is higher, and particularly the fat content of internal organ and muscle is little, confirmed the remarkable growth result of C group feed from the another side more, confirmed that also the suitable addition on this feed basis is better about 300mg.kg.
Description of drawings
Fig. 1 is the physiological and biochemical procedure schematic diagram of leukotrienes under the effect of enzyme
Specific embodiment (totally 6 examples)
Embodiment 1:
With 90 parts of purple common perilla seed Purple Perilla Seed Oils and 32 parts of filler white carbons and 8 parts of auxiliary agent linoleic acid after mixing in the double worm mixer, change K-enamel reaction still over to, activation is 2 hours under 68 ℃ and 96kpa condition, then at 52 ℃, 103kpa makes 18 hours stabilization processes, and packing is dispatched from the factory after crushed.
Embodiment 2:
After mixing in the double worm mixer, in 76kpa, activation is 8 hours under 38 ℃ the condition with 56 parts of purple common perilla seed Purple Perilla Seed Oils and 46 parts of diatomite and 2 parts of linoleic acid, again at 42 ℃, and 103kpa stabilization processes 2 hours, packing is dispatched from the factory after crushed.
Embodiment 3:
With 60 parts of purple common perilla seed Purple Perilla Seed Oils and 45 parts of diatomite and 7 parts of auxiliary agents, in double worm mixer, mix, 84 ℃ and 86kpa activation processing 10 hours, at 48 ℃, 102kpa made stabilization processes 36 hours, pulverized the back packing and dispatched from the factory again.
Embodiment 4:
40 parts of purple common perilla seed Purple Perilla Seed Oils and 60 parts of diatomite and 10 parts of auxiliary agents are mixed in double worm mixer, change K-enamel reaction still over to, at 84 ℃, under the condition of 96kpa, through activation in 6 hours,, made stabilization processes under the 103kpa condition 42 hours again through 58 ℃.
Embodiment 5:
With 1 part in 10 parts of purple common perilla seed Purple Perilla Seed Oils and 20 parts of auxiliary agents and diatomite, after mixing in K-enamel reaction still, in 38 ℃, after making 32 hours activation processing under the 76pka condition, at 103kpa, made stabilization processes 36 hours for 42 ℃ again, pulverize the back packing and sell.
Embodiment 6:
With 30 parts of purple common perilla seed Purple Perilla Seed Oils, 80 parts in diatomite, 12 parts of auxiliary agents, in mixer in the double worm mixer, mix, again at 96kpa, activation is 26 hours under 55 ℃ of conditions, then at 101kpa, 46 ℃ of stabilisations crushing packing after 26 hours.
Claims (4)
1. purple common perilla seed feedstuff additive is characterized in that by following method preparation:
(1) gets Purple Perilla Seed Oil 10～90 by weight, auxiliary agent 2～20, filler 1～80; Wherein said Purple Perilla Seed Oil is to take supercritical CO
2The extract of extraction purple perilla seed; Described auxiliary agent is linoleic acid or oleic acid or oleic acid and linoleic mixture;
(2) activation mixes according to the prescription consumption Purple Perilla Seed Oil and auxiliary agent and filler in Conicaldoublewormmixer, changes in the K-enamel reaction still again, 38～84 ℃ of temperature, activates 0.5～36 hour under the condition of pressure maintenance 76～96kpa;
(3) stabilisation changes in the stabilisation device, with 36～58 ℃, carries out stabilization processes under 101～103kpa condition 2～46 hours;
(4) can pack after taking-up is pulverized and dispatch from the factory.
2. purple common perilla seed feedstuff additive as claimed in claim 1, wherein the described filler of step (1) is a zeolite powder.
3. purple common perilla seed feedstuff additive as claimed in claim 1, wherein the described filler of step (1) is a diatomite.
4. purple common perilla seed feedstuff additive as claimed in claim 1, wherein the described filler of step (1) is a white carbon.
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| CN102326705B (en) * | 2011-08-25 | 2014-10-29 | 山东新希望六和集团有限公司 | Compound feed for enhancing production performance and carcass quality of table poultry and preparation method thereof |
| CN103636948A (en) * | 2013-12-26 | 2014-03-19 | 重庆市优胜科技发展有限公司 | Liquorice extract feed additive |
| CN104068239A (en) * | 2014-05-13 | 2014-10-01 | 范治淮 | Wine-flavor multi-element crucian feed and preparing method of wine-flavor multi-element crucian feed |
| CN104206797A (en) * | 2014-07-15 | 2014-12-17 | 浙江大学 | Natural productpreparation for increasing content of CLA in milk and meat of ruminant |
| CN106858083A (en) * | 2017-02-23 | 2017-06-20 | 西南大学 | A kind of feed for improving milk production of cow and coffin hardness and preparation method thereof |
| CN107242386A (en) * | 2017-06-29 | 2017-10-13 | 重庆市万源禽蛋食品有限公司 | Chicken feed and its preparation method and application |
| CN109043147A (en) * | 2018-09-18 | 2018-12-21 | 重庆市优胜科技发展有限公司 | Enhance the composition and preparation method thereof of animal immunizing power |
| CN109287872A (en) * | 2018-11-29 | 2019-02-01 | 佛山市南海东方澳龙制药有限公司 | For improving the additive and its preparation method and application of poultry immunity of organisms |
| CN110169514A (en) * | 2019-06-03 | 2019-08-27 | 天津农学院 | It is a kind of to improve the feed formula of Omega-3 polyunsaturated fatty acid and application in broiler chicken product |
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Non-Patent Citations (2)
| Title |
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| 日粮中添加紫苏籽对鸡蛋黄脂肪酸组成及ω_3、ω_6影响的研究.. 臧素敏等.河北农业大学学报.，第26卷第1期. 2003 |
| 日粮中添加紫苏籽对鸡蛋黄脂肪酸组成及ω_3、ω_6影响的研究.. 臧素敏等.河北农业大学学报.，第26卷第1期. 2003 * |
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Assignee: CHONGQING SUPER SCIENCE & TECHNOLOGY DEVELOPMENT CO., LTD. Assignor: Huang Zhigui Contract record no.: 2011500000053 Denomination of invention: Purple common perilla seed feedstuff additive and preparation method thereof Granted publication date: 20081001 License type: Exclusive License Open date: 20061011 Record date: 20110901 |