CH93492A - Process for the preparation of a dye of the phenyldinaphtylmethane series. - Google Patents
Process for the preparation of a dye of the phenyldinaphtylmethane series.Info
- Publication number
- CH93492A CH93492A CH93492DA CH93492A CH 93492 A CH93492 A CH 93492A CH 93492D A CH93492D A CH 93492DA CH 93492 A CH93492 A CH 93492A
- Authority
- CH
- Switzerland
- Prior art keywords
- dye
- acid
- preparation
- phenyldinaphtylmethane
- series
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B11/00—Diaryl- or thriarylmethane dyes
- C09B11/04—Diaryl- or thriarylmethane dyes derived from triarylmethanes, i.e. central C-atom is substituted by amino, cyano, alkyl
- C09B11/06—Hydroxy derivatives of triarylmethanes in which at least one OH group is bound to an aryl nucleus and their ethers or esters
Description
Verfahren zur Herstellung eines Farbstoffe-s der Plienyldinahhtylnietlianreihe. Es wurde- gefunden, dass, wenn man a12' 1-Naphtol-2-e,rbonsäiire 4-Clilorbenzoltri- chlorid in (-T'e"enwart eines säurebindenden Mittels.
vorzugsweise unter Zugabe eines Katalysators, einwirken lässt, ein neuer Farb- toff erhalten wird. Dieser Farbstoff gibt s<B>s</B> auf Wolle, aus saurein Bade gefärbt eine graue Färbung, welche beine Nachchroniieren in ein reines. N- orzüglicli echtes Grün über geht.
Beispiel: 752 Teile 1-Naphtol-2-carlionsäure -,ver- den - in 1900 Teilen Natronlauge von 30 Gew. und 500 Teilen -\Vasser gelöst. Hier auf gibt inan ! 34 Teile 4-Clilorbenzotrichlorid und 0,5 Teile Kupfer hinzu und rührt so lange, bis alles Benzotriclilorid verschwunden ist.
Das Natriumsalz des gebildeten Farb stoffes wird durch Aussalzen aus dein mit Wasser verdünnten Reaktionsgemisch abge schieden.
Process for the preparation of a dye of the Plienyldinahhtylnietlian reason. It has been found that if one converts a12 '1-naphthol-2-e, carbonic acid 4-chlorobenzene trichloride into (-T'e "in the presence of an acid-binding agent.
preferably with the addition of a catalyst, a new dye is obtained. This dye gives s <B> s </B> on wool, dyed from acidic bath a gray color, which is followed by post-chronizing into a pure. N- orzüglicli real green goes over.
Example: 752 parts of 1-naphthol-2-carlionic acid - dissolved in 1900 parts of 30% by weight sodium hydroxide solution and 500 parts of water. Give up here! Add 34 parts of 4-chlorobenzotrichloride and 0.5 part of copper and stir until all the benzotricliloride has disappeared.
The sodium salt of the dye formed is separated out by salting out the reaction mixture diluted with water.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH93492T | 1921-01-18 | ||
CH92406T | 1921-01-18 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH93492A true CH93492A (en) | 1922-03-01 |
Family
ID=25704488
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH93492D CH93492A (en) | 1921-01-18 | 1921-01-18 | Process for the preparation of a dye of the phenyldinaphtylmethane series. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH93492A (en) |
-
1921
- 1921-01-18 CH CH93492D patent/CH93492A/en unknown
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