CH692084A5 - Device for degreasing and drying mechanical components using ultrasound and non-halogen hydrocarbon solvent comprises airtight enclosure under controlled pressure and temperature - Google Patents

Device for degreasing and drying mechanical components using ultrasound and non-halogen hydrocarbon solvent comprises airtight enclosure under controlled pressure and temperature Download PDF

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Publication number
CH692084A5
CH692084A5 CH74198A CH74198A CH692084A5 CH 692084 A5 CH692084 A5 CH 692084A5 CH 74198 A CH74198 A CH 74198A CH 74198 A CH74198 A CH 74198A CH 692084 A5 CH692084 A5 CH 692084A5
Authority
CH
Switzerland
Prior art keywords
degreasing
solvent
temperature
ultrasound
mechanical components
Prior art date
Application number
CH74198A
Other languages
French (fr)
Inventor
Jean-Francois Fallot
Original Assignee
Egaclean Sa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Egaclean Sa filed Critical Egaclean Sa
Priority to CH74198A priority Critical patent/CH692084A5/en
Publication of CH692084A5 publication Critical patent/CH692084A5/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23GCLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G5/00Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents
    • C23G5/02Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents
    • C23G5/024Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents containing hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/50Solvents
    • C11D7/5004Organic solvents
    • C11D7/5027Hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23GCLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G5/00Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents
    • C23G5/02Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents
    • C23G5/04Apparatus
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22Organic compounds
    • C11D7/24Hydrocarbons

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Cleaning By Liquid Or Steam (AREA)
  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)

Abstract

A device for degreasing and drying mechanical components comprises an airtight enclosure containing a solvent, of non-halogen hydrocarbon-type with a flash point of 40-100 deg C, in which the components are immersed and a source of ultrasonic emissions greater than 15 kHz. The enclosure is maintained at at least 120 mbar and 60 deg C. Preferred Features: The device is such that the solvent can be changed and allows the components to be treated successively with several solvents with different chemical compositions adapted to the stains encountered on the components

Description

       

  



  Des solvants inflammables remplaçant les solvants chlorés sont utilisés dans l'industrie mécanique à une température n'excédant pas 15 DEG C au-dessous du point-éclair. 



  Les qualités de solvabilité du système de dégraissage présenté ci-dessus sont nettement améliorées par rapport aux systèmes actuellement en exploitation. 



  Cette amélioration est dûe d'une part à la température élevée qui accroît la solvabilité des huiles et graisses, d'autre part à l'effet du vide qui permet une meilleure pénétration du solvant dans les trous borgnes. En outre, le solvant est en permanence sous vide. Il est donc dégazé, ce qui améliore notablement l'efficacité des ultrasons. Les systèmes actuels pompent le solvant inflammable dans la chambre de travail à la pression atmosphérique, ce qui provoque un apport d'air dans la solution. Les ultrasons ont alors pour effet de dégazer la solution et non de caviter sur les pièces. Les temps de dégazage sont de l'ordre de quinze minutes alors que les temps de lavage sont en général inférieurs à cinq minutes.

   La mesure de la puissance des ultrasons dans une solution dégazée à une température supérieure à 60 DEG C démontre l'accroissement de puissance ultrasonore, par rapport à une solution non dégazée à moins de 40 DEG C. 



  Les phases d'injection de vapeur et de séchage qui complètent le cycle de dégraissage-séchage du système décrit ci-dessus sont identiques aux systèmes actuellement en exploitation. 



  La législation (OPAIR) impose des machines de lavage-séchage industriel recyclant les émissions de composés organiques volatils (COV) afin de minimiser ces émissions. 



  La présente invention permet d'améliorer l'efficacité du dégraissage et du séchage en utilisant des solvants de type hydrocarbures non halogénés dont le point-éclair est situé entre 40 DEG C et 100 DEG C. On utilise depuis quelques années des machines de dégraissage fermées exploitant des solvants de ce type à 15 DEG C au moins en-dessous du point-éclair. 



  La présente invention utilise ce type de solvants sous vide, au-dessus du point-éclair. Ce procédé améliore la qualité du nettoyage, en raison d'une meilleure solvabilité des huiles et graisses et facilite le séchage des pièces. La distillation du solvant selon les techniques usuelles permet de minimiser les pertes de solvant. 



  L'utilisation successive de différents solvants permet d'optimiser le cycle de nettoyage en utilisant des solvants non-polaires ou polaires. 



  L'invention garantit en outre la sécurité de l'installation, puisque le vide inférieur à 120 mbar empêche pratiquement la formation d'un mélange de gaz explosible. En outre même en cas de formation de mélange explosible et d'explosion, l'expansion de volume de sept fois le volume initial qui résulte de l'explosion permet de rester à une pression inférieure à 840 mbar, donc inférieure à la pression atmosphérique. Ceci élimine donc tout risque de dégât à l'installation et de risque pour l'opérateur.



  



  Flammable solvents replacing chlorinated solvents are used in the engineering industry at a temperature not exceeding 15 DEG C below the flash point.



  The solvency qualities of the degreasing system presented above are significantly improved compared to the systems currently in operation.



  This improvement is due on the one hand to the high temperature which increases the solvency of oils and greases, on the other hand to the effect of the vacuum which allows better penetration of the solvent into the blind holes. In addition, the solvent is permanently under vacuum. It is therefore degassed, which significantly improves the efficiency of ultrasound. Current systems pump the flammable solvent into the working chamber at atmospheric pressure, which causes air to enter the solution. The ultrasound then has the effect of degassing the solution and not of cavitating on the parts. The degassing times are of the order of fifteen minutes while the washing times are generally less than five minutes.

   Measuring the power of ultrasound in a degassed solution at a temperature above 60 DEG C demonstrates the increase in ultrasonic power, compared to a non-degassed solution at less than 40 DEG C.



  The steam injection and drying phases which complete the degreasing-drying cycle of the system described above are identical to the systems currently in operation.



  Legislation (OPAIR) imposes industrial washing-drying machines recycling volatile organic compound (VOC) emissions in order to minimize these emissions.



  The present invention makes it possible to improve the efficiency of degreasing and drying by using solvents of non-halogenated hydrocarbon type whose flash point is located between 40 DEG C and 100 DEG C. For a few years, closed degreasing machines have been used using solvents of this type at 15 DEG C at least below the flash point.



  The present invention uses this type of solvent under vacuum, above the flash point. This process improves the quality of cleaning, due to better solvency of oils and greases and facilitates the drying of parts. The distillation of the solvent according to the usual techniques makes it possible to minimize the losses of solvent.



  The successive use of different solvents makes it possible to optimize the cleaning cycle by using non-polar or polar solvents.



  The invention also guarantees the safety of the installation, since the vacuum of less than 120 mbar practically prevents the formation of an explosive gas mixture. Furthermore, even in the event of the formation of an explosive mixture and of an explosion, the volume expansion of seven times the initial volume which results from the explosion makes it possible to remain at a pressure below 840 mbar, therefore below atmospheric pressure. This therefore eliminates any risk of damage to the installation and of risk for the operator.


    

Claims (2)

1. Dispositif de dégraissage et séchage de pièces mécaniques, comportant une enceinte étanche, enceinte contenant un solvant dans lequel lesdites pièces sont immergées, et des moyens d'émission ultrasonore supérieure à 15 kHz, caractérisé en ce que ledit solvant est de type isoparaffine ou alcane, dont le point-éclair est situé entre 40 DEG C et 100 DEG C et en ce que ledit dispositif comporte des moyens pour maintenir la pression dans l'enceinte à moins de 120 mbar et la température à plus de 60 DEG C à l'intérieur de l'enceinte.   1. Degreasing and drying device for mechanical parts, comprising a sealed enclosure, enclosure containing a solvent in which said parts are immersed, and ultrasonic emission means greater than 15 kHz, characterized in that said solvent is of the isoparaffin type or alkane, the flash point of which is located between 40 DEG C and 100 DEG C and in that said device comprises means for maintaining the pressure in the enclosure at less than 120 mbar and the temperature at more than 60 DEG C at l inside the enclosure. 2. Dispositif selon la revendication 1, comportant des moyens de changer de solvant et traiter de manière successive lesdites pièces avec plusieurs solvants de type isoparaffine ou alcane, de composition chimiques différente, adaptée aux salissures rencontrées. 2. Device according to claim 1, comprising means for changing the solvent and successively treating said parts with several solvents of isoparaffin or alkane type, of different chemical composition, suitable for the dirt encountered.
CH74198A 1998-03-27 1998-03-27 Device for degreasing and drying mechanical components using ultrasound and non-halogen hydrocarbon solvent comprises airtight enclosure under controlled pressure and temperature CH692084A5 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CH74198A CH692084A5 (en) 1998-03-27 1998-03-27 Device for degreasing and drying mechanical components using ultrasound and non-halogen hydrocarbon solvent comprises airtight enclosure under controlled pressure and temperature

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH74198A CH692084A5 (en) 1998-03-27 1998-03-27 Device for degreasing and drying mechanical components using ultrasound and non-halogen hydrocarbon solvent comprises airtight enclosure under controlled pressure and temperature

Publications (1)

Publication Number Publication Date
CH692084A5 true CH692084A5 (en) 2002-01-31

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Family Applications (1)

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CH74198A CH692084A5 (en) 1998-03-27 1998-03-27 Device for degreasing and drying mechanical components using ultrasound and non-halogen hydrocarbon solvent comprises airtight enclosure under controlled pressure and temperature

Country Status (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1338680A1 (en) * 2002-02-22 2003-08-27 Egaclean AG Apparatus for degreasing and drying metallic, ceramic or polymeric articles
EP2260953A1 (en) * 2008-04-02 2010-12-15 Infinity Enterprises, Inc. Cleaning system

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1338680A1 (en) * 2002-02-22 2003-08-27 Egaclean AG Apparatus for degreasing and drying metallic, ceramic or polymeric articles
EP2260953A1 (en) * 2008-04-02 2010-12-15 Infinity Enterprises, Inc. Cleaning system
EP2260953A4 (en) * 2008-04-02 2012-07-04 Infinity Entpr Inc Cleaning system

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Owner name: AMSONIC AG

Free format text: EGACLEAN SA#RUE DES PRES 19#2017 BOUDRY (CH) -TRANSFER TO- AMSONIC AG#ZUERICHSTRASSE 3#2504 BIEL (CH)

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