WO2003006184A1 - Washing device and washing method - Google Patents

Washing device and washing method Download PDF

Info

Publication number
WO2003006184A1
WO2003006184A1 PCT/JP2002/007137 JP0207137W WO03006184A1 WO 2003006184 A1 WO2003006184 A1 WO 2003006184A1 JP 0207137 W JP0207137 W JP 0207137W WO 03006184 A1 WO03006184 A1 WO 03006184A1
Authority
WO
WIPO (PCT)
Prior art keywords
cleaning
vacuum
solution
drying
dried
Prior art date
Application number
PCT/JP2002/007137
Other languages
French (fr)
Japanese (ja)
Inventor
Kiyoshi Mito
Katsuhisa Ohta
Shinji Masuoka
Yutaka Asada
Original Assignee
Sharp Kabushiki Kaisha
Sharp Manufacturing System Kabushiki Kaisha
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP2001213459A external-priority patent/JP3818876B2/en
Priority claimed from JP2001229400A external-priority patent/JP2003039029A/en
Application filed by Sharp Kabushiki Kaisha, Sharp Manufacturing System Kabushiki Kaisha filed Critical Sharp Kabushiki Kaisha
Publication of WO2003006184A1 publication Critical patent/WO2003006184A1/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • B08B3/10Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
    • B08B3/12Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations

Definitions

  • the present invention relates to a cleaning apparatus for cleaning electronic, mechanical, and molding-related parts, and a method for cleaning such parts.
  • the present invention provides ultrasonic cleaning to water or a hydrocarbon-based cleaning liquid placed in a vacuum.
  • the present invention relates to a cleaning apparatus for cleaning a part immersed in a cleaning liquid, and a cleaning method for ultrasonically cleaning a part under vacuum and then drying the part in a vacuum.
  • fluorine-based solutions such as chlorofluorocarbons and chlorine-based solutions such as 1,1,1-trichloroethane have been often used as cleaning solutions for cleaning parts.
  • these vaporized solutions are said to have the property of depleting the ozone layer, and in 1987, the Montreal Protocol on Substances That Deplete the Ozone Layer, the force on the The phase-in convention was adopted in accordance with the stipulations on the gradual reduction and regulation of production volume for specified CFCs. Since then, it has been reviewed several times, and revisions have been made, such as the addition of regulated substances and the advancement of the regulatory schedule.
  • water is used.
  • water itself is inexpensive, it requires many additional facilities related to water handling, and installation of such facilities requires a great deal of cost. That is.
  • ancillary equipment besides the washing equipment itself, for example, water storage equipment, sedimentation / purification / sludge treatment equipment, drainage equipment, or pretreatment equipment when low-purity water is used,
  • these installation spaces and auxiliary space for maintenance are required.
  • initial operation and maintenance costs are inevitable for the operation, maintenance, and drainage management of these facilities. In particular, in drainage management, care must be taken to ensure that the water quality standards are met when draining used water.
  • the expected cleaning effect may not be obtained due to the wettability of water.
  • the surface tension of water is 68.74 ⁇ 0.05 dy n / cm at 45 ° C, and 72.7 ⁇ 0.05 dyn / cm at 20 ° C, which is quite a base value. high.
  • CFC113 at 1 ° dyn / cm 2 at 25 ° C, 25 dyn / cm2 at 1,0,1,1-trichloroethane. Only 13-1 Z 4 for cm and water. In other words, it can be said that water has poor wettability as compared with a solution that has been frequently used in the past.
  • the internal oxygen concentration is extremely low, which can prevent ignition and, even if there is a defect in the piping system, the negative pressure does not cause the internal solution or vapor to leak out, ensuring safety. Because it leads to In addition, in the case of a cleaning apparatus, if the cleaning liquid is placed under reduced pressure when applying ultrasonic vibration to the cleaning liquid, it is possible to easily generate cavitation as a cleaning power, thereby improving the cleaning power. In the case of a drying device, the saturated vapor pressure is reduced under reduced pressure, so the boiling point of the solution is substantially reduced, and the solution can be easily evaporated compared to that in a normal pressure atmosphere, and the drying property is improved. This is because it is advantageous for.
  • a conventional vacuum ultrasonic cleaning apparatus for example, according to Japanese Patent Application Laid-Open No. 2000-33349, has a lid as shown in FIGS.
  • a vibration plate 103 integral with the cover 107 is disposed on the bottom wall of the washing tank 101 storing the washing liquid 102, and one end is connected to the solenoid valve 104 and the vacuum pump 105.
  • Connecting piping 1 0 6 a, 10 6 b force branching from the other end of 10 6 Connect to washing tank 10 1 and cover 10 7 respectively
  • a vibrator 108 covered with a case is disposed inside the cleaning tank 101 (throw-in type), and the piping 106a and 106b are respectively connected. It is connected to the cleaning tank 101 and the vibrator 108 (see Fig. 15).
  • the vacuum pump 105 by operating the vacuum pump 105 and opening the solenoid valve 104, the pressure inside the cleaning tank 101 is reduced to put the cleaning liquid 102 under vacuum, and the diaphragm is added to the cleaning liquid 102. Ultrasonic vibration is applied from 103 and the vibrator 108 to clean the immersed object to be cleaned.
  • the inside of the case that covers the cover 107 and the vibrator 108 is reduced in pressure through the same pipe 106, so that the case that covers the cover 107 and the vibrator 108 is also reduced. Since there is no pressure difference between the inside of the chamber and the inside of the washing tank 101, they can bend or deform without making the case that covers the diaphragm 103 and the vibrator 108 thicker. Disappears.
  • vent gas a compressed gas or air
  • a compressed gas or air (hereinafter sometimes referred to as “vent gas”) is introduced into the cleaning tank 101 to change the pressure from the vacuum state to the normal pressure.
  • a vacuum a compressed gas or air
  • vent gas is introduced into the cleaning tank 101 to perform this venting, the mist-like cleaning liquid 102 floating in the cleaning tank 101 is connected to the piping by negative pressure action.
  • diaphragm 1 or 3 108 is driven by electricity, and the charging section that controls the electric drive is provided inside the case that covers the cover 107 and the vibrator 108. If a flammable hydrocarbon-based cleaning solution is used, the live parts may become an ignition source and ignite the mist-like cleaning liquid 102 accumulated around the live parts, causing a fire or explosion. It also has the disadvantage that it is very likely to be caused.
  • the object to be dried to which the cleaning liquid is attached is placed in a vacuum container, and the state of vacuum is applied, whereby the cleaning liquid attached to the object to be dried is vaporized.
  • the necessary heat evaporation latent heat
  • the temperature of the material to be dried gradually decreases, and when this temperature falls below the saturated vapor pressure temperature, if the degree of vacuum in the vacuum vessel is in the same state, then, Since the boiling and evaporation of the cleaning liquid are stopped, in order to avoid this situation, generally, the vacuum capacity is further increased to increase the ultimate vacuum, or the temperature of the material to be dried at the start of evacuation is increased. In addition, a device for supplying heat to the material to be dried during evacuation is required.
  • the present invention has been made in view of the above-described problems, and suppresses a pressure difference between inside and outside of a main component and between the components, so that airtightness can be easily achieved without special consideration. It is an object of the present invention to provide a vacuum ultrasonic cleaning apparatus which is capable of maintaining the above conditions and which is excellent in safety against fire and explosion even when a flammable cleaning liquid is used.
  • a cleaning apparatus is directed to a cleaning apparatus for applying an ultrasonic vibration to a cleaning liquid placed under vacuum to clean an object to be cleaned immersed in the cleaning liquid,
  • a cleaning tank for storing and holding the object to be cleaned, and a vibrator having a predetermined space therein and applying ultrasonic vibration to the cleaning liquid, provided in a vacuum chamber for cleaning capable of maintaining a vacuum state,
  • a predetermined space is opened in the cleaning vacuum vessel. This allows the cleaning tank and the vibrating body to be under the same pressure, and there is no pressure difference between the inside and outside of the cleaning tank and the vibrating body. Airtightness can be maintained.
  • a charging section for generating ultrasonic vibration is generally provided in a predetermined space of the vibrating body, but if a flammable cleaning liquid such as a hydrocarbon-based cleaning liquid is used as the cleaning liquid, the cleaning liquid leaks. If there is a risk of causing a fire or explosion when the charged part is in a predetermined space due to an ignition source, a purge gas for purging a predetermined space of the vibrator is supplied to the predetermined space.
  • a purge gas supply means is provided.
  • a vibrator that emits ultrasonic vibration is provided in the predetermined space formed by a vibration plate through which ultrasonic vibration propagates and a cover mounted on the vibration plate.
  • the diaphragm is disposed so that the predetermined space faces the outside of the cleaning tank so as to close an opening formed in a bottom wall or a side wall of the cleaning tank. It is preferable that the diaphragm is fixed by inserting a bolt from a peripheral portion of the diaphragm into a through hole penetrating the bottom wall or the side wall of the cleaning tank.
  • the cleaning liquid stored in the cleaning tank may leak through the through-hole, but if the cleaning liquid leaks through the through-hole and does not enter the predetermined space, the vibrator may erode. Or the risk of fire or explosion from the charged part of the transducer as an ignition source is greatly reduced, so the cover is attached at the center side of the through hole on the diaphragm.
  • the center of the diaphragm is depressed with respect to the cleaning tank more than the peripheral portion having the through hole.
  • the cover is mounted on the central portion of the diaphragm.
  • the vibrating body provided on the side wall and bottom wall may be inadvertently wetted along the outer surface of the side wall.
  • the upper end of the side wall of the cleaning tank is bent outward and downward so as to keep away from the side wall of the tank.
  • the lower end of the side wall of the cleaning tank has a bottom end in order to prevent the cleaning liquid from wrapping around the bottom wall provided with the vibrator and the like. It is good to project below the wall. Furthermore, if the cleaning liquid flowing down the outer wall of the side wall can be collected at a predetermined position, the recovery becomes easier.For example, the edge of the lower end portion of the side wall of the cleaning tank is uneven or has a flat surface. It may be inclined.
  • the cleaning apparatus comprises: a cleaning tank for storing a cleaning liquid and accommodating an object to be cleaned; and a vibrator having a predetermined space therein and applying ultrasonic vibration to the cleaning liquid, comprising: A predetermined space of the vibrator is provided in the container, and the predetermined space of the vibrator is opened in the cleaning vacuum container. The cleaning liquid placed under vacuum is subjected to ultrasonic vibration to immerse the cleaning liquid in the cleaning liquid.
  • Cleaning means for cleaning the cleaning object a vacuum container for drying capable of holding the object to be cleaned which has been cleaned by the cleaning means as an object to be dried and taking a vacuum state; and a heating container for storing the heated solution And a pipe communicating the drying vacuum vessel and the heating vessel.
  • One end of the pipe is opened toward the object to be dried, and the other end of the pipe is immersed in the solution.
  • a drying means which is opened and injects the solution in a boiling state from the one end of the pipe toward the object to be dried, and dries the object to be dried.
  • the object to be cleaned is first subjected to safe ultrasonic cleaning under vacuum by the cleaning means, and then the heat is efficiently applied to the object to be dried in the vacuum state by the drying means. Dry in time Dried.
  • the solution sprayed toward the object to be dried has a low latent heat of vaporization that can be evaporated even if the temperature of the object to be dried is not so high.
  • the solution is a hydrocarbon-based solution Good.
  • the heating vessel is divided into two chambers by partition walls. It is preferable that one side contains the solution and the other side is provided with a heat source, and the heat from the heat source is applied to the solution through the partition wall so that the solution is heated.
  • a drive valve is provided in the pipe path, and the It is preferable that the degree of opening and closing of the drive valve is adjusted based on a pressure in a vacuum vessel, a pressure in the heating vessel containing the solution, and a temperature of the solution.
  • the condensed solution is heated by applying heat to the object to be dried and vaporized again to heat the object to be dried or the temperature in the vacuum vessel can be increased more rapidly, the efficiency will increase.
  • at least one of the inner side surface and the bottom surface of the drying vacuum container is provided with a heating means.
  • the solution is sprayed toward the object to be dried and the drying is performed in consideration of reuse of the solution without impairing the properties of the solution.
  • the solution injected toward the object to be dried is always in a purified new liquid state, and the solution injected toward the object to be dried and collected on the bottom surface of the vacuum chamber for drying is desirably used. It is preferable to provide a solution discharging means for collecting and discharging.
  • a cleaning method for achieving the above object, comprises: a cleaning tank that stores a cleaning liquid and stores an object to be cleaned; and a vibrator that has a predetermined space therein and applies ultrasonic vibration to the cleaning liquid.
  • a cleaning state that can be maintained in a vacuum state;
  • a space is opened in the vacuum chamber for cleaning, a cleaning step of applying ultrasonic vibration to the cleaning liquid placed under vacuum, and cleaning the object to be cleaned immersed in the cleaning liquid;
  • a vacuum container for drying capable of holding the object to be cleaned after drying as a material to be dried and maintaining a vacuum state, a heating container for storing a heated solution, and communicating the vacuum container for drying with the heating container.
  • One end of the pipe is opened toward the object to be dried, the other end of the pipe is immersed in the solution, and the pipe is evacuated when the drying vacuum container is in a vacuum state.
  • a drying step in which the solution is opened and the solution is sprayed in a boiling state from the one end of the pipe toward the object to be dried, and the object to be dried is dried.
  • FIG. 1 is a configuration diagram showing a configuration of an entire cleaning apparatus according to a first embodiment of the present invention
  • FIG. 2 is a sectional view of a main part of a cleaning unit in the cleaning apparatus of the first embodiment.
  • FIG. 3 is a diagram schematically showing a state of leakage of the cleaning liquid.
  • FIG. 4 is a diagram schematically showing a state in which the cleaning liquid drips.
  • FIG. 5 is a sectional view of a main part of a lower portion of a cleaning tank in a cleaning device according to a second embodiment.
  • FIG. 6 is a cross-sectional view of a main part of a cleaning unit in a cleaning device according to a third embodiment.
  • FIG. 7 is an enlarged view of part A of FIG. 6 schematically showing the state of leakage of the cleaning liquid.
  • FIG. 8 is a side view of the lower part of the cleaning tank in the cleaning device of the fourth embodiment.
  • FIG. 9 is a side view of the lower part of the cleaning tank in the cleaning device of the fifth embodiment.
  • FIG. 10 is a diagram illustrating an example of the physical properties of the cleaning liquid.
  • FIG. 11 is a configuration diagram showing the configuration of the entire drying apparatus according to the sixth embodiment.
  • FIG. 12 is a cross-sectional view of a main part of a drying unit in a drying device according to a sixth embodiment.
  • FIG. 13 is a cross-sectional view of a main part of a drying unit in the drying device according to the seventh embodiment.
  • FIG. 14 is a sectional view of a main part of a conventional cleaning apparatus.
  • FIG. 15 is a sectional view of a main part of another conventional cleaning apparatus. BEST MODE FOR CARRYING OUT THE INVENTION
  • FIG. 1 is a configuration diagram of the entire cleaning apparatus
  • FIG. 2 is a cross-sectional view of a main part of the cleaning unit in FIG.
  • the washing apparatus is roughly divided into a washing section and a distillation section.
  • the distillation section is composed of a still, a primary tank, a drain tank, a reheater, a condenser, cooling water, hot water, a water removal unit, etc., but is not directly related to the present invention. Omitted.
  • 1 is a vacuum vessel (hereinafter sometimes referred to as a “vacuum vessel for cleaning” to distinguish it from the vacuum vessel 201 for drying described later)
  • 2 is the lid of the vacuum vessel 1
  • 3 is related to electronics, machinery, and molding.
  • An object to be cleaned such as parts, 4 is a basket for storing the object to be cleaned 3, 5 is a hydrocarbon-based cleaning liquid, 6 is a cleaning tank for storing the object to be cleaned 3, and 7 is an ultrasonic vibrator unit.
  • the vacuum vessel 1 is formed in a cylindrical shape with an open upper end, and has a cleaning tank 6 and an ultrasonic oscillator unit 7 installed inside.
  • a lid that rotates around the base shaft 2a is located at the open upper end. It has two. In other words, with the lid 2 rotated and opened, the net-like basket 4 containing the object 3 to be washed is put in and out of the vacuum vessel 1, while the vacuum vessel 1 is closed and closed. It has become so.
  • vacuum evacuation ⁇ 1a is formed on the bottom wall of the vacuum vessel 1, and a pressure sensor 17 for detecting the pressure in the vacuum vessel 1 is provided on the lid 2.
  • the cleaning tank 6 is roughly divided into a storage section 6a for storing the cleaning liquid 5 and a overflow collecting section 6h for collecting the cleaning liquid 5 overflowing from the storage section 6a, sharing the bottom wall 6d.
  • a cleaning liquid supply ⁇ 6 g for supplying the cleaning liquid 5 is formed on the side wall of the storage tank section 6 a, an opening 6 f is formed above the cleaning liquid supply ⁇ 6 g, and a pair of upper and lower liquids sandwiching the opening ⁇ 6 f is formed.
  • Position sensor 15 is arranged.
  • the cleaning liquid 5 stored in the storage tank section 6a flows out of the opening ⁇ 6f to the overflow collecting section 6h when it exceeds the opening ⁇ 6f, and on the other hand, by the liquid level sensor 15.
  • the cleaning liquid supply port 6 g is connected to a liquid supply pipe 35 communicating with a cleaning liquid temperature control tank 30 described later, and an opening 6 i is formed in the bottom wall 6 d of the overflow liquid recovery section 6 h.
  • the storage section 6a is provided with a temperature sensor 16 for detecting the temperature of the cleaning liquid 5.
  • the upper end 6c of the side wall 6b of the cleaning tank 6 is bent outward and downward, while the lower end 6e protrudes below the bottom wall 6d.
  • the ultrasonic vibrator unit 7 includes a vibrating plate 8 through which ultrasonic vibration propagates, a plurality of vibrators 9 mounted on the lower surface of the vibrating plate 8 to generate ultrasonic vibrations, and a vibrator surrounding each of the vibrators 9.
  • An inner space 7 a is formed by a cover 10 attached to the lower surface of the plate 8 and surrounded by the vibration plate 8 and the cover 10.
  • the diaphragm 8 has a central portion 8a to which the respective vibrators 9 are attached, which is raised one step above the peripheral portion 8b, and the cover 10 is attached on the central portion 8a. I have.
  • An opening 6j is formed in the bottom wall 6d of the storage tank 6a, and the diaphragm 8 is arranged so as to close the opening 6j with the upper surface of the central portion 8a of the diaphragm 8.
  • a bolt 1 2 is inserted into a through hole (not shown) that penetrates the peripheral portion 8 b of the diaphragm 8, the bottom wall 6 d of the cleaning tank 6, and a Teflon (R) packing 13 sandwiched therebetween. And is fastened.
  • the end of each of the vibrators 9 driven by electricity is provided with a charging section 9 a for controlling its electric drive.
  • the cover 10 has a suction port 10 a and a vacuum vessel 1. And an exhaust port 10b to which a check valve 11 that allows the internal space ⁇ a to be opened only toward the exhaust port is formed.
  • the vacuum exhaust port 1a of the vacuum vessel 1 is connected to one end of a vacuum exhaust pipe 20 provided with solenoid valves 21 and 22 in a path, and the other end of the vacuum exhaust pipe 20 is connected to a vacuum pump 25. It is linked to Further, a gas-liquid separator 26 is provided downstream of the vacuum pump 25.
  • the evacuation pipe 20 branches off between the solenoid valves 21 and 22 to form a branch pipe 20 a connected to the opening 6 i of the overflow collection part 6 h.
  • a solenoid valve 23 is provided in the path a. That is, by opening the solenoid valves 21 and 22, the pressure in the vacuum vessel 1 is reduced, and the cleaning tank 6 and the ultrasonic transducer unit 7 are reduced in pressure.
  • the internal space 7a of the ultrasonic transducer unit 7 is also depressurized through this.
  • the solenoid valve 23 By opening the solenoid valve 23, the cleaning liquid 5 flowing out to the overflow collection part 6h is sucked into the branch pipe 20a.
  • the air intake ⁇ 10a of the cover 10 will be described later in detail, but the purging of the internal space 7a of the ultrasonic vibrator unit 7 from the start of the depressurization to the completion of the cleaning, and the vent after the completion of the cleaning It is used when it is connected to one end of the intake pipe 46.
  • This intake pipe 46 has a flow meter 47, a check valve 48, etc.
  • the cleaning device of the present embodiment is a form in which the purging action and the venting action are shared.
  • the gas and air 43 in the gas cylinder 40 can be selected as the gas for purging and venting. Of course, it is sufficient to provide only one of them.
  • an inert gas as a purge and vent gas from the viewpoint of preventive safety.
  • a basket 4 containing an object to be cleaned 3 is stored in a cleaning tank 6 provided in a vacuum container 1, and the cleaning liquid 5 stored in a storage tank 6a is supplied to the cleaning tank 5. Immerse and leave lid 2 closed.
  • the vacuum pump 25 is operated and the solenoid valves 21 and 22 are opened, the air in the vacuum vessel 1 is sucked from the vacuum pump 1 a to the vacuum pump 25 through the vacuum pump pipe 20. Then, evacuation is started.
  • the solenoid valve 42 or the like or the solenoid valve 44 of the intake pipe 46 the internal space 7a of the ultrasonic vibrator unit 7 is called gas or air 43 in the gas cylinder 40.
  • the purge gas is introduced from the intake port 10a and purged, and at the same time, it is sucked from the exhaust port 10Ob via the check valve 11 and the pressure is reduced.
  • the solenoid valve 23 of the branch pipe 20a is also opened to suck the cleaning liquid 5 flowing out to the overflow collecting part 6h.
  • the vibrator 9 when the vibrator 9 is actuated when the pressure in the vacuum vessel 1 detected by the pressure gauge 17 reaches a predetermined value (vacuum state), the ultrasonic vibration propagates through the diaphragm 8 to the cleaning liquid 5. The cavitation is generated in the cleaning liquid 5 and the immersed object 3 is cleaned.
  • the cleaning of the object to be cleaned 3 is completed, and the process shifts to a vent.
  • the solenoid valve 22 or the solenoid valves 21 and 23 of the vacuum exhaust pipe 20 are closed, and then the solenoid valve 42 or the like or the solenoid valve 44 of the intake pipe 46 is opened, the gas cylinder 40 A vent gas such as a gas or air 43 is introduced from the check valve 11 through the intake unit 10a and the exhaust port 10b of the ultrasonic vibrator unit 7, and the pressure in the vacuum vessel 1 becomes normal pressure. Is returned to. Then, the lid 2 is opened, the basket 4 containing the washed object 3 is taken out of the vacuum vessel 1, and the process is completed.
  • the cleaning liquid 5 that has flowed out into the overflow collecting section 6 h and the mist-like cleaning liquid 5 existing in the pressure vessel 1 are discharged from the vacuum exhaust port la of the vacuum vessel 1 and the overflow collecting section 6 h.
  • the water is sucked from i through a vacuum exhaust pipe 20 to a vacuum pump 25 and purified through a gas-liquid separator 26 and a distillation unit.
  • the temperature is adjusted to about 40 ° C in the washing liquid temperature control tank 30 provided with the heating coil 31 and the cooling coil 32, and the liquid supply pump 36, the filter 37, and the solenoid valve 18 Are supplied from a cleaning liquid supply port 6 g to a storage tank 6 a via a liquid supply pipe 35 provided in the path.
  • This supply is performed by operating the liquid supply pump 36, the solenoid valve 18 and the like based on the output from the liquid level sensor 15 provided in the storage section 6a.
  • Examples of the vacuum pump 25 include a reciprocating type, a liquid ring type, and a rotary type vacuum pump.
  • a liquid ring type vacuum pump is used for the following reasons. Has adopted.
  • the liquid ring vacuum pump 25 sucks the cleaning liquid 5 flowing out from the opening 6 f of the storage tank section 6 a into the overflow collecting section 6 h and the mist cleaning liquid 5 existing in the pressure vessel 1.
  • the liquid ring vacuum pump 25 generates severe noise due to the cavity when the degree of vacuum used reaches the saturated vapor pressure of the replenisher, and the pump cannot be used.
  • an air ejector is arranged at the front stage of the path to suck air.
  • the role of the air ejector is replaced by the supply of purge gas. Since the inside space 7a of the ultrasonic vibrator unit 7 has been cut off from the outside except for the supply of the purge gas and the vent gas, the mist-like cleaning liquid 5 existing in the pressure vessel 1 is not filled.
  • the exhaust gas is forcibly discharged from the check valve 11 via the exhaust ⁇ 10 b.
  • the charged portion 9a of the vibrator 9 provided in the internal space 7a serves as an ignition source, and there is no occurrence of a state in which the cleaning solution 5 is ignited to cause a fire or explosion.
  • the explosion range is about 0.8 to 5.5 vol.% (See FIG. 10).
  • the internal space 7a is always purged. And venting to avoid this explosion area.
  • the cover 10 forming the internal space 7a of the ultrasonic vibrator unit 7 is attached to the diaphragm 8 on the center side from the bolt 12, the cleaning liquid 5 is temporarily provided. Even if it leaks through the through hole (2) and the packing (13) (hatched part in Fig. 3), it does not enter the internal space 7a. Moreover, by raising the central portion 8a of the diaphragm 8, it becomes more advantageous to prevent the above-mentioned leaked cleaning liquid 5 from entering the internal space 7a, and furthermore, from the shape thereof.
  • the cleaning tank 6 and the ultrasonic transducer unit 7, which are the main components, are both placed under the same vacuum in the vacuum vessel 1, and there is no pressure difference between the inside and outside. There is no load on the related parts to be connected. Therefore, for example, the plate thickness of the diaphragm 8 is usually about 3 to 4 mm in consideration of the strength with respect to the pressure difference and the propagation efficiency of ultrasonic vibration, but in the cleaning device of the present embodiment, Since it is not necessary to consider the pressure difference, a plate thickness of about 2-3 mm used under normal pressure is sufficient.
  • the transducer unit 7 is wetted carelessly.
  • the internal space 7a of the ultrasonic vibrator unit 7 is provided with a charged portion 9a of the vibrator 9 serving as an ignition source, from the viewpoint of safety against fire and explosion, It is preferable to avoid the situation. Therefore, in the cleaning apparatus of the present embodiment, the droplet 5a is moved away from the side wall 6b of the cleaning tank 6 by the upper end 6c of the side wall 6b of the cleaning tank 6 bent outward and downward, and the cleaning is performed.
  • the lower end 6 e prevents the droplet 5 a flowing down the outer surface of the side wall 6 b of the cleaning tank 6 from flowing around the bottom wall 6 d provided with the ultrasonic vibrator unit 7. .
  • FIG. 5 is a sectional view showing a main part of a lower portion of a cleaning tank in the cleaning apparatus according to the second embodiment.
  • parts having the same names and the same functions as those of the cleaning device of the first embodiment are denoted by the same reference numerals, overlapping description will be omitted, and different points will be described. The same applies to the cleaning device of the embodiment.
  • FIG. 6 is a cross-sectional view of a main part of a cleaning unit in the cleaning device of the third embodiment
  • FIG. 7 is an enlarged view of part A of FIG. 6 showing leakage of the cleaning liquid.
  • a feature of the cleaning apparatus of the third embodiment is that the cleaning tank 6 is vertically long, and the ultrasonic vibrator unit 7 is provided on the side wall 6 b of the cleaning tank 6.
  • the washing tank 6 is roughly divided into a storage tank section 6a and an overflow liquid collecting section 6h, sharing the bottom wall 6d and one side wall 6b.
  • An opening 6 k is formed in one side wall 6 b of the storage tank 6 a, and the diaphragm 8 is arranged so as to close the opening 6 k at the center 8 a of the diaphragm 8.
  • Bolts 12 are fastened to through holes (not shown) that penetrate the peripheral portion 8 b, one side wall 6 b of the cleaning tank 6, and the packing 13 sandwiched therebetween.
  • a gutter-like projection 8c is provided on the periphery 8b of the diaphragm 8 so as to surround the bolts 12 so as to surround the bolts 12.
  • the object 3 to be cleaned is used for screen printing.
  • ultrasonic vibration can be applied from the side while the object to be cleaned 3 is standing, and cleaning can be performed efficiently.
  • the cleaning liquid 5 leaks through the through hole of the bolt 12 and the packing 13 (the hatched portion in FIG. 7), Since it can be received by the gutter-shaped projection 8 c provided on the plate 8, it does not enter the internal space 7 a of the ultrasonic vibrator unit 7.
  • the upper end portion 6c of the side wall 6b of the cleaning tank 6 bent outward and downward causes droplets that drip when removing the object 3 to be cleaned after cleaning.
  • the ultrasonic vibrator unit 7 provided on one side wall 6b of the cleaning layer 6 is removed because it is collected in the cleaning tank 6 or is further distant from the side wall 6b of the cleaning tank 6. Do not inadvertently get wet. In other words, even if the cleaning liquid 5 is flammable, there is no situation in which the charging section 9a of the vibrator 9 provided in the internal space 7a of the ultrasonic vibrator unit 7 becomes a source of ignition and a fire or Safety against explosion can be ensured.
  • FIG. 8 is a side view of the lower portion of the cleaning tank in the cleaning device of the fourth embodiment
  • FIG. 9 is a side view of the lower portion of the cleaning tank in the cleaning device of the fifth embodiment.
  • a feature of the cleaning apparatuses of the fourth and fifth embodiments is that the edge of the lower end 6e of the cleaning tank 6 in the cleaning apparatus of the first embodiment is deformed.
  • the edge of the lower end 6 e is uneven, so that the droplet a flows down along the outer surface of the side wall 6 b of the cleaning tank 6, and collects and drops on the convex portion by its own weight.
  • the edge of the lower end 6e is inclined with respect to the horizontal plane, so that the droplet 5a is applied to the outer surface of the side wall 6b of the cleaning tank 6. It flows down and gathers on the lowest slope part due to its own weight and drops. Therefore, since the position where the droplet 5a is dropped is determined, the recovery of the droplet 5a becomes easy.
  • FIG. 11 is a configuration diagram of the entire drying apparatus
  • FIG. 12 is a sectional view of a main part of the drying unit in FIG. 11.
  • the drying apparatus is roughly divided into a drying section and a distillation section, as shown in FIG.
  • the distillation section includes a still, a reheater, a condenser, a cold heat source, a warm heat source, a moisture removal unit, and the like.
  • the distilling unit is not directly related to the present invention, a detailed description thereof will be omitted.
  • 201 is a vacuum vessel (below, ), 202 is the lid of the vacuum vessel 201, and 203 is the object to be dried, such as electronics, machinery, molding parts, etc., which has been washed with the cleaning liquid.
  • 204 is a basket for storing the object to be dried 203
  • 205 is a heating vessel
  • 206 is a hydrocarbon-based solution
  • 2007 is A coiled heater
  • 208 is a heating medium
  • 209 is a communication pipe for communicating the vacuum vessel 201 with the heating vessel 205
  • 210 is an air-driven valve for opening and closing the communication pipe 209.
  • the vacuum vessel 201 is formed in a cylindrical shape with the upper part opened above the drying part, and the open upper part is provided with a lid 202 that rotates about a base shaft 202a.
  • a vacuum exhaust port 201 a and an intake port 201 b are formed on the side of the vacuum vessel 201, and heaters 221, 222 are provided on a bottom face and an inner face of the vacuum vessel 201, respectively.
  • a pressure sensor 231, a temperature sensor 232, and a liquid level sensor 233 are provided.
  • the heating vessel 205 forms the lower part of the drying section and is divided into two upper and lower chambers by a metal partition wall 205a having excellent heat conductivity.
  • the upper chamber 205b contains a solution 206.
  • a pressure sensor 241, a temperature sensor 242, and a liquid level sensor 243 are provided.
  • the lower chamber 205c is provided with a heater 207, a pressure sensor 244, a temperature sensor 245, and an overheating prevention switch 246, and contains a heating medium 208.
  • the T heating medium 208 is heated by the operation of the heater 207, and the heat of the heated heating medium 208 is indirectly heated to the solution 206 through the partition wall 205a.
  • the heating temperature of the solution 206 is directly detected by the temperature sensor 242 and indirectly detected by the temperature sensor 245. If the temperature rises abnormally, the overheating prevention switch 246 detects the heating temperature of the heater 207. Because of this, it can be said that the structure has extremely low risk of fire and explosion.
  • the upper chamber 205b is provided with an exhaust CD 205d, a liquid supply d 205e, and an exhaust boil 205f.
  • the communication pipe 209 connects the vacuum vessel 201 and the heating vessel 205 to each other.
  • the end 209a is open to the bottom of the vacuum vessel 201, the lower end 209b is immersed in the solution 206, and an air drive valve 210 is provided in the path.
  • the vacuum exhaust port 201 a of the vacuum vessel 201 and the exhaust D 205 d of the upper chamber 205 a of the heating vessel 205 are connected to each of two ends branched from the vacuum exhaust pipe 250, and the branched vacuum exhaust is performed.
  • Air drive valves 251 and 252 are provided in the path of the pipe 250, respectively, while the other end of the vacuum exhaust pipe 250 is connected to a vacuum pump 253. Further, a separator 254 is provided downstream of the vacuum pump 253. That is, the upper chamber 205a of the vacuum vessel 201 or the heating vessel 205 is depressurized by opening and closing the air drive valve 251 or 252.
  • the suction port 201b of the vacuum vessel 201 is used for returning the vacuum state of the vacuum vessel 201 to normal pressure (venting) after the drying, which will be described in detail later, is completed.
  • 1 is connected to one end.
  • the other end of the vent gas pipe 26 1 is branched into two pipes.
  • One is a gas cylinder sealed with an inert gas such as nitrogen gas via an air drive valve 262 ⁇
  • the other end is connected to an air 267 such as compressed air or open air through a check valve 265 and an air drive valve 266.
  • the drying apparatus of the present embodiment has a configuration in which the gas in the gas cylinder 264 and the air 267 can be selected as the vent gas, but of course, only one of them is provided. I'll do it. From the viewpoint of preventive safety, it is preferable to use an inert gas as the vent gas.
  • a packet 204 containing the material 203 to be dried is housed in a vacuum vessel 201, the lid 202 is closed, the vacuum pump 253 is operated, and the air-driven valve 25 1 Open 2 52. Then, the air in the vacuum vessel 201 is sucked from the vacuum exhaust ⁇ 201 a through the vacuum exhaust pipe 250 to the vacuum pump 253 to start vacuuming, and the upper chamber 205 b of the heating vessel 205 is started. The inside air is sucked from the exhaust ⁇ 205 d to the vacuum pump 253 via the vacuum exhaust pipe 250, and the decompression is started. In addition, the heater 207 in the lower chamber 205c of the heating vessel 205 is operated to heat the solution 206 contained in the upper chamber 205b.
  • the air-driven valve 210 of the communication pipe 209 is opened.
  • the solution 206 is rapidly sucked from the lower end 209 b of the communication pipe 209 to the upper end 209 a and is jetted upward in a boiling state, so that the temperature in the vacuum vessel 201 rises rapidly.
  • heat is applied to the object 203 in the basket 204 to rapidly heat the object 203.
  • the solution 206 that has given heat to the material 203 to be dried loses enthalpy and falls, and accumulates on the bottom surface of the vacuum container 201.
  • the solution 206 is injected into the solution 206 injected from the upper end 209a of the communication pipe 209. Therefore, the injection which also has an active bubbling effect is maintained and does not cause any substantial obstacle. However, if the amount exceeds a certain amount, an adverse effect occurs. Therefore, the liquid level sensor 233 detects this amount.
  • the heating of the object to be dried 203 is completed, and the process proceeds to drying.
  • the solution 206 accumulated on the bottom surface of the vacuum vessel 201 has an adverse effect on drying, and therefore, it is necessary to discharge the solution 206 from the vacuum vessel 201 before the drying is started. Therefore, in the drying apparatus of the present embodiment, the air drive valve 252 provided in the vacuum exhaust pipe 250 is further opened to reduce the pressure in the upper chamber 205b of the heating vessel 205.
  • the injection of the solution 206 from the upper end 209 a of the communication pipe 209 gradually decreases, and when the pressure in the upper chamber 205 b of the heating vessel 205 becomes equal to the pressure in the vacuum vessel 201, the vacuum vessel 20
  • the solution 206 stored on the bottom surface of 1 is drawn back into the upper chamber 205 b of the heating vessel 205 by its own weight, and is discharged from the vacuum vessel 201.
  • the air drive valve 251 may be temporarily closed.
  • the air drive valve 210 of the communication pipe 209 is closed, and the evacuation of the vacuum vessel 201 is continued.
  • the cleaning liquid adhering to the dried material 203 (for example, the cleaning liquid 5 when the cleaning is performed using the above-described cleaning apparatus) and the solution 206 evaporate while removing latent heat of evaporation from the material 203 to be dried, and are dried. .
  • the upper chamber 205b of the ripening vessel 205 is always in a negative pressure environment.
  • the air drive valve 25 1 of the vacuum exhaust pipe 250 is closed.
  • the air drive valve 262 or 266 of the vent gas pipe 26 1 is opened, and the gas or air 267 in the gas cylinder 264 is introduced from the suction vent 201 b of the vacuum vessel 201, and the vacuum vessel 201
  • the internal pressure is returned to normal pressure.
  • the lid 202 is opened, the basket 204 containing the dried material to be dried 203 is taken out of the vacuum vessel 201, and the process is completed.
  • the vaporized cleaning solution / solution 206 present in the vacuum vessel 201 is sucked from the vacuum pump 201 a to the vacuum pump 253 via the vacuum pump pipe 250. After being purified through the separator 254 and the distillation section, it is filtered from the liquid supply port 205 e via the liquid supply port 205 e via the filter pipe 256 and the air drive valve 257 through the liquid supply pipe 255. It is thrown into the upper room 205 b of 205. This injection uses the negative pressure of the vacuum pump 253, so it can be performed only by opening and closing the air drive valve 257 without providing a dedicated pump. It operates according to the output of.
  • the vacuum pump 253 may be a reciprocating type, a liquid ring type, a rotary type, or the like, but the drying device of the present embodiment employs a liquid ring type vacuum pump for the following reasons. are doing. Even if the cleaning liquid or solution 206 vaporized in the vacuum vessel 201 is sucked in, the liquid comes into contact with the pump rotating part via the liquid, so that unlike a normal seal-type vacuum pump, a metal slide is used. This is because sparks and heat generated by moving surface friction are small, and the safety is high and there is no problem.
  • the drying apparatus of the present embodiment is provided with a heater 22 1 on the bottom face of the vacuum vessel 201.
  • the solution 206 stored on the bottom surface of the vacuum vessel 201 is heated and vaporized by the heater 22 1, diffuses into the vacuum vessel 201, and gives heat again to the object 203 to be dried.
  • the drying time can be reduced by 20 to 25%, and this effect is extremely effective.
  • a heater 222 is provided on the inner surface of the vacuum vessel 201 in order to raise the temperature inside the vacuum vessel 201 more rapidly.
  • the side surface of the vacuum vessel 201 has a large heat capacity, so it is difficult to raise the temperature. If the vaporized solution 206 in the vacuum vessel 201 comes into contact with this side face and condenses, the drying will be hindered. There is a possibility that the installation of this heater 222 The drying time was reduced by about 5% in our experiments.
  • the air-driven valve 210 provided in the communication pipe 209 includes a pressure sensor 231 of the vacuum vessel 201, a pressure sensor 241 of the heating vessel 205, and a temperature sensor 242.
  • the degree of opening and closing is automatically adjusted based on the value output from the. Therefore, the state of the boiling solution 206 which is sprayed toward the object to be dried 203 and the state of the temperature of the object to be dried 203 can always be stabilized to an appropriate state.
  • the air-driven valve 210 may be kept open and the solution 206 may be constantly jetted, but in particular, a complicated shaped cover may be used.
  • FIG. 13 is a sectional view of a main part of a drying unit in the drying apparatus according to the seventh embodiment.
  • the 6 denoted by the same reference numerals perform the same functions with the same name as the drying device of the embodiment in the figure, and duplicate explanations are omitted describes points different (first, drying of the embodiment
  • the object to be dried after cleaning is not completely free of dirt and foreign matters such as adherents (the shape and size of the parts to be dried). Or, depending on the degree of contamination, if it is expressed as an index with the adhesion weight of dirt and foreign matter being 100, it is sufficient if about 70 to 80 dirt or foreign matter can be removed by washing.
  • the drying device of the present embodiment is intended to solve such a problem.
  • a condensing coil 271 is provided on the inner surface of the vacuum vessel 201.
  • the inside of the condensation coil 27 1 is provided with a cylindrical partition wall 27 2.
  • a gutter-like portion 272a is formed at the lower portion of the partition 272, and a vacuum exhaust port 201a is formed near the gutter-like portion 272a.
  • the heating vessel 205 is divided into a right chamber 205 h and a left chamber 205 i by a partition wall 205 g, and a heater 207 is provided in the right chamber 205 h, and the heater 207 is directly heated by the heater 207.
  • the solution 206 to be removed is stored.
  • heating may be performed indirectly via a heating medium.
  • the right chamber 205 h is provided with an exhaust ⁇ 205 d, a liquid supply port 205 e, and a discharge port 205 f, and a temperature sensor 242, an overheating prevention switch 246, and a liquid level sensor 243. Is provided.
  • the upper end 209a of the communication pipe 209 that communicates the vacuum chamber 201 with the right chamber 205h of the heating vessel 205 passes through the bottom of the vacuum vessel 201 and opens inside the vacuum vessel 201, and the lower end 209b has the lower end 209b.
  • the left chamber 205 i is immersed in the solution 206 ( while the left chamber 205 i serves as a collection tank for collecting the solution 206 collected on the bottom surface of the vacuum vessel 201, which will be described later).
  • the upper end 2 1 1a of the collection pipe 2 1 1 is open to the bottom of the vacuum vessel 201, and the lower end 2 1 lb is open to the upper surface of the left chamber 205 i.
  • An exhaust port 205 j and an exhaust port 205 k are formed in the chamber 205 i, and a liquid level sensor 247 is provided.
  • the vaporized cleaning liquid and the solution 206 existing in the vacuum vessel 201 are sucked from the vacuum exhaust 201 a by the suction force from the side wall and the partition wall 2 of the vacuum vessel 201. It passes through the gap with 72 and is cooled by the condensation coil 27 1 and liquefied.
  • the liquefied solution 206 collects in the gutter-like portion 27 2 a, and is sucked from the vacuum exhaust port 201 a through the vacuum exhaust pipe 250 to the vacuum pump 253 via the edge X kuta 257 and the like.
  • the filter 254 After being purified and passed through the separator 254, the filter 25
  • the solution 206 collected on the bottom surface of the vacuum vessel 201 is not drawn back through the communication pipe 209 as in the drying device of the sixth embodiment, but is collected by the collection pipe 21.
  • the left chamber 2005 i which is a collection tank, through 1.
  • This is an exhaust 205
  • This can be achieved by opening the air drive valves 256, 258 provided in the vacuum exhaust pipe 250 connected to the vacuum pump 253 from j, and reducing the pressure in the left chamber 205i. Therefore, the solution 206 collected on the bottom of the vacuum vessel 201 contains dirt, foreign matter, oil, etc. remaining on the object 203 after washing, but the individual collection tank (left)
  • the solution 206 in the right chamber 205 h is always kept in a clean, uncontaminated, fresh liquid state by being collected in the chamber 205 i), and is repeatedly dried, for example. Even if it does not impair the appearance of the object to be dried after drying.
  • the present invention is not limited to the first to seventh embodiments, and various changes can be made without departing from the spirit of the present invention.
  • the ultrasonic vibrator unit 7 is provided inside the storage tank portion 6a of the cleaning tank 6 (throw-in type), and the ultrasonic vibrator unit 7
  • the check valve 11 connected to the exhaust port 10 b may be penetrated through the cleaning tank 6 and opened into the vacuum vessel 1.
  • diaphragm 8 may have a flat shape in which central portion 8a is not raised with respect to peripheral portion 8b.
  • non-flammable water may be used as the solution 206 instead of the hydrocarbon-based solution, but the drying property is taken into consideration. It is preferable to use a hydrocarbon-based solution whose latent heat of vaporization is as low as about 1Z10 with respect to water.
  • the drying apparatus may include a cleaning step. In this case, it is preferable that the cleaning liquid used for cleaning before drying and the solution 206 used for the drying step are of the same type.
  • the heater 221 provided on the bottom surface of the vacuum vessel 201 can be used to heat and vaporize the solution 206 stored on the bottom face of the vacuum vessel 201 as long as it can be vaporized. It may be a jacket-type heater that covers the area.
  • the cleaning device and the drying device of the above embodiment can be appropriately combined, and in this case, the process from cleaning to drying can be performed efficiently and safely, which is extremely useful.
  • the cleaning apparatus and the cleaning method of the present invention are useful for cleaning and drying of electronic, mechanical, and molding-related parts. '

Landscapes

  • Cleaning By Liquid Or Steam (AREA)

Abstract

A vacuum ultrasonic washing device capable of easily maintaining airtightness without taking any special consideration by suppressing pressure differences between the inside and outside of major component parts and between the main component parts and providing an excellence in safety against fire and explosion even if inflammable washing fluid is used, wherein a washing tank (6) having a storage part (6a) for storing washing fluid (5) and storing a washed matter (3) in the storage part (6a) and an ultrasonic vibrator unit (7) having a specified space (7a) therein and providing ultrasonic vibration to the washing fluid (5) are installed in a vacuum container (1) allowed to be brought into a vacuum state, and the specified space (7a) of the ultrasonic vibrator unit (7) is open from an inlet (10a) into the vacuum container (1) through a check valve (11).

Description

明 細 書 洗浄装置、 及び洗浄方法 技術分野  Description Cleaning equipment and cleaning method
本発明は、 電子、 機械、 成形関連等の部品を洗浄する洗浄装置、 及びその部品 の洗浄方法に関し、 特に、 真空下におかれた水又は炭化水素系等の洗浄液に超音 波振動を与え洗浄液に浸漬した部品を洗浄する洗浄装置、 及び、 真空下で部品を 超音波洗浄した後更にその部品を真空状態で乾燥させる洗浄方法に関する。 背景技術  The present invention relates to a cleaning apparatus for cleaning electronic, mechanical, and molding-related parts, and a method for cleaning such parts. In particular, the present invention provides ultrasonic cleaning to water or a hydrocarbon-based cleaning liquid placed in a vacuum. The present invention relates to a cleaning apparatus for cleaning a part immersed in a cleaning liquid, and a cleaning method for ultrasonically cleaning a part under vacuum and then drying the part in a vacuum. Background art
従来よ り、 部品を洗浄する洗浄液と しては、 フロン等のフッ素系や、 1 , 1 , 1 -ト リ クロロエタン等の塩素系の溶液が多く 用いられてきた。 しかしながら、 気化し たこれらの溶液はオゾン層を破壊する性質を有しているとされ、 1 9 8 7年に、 「オゾン層を破壊する物質に関するモン ト リオール議定書」 力 「オゾン層保護 に関するウイ ーン条約」 に基づき採択されて、 特定フロン等を対象に生産量の段 階的な削減や規制等が規定された。 その後も何度か見直しがなされており、 規制 物質の追加や規制スケジュールの前倒し等の改正が行われている。  Conventionally, fluorine-based solutions such as chlorofluorocarbons and chlorine-based solutions such as 1,1,1-trichloroethane have been often used as cleaning solutions for cleaning parts. However, these vaporized solutions are said to have the property of depleting the ozone layer, and in 1987, the Montreal Protocol on Substances That Deplete the Ozone Layer, the force on the The phase-in convention was adopted in accordance with the stipulations on the gradual reduction and regulation of production volume for specified CFCs. Since then, it has been reviewed several times, and revisions have been made, such as the addition of regulated substances and the advancement of the regulatory schedule.
日本においては、 1 9 9 8年 9月 3 0 日に、 上記したウ イ ーン条約及びモン ト リオ一ル議定書が批准された。 この議定書では、 C F C (塩素 · フッ素 · 炭素化 合物) に代わるフッ素系である H C F C (水素 · 塩素 · フ ッ素 · 炭素化合物) に ついても、 2 0 2 0年までに全廃することが決められており、 その全廃時期につ いては、 今後更に、 前倒しが予想される。 また、 これらに関連して、 塩素系に対 しても、 水質や大気汚染に関する規制の見直しが図られており、 年毎にその規制 が強化されつつある。  In Japan, the aforementioned Wien Treaty and the Montreal Protocol were ratified on September 30, 1998. This protocol determines that HCFC (hydrogen, chlorine, fluorine, and carbon compounds), which replaces CFCs (chlorine, fluorine, and carbon compounds), will be completely abolished by 2010. It is anticipated that the total abolition period will be further advanced in the future. In relation to these, regulations on water quality and air pollution are also being reviewed for chlorine systems, and the regulations are being strengthened every year.
一方、 地球温暖化防止に関する活動も活発になってきており、 1 9 9 7年 1 2 月の 「地球温暖化防止京都会議」 では、 日本に対して、 温暖化ガスの 6 %削減が 義務づけられた。 この温暖化ガスの対象としては、 代替フロンである H F C (水 素 · フッ素 · 炭素化合物) やパーフルォロカーボンも含まれており、 更に代替フ ロンにおいても排出規制が強化されることになつた訳である。 従って、 今後、 規 制動向に対して十二分なウォッチが必要であるとともに、 早急に対処策を講じて いく ことが強く要求される。 On the other hand, activities related to the prevention of global warming are also becoming active.The Kyoto Conference on Global Warming Prevention in January 1997, obliged Japan to reduce greenhouse gases by 6%. Was. The targets of this greenhouse gas include HFCs (hydrogen, fluorine and carbon compounds) and perfluorocarbons, which are alternative fluorocarbons. This has also led to tighter emission regulations in Ron. Therefore, in the future, there is a need to have more than enough watch on regulatory trends, and it is also strongly required to take immediate measures.
このような背景のもと、 近年、 オゾン層破壊のおそれが少ないとされる水又は 非塩素系の溶液を用いて部品を洗浄することが注目されているが、 以下の点に留 意する必要がある。  Against this background, attention has recently been paid to cleaning parts using water or non-chlorine-based solutions, which are considered to be less likely to cause ozone layer destruction, but it is necessary to pay attention to the following points: There is.
先ず、 水を用いる場合であるが、 第 1 に、 水自体は安価である反面、 水の取り 扱いに関連する多く の付帯設備を必要と し、 その付帯設備の据え付けに多大な費 用が生じることである。 付帯設備と しては、 洗浄装置本体の他に、 例えば、 貯水 設備、 沈澱 · 浄化 · 汚泥処理設備、 排水設備、 或いは、 純度の低い水を用いた場 合の前処理用設備が挙げられ、 しかも、 これらの設置スペースや、 メ ンテナンス のための補助スペースも必要となる。 また: これら付帯設備の運転、 保守、 或い は、 排水管理等には、 初期投資とともに、 維持に係わる経費も必然的に発生する ことはいうまでもない。 特に、 排水管理においては、 使用後の水を排水する際に 水質基準値を満足し得るような配慮が必要である。  First, water is used.First, although water itself is inexpensive, it requires many additional facilities related to water handling, and installation of such facilities requires a great deal of cost. That is. As ancillary equipment, besides the washing equipment itself, for example, water storage equipment, sedimentation / purification / sludge treatment equipment, drainage equipment, or pretreatment equipment when low-purity water is used, In addition, these installation spaces and auxiliary space for maintenance are required. Also: Needless to say, initial operation and maintenance costs are inevitable for the operation, maintenance, and drainage management of these facilities. In particular, in drainage management, care must be taken to ensure that the water quality standards are met when draining used water.
第 2に、 水の有する濡れ性により、 期待される程の洗浄効果が得られない可能 性があることである。 水の表面張力は、 4 5 °Cにおいて 6 8 . 7 4 ± 0 . 0 5 dy n/cm、 2 0 °Cにおいて 7 2 . 7 5 ± 0 . 0 5 dyn/cmとべ一ス値がかなり高い。 一 方、 従来多用されてきたフッ素系や塩素系の溶液では、 例えば、 フロン C F C 1 1 3が 2 0 °Cにおいて 1 Ί dyn/cm , 1 , 1, 1-ト リ クロロェタンが 2 5 dyn/cmと水に 対して 1 3〜 1 Z 4に過ぎない。 つまり、 水は、 従来多用されてきた溶液と比 較して濡れ性が悪いということがいえる。 従って、 水を用いて従来と同様の手法 で洗浄が行われた場合、 部品同士の重なり部分や密着部分、 或いは、 部品に形成 されている小さな穴や隅部等には、 水は容易に浸透、 進入できなく なり、 これら の部分に付着し存在している汚れ等を洗浄できず、 洗浄効果が劣つてしまうこと になる。  Second, the expected cleaning effect may not be obtained due to the wettability of water. The surface tension of water is 68.74 ± 0.05 dy n / cm at 45 ° C, and 72.7 ± 0.05 dyn / cm at 20 ° C, which is quite a base value. high. On the other hand, in conventional fluorine-based and chlorine-based solutions, for example, CFC113 at 1 ° dyn / cm 2 at 25 ° C, 25 dyn / cm2 at 1,0,1,1-trichloroethane. Only 13-1 Z 4 for cm and water. In other words, it can be said that water has poor wettability as compared with a solution that has been frequently used in the past. Therefore, when cleaning is performed using water in the same manner as in the past, water easily penetrates into overlapping parts and close contact parts between parts, or small holes and corners formed in parts. As a result, it becomes impossible to enter, and dirt or the like adhering to these portions cannot be cleaned, resulting in a poor cleaning effect.
第 3に、 空気が混在する雰囲気や、 加温された常圧等の環境下で洗浄が行われ た場合、 洗浄される部品が金属部分を有すると、 水の有する酸化力により鯖が誘 発され易く なるため、 防鍩対策が不可欠となる。 特に、 そのような環境下では乾 燥時間が長く なるため、 水シミ等も発生し易く、 折角洗浄しても外観が損なわれ てしまう。 Third, when cleaning is performed in an atmosphere with air mixed or in an environment such as a heated normal pressure, if the part to be cleaned has a metal part, the oxidizing power of the water will induce the mackerel. Therefore, prevention measures are indispensable. Especially in such an environment, Since the drying time is prolonged, water spots and the like are liable to occur, and the appearance is impaired even if the corners are washed.
一方、 非塩素系であるシ リ コン系、 炭化水素系、 或いは、 アルコール系等の溶 液を用いる場合であるが、 第 1 に、 その沸点が高いもので 2 0 0 °C程度もあるた め、 常圧下でその溶液を蒸気化して蒸気による部品洗浄が行われる場合、 蒸気温 度が極めて高く なり、 洗浄される部品の熱変形や変質等の問題が発生する。 しか も、 従来多用されてきたフッ素系や塩素系の溶液と比較して、 乾燥性が劣るとい う問題もある。 第 2に、 炭化水素系の溶液は引火点が 5 0〜 8 0 °Cと低いため、 火災、 爆発等に対して安全性の確保が強く要求される。  On the other hand, when a non-chlorine-based solution such as a silicon-based, hydrocarbon-based, or alcohol-based solution is used, firstly, its boiling point is as high as about 200 ° C. Therefore, when the solution is vaporized under normal pressure and the parts are cleaned with steam, the steam temperature becomes extremely high, and problems such as thermal deformation and deterioration of the parts to be cleaned occur. However, there is also a problem that the drying property is inferior to that of a fluorine-based or chlorine-based solution that has been frequently used in the past. Second, hydrocarbon solutions have a low flash point of 50 to 80 ° C, so it is strongly required to ensure safety against fires and explosions.
このように、 水又は非塩素系の洗浄液を用いる場合の留意点は種々あるが、 特 に、 洗浄力や乾燥性の向上、 及び、 炭化水素系に対する安全性の確保という点に 対しては、 減圧環境下におかれた洗浄液に超音波振動を与えて、 洗浄液に浸潰し た部品を洗浄するいわゆる真空超音波方式の洗浄装置や、 減圧環境下で乾燥が行 える真空方式の乾燥装置が望ましい。 何故ならば、 減圧環境を形成する洗浄装置 や乾燥装置は、 真空容器を含む配管系が密閉構造となった、 いわゆる、 クローズ ドシステムとなるので、 配管系内部を負圧に保つことによって、 その内部の酸素 濃度が極めて低く なり引火を抑止できるし、 万一配管系に欠損箇所があったと し ても、 その負圧により内部の溶液や蒸気が外部に漏れ出ることはなく、 安全性の 確保につながるからである。 しかも、 洗浄装置の場合、 洗浄液に超音波振動を与 える際に洗浄液が減圧下におかれていると、 洗浄力となるキヤビテーシヨ ンを容 易に発生させることができるので、 洗浄力の向上に対して有利となる し、 また乾 燥装置の場合、 減圧下では飽和蒸気圧が下がるので、 溶液の沸点が実質下がり、 常圧雰囲気下と比較して溶液は容易に蒸発でき、 乾燥性の向上に対して有利とな るからである。  As described above, there are various points to keep in mind when using water or a non-chlorine-based cleaning solution.However, in particular, with regard to the improvement of detergency and drying property and the securing of safety against hydrocarbons, It is desirable to use a so-called vacuum ultrasonic cleaning device that applies ultrasonic vibration to the cleaning liquid placed in a reduced-pressure environment to clean parts immersed in the cleaning liquid, or a vacuum-type drying device that can dry in a reduced-pressure environment. . This is because the cleaning and drying equipment that creates a reduced-pressure environment is a so-called closed system in which the piping system including the vacuum vessel has a closed structure. The internal oxygen concentration is extremely low, which can prevent ignition and, even if there is a defect in the piping system, the negative pressure does not cause the internal solution or vapor to leak out, ensuring safety. Because it leads to In addition, in the case of a cleaning apparatus, if the cleaning liquid is placed under reduced pressure when applying ultrasonic vibration to the cleaning liquid, it is possible to easily generate cavitation as a cleaning power, thereby improving the cleaning power. In the case of a drying device, the saturated vapor pressure is reduced under reduced pressure, so the boiling point of the solution is substantially reduced, and the solution can be easily evaporated compared to that in a normal pressure atmosphere, and the drying property is improved. This is because it is advantageous for.
ここで先ず、 従来の真空超音波方式の洗浄装置は、 例えば、 特開 2 0 0 0— 3 3 3 4 9号公報によれば、 第 1 4、 1 5図に示されるよう に、 蓋を有し洗浄液 1 0 2を貯留する洗浄槽 1 0 1 の底壁にカバ一 1 0 7と一体の振動板 1 0 3が配設 され、 一端が電磁弁 1 0 4及び真空ポンプ 1 0 5に通ずる配管 1 0 6の他端から 分岐した配管 1 0 6 a、 1 0 6 b力 それぞれ洗浄槽 1 0 1、 カバ一 1 0 7に連 結されたり (第 1 4図参照) 、 洗浄槽 1 0 1 の内部にケースで覆われた振動子 1 0 8が配設され (投げ込み式) 、 配管 1 0 6 a、 1 0 6 bがそれぞれ洗浄槽 1 0 1、 振動子 1 0 8に連結されたり (第 1 5図参照) している。 Here, first, a conventional vacuum ultrasonic cleaning apparatus, for example, according to Japanese Patent Application Laid-Open No. 2000-33349, has a lid as shown in FIGS. A vibration plate 103 integral with the cover 107 is disposed on the bottom wall of the washing tank 101 storing the washing liquid 102, and one end is connected to the solenoid valve 104 and the vacuum pump 105. Connecting piping 1 0 6 a, 10 6 b force branching from the other end of 10 6 Connect to washing tank 10 1 and cover 10 7 respectively A vibrator 108 covered with a case is disposed inside the cleaning tank 101 (throw-in type), and the piping 106a and 106b are respectively connected. It is connected to the cleaning tank 101 and the vibrator 108 (see Fig. 15).
従って、 真空ポンプ 1 0 5を作動させ電磁弁 1 0 4を開く ことによ り、 洗浄槽 1 0 1 内を減圧して洗浄液 1 0 2を真空下におき、 この洗浄液 1 0 2 に振動板 1 0 3や振動子 1 0 8から超音波振動を与え、 浸潰した被洗浄物を洗浄することが できる。 しかも、 これと同時に、 同一の配管 1 0 6を通じてカバ一 1 0 7や振動 子 1 0 8を覆うケースの内部が減圧されることから、 カバ一 1 0 7や振動子 1 0 8を覆うケースの内部と洗浄槽 1 0 1 内とで圧力差が生じなく なるので、 振動板 1 0 3や振動子 1 0 8を覆うケースを厚く しなく とも、 それらが撓んだり変形し たりすることがなく なる。  Therefore, by operating the vacuum pump 105 and opening the solenoid valve 104, the pressure inside the cleaning tank 101 is reduced to put the cleaning liquid 102 under vacuum, and the diaphragm is added to the cleaning liquid 102. Ultrasonic vibration is applied from 103 and the vibrator 108 to clean the immersed object to be cleaned. In addition, at the same time, the inside of the case that covers the cover 107 and the vibrator 108 is reduced in pressure through the same pipe 106, so that the case that covers the cover 107 and the vibrator 108 is also reduced. Since there is no pressure difference between the inside of the chamber and the inside of the washing tank 101, they can bend or deform without making the case that covers the diaphragm 103 and the vibrator 108 thicker. Disappears.
しかし、 このような洗浄装置では、 洗浄槽 1 0 1や配管 1 0 6 a、 1 0 6 bの 内外、 及び、 第 1 4図ではカバー 1 0 7の内外で圧力差が生じるため、 これら構 成部品同士の気密性を維持すべく、 格別な配慮が必要である。 例えば、 気密性に 対して特に弱い部分である配管 1 0 6 aと洗浄槽 1 0 1 との連結部、 振動板 1 0 3 とカバー 1 0 7 との連結部、 配管 1 0 6 b とカバ一 1 0 7 (第 1 4図参照) 又 は洗浄槽 1 0 1 (第 1 5図参照) との連結部等には、 シール材ゃ溶接材ゃフイ ツ ティ ング類等といつた封止材ゃ封止方法の適正な選定が設計上で重要となるし、 更に、 経年使用に伴うこれら封止材ゃ封止方法の劣化に対しても十分に配慮して おく 必要がある。  However, in such a cleaning device, a pressure difference is generated between the inside and outside of the washing tank 101 and the pipes 106a and 106b, and in FIG. Special care must be taken to maintain the airtightness between the components. For example, the connection between the pipe 106a and the cleaning tank 101, which are particularly weak parts for airtightness, the connection between the diaphragm 103 and the cover 107, and the pipe 106b and the cover At the connecting part with 107 (see Fig. 14) or cleaning tank 101 (see Fig. 15), seal with sealing material, welding material, fittings, etc. Appropriate selection of materials and sealing methods is important in design, and it is also necessary to give due consideration to deterioration of these sealing materials and sealing methods due to aging.
また、 真空下での洗浄が完了した後、 通常、 洗浄槽 1 0 1 内に圧縮ガスや大気 等 (以下、 「ベン トガス」 と記すこ とがある) を導入して、 真空状態から常圧に 戻す動作 (以下、 「ベン ト」 と記すことがある) が行われる。 これは、 洗浄槽 1 0 1 から被洗浄物を取り出すに際し先ず蓋を開く 必要があるが、 洗浄槽 1 0 1 内 が真空状態のままであると、 蓋が圧着された状態となっており、 蓋を開く ことが 極めて困難となるからである。 このベン トを行うために洗浄槽 1 0 1 内にベン ト ガスを導入し始めると、 洗浄槽 1 0 1 内に浮遊しているミ ス ト状の洗浄液 1 0 2 は、 負圧作用で配管 1 0 6 a、 1 0 6 bに吸引され、 カバー 1 0 7や振動子 1 0 8を覆うケースの内部に到達し蓄積されていく。 一般に、 振動板 1 ひ 3や振動子 1 0 8は電気で駆動され、 その電気駆動を司る充電部がカバ一 1 0 7や振動子 1 0 8を覆うケースの内部に備えられているので、 例えば、 洗浄液 1 0 2と して可 燃性の炭化水素系の洗浄液が用いられた場合、 充電部が着火源となってその充電 部の周囲に蓄積されているミス ト状の洗浄液 1 0 2に引火して、 火災や爆発を引 き起こすおそれが極めて高いという欠点もある。 After the cleaning under vacuum is completed, usually, a compressed gas or air (hereinafter sometimes referred to as “vent gas”) is introduced into the cleaning tank 101 to change the pressure from the vacuum state to the normal pressure. (Hereinafter, may be referred to as a “vent”). This is because when removing the object to be cleaned from the cleaning tank 101, it is necessary to open the lid first, but if the inside of the cleaning tank 101 is kept in a vacuum state, the lid is crimped, This is because it is extremely difficult to open the lid. When vent gas is introduced into the cleaning tank 101 to perform this venting, the mist-like cleaning liquid 102 floating in the cleaning tank 101 is connected to the piping by negative pressure action. It is sucked by 106 a and 106 b, reaches the inside of the case that covers the cover 107 and the vibrator 108, and accumulates. Generally, diaphragm 1 or 3 108 is driven by electricity, and the charging section that controls the electric drive is provided inside the case that covers the cover 107 and the vibrator 108. If a flammable hydrocarbon-based cleaning solution is used, the live parts may become an ignition source and ignite the mist-like cleaning liquid 102 accumulated around the live parts, causing a fire or explosion. It also has the disadvantage that it is very likely to be caused.
次に、 従来の真空方式の乾燥装置では、 洗浄液が付着している被乾燥物を真空 容器内に置き、 真空状態にすることによって、 被乾燥物に付着している洗浄液が、 気化するために必要な熱 (蒸発潜熱) を被乾燥物から奪いながら沸騰、 蒸発し、 真空乾燥が進行する。 一方、 乾燥が進行するに伴い被乾燥物の品温は徐々に低下 し、 この品温が飽和蒸気圧温度を下回ると、 真空容器内の真空度が同一状態であ るならば、 その時点で洗浄液の沸騰、 蒸発は停止してしまうので、 この事態を回 避するために、 一般には、 更に真空能力を上げ到達真空度を高めたり、 真空引き 開始時点の被乾燥物の品温を高めたり、 真空引き中の被乾燥物に熱を供給したり する工夫が必要とされる。  Next, in a conventional vacuum-type drying apparatus, the object to be dried to which the cleaning liquid is attached is placed in a vacuum container, and the state of vacuum is applied, whereby the cleaning liquid attached to the object to be dried is vaporized. The necessary heat (evaporation latent heat) is removed from the material to be dried while boiling and evaporating, and vacuum drying proceeds. On the other hand, as the drying proceeds, the temperature of the material to be dried gradually decreases, and when this temperature falls below the saturated vapor pressure temperature, if the degree of vacuum in the vacuum vessel is in the same state, then, Since the boiling and evaporation of the cleaning liquid are stopped, in order to avoid this situation, generally, the vacuum capacity is further increased to increase the ultimate vacuum, or the temperature of the material to be dried at the start of evacuation is increased. In addition, a device for supplying heat to the material to be dried during evacuation is required.
例えば、 真空引き開始時点の被乾燥物の品温を高める簡便な手法と して、 真空 容器内に温風を吹き込む温風加熱方式があ^)。 しかし、 限られた時間の加熱では、 真空容器の側壁の温度が十分上昇しないままで乾燥状態に入ることになるため、 蒸発した洗浄液のガスはその側壁に接して冷却、 凝縮し、 その凝縮状態のまま真 空容器内に残留して、 乾燥を阻害するという問題があった。 更に、 細管や入り組 んだ形状を有する複雑な形状の被乾燥物を乾燥させる場合は、 特に部位毎に品温 差が生じ易く 、 この品温差により、 部位毎の乾燥状態が不均一となって輪ジミゃ 発銪の要因となり、 洗浄、 乾燥させた被乾燥物の外観を著しく損ねるという問題 もあった。 また、 別の手法と して、 蒸気を被乾燥物に向けて強制的に噴射させる 蒸気噴射加熱方式もあるが、 蒸気化に伴う設備や噴射用のポンプを設ける必要が あり、 コス ト アップが生じてしまう。 発明の開示  For example, there is a hot air heating method in which hot air is blown into a vacuum vessel as a simple method to raise the temperature of the material to be dried at the start of evacuation ^). However, heating for a limited time causes the vacuum vessel to enter a dry state without the temperature of the side wall rising sufficiently, so that the gas of the evaporated cleaning solution contacts the side wall and cools and condenses. As a result, there is a problem in that it remains in the vacuum container and inhibits drying. Furthermore, when drying a dried object having a complicated shape having a thin tube or a complicated shape, a temperature difference is likely to occur particularly in each part, and the drying state in each part becomes uneven due to the temperature difference. As a result, there is a problem that the appearance of the washed and dried object to be dried is significantly impaired. As another method, there is also a steam injection heating method in which steam is forcibly injected toward the material to be dried.However, it is necessary to provide equipment for evaporating and a pump for injection to increase the cost. Will happen. Disclosure of the invention
本発明は、 上記の問題に鑑みてなされたものであり、 主要構成部品内外及びそ の構成部品同士での圧力差を抑制して、 格別な配慮を施すことなく容易に気密性 を維持でき、 しかも、 可燃性の洗浄液が用いられた場合でも、 火災や爆発に対し て安全性に優れた真空超音波方式の洗浄装置を提供することを目的とするもので ある。 The present invention has been made in view of the above-described problems, and suppresses a pressure difference between inside and outside of a main component and between the components, so that airtightness can be easily achieved without special consideration. It is an object of the present invention to provide a vacuum ultrasonic cleaning apparatus which is capable of maintaining the above conditions and which is excellent in safety against fire and explosion even when a flammable cleaning liquid is used.
また、 本発明の目的は、 電子、 機械、 成形関連等の部品に対し効率よく かつ安 全に洗浄から乾燥までし得る洗浄方法を提供することにある。  It is another object of the present invention to provide a cleaning method capable of efficiently and safely cleaning and drying electronic, mechanical, and molding-related parts.
上記目的を達成するため、 本発明による洗浄装置は、 真空下におかれた洗浄液 に超音波振動を与えて、 前記洗浄液に浸潰した被洗浄物を洗浄する洗浄装置にお いて、 前記洗浄液を貯留し前記被洗浄物を収容する洗浄槽と、 内部に所定空間を 有し前記洗浄液に超音波振動を与える振動体とを、 真空状態を取り得る洗浄用真 空容器内に備え、 前記振動体の所定空間が前記洗浄用真空容器内に開口している これにより、 洗浄槽と振動体とを同一圧力下におけるとともに、 それらの内外で 圧力差が生じないため、 格別な配慮を施すことなく容易に気密性を維持できる。 その振動体の所定空間には、 一般に、 超音波振動を起こすための充電部が備え られているが、 仮に、 洗浄液として炭化水素系のような可燃性の洗浄液が用いら れ、 その洗浄液が漏洩やベン ト等によって所定空間に存した場合、 充電部が着火 源となつて火災や爆発を引き起こす危険性が生じるので、 前記振動体の所定空間 をパージするためのパージガスを前記所定空間に供給するパージガス供給手段を 備えているこ とが好ましい。  In order to achieve the above object, a cleaning apparatus according to the present invention is directed to a cleaning apparatus for applying an ultrasonic vibration to a cleaning liquid placed under vacuum to clean an object to be cleaned immersed in the cleaning liquid, A cleaning tank for storing and holding the object to be cleaned, and a vibrator having a predetermined space therein and applying ultrasonic vibration to the cleaning liquid, provided in a vacuum chamber for cleaning capable of maintaining a vacuum state, A predetermined space is opened in the cleaning vacuum vessel. This allows the cleaning tank and the vibrating body to be under the same pressure, and there is no pressure difference between the inside and outside of the cleaning tank and the vibrating body. Airtightness can be maintained. A charging section for generating ultrasonic vibration is generally provided in a predetermined space of the vibrating body, but if a flammable cleaning liquid such as a hydrocarbon-based cleaning liquid is used as the cleaning liquid, the cleaning liquid leaks. If there is a risk of causing a fire or explosion when the charged part is in a predetermined space due to an ignition source, a purge gas for purging a predetermined space of the vibrator is supplied to the predetermined space. Preferably, a purge gas supply means is provided.
また、 振動体を容易に備える観点から、 超音波振動が伝播する振動板と、 この 振動板上に取り付けられたカバーとにより形成された前記所定空間に、 超音波振 動を発する振動子が設けられていて、 前記洗浄槽の底壁又は側壁に形成された開 口を閉塞するように、 前記振動板が前記所定空間を前記洗浄槽の外側に向けて配 置されるとと もに、 前記振動板の周縁部から前記洗浄槽の底壁又は側壁を貫通す る貫通穴にボルトを挿通して固定されるとよい。 ただし、 洗浄槽に貯留している 洗浄液が貫通穴を通じて漏洩するおそれがあるが、 仮に、 その洗浄液が貫通穴を 通じて漏洩しても、 所定空間内へ侵入しなければ、 振動子が浸食を受けたり、 振 動子が備えた充電部を着火源として火災や爆発が生じたりする危険性は格段に減 少するので、 前記カバーが前記振動板上の前記貫通穴より も中央側で取り付けら れている。 更に、 その貫通穴から漏洩した洗浄液が所定空間へ侵入するのをより確実に防 止する目的から、 前記振動板の中央部が前記貫通穴を有する周縁部よりも前記洗 浄槽に対して陥没しており、 前記カバーが前記振動板の前記中央部上に取り付け られることが好ましい。 In addition, from the viewpoint of easily providing a vibrating body, a vibrator that emits ultrasonic vibration is provided in the predetermined space formed by a vibration plate through which ultrasonic vibration propagates and a cover mounted on the vibration plate. Wherein the diaphragm is disposed so that the predetermined space faces the outside of the cleaning tank so as to close an opening formed in a bottom wall or a side wall of the cleaning tank. It is preferable that the diaphragm is fixed by inserting a bolt from a peripheral portion of the diaphragm into a through hole penetrating the bottom wall or the side wall of the cleaning tank. However, the cleaning liquid stored in the cleaning tank may leak through the through-hole, but if the cleaning liquid leaks through the through-hole and does not enter the predetermined space, the vibrator may erode. Or the risk of fire or explosion from the charged part of the transducer as an ignition source is greatly reduced, so the cover is attached at the center side of the through hole on the diaphragm. Have been Further, in order to more reliably prevent the cleaning liquid leaking from the through hole from entering the predetermined space, the center of the diaphragm is depressed with respect to the cleaning tank more than the peripheral portion having the through hole. Preferably, the cover is mounted on the central portion of the diaphragm.
また、 洗浄後の被洗浄物を洗浄液から洗浄槽の上方へ取り出す際、 洗浄液の一 部は、 被洗浄物に付着して持ち出されながら滴り落ち、 洗浄槽の周囲を無秩序に 汚したり、 洗浄槽の側壁外面を伝って流下し側壁や底壁に設けた振動体を不用意 に濡らしたり してしまうので、 これを避けるべく、 滴り落ちた洗浄液をガイ ドし て洗浄槽に回収したり、 洗浄槽の側壁から遠ざけたりするように、 前記洗浄槽の 側壁上端部が外側下方に向けて折り曲げられていることが好ましい。  When the object to be cleaned after cleaning is removed from the cleaning liquid to above the cleaning tank, a portion of the cleaning liquid adheres to the object to be cleaned and drops out while being taken out, and the surroundings of the cleaning tank are randomly disordered, and the cleaning tank is not cleaned. To avoid this, the vibrating body provided on the side wall and bottom wall may be inadvertently wetted along the outer surface of the side wall. Preferably, the upper end of the side wall of the cleaning tank is bent outward and downward so as to keep away from the side wall of the tank.
また、 仮に、 滴り落ちた洗浄液が洗浄槽の側壁外面を伝って流下しても、 振動 体等が設けられている底壁へ回り込まないようにする目的で、 前記洗浄槽の側壁 下端部が底壁より下方に突出しているとよい。 更に、 側壁外面を伝って流下する 洗浄液を所定位置に集めることができれば、 回収が容易になるので、 例えば、 前 記洗浄槽の側壁下端部の縁が、 凹凸状であったり、 水平面に対して傾斜していた り してもよい。  Also, even if the dripped cleaning liquid flows down along the outer surface of the side wall of the cleaning tank, the lower end of the side wall of the cleaning tank has a bottom end in order to prevent the cleaning liquid from wrapping around the bottom wall provided with the vibrator and the like. It is good to project below the wall. Furthermore, if the cleaning liquid flowing down the outer wall of the side wall can be collected at a predetermined position, the recovery becomes easier.For example, the edge of the lower end portion of the side wall of the cleaning tank is uneven or has a flat surface. It may be inclined.
また本発明による洗浄装置は、 洗浄液を貯留し被洗浄物を収容する洗浄槽と、 内部に所定空間を有し前記洗浄液に超音波振動を与える振動体とを、 真空状態を 取り得る洗浄用真空容器内に備え、 前記振動体の所定空間が前記洗浄用真空容器 内に開口しており、 真空下におかれた前記洗浄液に超音波振動を与えて、 この洗 浄液に浸潰した前記被洗浄物を洗浄する洗浄手段と、 この洗浄手段で洗浄された 前記被洗浄物を被乾燥物と して収容し真空状態を取り得る乾燥用真空容器と、 加 熱された溶液を収容する加熱容器と、 前記乾燥用真空容器と前記加熱容器を連通 する配管と、 を備え、 前記配管の一端は前記被乾燥物に向けて開口し、 前記配管 の他端は前記溶液に浸潰しており、 前記乾燥用真空容器が真空状態のときに前記 配管が開放されて、 前記溶液が沸騰状態で前記配管の前記一端から前記被乾燥物 に向けて噴射され、 この被乾燥物を乾燥させる乾燥手段と、 よりなる。 これによ り、 被洗浄物は、 先ず洗浄手段によ って真空下で安全に超音波洗浄され、 次いで 乾燥手段によつて被乾燥物と して真空状態で効率よく 熱が与えられ、 短時間で乾 燥される。 Further, the cleaning apparatus according to the present invention comprises: a cleaning tank for storing a cleaning liquid and accommodating an object to be cleaned; and a vibrator having a predetermined space therein and applying ultrasonic vibration to the cleaning liquid, comprising: A predetermined space of the vibrator is provided in the container, and the predetermined space of the vibrator is opened in the cleaning vacuum container. The cleaning liquid placed under vacuum is subjected to ultrasonic vibration to immerse the cleaning liquid in the cleaning liquid. Cleaning means for cleaning the cleaning object; a vacuum container for drying capable of holding the object to be cleaned which has been cleaned by the cleaning means as an object to be dried and taking a vacuum state; and a heating container for storing the heated solution And a pipe communicating the drying vacuum vessel and the heating vessel. One end of the pipe is opened toward the object to be dried, and the other end of the pipe is immersed in the solution. When the vacuum vessel for drying is in a vacuum state, A drying means which is opened and injects the solution in a boiling state from the one end of the pipe toward the object to be dried, and dries the object to be dried. As a result, the object to be cleaned is first subjected to safe ultrasonic cleaning under vacuum by the cleaning means, and then the heat is efficiently applied to the object to be dried in the vacuum state by the drying means. Dry in time Dried.
被乾燥物に向けて噴射される溶液は、 被乾燥物の品温がそれほど高く なく ても 蒸発できる蒸発潜熱の低いものであることが望ましく、 例えば、 前記溶液は炭化 水素系の溶液であるとよい。  It is desirable that the solution sprayed toward the object to be dried has a low latent heat of vaporization that can be evaporated even if the temperature of the object to be dried is not so high.For example, if the solution is a hydrocarbon-based solution Good.
また、 溶液を加熱する際、 ヒータ等の熱源が直接溶液に触れると、 火災や爆発 のおそれがあるため、 これを回避する目的から、 前記加熱容器は隔壁で 2室に分 割されていて、 一方に前記溶液を収容し、 他方に熱源を設けており、 前記熱源か らの熱が前記隔壁を通じて前記溶液に与えられ、 前記溶液が加熱されるようにな つていることが好ま しい。  Also, when heating the solution, if a heat source such as a heater directly touches the solution, there is a risk of fire or explosion.To avoid this, the heating vessel is divided into two chambers by partition walls. It is preferable that one side contains the solution and the other side is provided with a heat source, and the heat from the heat source is applied to the solution through the partition wall so that the solution is heated.
被乾燥物に向けて噴射された沸騰状態の溶液の状態、 及び、 被乾燥物の品温状 態を安定化させる観点から、 前記配管の経路に駆動弁が設けられており、 前記乾 燥用真空容器内の圧力と、 前記溶液が収容されている前記加熱容器内の圧力と、 前記溶液の温度とに基づき、 前記駆動弁の開閉度合いが調節されるようになって いることが好ま しい。  In order to stabilize the state of the boiling solution sprayed toward the object to be dried and the temperature of the product to be dried, a drive valve is provided in the pipe path, and the It is preferable that the degree of opening and closing of the drive valve is adjusted based on a pressure in a vacuum vessel, a pressure in the heating vessel containing the solution, and a temperature of the solution.
更に、 被乾燥物に熱を与えて凝縮した溶液が再度蒸気化して被乾燥物に熱を与 えたり、 真空容器内の温度をより急速に高めるたりすることができれば、 より効 率が上がるので、 前記乾燥用真空容器の内側面と底面とのうち、 少なく とも 1 つ に加熱手段を設けるとよい。  In addition, if the condensed solution is heated by applying heat to the object to be dried and vaporized again to heat the object to be dried or the temperature in the vacuum vessel can be increased more rapidly, the efficiency will increase. Preferably, at least one of the inner side surface and the bottom surface of the drying vacuum container is provided with a heating means.
そして、 被乾燥物に向けて噴射される溶液のランニングコス トを抑える観点か ら、 溶液の性質を損なわず再利用することを考慮して、 前記被乾燥物に向けて噴 射されて前記乾燥用真空容器内に存する蒸気化した前記溶液を回収し凝縮させる 溶液凝縮手段と、 前記溶液凝縮手段により凝縮した前記溶液を前記加熱容器に供 給する供給手段とを備えることが好ま しい。  Then, from the viewpoint of suppressing the running cost of the solution sprayed toward the object to be dried, the solution is sprayed toward the object to be dried and the drying is performed in consideration of reuse of the solution without impairing the properties of the solution. It is preferable to include a solution condensing means for collecting and condensing the vaporized solution present in the vacuum container for use, and a supply means for supplying the solution condensed by the solution condensing means to the heating container.
更に、 被乾燥物に向けて噴射される溶液は常に浄化された新液状態であること が望ま しく、 前記被乾燥物に向けて噴射されて前記乾燥用真空容器の底面に溜ま つた前記溶液を回収して排出する溶液排出手段を備えるとよい。  Further, it is desirable that the solution injected toward the object to be dried is always in a purified new liquid state, and the solution injected toward the object to be dried and collected on the bottom surface of the vacuum chamber for drying is desirably used. It is preferable to provide a solution discharging means for collecting and discharging.
また上記目的を達成するための本発明による洗浄方法は、 洗浄液を貯留し被洗 浄物を収容する洗浄槽と、 内部に所定空間を有し前記洗浄液に超音波振動を与え る振動体とを、 真空状態を取り得る洗浄用真空容器内に備え、 前記振動体の所定 空間が前記洗浄用真空容器内に開口 しており、 真空下におかれた前記洗浄液に超 音波振動を与えて、 この洗浄液に浸潰した前記被洗浄物を洗浄する洗浄工程と、 この洗浄工程を経た前記被洗浄物を被乾燥物と して収容し真空状態を取り得る乾 燥用真空容器と、 加熱された溶液を収容する加熱容器と、 前記乾燥用真空容器と 前記加熱容器を連通する配管と、 を備え、 前記配管の一端は前記被乾燥物に向け て開口し、 前記配管の他端は前記溶液に浸潰しており、 前記乾燥用真空容器が真 空状態のときに前記配管が開放されて、 前記溶液が沸騰状態で前記配管の前記一 端から前記被乾燥物に向けて噴射され、 この被乾燥物を乾燥させる乾燥工程と、 よりなる。 図面の簡単な説明 Further, a cleaning method according to the present invention for achieving the above object, comprises: a cleaning tank that stores a cleaning liquid and stores an object to be cleaned; and a vibrator that has a predetermined space therein and applies ultrasonic vibration to the cleaning liquid. A cleaning state that can be maintained in a vacuum state; A space is opened in the vacuum chamber for cleaning, a cleaning step of applying ultrasonic vibration to the cleaning liquid placed under vacuum, and cleaning the object to be cleaned immersed in the cleaning liquid; A vacuum container for drying capable of holding the object to be cleaned after drying as a material to be dried and maintaining a vacuum state, a heating container for storing a heated solution, and communicating the vacuum container for drying with the heating container. One end of the pipe is opened toward the object to be dried, the other end of the pipe is immersed in the solution, and the pipe is evacuated when the drying vacuum container is in a vacuum state. A drying step in which the solution is opened and the solution is sprayed in a boiling state from the one end of the pipe toward the object to be dried, and the object to be dried is dried. BRIEF DESCRIPTION OF THE FIGURES
第 1図は本発明の第 1 実施形態である洗浄装置全体の構成を表す構成図である ( 第 2図は第 1 実施形態の洗浄装置における洗浄部の要部断面図である。 FIG. 1 is a configuration diagram showing a configuration of an entire cleaning apparatus according to a first embodiment of the present invention ( FIG. 2 is a sectional view of a main part of a cleaning unit in the cleaning apparatus of the first embodiment).
第 3図は洗浄液の漏洩状態を模式的に表す図である。  FIG. 3 is a diagram schematically showing a state of leakage of the cleaning liquid.
第 4図は洗浄液が滴り落ちる状態を模式的に表す図である。  FIG. 4 is a diagram schematically showing a state in which the cleaning liquid drips.
第 5図は第 2実施形態の洗浄装置における洗浄槽下部の要部断面図である。 第 6図は第 3実施形態の洗浄装置における洗浄部の要部断面図である。  FIG. 5 is a sectional view of a main part of a lower portion of a cleaning tank in a cleaning device according to a second embodiment. FIG. 6 is a cross-sectional view of a main part of a cleaning unit in a cleaning device according to a third embodiment.
第 7図は洗浄液の漏洩状態を模式的に表す第 6図の A部の拡大図である。  FIG. 7 is an enlarged view of part A of FIG. 6 schematically showing the state of leakage of the cleaning liquid.
第 8図は第 4実施形態の洗浄装置における洗浄槽下部の側面図である。  FIG. 8 is a side view of the lower part of the cleaning tank in the cleaning device of the fourth embodiment.
第 9図は第 5実施形態の洗浄装置における洗浄槽下部の側面図である。  FIG. 9 is a side view of the lower part of the cleaning tank in the cleaning device of the fifth embodiment.
第 1 0図は洗浄液の物性の一例を表す図である。  FIG. 10 is a diagram illustrating an example of the physical properties of the cleaning liquid.
第 1 1図は第 6実施形態である乾燥装置全体の構成を表す構成図である。  FIG. 11 is a configuration diagram showing the configuration of the entire drying apparatus according to the sixth embodiment.
第 1 2図は第 6実施形態の乾燥装置における乾燥部の要部断面図である。  FIG. 12 is a cross-sectional view of a main part of a drying unit in a drying device according to a sixth embodiment.
第 1 3図は第 7実施形態の乾燥装置における乾燥部の要部断面図である。  FIG. 13 is a cross-sectional view of a main part of a drying unit in the drying device according to the seventh embodiment.
第 1 4図は従来の洗浄装置の要部断面図である。  FIG. 14 is a sectional view of a main part of a conventional cleaning apparatus.
第 1 5図は従来の他の洗浄装置の要部断面図である。 発明を実施するための最良の形態  FIG. 15 is a sectional view of a main part of another conventional cleaning apparatus. BEST MODE FOR CARRYING OUT THE INVENTION
以下、 本発明の実施形態である洗浄装置及び乾燥装置について、 順に図面を参 照しながら詳述する。 先ず、 本発明の第 1実施形態である洗浄装置について説明 する。 第 1図は洗浄装置全体の構成図が、 第 2図は第 1 図における洗浄部の要部 断面図がそれぞれ示されている。 洗浄装置 、 第 1図に示されるように、 概略、 洗浄部と蒸留部とに大別される。 なお、 蒸留部は、 蒸留器、 一次槽、 ドレン槽、 再熱器、 凝縮器、 冷却水、 温水、 水分除去ユニッ ト等で構成されるが、 本発明と 直接関係しないので、 詳細の説明は省略する。 Hereinafter, a cleaning device and a drying device according to an embodiment of the present invention will be sequentially described with reference to the drawings. It will be described in detail with reference to FIG. First, a cleaning device according to a first embodiment of the present invention will be described. FIG. 1 is a configuration diagram of the entire cleaning apparatus, and FIG. 2 is a cross-sectional view of a main part of the cleaning unit in FIG. As shown in FIG. 1, the washing apparatus is roughly divided into a washing section and a distillation section. The distillation section is composed of a still, a primary tank, a drain tank, a reheater, a condenser, cooling water, hot water, a water removal unit, etc., but is not directly related to the present invention. Omitted.
先ず、 洗浄部の要部構成を以下に説明する。 1 は真空容器 (以下、 後述する乾 燥用真空容器 2 0 1 と区別して 「洗浄用真空容器」 と記すことがある) 、 2は真 空容器 1 の蓋、 3は電子、 機械、 成形関連部品等の被洗浄物、 4は被洗浄物 3を 入れるバスケ ッ ト、 5は炭化水素系の洗浄液、 6は被洗浄物 3を収容する洗浄槽, 7は超音波振動子ュニッ トである。  First, the main configuration of the cleaning unit will be described below. 1 is a vacuum vessel (hereinafter sometimes referred to as a “vacuum vessel for cleaning” to distinguish it from the vacuum vessel 201 for drying described later), 2 is the lid of the vacuum vessel 1, and 3 is related to electronics, machinery, and molding. An object to be cleaned such as parts, 4 is a basket for storing the object to be cleaned 3, 5 is a hydrocarbon-based cleaning liquid, 6 is a cleaning tank for storing the object to be cleaned 3, and 7 is an ultrasonic vibrator unit.
真空容器 1 は、 上端が開放した円筒状に形成され、 内部に洗浄槽 6 と超音波振 動子ユニッ ト 7を配備しており、 開放した上端には基軸 2 aを中心に回動する蓋 2を備えている。 つまり、 蓋 2を回動させて開いた状態で、 被洗浄物 3の入った 網状のバスケ ッ ト 4が真空容器 1 の内外へ出し入れされ、 一方、 閉じた状態で真 空容器 1が密閉されるようになっている。 なお、 真空容器 1 の底壁には真空排気 □ 1 aが形成され、 蓋 2 には真空容器 1 内の圧力を検出する圧力センサ 1 7が設 けられている。  The vacuum vessel 1 is formed in a cylindrical shape with an open upper end, and has a cleaning tank 6 and an ultrasonic oscillator unit 7 installed inside.A lid that rotates around the base shaft 2a is located at the open upper end. It has two. In other words, with the lid 2 rotated and opened, the net-like basket 4 containing the object 3 to be washed is put in and out of the vacuum vessel 1, while the vacuum vessel 1 is closed and closed. It has become so. In addition, vacuum evacuation □ 1a is formed on the bottom wall of the vacuum vessel 1, and a pressure sensor 17 for detecting the pressure in the vacuum vessel 1 is provided on the lid 2.
洗浄槽 6は、 底壁 6 dを共用して、 洗浄液 5を貯留する貯槽部 6 a と、 貯槽部 6 aから溢れた洗浄液 5を回収する溢液回収部 6 hとに大別される。 貯槽部 6 a には、 洗浄液 5を供給する洗浄液供給□ 6 gが側壁に形成され、 その洗浄液供給 □ 6 gの上方に開口 6 f が形成され、 その開□ 6 f を挟み込む上下一対の液位セ ンサ 1 5が配置されている。 ここで、 貯槽部 6 aに貯留されている洗浄液 5は、 開□ 6 f を超えると開□ 6 f から溢液回収部 6 hに流出し、 一方では、 液位セン サ 1 5によつて液位が検知され、 その液位が下がると新たに洗浄液 5が洗浄液供 給 D 6 gから供給されて、 常時一定の液位が保たれるようになつている。 なお、 洗浄液供給口 6 gは、 後述する洗浄液調温槽 3 0に連通した給液配管 3 5に連結 され、 また、 溢液回収部 6 hの底壁 6 dには開口 6 i が形成され、 貯槽部 6 aに は洗浄液 5の液温を検出する温度センサ 1 6が設けられている。 また、 洗浄槽 6の側壁 6 bの上端部 6 cは、 外側下方に向けて折り曲げられ、 一方、 下端部 6 eは底壁 6 dより下方に突出している。 The cleaning tank 6 is roughly divided into a storage section 6a for storing the cleaning liquid 5 and a overflow collecting section 6h for collecting the cleaning liquid 5 overflowing from the storage section 6a, sharing the bottom wall 6d. A cleaning liquid supply □ 6 g for supplying the cleaning liquid 5 is formed on the side wall of the storage tank section 6 a, an opening 6 f is formed above the cleaning liquid supply □ 6 g, and a pair of upper and lower liquids sandwiching the opening □ 6 f is formed. Position sensor 15 is arranged. Here, the cleaning liquid 5 stored in the storage tank section 6a flows out of the opening □ 6f to the overflow collecting section 6h when it exceeds the opening □ 6f, and on the other hand, by the liquid level sensor 15. When the liquid level is detected and the liquid level drops, a new cleaning liquid 5 is supplied from the cleaning liquid supply D 6 g, so that a constant liquid level is always maintained. The cleaning liquid supply port 6 g is connected to a liquid supply pipe 35 communicating with a cleaning liquid temperature control tank 30 described later, and an opening 6 i is formed in the bottom wall 6 d of the overflow liquid recovery section 6 h. The storage section 6a is provided with a temperature sensor 16 for detecting the temperature of the cleaning liquid 5. The upper end 6c of the side wall 6b of the cleaning tank 6 is bent outward and downward, while the lower end 6e protrudes below the bottom wall 6d.
超音波振動子ユニッ ト 7は、 超音波振動が伝播する振動板 8と、 この振動板 8 の下面に取り付けられ超音波振動を発する複数の振動子 9 と、 これら各振動子 9 を包囲し振動板 8の下面に取り付けられたカバー 1 0 とから構成されていて、 振 動板 8 とカバ一 1 0とにより囲まれた内部空間 7 aが形成されている。 振動板 8 は、 各振動子 9が取り付けられた中央部 8 aが、 周縁部 8 bより も上面側に 1段 隆起しており、 カバ一 1 0はその中央部 8 a上に取り付けられている。  The ultrasonic vibrator unit 7 includes a vibrating plate 8 through which ultrasonic vibration propagates, a plurality of vibrators 9 mounted on the lower surface of the vibrating plate 8 to generate ultrasonic vibrations, and a vibrator surrounding each of the vibrators 9. An inner space 7 a is formed by a cover 10 attached to the lower surface of the plate 8 and surrounded by the vibration plate 8 and the cover 10. The diaphragm 8 has a central portion 8a to which the respective vibrators 9 are attached, which is raised one step above the peripheral portion 8b, and the cover 10 is attached on the central portion 8a. I have.
また、 貯槽部 6 aの底壁 6 dには開口 6 j が形成されており、 振動板 8は、 そ の開口 6 j を振動板 8の中央部 8 aの上面で閉塞するよう に配置され、 振動板 8 の周縁部 8 b と、 洗浄槽 6の底壁 6 dと、 これらの間に挟んだテフロン (R ) 製 のパッキン 1 3 とを貫通する不図示の貫通穴に、 ボルト 1 2を挿通して締結され ている。 なお、 電気で駆動される各振動子 9の端部には、 その電気駆動を司る充 電部 9 aが備えられ、 カバ一 1 0には、 吸気□ 1 0 aと、 真空容器 1 内に向けて のみ内部空間 Ί aを開放可能にする逆止弁 1 1 が連結された排気口 1 0 b と、 が 形成されている。  An opening 6j is formed in the bottom wall 6d of the storage tank 6a, and the diaphragm 8 is arranged so as to close the opening 6j with the upper surface of the central portion 8a of the diaphragm 8. A bolt 1 2 is inserted into a through hole (not shown) that penetrates the peripheral portion 8 b of the diaphragm 8, the bottom wall 6 d of the cleaning tank 6, and a Teflon (R) packing 13 sandwiched therebetween. And is fastened. The end of each of the vibrators 9 driven by electricity is provided with a charging section 9 a for controlling its electric drive. The cover 10 has a suction port 10 a and a vacuum vessel 1. And an exhaust port 10b to which a check valve 11 that allows the internal space Ίa to be opened only toward the exhaust port is formed.
真空容器 1 の真空排気口 1 aは、 電磁弁 2 1、 2 2を経路に備えた真空排気配 管 2 0の一端に連結され、 その真空排気配管 2 0の他端は、 真空ポンプ 2 5に連 結されている。 更に、 真空ポンプ 2 5の下流側には気液分離器 2 6が設けられて いる。 一方、 真空排気配管 2 0は電磁弁 2 1 と 2 2との間で分岐し、 溢液回収部 6 hの開口 6 i に連結された分岐配管 2 0 aが形成され、 その分岐配管 2 0 aの 経路に電磁弁 2 3が備えられている。 つまり、 電磁弁 2 1、 2 2を開く ことによ つて、 真空容器 1 内が減圧されて、 洗浄槽 6及び超音波振動子ユニッ ト 7が減圧 下におかれ、 更に、 逆止弁 1 1 を介して超音波振動子ユニッ ト 7の内部空間 7 a も減圧されるようになっている。 一方、 電磁弁 2 3を開く ことによって、 溢液回 収部 6 hに流出した洗浄液 5を分岐配管 2 0 aに吸引するようになっている。 カバー 1 0の吸気□ 1 0 aは、 詳細は後述するが、 減圧開始から洗浄完了にか けて超音波振動子ュニッ ト 7の内部空間 7 aをパージするときと、 洗浄完了後の ベン トのときに活用され、 吸気配管 4 6の一端に接続されている。 この吸気配管 4 6は、 経路に流量計 4 7や逆止弁 4 8等を備えて他端が 2本に分岐しており、 一方は、 レギユ レ一夕 4 1や電磁弁 4 2等を介して、 窒素ガス等の不活性ガスを 封したガスボンベ 4 0に接続され、 他方は、 電磁弁 4 4や逆止弁 4 5を介して、 圧縮空気や開放した大気等の空気 4 3に接続されている。 つまり、 本実施形態の 洗浄装置は、 パージ作用とベン ト作用を共用した形態である。 更に、 パージ及び ベン ト用ガスと してガスボンべ 4 0中のガスと空気 4 3 との 2者を選択できるよ うにした形態であるが、 もちろん、 一方のみ備えていれば足りる。 なお、 予防安 全面の観点から、 パージ及びベン ト用ガスと しては不活性ガスを用いる方が好ま しい。 The vacuum exhaust port 1a of the vacuum vessel 1 is connected to one end of a vacuum exhaust pipe 20 provided with solenoid valves 21 and 22 in a path, and the other end of the vacuum exhaust pipe 20 is connected to a vacuum pump 25. It is linked to Further, a gas-liquid separator 26 is provided downstream of the vacuum pump 25. On the other hand, the evacuation pipe 20 branches off between the solenoid valves 21 and 22 to form a branch pipe 20 a connected to the opening 6 i of the overflow collection part 6 h. A solenoid valve 23 is provided in the path a. That is, by opening the solenoid valves 21 and 22, the pressure in the vacuum vessel 1 is reduced, and the cleaning tank 6 and the ultrasonic transducer unit 7 are reduced in pressure. The internal space 7a of the ultrasonic transducer unit 7 is also depressurized through this. On the other hand, by opening the solenoid valve 23, the cleaning liquid 5 flowing out to the overflow collection part 6h is sucked into the branch pipe 20a. The air intake □ 10a of the cover 10 will be described later in detail, but the purging of the internal space 7a of the ultrasonic vibrator unit 7 from the start of the depressurization to the completion of the cleaning, and the vent after the completion of the cleaning It is used when it is connected to one end of the intake pipe 46. This intake pipe 46 has a flow meter 47, a check valve 48, etc. in the path, and the other end is branched into two, one of which is connected via a regulator 41, a solenoid valve 42, etc. It is connected to a gas cylinder 40 sealed with an inert gas such as nitrogen gas, and the other is connected to air 43 such as compressed air or open air via a solenoid valve 44 or a check valve 45. . That is, the cleaning device of the present embodiment is a form in which the purging action and the venting action are shared. Further, the gas and air 43 in the gas cylinder 40 can be selected as the gas for purging and venting. Of course, it is sufficient to provide only one of them. In addition, it is preferable to use an inert gas as a purge and vent gas from the viewpoint of preventive safety.
このような構成の洗浄装置の動作、 及びミ その動作中の様子について、 以下に 説明する。 第 1、 2図に示されるように、 被洗浄物 3を入れたバスケッ ト 4を真 空容器 1 内に備えた洗浄槽 6に収容して、 貯槽部 6 aに貯留されている洗浄液 5 に浸漬させ、 蓋 2を閉じた状態にする。 次いで、 真空ポンプ 2 5を作動させると ともに電磁弁 2 1、 2 2を開く と、 真空容器 1 内の空気が、 真空排気ロ 1 aから 真空排気配管 2 0を経て真空ポンプ 2 5へ吸引されて、 真空引きが開始される。 この際、 吸気配管 4 6の電磁弁 4 2等又は電磁弁 4 4を開く ことによ り、 超音波 振動子ュニッ ト 7の内部空間 7 aは、 ガスボンベ 4 0中のガス又は空気 4 3とい つたパージガスが吸気口 1 0 aから導入されてパージが行われると同時に、 排気 口 1 O bから逆止弁 1 1 を介して吸引され減圧されていく。 また、 分岐配管 2 0 aの電磁弁 2 3 も開き、 溢液回収部 6 hに流出した洗浄液 5を吸引する。  The operation of the cleaning apparatus having such a configuration and the state during the operation will be described below. As shown in FIGS. 1 and 2, a basket 4 containing an object to be cleaned 3 is stored in a cleaning tank 6 provided in a vacuum container 1, and the cleaning liquid 5 stored in a storage tank 6a is supplied to the cleaning tank 5. Immerse and leave lid 2 closed. Next, when the vacuum pump 25 is operated and the solenoid valves 21 and 22 are opened, the air in the vacuum vessel 1 is sucked from the vacuum pump 1 a to the vacuum pump 25 through the vacuum pump pipe 20. Then, evacuation is started. At this time, by opening the solenoid valve 42 or the like or the solenoid valve 44 of the intake pipe 46, the internal space 7a of the ultrasonic vibrator unit 7 is called gas or air 43 in the gas cylinder 40. The purge gas is introduced from the intake port 10a and purged, and at the same time, it is sucked from the exhaust port 10Ob via the check valve 11 and the pressure is reduced. In addition, the solenoid valve 23 of the branch pipe 20a is also opened to suck the cleaning liquid 5 flowing out to the overflow collecting part 6h.
その後、 圧力計 1 7で検出される真空容器 1 内の圧力が所定値 (真空状態) に なつた時点で振動子 9を作動させると、 超音波振動が振動板 8を伝播して洗浄液 5 に与えられ、 その洗浄液 5中にキ ヤビテーシ ヨ ンが発生して、 浸漬している被 洗浄物 3の洗浄が行われる。  Then, when the vibrator 9 is actuated when the pressure in the vacuum vessel 1 detected by the pressure gauge 17 reaches a predetermined value (vacuum state), the ultrasonic vibration propagates through the diaphragm 8 to the cleaning liquid 5. The cavitation is generated in the cleaning liquid 5 and the immersed object 3 is cleaned.
所定時間が経過した後、 被洗浄物 3の洗浄が完了しベン トに移行する。 真空排 気配管 2 0の電磁弁 2 2、 又は、 電磁弁 2 1、 2 3を閉じ、 次いで、 吸気配管 4 6の電磁弁 4 2等又は電磁弁 4 4をより開く と、 ガスボンベ 4 0中のガス又は空 気 4 3 といったベン トガスが超音波振動子ュニッ ト 7の吸気ロ 1 0 a及び排気口 1 0 bを経て逆止弁 1 1 から導入され、 真空容器 1内の圧力が常圧に戻される。 そして、 蓋 2を開き、 洗浄した被洗浄物 3を入れたバスケッ ト 4を真空容器 1 か ら取り出して、 終了する。 After a lapse of a predetermined time, the cleaning of the object to be cleaned 3 is completed, and the process shifts to a vent. When the solenoid valve 22 or the solenoid valves 21 and 23 of the vacuum exhaust pipe 20 are closed, and then the solenoid valve 42 or the like or the solenoid valve 44 of the intake pipe 46 is opened, the gas cylinder 40 A vent gas such as a gas or air 43 is introduced from the check valve 11 through the intake unit 10a and the exhaust port 10b of the ultrasonic vibrator unit 7, and the pressure in the vacuum vessel 1 becomes normal pressure. Is returned to. Then, the lid 2 is opened, the basket 4 containing the washed object 3 is taken out of the vacuum vessel 1, and the process is completed.
ここで、 溢液回収部 6 hに流出した洗浄液 5や、 圧力容器 1 内に存するミス ト 状の洗浄液 5は、 真空容器 1 の真空排気口 l aや、 溢液回収部 6 hの開 0 6 i か ら真空排気配管 2 0を経て真空ポンプ 2 5へ吸引され、 気液分離器 2 6や蒸留部 を経由して浄化される。 その後、 加熱用コイル 3 1や冷却用コイル 3 2が設けら れた洗浄液調温槽 3 0で 4 0 °C程度に調温され、 給液ポンプ 3 6やフ ィルタ 3 7 や電磁弁 1 8等が経路に設けられた給液配管 3 5を介して、 洗浄液供給口 6 gか ら貯槽部 6 aに供給される。 この供給は、 貯槽部 6 aに設けた液位センサ 1 5か らの出力によ り給液ポンプ 3 6や電磁弁 1 8等を作動させて行われるようになつ ている。  Here, the cleaning liquid 5 that has flowed out into the overflow collecting section 6 h and the mist-like cleaning liquid 5 existing in the pressure vessel 1 are discharged from the vacuum exhaust port la of the vacuum vessel 1 and the overflow collecting section 6 h. The water is sucked from i through a vacuum exhaust pipe 20 to a vacuum pump 25 and purified through a gas-liquid separator 26 and a distillation unit. After that, the temperature is adjusted to about 40 ° C in the washing liquid temperature control tank 30 provided with the heating coil 31 and the cooling coil 32, and the liquid supply pump 36, the filter 37, and the solenoid valve 18 Are supplied from a cleaning liquid supply port 6 g to a storage tank 6 a via a liquid supply pipe 35 provided in the path. This supply is performed by operating the liquid supply pump 36, the solenoid valve 18 and the like based on the output from the liquid level sensor 15 provided in the storage section 6a.
また、 真空ポンプ 2 5 と しては、 往復式、 液封式、 回転式等の真空ポンプが挙 げられるが、 本実施形態の洗浄装置では、 以下の理由から、 液封式の真空ポンプ を採用している。 液封式の真空ポンプ 2 5は、 貯槽部 6 aの開口 6 f から溢液回 収部 6 hに流出した洗浄液 5や、 圧力容器 1 内に存するミ ス ト状の洗浄液 5が吸 入されても、 液体を隔ててポンプ回転部と接触するようになっているので、 通常 のシール方式の真空ポンプとは異なり金属摺動面摩擦による火花や熱の発生が少 なく安全性に富み、 支障もないからである。 一方、 液封式の真空ポンプ 2 5は、 使用真空度が補給液の飽和蒸気圧に達するとキ ヤビテーシ ヨ ンによる激しい騒音 を発生して使用に耐えれなく なるので、 これを回避するために、 一般的にはエア ーェゼクタを経路の前段に配置して空気を吸い込ませているが、 本実施形態の洗 浄装置では、 そのエア一ェゼク夕の役割をパージガスの供給で代替している。 なお、 超音波振動子ユニッ ト 7の内部空間 7 aは、 パ一ジガスやベン トガスの 供給以外に外部からの侵入が断たれているので、 圧力容器 1 内に存するミス ト状 の洗浄液 5がその内部空間 7 a内に侵入するこ とはなく、 また、 常時パージ及び ベン ト状態に保たれているので、 仮に振動板 8の欠損等で洗浄液 5が内部空間 7 a内に漏洩しても、 排気□ 1 0 bを経て逆止弁 1 1から強制的に排出される。 つ まり、 その内部空間 7 a内に備えた振動子 9の充電部 9 aが着火源となって、 洗 浄液 5に引火して火災や爆発を引き起こすような状態は全く生じない。 ちなみに, 洗浄液 5が炭化水素系の場合、 爆発範囲は 0 . 8〜5 . 5 vo l . %程度 (第 1 0図 参照) であるが、 本実施形態の洗浄装置では、 常時内部空間 7 aをパージ及びべ ン ト状態にすることによ り、 この爆発範囲を回避させている。 Examples of the vacuum pump 25 include a reciprocating type, a liquid ring type, and a rotary type vacuum pump. In the cleaning apparatus of the present embodiment, a liquid ring type vacuum pump is used for the following reasons. Has adopted. The liquid ring vacuum pump 25 sucks the cleaning liquid 5 flowing out from the opening 6 f of the storage tank section 6 a into the overflow collecting section 6 h and the mist cleaning liquid 5 existing in the pressure vessel 1. However, unlike a normal seal-type vacuum pump, there is little spark or heat generation due to friction on the metal sliding surface, so that the liquid is in contact with the rotating part of the pump with a liquid in between, and the safety is high. Because there is no. On the other hand, the liquid ring vacuum pump 25 generates severe noise due to the cavity when the degree of vacuum used reaches the saturated vapor pressure of the replenisher, and the pump cannot be used. Generally, an air ejector is arranged at the front stage of the path to suck air. However, in the cleaning device of the present embodiment, the role of the air ejector is replaced by the supply of purge gas. Since the inside space 7a of the ultrasonic vibrator unit 7 has been cut off from the outside except for the supply of the purge gas and the vent gas, the mist-like cleaning liquid 5 existing in the pressure vessel 1 is not filled. Since it does not enter the internal space 7a and is always kept in a purged and vented state, even if the cleaning liquid 5 leaks into the internal space 7a due to a defect of the diaphragm 8, etc. The exhaust gas is forcibly discharged from the check valve 11 via the exhaust □ 10 b. In other words, the charged portion 9a of the vibrator 9 provided in the internal space 7a serves as an ignition source, and there is no occurrence of a state in which the cleaning solution 5 is ignited to cause a fire or explosion. By the way, When the cleaning liquid 5 is a hydrocarbon, the explosion range is about 0.8 to 5.5 vol.% (See FIG. 10). However, in the cleaning apparatus of this embodiment, the internal space 7a is always purged. And venting to avoid this explosion area.
また、 超音波振動子ユニッ ト 7の内部空間 7 aを形成するカバ一 1 0が、 ボル ト 1 2よりも中央側で振動板 8に取り付けられているので、 仮に、 洗浄液 5がボ ルト 1 2の貫通穴ゃパッキン 1 3を通じて漏洩 (第 3図のハッチング部) しても、 内部空間 7 a内へ侵入することはない。 しかも、 振動板 8の中央部 8 aを隆起さ せることによ り、 上記の漏洩した洗浄液 5の内部空間 7 a内への侵入防止に対し て、 より有利になるし、 更に、 その形状から振動板 8 自体の変形抵抗が増すため, 振動板 8のボルト締結の際、 締め付け トルクに起因する振動板 8の波打ちやうね り等の変形が生じ難く なり、 慎重な締め付けトルクの管理が大幅に削減できると いう効果も生む。 例えば、 発明者らの実験においては、 2割程度の取り付け工数 の低減が図れた。  Further, since the cover 10 forming the internal space 7a of the ultrasonic vibrator unit 7 is attached to the diaphragm 8 on the center side from the bolt 12, the cleaning liquid 5 is temporarily provided. Even if it leaks through the through hole (2) and the packing (13) (hatched part in Fig. 3), it does not enter the internal space 7a. Moreover, by raising the central portion 8a of the diaphragm 8, it becomes more advantageous to prevent the above-mentioned leaked cleaning liquid 5 from entering the internal space 7a, and furthermore, from the shape thereof. Since the deformation resistance of the diaphragm 8 itself increases, when the bolts of the diaphragm 8 are fastened, deformation such as waving or undulation of the diaphragm 8 due to the tightening torque is less likely to occur, and careful management of the tightening torque is greatly improved. This also has the effect of reducing emissions. For example, in experiments conducted by the inventors, the number of installation steps was reduced by about 20%.
そして、 主要構成部品である洗浄槽 6 と超音波振動子ユニッ ト 7が、 ともに真 空容器 1 内で同一の真空下におかれるとともに、 各々の内外でも圧力差が生じな いため、 各々のみならず連結する関連部品にも負荷が生じない。 従って、 例えば, 振動板 8の板厚に関しては、 通常、 圧力差に対する強度や超音波振動の伝播効率 を考慮して 3〜4 mm程度の板厚であるが、 本実施形態の洗浄装置では、 圧力差の 考慮が不要となるので、 常圧下で用いられる 2〜 3 mm程度の板厚で十分である。 ところで、 第 4図に示されるように、 洗浄後の被洗浄物 3を洗浄液 5から洗浄 槽 6の上方へ取り出す際、 洗浄液 5の一部は、 被洗浄物 3やバスケッ ト 4に付着 して持ち出されながら滴り落ちる液滴 5 aとなり、 洗浄槽 6の周囲を無秩序に汚 したり、 洗浄槽 6の側壁 6 bの外面を伝って流下し側壁 6 bや底壁 6 dに設けた 超音波振動子ユニッ ト 7を不用意に濡らしたり してしまう。 特に、 超音波振動子 ュニッ ト 7の内部空間 7 aには、 着火源となる振動子 9の充電部 9 aが備えられ ているので、 火災や爆発に対する安全性の観点から、 このような状況は避けるこ とが好ま しい。 そこで、 本実施形態の洗浄装置では、 外側下方に向けて折り曲げ られた洗浄槽 6の側壁 6 bの上端部 6 c によって、 液滴 5 aが洗浄槽 6の側壁 6 bから遠ざけられたり、 洗浄槽 6の底壁 6 dより下方に突出している側壁 6 bの 下端部 6 eによって、 洗浄槽 6の側壁 6 bの外面を伝って流下した液滴 5 aが、 超音波振動子ユニッ ト 7を設けた底壁 6 dへ回り込まないようにさせたり してい る。 The cleaning tank 6 and the ultrasonic transducer unit 7, which are the main components, are both placed under the same vacuum in the vacuum vessel 1, and there is no pressure difference between the inside and outside. There is no load on the related parts to be connected. Therefore, for example, the plate thickness of the diaphragm 8 is usually about 3 to 4 mm in consideration of the strength with respect to the pressure difference and the propagation efficiency of ultrasonic vibration, but in the cleaning device of the present embodiment, Since it is not necessary to consider the pressure difference, a plate thickness of about 2-3 mm used under normal pressure is sufficient. By the way, as shown in FIG. 4, when removing the cleaning target 3 from the cleaning liquid 5 above the cleaning tank 6, part of the cleaning liquid 5 adheres to the cleaning target 3 and the basket 4. Droplets 5 a dropping out while being taken out, dirty randomly around the cleaning tank 6, and flow down along the outer surface of the side wall 6 b of the cleaning tank 6, and ultrasonic waves provided on the side wall 6 b and bottom wall 6 d The transducer unit 7 is wetted carelessly. In particular, since the internal space 7a of the ultrasonic vibrator unit 7 is provided with a charged portion 9a of the vibrator 9 serving as an ignition source, from the viewpoint of safety against fire and explosion, It is preferable to avoid the situation. Therefore, in the cleaning apparatus of the present embodiment, the droplet 5a is moved away from the side wall 6b of the cleaning tank 6 by the upper end 6c of the side wall 6b of the cleaning tank 6 bent outward and downward, and the cleaning is performed. Of the side wall 6 b projecting below the bottom wall 6 d of the tank 6 The lower end 6 e prevents the droplet 5 a flowing down the outer surface of the side wall 6 b of the cleaning tank 6 from flowing around the bottom wall 6 d provided with the ultrasonic vibrator unit 7. .
次に、 本発明の第 2実施形態の洗浄装置について、 第 5図を参照しながら説明 する。 第 5図は第 2実施形態の洗浄装置における洗浄槽下部の要部断面図が示さ れている。 なお、 図中で第 1実施形態の洗浄装置と同じ名称で同じ機能を果たす 部分には同一の符号を付し、 重複する説明は省略し、 相違する点について述べる c 後述する第 3〜 5実施形態の洗浄装置においても同様とする。 Next, a cleaning device according to a second embodiment of the present invention will be described with reference to FIG. FIG. 5 is a sectional view showing a main part of a lower portion of a cleaning tank in the cleaning apparatus according to the second embodiment. In the drawings, parts having the same names and the same functions as those of the cleaning device of the first embodiment are denoted by the same reference numerals, overlapping description will be omitted, and different points will be described. The same applies to the cleaning device of the embodiment.
第 2実施形態の洗浄装置の特徴は、 第 1実施形態の洗浄装置における洗浄槽 6 の底壁 6 dの内面が面一になるように超音波振動子ュニッ ト 7を備えた点にある £ 振動板 8の隆起した中央部 8 aを洗浄槽 6の開□ 6 j に嵌めて、 底壁 6 dの内面 が面一になるように振動板 8を取り付けている。 従って、 被洗浄物 3から洗浄液 5に取り込まれた異物や残渣が澱み難く なるので、 洗浄液 5全体に速やかに拡散 して高品位の洗浄性が確保でき、 しかも、 清掃やメンテナンス等が容易となる。 次に、 本発明の第 3実施形態の洗浄装置について、 第 6、 7図を参照しながら 説明する。 第 6図は第 3実施形態の洗浄装置における洗浄部の要部断面図が、 第 7図は洗浄液の漏洩を表す第 6図の A部の拡大図がそれぞれ示されている。 Features of the cleaning apparatus of the second embodiment is that the bottom wall 6 d inner surface of the cleaning tank 6 in the cleaning apparatus of the first embodiment is provided with the ultrasonic vibrator Yuni' preparative 7 to be flush £ The raised central portion 8a of the diaphragm 8 is fitted into the opening 6j of the cleaning tank 6, and the diaphragm 8 is attached so that the inner surface of the bottom wall 6d is flush. Therefore, foreign substances and residues taken into the cleaning liquid 5 from the cleaning object 3 are unlikely to stagnate, and are quickly diffused throughout the cleaning liquid 5 to ensure high-quality cleaning performance, and also facilitate cleaning and maintenance. . Next, a cleaning apparatus according to a third embodiment of the present invention will be described with reference to FIGS. FIG. 6 is a cross-sectional view of a main part of a cleaning unit in the cleaning device of the third embodiment, and FIG. 7 is an enlarged view of part A of FIG. 6 showing leakage of the cleaning liquid.
第 3実施形態の洗浄装置の特徴は、 洗浄槽 6を縦長にし、 超音波振動子ュニッ ト 7をその洗浄槽 6の側壁 6 bに備えた点にある。 洗浄槽 6は、 底壁 6 d と一側 壁 6 bを共用して、 貯槽部 6 aと、 溢液回収部 6 hとに大別される。 貯槽部 6 a の一側壁 6 b には開口 6 kが形成されており、 振動板 8は、 その開口 6 kを振動 板 8の中央部 8 aで閉塞するように配置され、 振動板 8の周縁部 8 b と、 洗浄槽 6の一側壁 6 b と、 これらの間に挟んだパッキン 1 3とを貫通する不図示の貫通 穴に、 ボルト 1 2を挿通して締結されている。 更に、 振動板 8の周縁部 8 bには, ボルト 1 2を包囲するように全周に突設した樋状の突起部 8 cが設けられている < 従って、 被洗浄物 3がスクリーン印刷用めシルクスクリーン板等のように比較 的大型で細長い形状の場合、 その被洗浄物 3を立てた状態で側方から超音波振動 を与えることができ、 効率よく洗浄が行える。 また、 仮に、 洗浄液 5がボルト 1 2の貫通穴ゃパッキン 1 3を通じて漏洩 (第 7図のハッチング部) しても、 振動 板 8に設けた樋状の突起部 8 cで受けることができるので、 超音波振動子ュニッ ト 7の内部空間 7 a内へ侵入することはない。 A feature of the cleaning apparatus of the third embodiment is that the cleaning tank 6 is vertically long, and the ultrasonic vibrator unit 7 is provided on the side wall 6 b of the cleaning tank 6. The washing tank 6 is roughly divided into a storage tank section 6a and an overflow liquid collecting section 6h, sharing the bottom wall 6d and one side wall 6b. An opening 6 k is formed in one side wall 6 b of the storage tank 6 a, and the diaphragm 8 is arranged so as to close the opening 6 k at the center 8 a of the diaphragm 8. Bolts 12 are fastened to through holes (not shown) that penetrate the peripheral portion 8 b, one side wall 6 b of the cleaning tank 6, and the packing 13 sandwiched therebetween. Further, a gutter-like projection 8c is provided on the periphery 8b of the diaphragm 8 so as to surround the bolts 12 so as to surround the bolts 12. <Thus, the object 3 to be cleaned is used for screen printing. In the case of a relatively large and slender shape such as a silk screen plate, ultrasonic vibration can be applied from the side while the object to be cleaned 3 is standing, and cleaning can be performed efficiently. Also, even if the cleaning liquid 5 leaks through the through hole of the bolt 12 and the packing 13 (the hatched portion in FIG. 7), Since it can be received by the gutter-shaped projection 8 c provided on the plate 8, it does not enter the internal space 7 a of the ultrasonic vibrator unit 7.
また、 本実施形態の洗浄装置では、 外側下方に向けて折り曲げられた洗浄槽 6 の側壁 6 bの上端部 6 c によって、 洗浄後の被洗浄物 3を取り出す際に滴り落ち た液滴が、 洗浄槽 6に回収されたり、 洗浄槽 6の側壁 6 bからより遠ざけられた りするようになっているので、 洗浄層 6の一側壁 6 bに設けた超音波振動子ュニ ッ ト 7を不用意に濡らすことはない。 つまり、 洗浄液 5が可燃性であっても、 超 音波振動子ュニッ ト 7の内部空間 7 aに設けた振動子 9の充電部 9 a力 着火源 となるような状況は生じず、 火災や爆発に対する安全性を確保できる。  Further, in the cleaning device of the present embodiment, the upper end portion 6c of the side wall 6b of the cleaning tank 6 bent outward and downward causes droplets that drip when removing the object 3 to be cleaned after cleaning. The ultrasonic vibrator unit 7 provided on one side wall 6b of the cleaning layer 6 is removed because it is collected in the cleaning tank 6 or is further distant from the side wall 6b of the cleaning tank 6. Do not inadvertently get wet. In other words, even if the cleaning liquid 5 is flammable, there is no situation in which the charging section 9a of the vibrator 9 provided in the internal space 7a of the ultrasonic vibrator unit 7 becomes a source of ignition and a fire or Safety against explosion can be ensured.
次に、 本発明の第 4、 5実施形態の洗浄装置について、 第 8、 9図を参照しな がら説明する。 第 8図は第 4実施形態の洗浄装置における洗浄槽下部の側面図が、 第 9図は第 5実施形態の洗浄装置における洗浄槽下部の側面図がそれぞれ示され ている。  Next, cleaning apparatuses according to fourth and fifth embodiments of the present invention will be described with reference to FIGS. FIG. 8 is a side view of the lower portion of the cleaning tank in the cleaning device of the fourth embodiment, and FIG. 9 is a side view of the lower portion of the cleaning tank in the cleaning device of the fifth embodiment.
第 4、 5実施形態の洗浄装置の特徴は、 第 1 実施形態の洗浄装置における洗浄 槽 6の下端部 6 eの縁を変形させた点にある。 第 4実施形態の洗浄装置では、 第 8図に示されるように、 下端部 6 e の縁が凹凸状になっているので、 洗浄後の被 洗浄物 3を取り出す際に滴り落ちた液滴 5 aは、 洗浄槽 6の側壁 6 bの外面を伝 つて流下し、 自重によって凸状部分に集まり滴下する。 第 5実施形態の洗浄装置 では、 第 9図に示されるように、 下端部 6 eの縁が水平面に対して傾斜している ので、 液滴 5 aは洗浄槽 6の側壁 6 bの外面を伝って流下し、 自重によって最も 低い傾斜部分に集まり滴下する。 従って、 液滴 5 aの滴下する位置が定まるので, その液滴 5 aの回収が容易となる。  A feature of the cleaning apparatuses of the fourth and fifth embodiments is that the edge of the lower end 6e of the cleaning tank 6 in the cleaning apparatus of the first embodiment is deformed. In the cleaning device of the fourth embodiment, as shown in FIG. 8, the edge of the lower end 6 e is uneven, so that the droplet a flows down along the outer surface of the side wall 6 b of the cleaning tank 6, and collects and drops on the convex portion by its own weight. In the cleaning device of the fifth embodiment, as shown in FIG. 9, the edge of the lower end 6e is inclined with respect to the horizontal plane, so that the droplet 5a is applied to the outer surface of the side wall 6b of the cleaning tank 6. It flows down and gathers on the lowest slope part due to its own weight and drops. Therefore, since the position where the droplet 5a is dropped is determined, the recovery of the droplet 5a becomes easy.
引き続き、 本発明の第 6実施形態である乾燥装置について説明する。 第 1 1図 は乾燥装置全体の構成図が、 第 1 2図は第 1 1 図における乾燥部の要部断面図が それぞれ示されている。 乾燥装置は、 第 1 1図に示されるように、 概略、 乾燥部 と蒸留部とに大別される。 なお、 蒸留部は、 蒸留器、 再熱器、 凝縮器、 冷熱源、 温熱源、 水分除去ュニッ ト等で構成されるが、 本発明と直接関係しないので、 詳 細の説明は省略する。  Subsequently, a drying apparatus according to a sixth embodiment of the present invention will be described. FIG. 11 is a configuration diagram of the entire drying apparatus, and FIG. 12 is a sectional view of a main part of the drying unit in FIG. 11. The drying apparatus is roughly divided into a drying section and a distillation section, as shown in FIG. The distillation section includes a still, a reheater, a condenser, a cold heat source, a warm heat source, a moisture removal unit, and the like. However, since the distilling unit is not directly related to the present invention, a detailed description thereof will be omitted.
先ず、 乾燥部の要部構成を以下に説明する。 2 0 1 は真空容器 (以下、 前述し た洗浄用真空容器 1 と区別して 「乾燥用真空容器」 と記すことがある) 、 202 は真空容器 20 1の蓋、 203は洗浄液で洗浄された電子、 機械、 成形関連部品 等の被乾燥物 (例えば、 上記の洗浄装置を用いて洗浄液 5で洗浄された被洗浄物 3) 、 204は被乾燥物 203を入れるバスケッ ト、 20 5は加熱容器、 206 は炭化水素系の溶液、 2 07はコイル状のヒー夕、 208は加熱媒体、 209は 真空容器 20 1 と加熱容器 205を連通する連通配管、 2 1 0は連通配管 209 の開閉を司るエアー駆動弁である。 First, the main configuration of the drying section will be described below. 201 is a vacuum vessel (below, ), 202 is the lid of the vacuum vessel 201, and 203 is the object to be dried, such as electronics, machinery, molding parts, etc., which has been washed with the cleaning liquid. (For example, the object to be cleaned 3 washed with the cleaning liquid 5 using the above-described cleaning apparatus), 204 is a basket for storing the object to be dried 203, 205 is a heating vessel, 206 is a hydrocarbon-based solution, and 2007 is A coiled heater, 208 is a heating medium, 209 is a communication pipe for communicating the vacuum vessel 201 with the heating vessel 205, and 210 is an air-driven valve for opening and closing the communication pipe 209.
真空容器 20 1は、 乾燥部の上方を形成し、 上部が開放した円筒状に形成され ており、 その開放した上部には、 基軸 202 aを中心に回動する蓋 202を備え ている。 つま り、 蓋 20 2を回動させて開いた状態で、 被乾燥物 203の入った 網状のバスケ ッ ト 204が真空容器 20 1の内外へ出し入れされ、 一方、 閉じた 状態で真空容器 20 1が密閉されるようになっている。 なお、 真空容器 20 1の 側面には真空排気口 20 1 aや吸気口 20 1 bが形成され、 真空容器 20 1の底 面、 内側面には各々ヒータ 22 1、 222が設けられており、 また、 圧力センサ 23 1、 温度センサ 23 2、 及び、 液位センサ 233も設けられている。  The vacuum vessel 201 is formed in a cylindrical shape with the upper part opened above the drying part, and the open upper part is provided with a lid 202 that rotates about a base shaft 202a. In other words, in a state where the lid 202 is rotated and opened, the net-like basket 204 containing the material 203 to be dried is put in and out of the vacuum container 201, while the vacuum container 201 is closed and closed. Is to be sealed. In addition, a vacuum exhaust port 201 a and an intake port 201 b are formed on the side of the vacuum vessel 201, and heaters 221, 222 are provided on a bottom face and an inner face of the vacuum vessel 201, respectively. Further, a pressure sensor 231, a temperature sensor 232, and a liquid level sensor 233 are provided.
加熱容器 2 05は、 乾燥部の下方を形成し、 熱伝導性の優れた金属製の隔壁 2 0 5 aで上下 2室に分割されていて、 上室 20 5 bには、 溶液 206が収容され, 圧力センサ 24 1、 温度センサ 24 2、 及び、 液位センサ 243が設けられてい る。 一方、 下室 205 cにはヒー夕 207、 圧力センサ 244、 温度センサ 24 5、 及び、 過昇温防止スィ ッチ 24 6が設けられ、 加熱媒体 208が収容されて いる。 つまり、 ヒー夕 207の作動によつ T加熱媒体 208が加熱され、 その加 熱された加熱媒体 208の熱が隔壁 205 aを通じて、 間接的に溶液 206が加 熱されるよう になつており、 しかも、 溶液 206の加熱温度が、 直接的には温度 センサ 242で、 間接的には温度センサ 24 5で検知され、 仮にその温度が異常 上昇した場合には過昇温防止スィ ツチ 246により、 ヒータ 207を停止させる ようになつていることから、 火災や爆発の危険性が極めて少ない構造といえる。 なお、 上室 2 05 bには、 排気 CD 205 d、 供液 d 205 e、 及び、 排出ロ 20 5 f が形成されている。  The heating vessel 205 forms the lower part of the drying section and is divided into two upper and lower chambers by a metal partition wall 205a having excellent heat conductivity.The upper chamber 205b contains a solution 206. A pressure sensor 241, a temperature sensor 242, and a liquid level sensor 243 are provided. On the other hand, the lower chamber 205c is provided with a heater 207, a pressure sensor 244, a temperature sensor 245, and an overheating prevention switch 246, and contains a heating medium 208. In other words, the T heating medium 208 is heated by the operation of the heater 207, and the heat of the heated heating medium 208 is indirectly heated to the solution 206 through the partition wall 205a. The heating temperature of the solution 206 is directly detected by the temperature sensor 242 and indirectly detected by the temperature sensor 245. If the temperature rises abnormally, the overheating prevention switch 246 detects the heating temperature of the heater 207. Because of this, it can be said that the structure has extremely low risk of fire and explosion. The upper chamber 205b is provided with an exhaust CD 205d, a liquid supply d 205e, and an exhaust boil 205f.
また、 連通配管 209は真空容器 20 1 と加熱容器 20 5を連通しており、 上 端 209 aが真空容器 20 1の底面に開口し、 下端 209 bが溶液 206に浸漬 していて、 その経路にエアー駆動弁 2 1 0が設けられている。 The communication pipe 209 connects the vacuum vessel 201 and the heating vessel 205 to each other. The end 209a is open to the bottom of the vacuum vessel 201, the lower end 209b is immersed in the solution 206, and an air drive valve 210 is provided in the path.
真空容器 20 1の真空排気口 20 1 a、 及び、 加熱容器 205の上室 205 a の排気 D 20 5 dは、 真空排気配管 250から分岐した 2つの端各々に連結され、 その分岐した真空排気配管 2 50の経路には各々エアー駆動弁 25 1、 2 52が 設けられていて、 一方、 真空排気配管 2 50の他端は真空ポンプ 25 3に連結さ れている。 更に、 真空ポンプ 253の下流側にはセパレー夕 254が設けられて いる。 つまり、 エアー駆動弁 25 1又は 252の開閉によって、 真空容器 20 1 又は加熱容器 20 5の上室 205 aが減圧されるようになっている。  The vacuum exhaust port 201 a of the vacuum vessel 201 and the exhaust D 205 d of the upper chamber 205 a of the heating vessel 205 are connected to each of two ends branched from the vacuum exhaust pipe 250, and the branched vacuum exhaust is performed. Air drive valves 251 and 252 are provided in the path of the pipe 250, respectively, while the other end of the vacuum exhaust pipe 250 is connected to a vacuum pump 253. Further, a separator 254 is provided downstream of the vacuum pump 253. That is, the upper chamber 205a of the vacuum vessel 201 or the heating vessel 205 is depressurized by opening and closing the air drive valve 251 or 252.
真空容器 2 0 1の吸気口 20 1 bは、 詳細は後述する乾燥が完了した後の真空 容器 20 1の真空状態を常圧に戻す (ベント) ときに活用ざれ、 ベン ト用ガス配 管 26 1の一端に接続されている。 このベン ト用ガス配管 26 1の他端は、 2本 に分岐しており、 一方は、 エアー駆動弁 262ゃレギユレ一夕 263等を介して, 窒素ガス等の不活性ガスを封したガスボンベ 2 64に接続され、 他方は、 逆止弁 265及びエアー駆動弁 266を介して、 圧縮空気や開放した大気等の空気 26 7に接続されている。 つまり、 本実施形態の乾燥装置は、 ベン ト用ガスと してガ スボンべ 264中のガスと空気 26 7との 2者を選択できるようにした形態であ るが、 もちろん、 一方のみ備えていれば足.りる。 なお、 予防安全面の観点から、 ベン ト用ガスと しては不活性ガスを用いる方が好ましい。  The suction port 201b of the vacuum vessel 201 is used for returning the vacuum state of the vacuum vessel 201 to normal pressure (venting) after the drying, which will be described in detail later, is completed. 1 is connected to one end. The other end of the vent gas pipe 26 1 is branched into two pipes. One is a gas cylinder sealed with an inert gas such as nitrogen gas via an air drive valve 262 ゃThe other end is connected to an air 267 such as compressed air or open air through a check valve 265 and an air drive valve 266. In other words, the drying apparatus of the present embodiment has a configuration in which the gas in the gas cylinder 264 and the air 267 can be selected as the vent gas, but of course, only one of them is provided. I'll do it. From the viewpoint of preventive safety, it is preferable to use an inert gas as the vent gas.
このような構成の乾燥装置の動作、 及び、 その動作中の様子について、 以下に 説明する。 第 1 1図に示されるよう に、 被乾燥物 203を入れたパスケッ ト 20 4を真空容器 20 1内に収容して蓋 202を閉じ、 真空ポンプ 253を作動させ るとともにエアー駆動弁 2 5 1、 2 52を開く。 すると、 真空容器 2 0 1内の空 気が、 真空排気□ 20 1 aから真空排気配管 2 50を経て真空ポンプ 253へ吸 引されて真空引きが開始され、 加熱容器 205の上室 20 5 b内の空気が、 排気 □ 205 dから真空排気配管 250を経て真空ポンプ 2 5 3へ吸引されて減圧が 開始される。 また、 加熱容器 205の下室 20 5 cのヒー夕 207を作動させて、 上室 205 bに収容している溶液 2 06を加熱する。  The operation of the drying apparatus having such a configuration and the state during the operation will be described below. As shown in FIG. 11, a packet 204 containing the material 203 to be dried is housed in a vacuum vessel 201, the lid 202 is closed, the vacuum pump 253 is operated, and the air-driven valve 25 1 Open 2 52. Then, the air in the vacuum vessel 201 is sucked from the vacuum exhaust □ 201 a through the vacuum exhaust pipe 250 to the vacuum pump 253 to start vacuuming, and the upper chamber 205 b of the heating vessel 205 is started. The inside air is sucked from the exhaust □ 205 d to the vacuum pump 253 via the vacuum exhaust pipe 250, and the decompression is started. In addition, the heater 207 in the lower chamber 205c of the heating vessel 205 is operated to heat the solution 206 contained in the upper chamber 205b.
その後、 真空容器 20 1内の圧力、 加熱容器 205の上室 205 b内の圧力、 及び、 溶液 206の温度が所定値になった時点で、 連通配管 209のエア一駆動 弁 2 1 0を開く。 すると、 第 1 2図に示されるように、 溶液 206は、 連通配管 209の下端 209 bから上端 209 aに急激に吸い上げられ、 沸騰状態で上方 に噴射され、 真空容器 20 1内の温度を急上昇させるとともに、 バスケッ ト 20 4内にある被乾燥物 203に熱を与え、 被乾燥物 203を急速に加熱する。 ここ で、 被乾燥物 203に熱を与えた溶液 206は、 ェンタルピを失って落下し、 真 空容器 20 1の底面に溜まっていく 力 連通配管 209の上端 209 aから噴射 される溶液 206にとつて、 ァクティ ブなバプリ ング効果も有する噴射が維持さ れ、 実質的な障害とはならない。 ただし、 ある程度の量を超えると、 悪影響が生 じるため、 液位センサ 2 33により この量を検知するよう になっている。 Then, the pressure in the vacuum vessel 201, the pressure in the upper chamber 205b of the heating vessel 205, When the temperature of the solution 206 reaches a predetermined value, the air-driven valve 210 of the communication pipe 209 is opened. Then, as shown in FIG. 12, the solution 206 is rapidly sucked from the lower end 209 b of the communication pipe 209 to the upper end 209 a and is jetted upward in a boiling state, so that the temperature in the vacuum vessel 201 rises rapidly. At the same time, heat is applied to the object 203 in the basket 204 to rapidly heat the object 203. Here, the solution 206 that has given heat to the material 203 to be dried loses enthalpy and falls, and accumulates on the bottom surface of the vacuum container 201.The solution 206 is injected into the solution 206 injected from the upper end 209a of the communication pipe 209. Therefore, the injection which also has an active bubbling effect is maintained and does not cause any substantial obstacle. However, if the amount exceeds a certain amount, an adverse effect occurs. Therefore, the liquid level sensor 233 detects this amount.
次いで、 被乾燥物 20 3の品温が 80〜 1 00 °C程度になるような所定時間が 経過した後、 被乾燥物 2 03の加熱が完了し乾燥に移行する。 ここで、 真空容器 20 1の底面に溜まつている溶液 206は乾燥にとって悪影響を及ぼすので、 乾 燥に移行する際に、 真空容器 20 1から排出しておく必要がある。 そこで、 本実 施形態の乾燥装置では、 真空排気配管 250に設けられたエアー駆動弁 2 52を 更に開き、 加熱容器 20 5の上室 205 b内を減圧していく。 すると、 連通配管 209の上端 209 aからの溶液 206の噴射は徐々に低下していき、 加熱容器 205の上室 205 b内の圧力が真空容器 20 1 内の圧力と同等になると、 真空 容器 20 1の底面に溜ま っている溶液 206は、 自重で加熱容器 20 5の上室 2 05 b内に引き戻され、 真空容器 20 1からの排出がなされる。 なお、 この排出 時間を短縮するためには、 真空容器 20 1の真空引きを停止させることが有効で あり、 エアー駆動弁 25 1を一時的に閉じてもよい。  Next, after a lapse of a predetermined time such that the temperature of the object to be dried 203 becomes about 80 to 100 ° C., the heating of the object to be dried 203 is completed, and the process proceeds to drying. Here, the solution 206 accumulated on the bottom surface of the vacuum vessel 201 has an adverse effect on drying, and therefore, it is necessary to discharge the solution 206 from the vacuum vessel 201 before the drying is started. Therefore, in the drying apparatus of the present embodiment, the air drive valve 252 provided in the vacuum exhaust pipe 250 is further opened to reduce the pressure in the upper chamber 205b of the heating vessel 205. Then, the injection of the solution 206 from the upper end 209 a of the communication pipe 209 gradually decreases, and when the pressure in the upper chamber 205 b of the heating vessel 205 becomes equal to the pressure in the vacuum vessel 201, the vacuum vessel 20 The solution 206 stored on the bottom surface of 1 is drawn back into the upper chamber 205 b of the heating vessel 205 by its own weight, and is discharged from the vacuum vessel 201. In order to shorten the discharge time, it is effective to stop the evacuation of the vacuum vessel 201, and the air drive valve 251 may be temporarily closed.
そして、 真空容器 20 1の底面に溜まっている溶液 206の排出がなされた後、 連通配管 209のエアー駆動弁 2 1 0を閉じ、 真空容器 20 1の真空引きを継続 すると、 加温された被乾燥物 203に付着している洗浄液 (例えば、 上記の洗浄 装置を用いて洗浄がなされた場合の洗浄液 5 ) や溶液 206は、 被乾燥物 203 から蒸発潜熱を奪いながら蒸発し、 乾燥が行われる。 なお、 加熟容器 20 5の上 室 205 bは常に負圧環境におかれていることはいうまでもない。  After the solution 206 remaining on the bottom surface of the vacuum vessel 201 is discharged, the air drive valve 210 of the communication pipe 209 is closed, and the evacuation of the vacuum vessel 201 is continued. The cleaning liquid adhering to the dried material 203 (for example, the cleaning liquid 5 when the cleaning is performed using the above-described cleaning apparatus) and the solution 206 evaporate while removing latent heat of evaporation from the material 203 to be dried, and are dried. . Needless to say, the upper chamber 205b of the ripening vessel 205 is always in a negative pressure environment.
乾燥が完了すると、 真空排気配管 2 50のエアー駆動弁 2 5 1 を閉じる。 次い で、 ベン ト用ガス配管 2 6 1のエアー駆動弁 2 62又は 2 66を開き、 ガスボン ベ 264中のガス又は空気 267を真空容器 20 1の吸気ロ 20 1 bから導入し、 真空容器 20 1 内の圧力を常圧に戻す。 そして、 蓋 202を開き、 乾燥した被乾 燥物 203を入れたバスケッ ト 204を真空容器 20 1から取り出して、 終了す る。 When the drying is completed, the air drive valve 25 1 of the vacuum exhaust pipe 250 is closed. Next Then, the air drive valve 262 or 266 of the vent gas pipe 26 1 is opened, and the gas or air 267 in the gas cylinder 264 is introduced from the suction vent 201 b of the vacuum vessel 201, and the vacuum vessel 201 The internal pressure is returned to normal pressure. Then, the lid 202 is opened, the basket 204 containing the dried material to be dried 203 is taken out of the vacuum vessel 201, and the process is completed.
なお、 被乾燥物 203の加熱や乾燥中、 真空容器 20 1 内に存する気化した洗 浄液ゃ溶液 206は、 真空排気ロ 2 0 1 aから真空排気配管 250を経て真空ポ ンプ 2 53へ吸引され、 セパレー夕 2 54や蒸留部を経由して浄化された後、 フ ィルタ 2 56やエアー駆動弁 257が経路に設けられた給液配管 25 5を介して, 供液口 205 eから加熱容器 205の上室 20 5 bに投入される。 この投入は、 真空ポンプ 2 53による負圧力を利用するので専用のポンプを設けなく ともエア 一駆動弁 25 7の開閉動作のみで行え、 また、 このエアー駆動弁 25 7は、 液位 センサ 243からの出力により作動するようになっている。  During the heating and drying of the object 203 to be dried, the vaporized cleaning solution / solution 206 present in the vacuum vessel 201 is sucked from the vacuum pump 201 a to the vacuum pump 253 via the vacuum pump pipe 250. After being purified through the separator 254 and the distillation section, it is filtered from the liquid supply port 205 e via the liquid supply port 205 e via the filter pipe 256 and the air drive valve 257 through the liquid supply pipe 255. It is thrown into the upper room 205 b of 205. This injection uses the negative pressure of the vacuum pump 253, so it can be performed only by opening and closing the air drive valve 257 without providing a dedicated pump. It operates according to the output of.
ここで、 真空ポンプ 2 53としては、 往復式、 液封式、 回転式等の真空ポンプ が挙げられるが、 本実施形態の乾燥装置では、 以下の理由から、 液封式の真空ポ ンプを採用している。 真空容器 20 1内で気化した洗浄液や溶液 206が吸入さ れても、 液体を隔ててポンプ回転部と接触するようになっているので、 通常のシ ール方式の真空ポンプとは異なり金属摺動面摩擦による火花や熱の発生が少なく 安全性に富み、 支障もないからである。  Here, the vacuum pump 253 may be a reciprocating type, a liquid ring type, a rotary type, or the like, but the drying device of the present embodiment employs a liquid ring type vacuum pump for the following reasons. are doing. Even if the cleaning liquid or solution 206 vaporized in the vacuum vessel 201 is sucked in, the liquid comes into contact with the pump rotating part via the liquid, so that unlike a normal seal-type vacuum pump, a metal slide is used. This is because sparks and heat generated by moving surface friction are small, and the safety is high and there is no problem.
また、 真空容器 20 1の底面に溜まっている溶液 206を再度被乾燥物 203 の加熱に利用する目的で、 本実施形態の乾燥装置では、 真空容器 20 1の底面に ヒー夕 22 1 を設けている。 真空容器 20 1の底面に溜まっている溶液 206は, ヒータ 22 1 によって加熱、 蒸気化され、 真空容器 20 1 内に向かって拡散し、 被乾燥物 203に再度熱を与える。 発明者らの実験においては、 20〜25%の 乾燥時間の短縮が図れ、 この効果は極めて有効である。 更に、 真空容器 20 1内 の温度をより急速に高めるために、 真空容器 20 1の内側面にヒータ 222が設 けられている。 一般に、 真空容器 2 0 1の側面は熱容量が大きいため昇温し難く, 真空容器 20 1内に存する蒸気化した溶液 206がこの側面に接触、 凝縮して残 存すると、 乾燥を阻害してしまうおそれがあるが、 このヒータ 222の設置によ り改善が見込まれ、 発明者らの実験においては、 5 %程度の乾燥時間の短縮が図 れた。 Further, in order to utilize the solution 206 accumulated on the bottom surface of the vacuum vessel 201 again for heating the material 203 to be dried, the drying apparatus of the present embodiment is provided with a heater 22 1 on the bottom face of the vacuum vessel 201. I have. The solution 206 stored on the bottom surface of the vacuum vessel 201 is heated and vaporized by the heater 22 1, diffuses into the vacuum vessel 201, and gives heat again to the object 203 to be dried. In the experiments of the inventors, the drying time can be reduced by 20 to 25%, and this effect is extremely effective. Further, a heater 222 is provided on the inner surface of the vacuum vessel 201 in order to raise the temperature inside the vacuum vessel 201 more rapidly. Generally, the side surface of the vacuum vessel 201 has a large heat capacity, so it is difficult to raise the temperature. If the vaporized solution 206 in the vacuum vessel 201 comes into contact with this side face and condenses, the drying will be hindered. There is a possibility that the installation of this heater 222 The drying time was reduced by about 5% in our experiments.
また、 連通配管 2 0 9に設けられているエアー駆動弁 2 1 0は、 真空容器 2 0 1の圧力センサ 2 3 1 と、 加熱容器 2 0 5の圧力センサ 2 4 1 と温度センサ 2 4 2から出力される値に基づき、 開閉度合いが自動的に調節されるよう になってい る。 従って、 被乾燥物 2 0 3に向けて噴射された沸騰状態の溶液 2 0 6の状態、 及び、 被乾燥物 2 0 3の品温状態を常に適正状態に安定化させることができる。 もちろん、 このような開閉度合いの調節機構を備えずに、 エアー駆動弁 2 1 0を 開いた状態に維持させて溶液 2 0 6を常時噴射しても構わないが、 特に、 複雑な 形状の被乾燥物 2 0 3の場合、 例えば、 溶液 2 0 6を間欠噴射させるような調節 機構を備えると、 噴射が急激に立ち上がったり立ち下がったりする作用によって, 溶液 2 0 6が噴射される有効な領域が拡大し、 常時噴射では到達が困難な部位に も容易に到達できるので、 この調節機構は極めて有効といえる。  The air-driven valve 210 provided in the communication pipe 209 includes a pressure sensor 231 of the vacuum vessel 201, a pressure sensor 241 of the heating vessel 205, and a temperature sensor 242. The degree of opening and closing is automatically adjusted based on the value output from the. Therefore, the state of the boiling solution 206 which is sprayed toward the object to be dried 203 and the state of the temperature of the object to be dried 203 can always be stabilized to an appropriate state. Of course, without providing such a mechanism for adjusting the degree of opening and closing, the air-driven valve 210 may be kept open and the solution 206 may be constantly jetted, but in particular, a complicated shaped cover may be used. In the case of dry matter 203, for example, if an adjustment mechanism that intermittently sprays the solution 206 is provided, the effective area where the solution 206 is sprayed by the action that the spray rapidly rises and falls This adjustment mechanism can be said to be extremely effective because it can easily reach areas that are difficult to reach by continuous injection.
次に、 本発明の第 7実施形態の乾燥装置について、 第 1 3図を参照しながら説 明する。 第 1 3図は第 7実施形態の乾燥装置における乾燥部の要部断面図が示さ れている。 なお、 図中で第 6実施形態の乾燥装置と同じ名称で同じ機能を果たす 部分には同一の符号を付し、 重複する説明は省略し、 相違する点について述べる ( 先ず、 本実施形態の乾燥装置の目的について触れておく。 一般的に、 洗浄が行 われた被乾燥物は、 汚れや付着物である異物が完全に除去されている訳ではない ( 被乾燥物である部品の形状や大きさ、 或いは、 汚染の程度にもよるが、 仮に、 汚 れゃ異物の付着重量を 1 0 0 とした指標で表すと、 洗浄によって 7 0〜 8 0程度 の汚れや異物を除去できればよいとされ、 りの 2 0〜 3 0程度の汚れや異物は, 被乾燥物に残存して乾燥装置に持ち込まれてしまうことになる。 つま り、 この持 ち込まれる汚れや異物は、 1 つの被乾燥物に対しては微量であっても、 幾つもの 被乾燥物に対しては決して無視できず、 繰り返し乾燥が行われるにつれ、 特に、 被乾燥物を加熱する溶液に混入して蓄積され、 最終的に乾燥後の被乾燥物の表面 に残存し外観品位の低下につながることになる。 そこで、 本実施形態の乾燥装置 では、 このような問題の解決を図っている。 Next, a drying apparatus according to a seventh embodiment of the present invention will be described with reference to FIG. FIG. 13 is a sectional view of a main part of a drying unit in the drying apparatus according to the seventh embodiment. Note that the 6 denoted by the same reference numerals perform the same functions with the same name as the drying device of the embodiment in the figure, and duplicate explanations are omitted describes points different (first, drying of the embodiment In general, the object to be dried after cleaning is not completely free of dirt and foreign matters such as adherents (the shape and size of the parts to be dried). Or, depending on the degree of contamination, if it is expressed as an index with the adhesion weight of dirt and foreign matter being 100, it is sufficient if about 70 to 80 dirt or foreign matter can be removed by washing. On the other hand, about 20 to 30 pieces of dirt and foreign matter remain on the material to be dried and are brought into the drying device. A small amount for objects, but for several objects to be dried In particular, as the material is repeatedly dried, it is accumulated in the solution that heats the object to be dried and accumulates, and finally remains on the surface of the object to be dried after drying, leading to a deterioration in appearance quality. Therefore, the drying device of the present embodiment is intended to solve such a problem.
本実施形態の乾燥装置では、 真空容器 2 0 1 の内側面に凝縮コィル 2 7 1が設 けられ、 その凝縮コイル 27 1の内側に円筒状の隔壁 2 7 2が備えられている。 隔壁 272の下部は樋状部分 272 aが形成され、 その樋状部分 272 aの近傍 に真空排気口 20 1 aが形成されている。 また、 加熱容器 205は、 隔壁 205 gで右室 20 5 hと左室 205 i に分割されており、 右室 205 hには、 ヒータ 207が設けられ、 このヒータ 20 7によつて直接的加熱される溶液 206が収 容されている。 もちろん、 加熱媒体を介して間接的に加熱するようにしても構わ ない。 なお、 右室 205 hには排気□ 205 d、 供液口 205 e、 及び、 排出口 205 f が形成され、 温度センサ 242、 過昇温防止スィ ッチ 246、 及び、 液 位センサ 24 3が設けられている。 真空容器 20 1 と加熱容器 205の右室 20 5 hを連通する連通配管 209は、 上端 209 aが真空容器 20 1の底面を貫通 して真空容器 20 1の内部に開口し、 下端 209 bが溶液 206に浸漬している ( 一方、 左室 205 iは、 後述する真空容器 20 1の底面に溜まった溶液 206 が回収される回収タンクの役割を果たし、 回収配管 2 1 1で真空容器 20 1 と連 通しており、 その回収配管 2 1 1の上端 2 1 1 aは真空容器 20 1の底面に開口 し、 下端 2 1 l bは左室 20 5 iの上面に開口している。 なお、 左室 205 i に は排気口 20 5 j 及び排出口 205 kが形成され、 液位センサ 247が設けられ ている。 In the drying device of the present embodiment, a condensing coil 271 is provided on the inner surface of the vacuum vessel 201. The inside of the condensation coil 27 1 is provided with a cylindrical partition wall 27 2. A gutter-like portion 272a is formed at the lower portion of the partition 272, and a vacuum exhaust port 201a is formed near the gutter-like portion 272a. The heating vessel 205 is divided into a right chamber 205 h and a left chamber 205 i by a partition wall 205 g, and a heater 207 is provided in the right chamber 205 h, and the heater 207 is directly heated by the heater 207. The solution 206 to be removed is stored. Of course, heating may be performed indirectly via a heating medium. The right chamber 205 h is provided with an exhaust □ 205 d, a liquid supply port 205 e, and a discharge port 205 f, and a temperature sensor 242, an overheating prevention switch 246, and a liquid level sensor 243. Is provided. The upper end 209a of the communication pipe 209 that communicates the vacuum chamber 201 with the right chamber 205h of the heating vessel 205 passes through the bottom of the vacuum vessel 201 and opens inside the vacuum vessel 201, and the lower end 209b has the lower end 209b. The left chamber 205 i is immersed in the solution 206 ( while the left chamber 205 i serves as a collection tank for collecting the solution 206 collected on the bottom surface of the vacuum vessel 201, which will be described later). The upper end 2 1 1a of the collection pipe 2 1 1 is open to the bottom of the vacuum vessel 201, and the lower end 2 1 lb is open to the upper surface of the left chamber 205 i. An exhaust port 205 j and an exhaust port 205 k are formed in the chamber 205 i, and a liquid level sensor 247 is provided.
このような構成における乾燥装置の特筆すべき動作について以下に述べる。 第 The remarkable operation of the drying apparatus having such a configuration will be described below. No.
1 に、 被乾燥物 203の加熱や乾燥中、 真空容器 20 1内に存する気化した洗浄 液や溶液 206は、 真空排気□ 20 1 aからの吸引力により、 真空容器 20 1の 側壁と隔壁 2 72との隙間を上方から通過し、 凝縮コイル 27 1 によって冷却さ れて液化する。 その液化した溶液 2 06は、 樋状部分 27 2 aに集ま り、 真空排 気口 20 1 aから真空排気配管 2 5 0を経てェジ Xクタ 2 57等を介し真空ボン プ 253へ吸引され、 セパレ一タ 2 54を経由 して浄化された後、 フ ィルタ 25First, during heating and drying of the object 203 to be dried, the vaporized cleaning liquid and the solution 206 existing in the vacuum vessel 201 are sucked from the vacuum exhaust 201 a by the suction force from the side wall and the partition wall 2 of the vacuum vessel 201. It passes through the gap with 72 and is cooled by the condensation coil 27 1 and liquefied. The liquefied solution 206 collects in the gutter-like portion 27 2 a, and is sucked from the vacuum exhaust port 201 a through the vacuum exhaust pipe 250 to the vacuum pump 253 via the edge X kuta 257 and the like. After being purified and passed through the separator 254, the filter 25
6やエア一駆動弁 257が経路に設けられた給液配管 25 5を介して、 供液□ 26 and the air-driven valve 257 are supplied via the liquid supply pipe 25
05 eから加熱容器 205の右室 2 05 hに投入される。 From 05e, it is thrown into the right chamber 205h of the heating vessel 205.
第 2に、 真空容器 20 1の底面に溜まった溶液 206は、 第 6実施形態の乾燥 装置のように、 連通配管 209を通じて引き戻されるのではなく 、 回収配管 2 1 Second, the solution 206 collected on the bottom surface of the vacuum vessel 201 is not drawn back through the communication pipe 209 as in the drying device of the sixth embodiment, but is collected by the collection pipe 21.
1を通じて回収タンクである左室 2 05 i に回収される。 これは、 排気口 205 j から真空ポンプ 2 5 3へ通じる真空排気配管 2 5 0に設けられたエアー駆動弁 2 5 6、 2 5 8を開き、 左室 2 0 5 i 内を減圧していく こ とにより達成できる。 従って、 真空容器 2 0 1 の底面に溜まった溶液 2 0 6は、 洗浄後に被乾燥物 2 0 3に残存している汚れ、 異物、 油脂等が混入しているが、 個別の回収タンク (左 室 2 0 5 i ) に回収されることによ り、 右室 2 0 5 hにある溶液 2 0 6は常に汚 染されていない浄化された新液状態に維持され、 例え繰り返し乾燥が行われたと しても、 乾燥後の被乾燥物の外観品位を損なう ことは全く ない。 It is collected in the left chamber 2005 i, which is a collection tank, through 1. This is an exhaust 205 This can be achieved by opening the air drive valves 256, 258 provided in the vacuum exhaust pipe 250 connected to the vacuum pump 253 from j, and reducing the pressure in the left chamber 205i. Therefore, the solution 206 collected on the bottom of the vacuum vessel 201 contains dirt, foreign matter, oil, etc. remaining on the object 203 after washing, but the individual collection tank (left) The solution 206 in the right chamber 205 h is always kept in a clean, uncontaminated, fresh liquid state by being collected in the chamber 205 i), and is repeatedly dried, for example. Even if it does not impair the appearance of the object to be dried after drying.
なお、 本発明は上記第 1 〜 7実施形態に限定される訳ではなく、 本発明の趣旨 を逸脱しない範囲で、 種々の変更が可能である。 例えば、 第 1〜 5実施形態であ る洗浄装置においては、 超音波振動子ュニッ ト 7を洗浄槽 6の貯槽部 6 aの内部 に備え (投げ込み式) 、 その超音波振動子ュニッ ト 7の排気口 1 0 b に通ずる逆 止弁 1 1 を洗浄槽 6に貫通させて真空容器 1 内に開放させてもよい。 また、 振動 板 8は、 中央部 8 aが周縁部 8 b に対して隆起していないフラッ ト状であっても 構わない。  Note that the present invention is not limited to the first to seventh embodiments, and various changes can be made without departing from the spirit of the present invention. For example, in the cleaning apparatus according to the first to fifth embodiments, the ultrasonic vibrator unit 7 is provided inside the storage tank portion 6a of the cleaning tank 6 (throw-in type), and the ultrasonic vibrator unit 7 The check valve 11 connected to the exhaust port 10 b may be penetrated through the cleaning tank 6 and opened into the vacuum vessel 1. Further, diaphragm 8 may have a flat shape in which central portion 8a is not raised with respect to peripheral portion 8b.
他方、 第 6、 7実施形態である乾燥装置においては、 溶液 2 0 6 と して、 炭化 水素系の溶液の代わりに非燃性の水を適用しても構わないが、 乾燥性を考慮する と蒸発潜熱が水に対して 1 Z 1 0程度と格段に低い炭化水素系の溶液を適用する のが好ま しい。 また、 乾燥装置には洗浄工程を含んでいても構わず、 この際、 乾 燥前の洗浄に用いる洗浄液と乾燥工程に用いる溶液 2 0 6 とは、 同種であること が望ましい。 更に、 真空容器 2 0 1 の底面に設けられるヒータ 2 2 1 は、 その真 空容器 2 0 1 の底面に溜まっている溶液 2 0 6を加熱、 蒸気化することができる 限り、 真空容器の底面を覆うジャケ ッ トタイプのヒー夕であってもよい。  On the other hand, in the drying apparatuses according to the sixth and seventh embodiments, non-flammable water may be used as the solution 206 instead of the hydrocarbon-based solution, but the drying property is taken into consideration. It is preferable to use a hydrocarbon-based solution whose latent heat of vaporization is as low as about 1Z10 with respect to water. In addition, the drying apparatus may include a cleaning step. In this case, it is preferable that the cleaning liquid used for cleaning before drying and the solution 206 used for the drying step are of the same type. Furthermore, the heater 221 provided on the bottom surface of the vacuum vessel 201 can be used to heat and vaporize the solution 206 stored on the bottom face of the vacuum vessel 201 as long as it can be vaporized. It may be a jacket-type heater that covers the area.
勿論、 上記実施形態の洗浄装置と乾燥装置とを適宜組み合わせることも可能で あり、 この場合、 洗浄から乾燥までを効率よく かつ安全に行えるので極めて有益 である。 産業上の利用の可能性  Of course, the cleaning device and the drying device of the above embodiment can be appropriately combined, and in this case, the process from cleaning to drying can be performed efficiently and safely, which is extremely useful. Industrial applicability
本発明の洗浄装置及び洗浄方法は、 電子、 機械、 成形関連等の部品の洗浄や乾 燥に対して有用である。 '  INDUSTRIAL APPLICABILITY The cleaning apparatus and the cleaning method of the present invention are useful for cleaning and drying of electronic, mechanical, and molding-related parts. '

Claims

請求の範囲 The scope of the claims
1 . 真空下におかれた洗浄液に超音波振動を与えて、 前記洗浄液に浸潰した 被洗浄物を洗浄する洗浄装置において、 1. In a cleaning apparatus for applying an ultrasonic vibration to a cleaning liquid placed under vacuum to wash an object to be cleaned immersed in the cleaning liquid,
前記洗浄液を貯留し前記被洗浄物を収容する洗浄槽と、 内部に所定空間を有し 前記洗浄液に超音波振動を与える振動体とを、 真空状態を取り得る洗浄用真空容 器内に備え、 前記振動体の所定空間が前記洗浄用真空容器内に開口していること を特徴とする洗浄装置。  A cleaning tank that stores the cleaning liquid and stores the object to be cleaned, and a vibrator that has a predetermined space therein and applies ultrasonic vibration to the cleaning liquid is provided in a cleaning vacuum container that can take a vacuum state, A cleaning device, wherein a predetermined space of the vibrator is opened in the cleaning vacuum container.
2 . 請求の範囲 1 に記載の洗浄装置において、  2. The cleaning device according to claim 1,
前記振動体の所定空間をパージするためのパージガスを前記所定空間に供給す るパージガス供給手段を備える。  Purge gas supply means for supplying a purge gas for purging a predetermined space of the vibrating body to the predetermined space is provided.
3 . 請求の範囲 1又は 2に記載の洗浄装置において、  3. The cleaning device according to claim 1 or 2,
超音波振動が伝播する振動板と、 この振動板上に取り付けられたカバーとによ り形成された前記所定空間に、 超音波振動を発する振動子が設けられていて、 前記洗浄槽の底壁又は側壁に形成された開口を閉塞するように、 前記振動板が 前記所定空間を前記洗浄槽の外側に向けて配置されるとと もに、 前記振動板の周 縁部から前記洗浄槽の底壁又は側壁を貫通する貫通穴にボルトを揷通して固定さ れており、 前記カバーが前記振動板上の前記貫通穴よりも中央側で取り付けられ ている。  A vibrator that emits ultrasonic vibration is provided in the predetermined space formed by a vibration plate through which ultrasonic vibration propagates and a cover attached to the vibration plate, and a bottom wall of the cleaning tank is provided. Alternatively, the diaphragm is arranged so that the predetermined space faces the outside of the cleaning tank so as to close an opening formed in a side wall, and a bottom of the cleaning tank is arranged from a peripheral portion of the diaphragm. A bolt is passed through a through hole that penetrates a wall or a side wall, and the cover is attached to the diaphragm closer to the center than the through hole on the diaphragm.
4 . 請求の範囲 3に記載の洗浄装置において、  4. The cleaning device according to claim 3,
前記振動板の中央部が前記貫通穴を有する周縁部より も前記洗浄槽に対して陥 没しており、 前記カバーが前記振動板の前記中央部上に取り付けられている。  A central portion of the diaphragm is depressed with respect to the cleaning tank from a peripheral portion having the through hole, and the cover is mounted on the central portion of the diaphragm.
5 . 請求の範囲 1、 2又は 4のいずれかに記載の洗浄装置において、 前記洗浄槽の側壁上端部が外側下方に向けて折り曲げられている。  5. The cleaning apparatus according to any one of claims 1, 2 and 4, wherein an upper end portion of a side wall of the cleaning tank is bent outward and downward.
6 . 請求の範囲 1、 2又は 4のいずれかに記載の洗浄装置において、 前記洗浄槽の側壁下端部が底壁より下方に突出している。  6. The cleaning apparatus according to any one of claims 1, 2 and 4, wherein a lower end portion of a side wall of the cleaning tank projects below a bottom wall.
7 . 請求の範囲 6に記載の洗浄装置において、  7. The cleaning device according to claim 6, wherein
前記洗浄槽の側壁下端部の縁が凹凸状である。  The edge of the lower end of the side wall of the cleaning tank is uneven.
8 . 請求の範囲 6に記載の洗浄装置において、 前記洗浄槽の側壁下端部の縁が水平面に対して傾斜している。 8. The cleaning device according to claim 6, wherein The edge of the lower end of the side wall of the cleaning tank is inclined with respect to the horizontal plane.
9 . 洗浄液を貯留し被洗浄物を収容する洗浄槽と、 内部に所定空間を有し前 記洗浄液に超音波振動を与える振動体とを、 真空状態を取り得る洗浄用真空容器 内に備え、 前記振動体の所定空間が前記洗浄用真空容器内に開口しており、 真空 下におかれた前記洗浄液に超音波振動を与えて、 この洗浄液に浸潰した前記被洗 浄物を洗浄する洗浄手段と、  9. A cleaning tank that stores a cleaning liquid and stores an object to be cleaned, and a vibrator that has a predetermined space therein and applies ultrasonic vibration to the cleaning liquid are provided in a cleaning vacuum container that can take a vacuum state, A predetermined space of the vibrator is opened in the cleaning vacuum vessel, and the cleaning liquid placed under vacuum is subjected to ultrasonic vibration to wash the object to be cleaned immersed in the cleaning liquid. Means,
この洗浄手段で洗浄された前記被洗浄物を被乾燥物と して収容し真空状態を取 り得る乾燥用真空容器と、 加熱された溶液を収容する加熱容器と、 前記乾燥用真 空容器と前記加熱容器を連通する配管と、 を備え、 前記配管の一端は前記被乾燥 物に向けて開口し、 前記配管の他端は前記溶液に浸漬しており、 前記乾燥用真空 容器が真空状態のときに前記配管が開放されて、 前記溶液が沸騰状態で前記配管 の前記一端から前記被乾燥物に向けて噴射され、 この被乾燥物を乾燥させる乾燥 手段と、  A vacuum container for drying capable of holding the object to be cleaned, which has been washed by the cleaning means, as a material to be dried and capable of maintaining a vacuum state; a heating container for storing a heated solution; and a vacuum container for drying. A pipe communicating with the heating vessel, one end of the pipe is opened toward the object to be dried, the other end of the pipe is immersed in the solution, and the drying vacuum vessel is in a vacuum state. When the pipe is opened, the solution is sprayed from the one end of the pipe toward the object to be dried in a boiling state, and drying means for drying the object to be dried.
よりなることを特徴とする洗浄装置。  A cleaning device, comprising:
1 0 . 請求の範囲 9 に記載の洗浄装置において、  10. The cleaning apparatus according to claim 9, wherein
前記溶液は炭化水素系の溶液である。  The solution is a hydrocarbon-based solution.
1 1 . 請求の範囲 9又は 1 0に記載の洗浄装置において、  11. The cleaning device according to claim 9 or 10, wherein
前記加熱容器は隔壁で 2室に分割されていて、 一方に前記溶液を収容し、 他方 に熱源を設けており、  The heating container is divided into two chambers by a partition, one of which contains the solution, and the other of which is provided with a heat source,
前記熱源からの熱が前記隔壁を通じて前記溶液に与えられ、 前記溶液が加熱さ れる。  Heat from the heat source is applied to the solution through the partition, and the solution is heated.
1 2 . 請求の範囲 9又は 1 0に記載の洗浄装置において、  1 2. The cleaning device according to claim 9 or 10,
前記配管の経路に駆動弁が設けられており、  A drive valve is provided in the path of the pipe,
前記乾燥用真空容器内の圧力と、 前記溶液が収容されている前記加熱容器内の 圧力と、 前記溶液の温度とに基づき、 前記駆動弁の開閉度合いが調節される。  The degree of opening and closing of the drive valve is adjusted based on the pressure in the drying vacuum vessel, the pressure in the heating vessel containing the solution, and the temperature of the solution.
1 3 . 請求の範囲 9又は 1 0に記載の洗浄装置において、  13. The cleaning device according to claim 9 or 10, wherein
前記乾燥用真空容器の内側面と底面とのうち、 少なく とも 1つに加熱手段を設 ける。  A heating means is provided on at least one of the inner side surface and the bottom surface of the drying vacuum container.
1 4 . 請求の範囲 9又は 1 0に記載の洗浄装置において、 前記被乾燥物に向けて噴射されて前記乾燥用真空容器内に存する蒸気化した前 記溶液を回収し凝縮させる溶液凝縮手段と、 前記溶液凝縮手段により凝縮した前 記溶液を前記加熱容器に供給する供給手段とを備える。 14. The cleaning device according to claim 9 or 10, A solution condensing unit that collects and condenses the vaporized solution that is sprayed toward the object to be dried and that is present in the drying vacuum container, and supplies the solution condensed by the solution condensing unit to the heating container. Supply means.
1 5 . 請求の範囲 1 4に記載の洗浄装置において、  15. The cleaning device according to claim 14, wherein
更に、 前記被乾燥物に向けて噴射されて前記乾燥用真空容器の底面に溜まつた 前記溶液を回収して排出する溶液排出手段を備える。  Further, a solution discharging means is provided for collecting and discharging the solution sprayed toward the object to be dried and collected on the bottom surface of the drying vacuum container.
1 6 . 洗浄液を貯留し被洗浄物を収容する洗浄槽と、 内部に所定空間を有し 前記洗浄液に超音波振動を与える振動体とを、 真空状態を取り得る洗浄用真空容 器内に備え、 前記振動体の所定空間が前記洗浄用真空容器内に開口しており、 真 空下におかれた前記洗浄液に超音波振動を与えて、 この洗浄液に浸潰した前記被 洗浄物を洗浄する洗浄工程と、  16. A cleaning tank that stores a cleaning liquid and stores an object to be cleaned and a vibrator that has a predetermined space therein and applies ultrasonic vibration to the cleaning liquid are provided in a cleaning vacuum container that can take a vacuum state. A predetermined space of the vibrating body is opened in the cleaning vacuum vessel, and the cleaning liquid placed in a vacuum is subjected to ultrasonic vibration to clean the cleaning object immersed in the cleaning liquid. A washing step;
この洗浄工程を経た前記被洗浄物を被乾燥物と して収容し真空状態を取り得る 乾燥用真空容器と、 加熱された溶液を収容する加熱容器と、 前記乾燥用真空容器 と前記加熱容器を連通する配管と、 を備え、 前記配管の一端は前記被乾燥物に向 けて開口し、 前記配管の他端は前記溶液に浸潰しており、 前記乾燥用真空容器が 真空状態のときに前記配管が開放されて、 前記溶液が沸騰状態で前記配管の前記 一端から前記被乾燥物に向けて噴射され、 この被乾燥物を乾燥させる乾燥工程と. よ りなることを特徴とする洗浄方法。  A vacuum container for drying capable of holding the object to be cleaned having undergone the washing process as an object to be dried and taking a vacuum state; a heating container for storing a heated solution; a vacuum container for drying; and the heating container. One end of the pipe is opened toward the object to be dried, the other end of the pipe is immersed in the solution, and the drying vacuum vessel is in a vacuum state. A cleaning step, wherein the pipe is opened, and the solution is sprayed in a boiling state from the one end of the pipe toward the object to be dried, and the object to be dried is dried.
PCT/JP2002/007137 2001-07-13 2002-07-12 Washing device and washing method WO2003006184A1 (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2001-213459 2001-07-13
JP2001213459A JP3818876B2 (en) 2001-07-13 2001-07-13 Drying equipment
JP2001-229400 2001-07-30
JP2001229400A JP2003039029A (en) 2001-07-30 2001-07-30 Cleaning device

Publications (1)

Publication Number Publication Date
WO2003006184A1 true WO2003006184A1 (en) 2003-01-23

Family

ID=26618683

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2002/007137 WO2003006184A1 (en) 2001-07-13 2002-07-12 Washing device and washing method

Country Status (2)

Country Link
CN (1) CN1527749A (en)
WO (1) WO2003006184A1 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003084576A1 (en) * 2002-04-04 2003-10-16 Sharp Kabushiki Kaisha Vacuum ultrasonic cleaning and dezymotizing device
CN103769379A (en) * 2014-01-04 2014-05-07 福建奇妙电子科技有限公司 Manufacturing method of household water mist spraying equipment
CN114535210A (en) * 2022-02-25 2022-05-27 天津市成吉斯宾科技发展有限公司 Ultrasonic vacuum surface treatment cleaning method

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101810458B (en) * 2010-04-20 2012-09-19 姚建梁 Ultrasonic vacuum negative pressure cleaning device
CN102698977A (en) * 2011-03-28 2012-10-03 东莞新科技术研究开发有限公司 Vacuum cleaning device
JP5542749B2 (en) * 2011-06-30 2014-07-09 株式会社日立ハイテクノロジーズ Sample preparation apparatus, preparation method, and charged particle beam apparatus using the same
CN108049942B (en) * 2017-11-03 2020-11-17 宁波行泰环保科技有限公司 DPF cleaning method based on ultrasonic cleaning
CN114236298B (en) * 2022-02-24 2022-05-20 山东掌电电力科技有限公司 Power equipment on-line measuring device based on internet

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6310531A (en) * 1986-07-02 1988-01-18 Matsushita Electric Ind Co Ltd Treatment method
JPH06252118A (en) * 1993-02-25 1994-09-09 Dainippon Screen Mfg Co Ltd Substrate treating device
JPH06296940A (en) * 1991-02-28 1994-10-25 Hitachi Plant Eng & Constr Co Ltd Method and device for pressure-swinging cleaning
JPH0731942A (en) * 1993-05-18 1995-02-03 Yoshihide Shibano Method for ultrasonic washing and device therefor
JPH08309300A (en) * 1995-05-12 1996-11-26 Suzuki Motor Corp Ultrasonic washer
JP2000237703A (en) * 1999-02-18 2000-09-05 Akuatekku:Kk Vacuum washing/drying method and device

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6310531A (en) * 1986-07-02 1988-01-18 Matsushita Electric Ind Co Ltd Treatment method
JPH06296940A (en) * 1991-02-28 1994-10-25 Hitachi Plant Eng & Constr Co Ltd Method and device for pressure-swinging cleaning
JPH06252118A (en) * 1993-02-25 1994-09-09 Dainippon Screen Mfg Co Ltd Substrate treating device
JPH0731942A (en) * 1993-05-18 1995-02-03 Yoshihide Shibano Method for ultrasonic washing and device therefor
JPH08309300A (en) * 1995-05-12 1996-11-26 Suzuki Motor Corp Ultrasonic washer
JP2000237703A (en) * 1999-02-18 2000-09-05 Akuatekku:Kk Vacuum washing/drying method and device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003084576A1 (en) * 2002-04-04 2003-10-16 Sharp Kabushiki Kaisha Vacuum ultrasonic cleaning and dezymotizing device
CN103769379A (en) * 2014-01-04 2014-05-07 福建奇妙电子科技有限公司 Manufacturing method of household water mist spraying equipment
CN114535210A (en) * 2022-02-25 2022-05-27 天津市成吉斯宾科技发展有限公司 Ultrasonic vacuum surface treatment cleaning method

Also Published As

Publication number Publication date
CN1527749A (en) 2004-09-08

Similar Documents

Publication Publication Date Title
KR970007621B1 (en) Method &amp; apparatus for quantitative determination of trihalomethanes
JP4249208B2 (en) Vacuum distillation equipment
US5749159A (en) Method for precision cleaning and drying surfaces
US5752532A (en) Method for the precision cleaning and drying surfaces
US20120060868A1 (en) Microscale fluid delivery system
US7444761B2 (en) Intrinsically safe flammable solvent processing method and system
WO2003006184A1 (en) Washing device and washing method
JP3635026B2 (en) Sulfuric acid recycling equipment
JPH07227581A (en) Vacuum-cleaning and drying method and device therefor
JPH0615239A (en) Method for vacuum washing and drying and equipment therefor
JP3788588B2 (en) Parts washing and drying method
JP3989432B2 (en) Vacuum drying equipment
JP3818876B2 (en) Drying equipment
JP2003039029A (en) Cleaning device
JP3634718B2 (en) Cleaning device
JP6526858B2 (en) Cleaning solution distillation regenerating apparatus, parts cleaning apparatus, and method for regenerating distillation of cleaning solution
JP2902989B2 (en) Cleaning equipment
JPH05123658A (en) Method for cleaning body to be cleaned and apparatus therefor
JP3096241B2 (en) Cleaning equipment
US6413322B1 (en) Machine for vapor degreasing and process for doing same using an inflammable fluid
JP3052103B2 (en) Vacuum degreasing cleaning equipment
JPH0631103A (en) Vacuum distillation method of combustible solvent for work washing and vacuum distillation apparatus
JP4921229B2 (en) Cleaning device
JPH0326383A (en) Cleaning device using organic solvent
JP6320969B2 (en) Cleaning liquid distillation regeneration device and parts cleaning device

Legal Events

Date Code Title Description
AK Designated states

Kind code of ref document: A1

Designated state(s): AE AG AL AM AT AU AZ BA BB BG BR BY BZ CA CH CN CO CR CU CZ DE DK DM DZ EC EE ES FI GB GD GE GH GM HR HU ID IL IN IS KE KG KP KR KZ LC LK LR LS LT LU LV MA MD MG MK MN MW MX MZ NO NZ OM PH PL PT RO RU SD SE SG SI SK SL TJ TM TN TR TT TZ UA UG US UZ VN YU ZA ZM ZW

AL Designated countries for regional patents

Kind code of ref document: A1

Designated state(s): GH GM KE LS MW MZ SD SL SZ TZ UG ZM ZW AM AZ BY KG KZ MD RU TJ TM AT BE BG CH CY CZ DE DK EE ES FI FR GB GR IE IT LU MC NL PT SE SK TR BF BJ CF CG CI CM GA GN GQ GW ML MR NE SN TD TG

121 Ep: the epo has been informed by wipo that ep was designated in this application
WWE Wipo information: entry into national phase

Ref document number: 20028140990

Country of ref document: CN

DFPE Request for preliminary examination filed prior to expiration of 19th month from priority date (pct application filed before 20040101)
REG Reference to national code

Ref country code: DE

Ref legal event code: 8642

122 Ep: pct application non-entry in european phase