EP1338680A1 - Apparatus for degreasing and drying metallic, ceramic or polymeric articles - Google Patents

Apparatus for degreasing and drying metallic, ceramic or polymeric articles Download PDF

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Publication number
EP1338680A1
EP1338680A1 EP02406032A EP02406032A EP1338680A1 EP 1338680 A1 EP1338680 A1 EP 1338680A1 EP 02406032 A EP02406032 A EP 02406032A EP 02406032 A EP02406032 A EP 02406032A EP 1338680 A1 EP1338680 A1 EP 1338680A1
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EP
European Patent Office
Prior art keywords
deionized water
drying
degreasing
vacuum
mixture
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Granted
Application number
EP02406032A
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German (de)
French (fr)
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EP1338680B1 (en
Inventor
Jean-Francois Fallot
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
AMSONIC & RIOBEER AG
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Egaclean AG
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B21/00Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
    • F26B21/14Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects using gases or vapours other than air or steam, e.g. inert gases
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • B08B3/08Cleaning involving contact with liquid the liquid having chemical or dissolving effect
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/50Solvents
    • C11D7/5004Organic solvents
    • C11D7/5027Hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23GCLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G5/00Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents
    • C23G5/02Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents
    • C23G5/024Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents containing hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23GCLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G5/00Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents
    • C23G5/02Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents
    • C23G5/04Apparatus
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D2111/00Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
    • C11D2111/10Objects to be cleaned
    • C11D2111/14Hard surfaces
    • C11D2111/16Metals

Definitions

  • the present invention relates to a degreasing device and drying of mechanical parts or flammable solvents.
  • the CH-A-692 084 proposes the use of a solvent for flammable solvents to replace chlorinated solvents for degreasing-washing in the mechanical industry.
  • DE-A-43 29 178 offers the use of isoparaffinic solvents or modified alcohol.
  • the solvent according to this patent is of the isoparaffin or alkane type whose flash point is between 40 ° C and 100 ° C.
  • Metal parts are immersed in the solvent which is in an enclosure waterproof.
  • the pressure in the enclosure is less than 120 mbar and the temperature above 60 ° C inside the enclosure.
  • Legislation (OPAIR) requires machines using waterproof chlorinated solvents.
  • the mixture of chlorinated solvent and of water in a washing cycle is prohibited by law (OPEL).
  • Cleaning parts with non-polar soiling (mineral oils for example) and polar (particles, oxides, salts) cannot be resolved satisfactorily or with chlorinated or isoparaffinic solvents, or with detergents, their effectiveness being quickly inhibited by oils.
  • the object of the present invention is to propose a device for degreasing and drying of parts which improves the qualities of the degreasing system.
  • the device uses in a first phase washing a mixture of isoparaffin solvents at a temperature higher than the flash point, under vacuum or at temperature minus 15 ° C below the flash point, when the installation does not not work in vacuum.
  • a second phase the device uses an aqueous solution heated above 45 ° C, consisting deionized water, said washing being followed by a rinsing carried out deionized water and then drying carried out under vacuum.
  • a single-tank installation is used to immerse the parts to be cleaned in different solvents and rinsing agents.
  • the entire hydrocarbon solvent circuit is under vacuum about 120 mbar, to ensure the safety of the installation when the solvent is heated above the flash point.
  • the device presented here represents a development of the patent No 692084. Said patent uses only isoparaffin solvent.
  • the device described here first uses a solvent of the type isoparaffin, under vacuum, above the flash point and secondly an aqueous solution of composition suitable for metals to treat.
  • the aqueous solution is made with deionized water and contains less than 1% detergents, so reduce entrainment in the flushing circuit.
  • Rinsing is carried out in the enclosure in deionized water.
  • Drying is carried out in the enclosure, under vacuum.
  • the flash point is the temperature the lowest vapor concentration sufficient to produce a deflagration on contact of a flame but insufficient to produce the propagation of combustion in the absence of the pilot flame.
  • the main advantage is to perform high cleaning quality, because the isoparaffinic solvent removes dirt non-polar (fat in particular), while the solution aqueous removes polar soils (inorganic matter and particles).
  • the aqueous solution is practically not polluted by organic soils, since these were dissolved during the first wash. Soiling inorganics are practically not eliminated by solvents isoparaffins. They are however easily dissolved by a aqueous solution.
  • the cleaning sequence is therefore an element paramount.
  • a device having reservoirs allowing the use of one or more different aqueous solutions and a production facility deionized water in a closed circuit.
  • Final drying can optionally be carried out by a vapor phase with isoparaffin solvent followed by drying under vacuum, which protects the parts against corrosion.
  • the figure shows schematically a degreasing device and drying of metallic, ceramic or polymer parts.
  • the figure shows a reservoir 1 of primary isoparaffinic solvents, a reservoir 2 of secondary isoparaffinic solvents, a working chamber 3 of the single-tank installation, a distiller 4 of isoparaffinic solvents, a device 5 for producing deionized water in a closed circuit, tanks 6 of detergent solvents and a distillation resentant 7.
  • the solvent in tank 1 and the distillate in tank 2 is a mixture of isoparaffin solvents C g to C 11 .
  • the device is equipped with a vacuum system, which makes it possible to maintain a pressure below 12o mbar and to use the isoparaffin solvent above the flash point and to dry the parts under vacuum, after a first or a second washing. It is possible to add an isoparaffinic solvent vapor phase and vacuum drying after washing with detergent, to protect the parts against corrosion.
  • a mixture of isoparaffin solvents C 9 to C 11 is used at a temperature above the flash point under vacuum or at a temperature of at least 15 ° C below the flash point, when the installation does not work under vacuum.
  • the device uses an aqueous solution heated above 45 ° C. This aqueous solution consists of deionized water and a composition suitable for the parts to be cleaned. Washing is followed by rinsing with deionized water and then drying carried out under vacuum.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Metallurgy (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
  • Cleaning By Liquid Or Steam (AREA)

Abstract

Device for degreasing and drying metallic, ceramic or polymer components uses the following stages a primary washing stage with a mixture of isoparaffin solvents, a secondary operation using an aqueous solution, rinsing with the deionized water and drying under a vacuum. Device for degreasing and drying metallic, ceramic or polymer components uses the following stages: (1) a primary washing stage with a mixture of isoparaffin solvents under a vacuum at a temperature greater than the flash point, or at a temperature of at least 15 degrees C below the flash point when not under a vacuum; (2) a secondary operation using an aqueous solution heated to above 45 degrees C, made up of deionized water and a composition adapted to the components being cleaned; (3) rinsing with deionized water; and (4) drying under a vacuum. The primary washing operation uses a mixture of C9 to C11 isoparaffin solvents.

Description

La présente invention concerne un dispositif de dégraissage et séchage de pièces mécaniques ou de solvants inflammables. Le CH-A-692 084 propose l'utilisation d'un solvant de solvants inflammables pour remplacer des solvants chlorés pour le dégraissage-lavage dans l'industrie mécanique. Le DE-A-43 29 178 propose l'utilisation de solvants isoparaffiniques ou alcool modifié.The present invention relates to a degreasing device and drying of mechanical parts or flammable solvents. The CH-A-692 084 proposes the use of a solvent for flammable solvents to replace chlorinated solvents for degreasing-washing in the mechanical industry. DE-A-43 29 178 offers the use of isoparaffinic solvents or modified alcohol.

Le solvant selon de ce brevet est du type isoparaffine ou alcane dont le point-éclair est situé entre 40°C 100°C. Les pièces métalliques sont immergées dans le solvant qui est dans une enceinte étanche. La pression dans l'enceinte est à moins de 120 mbar et la température à plus de 60°C à l'intérieur de l'enceinte. La législation (OPAIR) impose des machines utilisant des solvants chlorés étanches. Le mélange de solvant chloré et d'eau dans un cycle de lavage est proscrit par la législation (OPEL). Le nettoyage de pièces présentant des salissures non-polaires (huiles minérales par exemple) et polaires (particules, oxydes, sels) ne peut être résolu de manière satisfaisante ni avec des solvants chlorés ou isoparaffiniques, ni avec des lessives, leur efficacité étant rapidement inhibée par les huiles. The solvent according to this patent is of the isoparaffin or alkane type whose flash point is between 40 ° C and 100 ° C. Metal parts are immersed in the solvent which is in an enclosure waterproof. The pressure in the enclosure is less than 120 mbar and the temperature above 60 ° C inside the enclosure. Legislation (OPAIR) requires machines using waterproof chlorinated solvents. The mixture of chlorinated solvent and of water in a washing cycle is prohibited by law (OPEL). Cleaning parts with non-polar soiling (mineral oils for example) and polar (particles, oxides, salts) cannot be resolved satisfactorily or with chlorinated or isoparaffinic solvents, or with detergents, their effectiveness being quickly inhibited by oils.

La présente invention a pour but de proposer un dispositif de dégraissage et séchage de pièces qui améliore les qualités du système de dégraissage.The object of the present invention is to propose a device for degreasing and drying of parts which improves the qualities of the degreasing system.

Selon l'invention le dispositif utilise dans une première phase de lavage un mélange de solvants isoparaffines à une température supérieure au point-éclair, sous vide ou à la température d'au moins 15°C en-dessous du point-éclair, lorsque l'installation ne travaille pas sous vide. Dans une deuxième phase le dispositif utilise une solution aqueuse chauffée au-dessus de 45°C, constituée d'eau désionisée, ledit lavage étant suivi d'un rinçage effectué de l'eau désionisée puis d'un séchage réalisé sous vide.According to the invention the device uses in a first phase washing a mixture of isoparaffin solvents at a temperature higher than the flash point, under vacuum or at temperature minus 15 ° C below the flash point, when the installation does not not work in vacuum. In a second phase the device uses an aqueous solution heated above 45 ° C, consisting deionized water, said washing being followed by a rinsing carried out deionized water and then drying carried out under vacuum.

Une installation monocuve est utilisée pour immerger les pièces à nettoyer dans différents solvants et agents de rinçage.A single-tank installation is used to immerse the parts to be cleaned in different solvents and rinsing agents.

L'ensemble du circuit de solvant hydrocarbure est sous vide d'environ 120 mbar, afin d'assurer la sécurité de l'installation lorsque le solvant est chauffé au-dessus du point-éclair. Le dispositif présenté ici représente un développement du brevet No 692084. Ledit brevet n'utilise que du solvant isoparaffine. Le dispositif décrit ici utilise premièrement un solvant de type isoparaffine, sous vide, au-dessus du point-éclair et deuxièmement une solution aqueuse de composition adaptée aux métaux à traiter. La solution aqueuse est réalisée avec de l'eau désionisée et contient moins de 1% d'agents détergents, de manière à réduire les entraínements dans le circuit de rinçage. Le rinçage est réalisé dans l'enceinte en eau désionisée. Le séchage est effectué dans l'enceinte, sous vide. Le point-éclair est la température la plus basse à laquelle la concentration de vapeur émise est suffisante pour produire une déflagration au contact d'une flamme mais insuffisante pour produire la propagation de la combustion en l'absence de la flamme pilote.The entire hydrocarbon solvent circuit is under vacuum about 120 mbar, to ensure the safety of the installation when the solvent is heated above the flash point. The device presented here represents a development of the patent No 692084. Said patent uses only isoparaffin solvent. The device described here first uses a solvent of the type isoparaffin, under vacuum, above the flash point and secondly an aqueous solution of composition suitable for metals to treat. The aqueous solution is made with deionized water and contains less than 1% detergents, so reduce entrainment in the flushing circuit. Rinsing is carried out in the enclosure in deionized water. Drying is carried out in the enclosure, under vacuum. The flash point is the temperature the lowest vapor concentration sufficient to produce a deflagration on contact of a flame but insufficient to produce the propagation of combustion in the absence of the pilot flame.

Le principal avantage consiste à réaliser un nettoyage de haute qualité, car le solvant isoparaffinique élimine les salissures non-polaires (matières grasses en particulier), alors que la solution aqueuse élimine les salissures polaires (matières inorganiques et particules). La solution aqueuse n'est pratiquement pas polluée par les salissures organiques, étant donné que celles-ci ont été dissoutes lors du premier lavage. Les salissures inorganiques ne sont pratiquement pas éliminées par les solvants isoparaffines. Elle sont par contre facilement dissoutes par une solution aqueuse. La séquence des nettoyages est donc un élément primordial.The main advantage is to perform high cleaning quality, because the isoparaffinic solvent removes dirt non-polar (fat in particular), while the solution aqueous removes polar soils (inorganic matter and particles). The aqueous solution is practically not polluted by organic soils, since these were dissolved during the first wash. Soiling inorganics are practically not eliminated by solvents isoparaffins. They are however easily dissolved by a aqueous solution. The cleaning sequence is therefore an element paramount.

Selon un variante de l'invention, il est prévu un dispositif comportant des réservoirs permettant d'utiliser une ou plusieurs solutions aqueuses différentes et une installation de production d'eau désionisée en circuit fermé.According to a variant of the invention, a device is provided having reservoirs allowing the use of one or more different aqueous solutions and a production facility deionized water in a closed circuit.

Différentes solutions permettent de nettoyer des substrats métalliques variés, en fonction de leur potentiel électrochimique.Different solutions can be used to clean metal substrates varied, depending on their electrochemical potential.

Le séchage final peut être réalisé en option par une phase vapeur avec du solvant isoparaffine suivie d'un séchage sous vide, ce qui permet de protéger les pièces contre la corrosion.Final drying can optionally be carried out by a vapor phase with isoparaffin solvent followed by drying under vacuum, which protects the parts against corrosion.

A présent, on va décrire un exemple de réalisation non limitatif de l'invention en regard de la seule figure annexée.Now, we will describe a non-limiting example of embodiment of the invention with reference to the single appended figure.

La figure représente schématiquement un dispositif de dégraissage et séchage de pièces métalliques, céramiques ou polymères. The figure shows schematically a degreasing device and drying of metallic, ceramic or polymer parts.

La figure montre un réservoir 1 de solvants isoparaffiniques primaires, un réservoir 2 de solvants isoparaffiniques secondaires, une chambre 3 de travail de l'installation monocuve, un distillateur 4 de solvants isoparaffiniques, un dispositif 5 de production d'eau désionisée en circuit fermé, des réservoirs 6 de solvants lessiviels et un retentant de destillation 7. Le solvant dans le réservoir 1 et le distillat dans le réservoir 2 est un mélange de solvants isoparaffines Cg à C11. Le dispositif est équipé d'un système de vide, ce qui permet de maintenir une pression inférieure à 12o mbar et d'utiliser le solvant isoparaffine au-dessus du point-éclair et de sécher les pièces sous vide, après un premier ou un second lavage. Il est possible d'ajouter une phase vapeur de solvant isoparaffinique et un séchage sous vide après un lavage lessiviel, afin de protéger les pièces contre la corrosion.The figure shows a reservoir 1 of primary isoparaffinic solvents, a reservoir 2 of secondary isoparaffinic solvents, a working chamber 3 of the single-tank installation, a distiller 4 of isoparaffinic solvents, a device 5 for producing deionized water in a closed circuit, tanks 6 of detergent solvents and a distillation resentant 7. The solvent in tank 1 and the distillate in tank 2 is a mixture of isoparaffin solvents C g to C 11 . The device is equipped with a vacuum system, which makes it possible to maintain a pressure below 12o mbar and to use the isoparaffin solvent above the flash point and to dry the parts under vacuum, after a first or a second washing. It is possible to add an isoparaffinic solvent vapor phase and vacuum drying after washing with detergent, to protect the parts against corrosion.

Dans une première phase de lavage on utilise un mélange de solvants isoparaffines C9 à C11 à une température supérieure au point-éclair sous vide ou à la température d'au moins 15°C en-dessous du point-éclair, lorsque l'installation ne travaille pas sous vide. Dans une deuxième phase le dispositif utilise une solution aqueuse chauffée au-dessus de 45°C. Cette solution aqueuse est constituée d'eau désionisée et de composition adaptée aux pièces à nettoyer. Le lavage est suivi d'un rinçage effectué avec de l'eau désionisée puis d'un séchage réalisé sous vide.In a first washing phase, a mixture of isoparaffin solvents C 9 to C 11 is used at a temperature above the flash point under vacuum or at a temperature of at least 15 ° C below the flash point, when the installation does not work under vacuum. In a second phase, the device uses an aqueous solution heated above 45 ° C. This aqueous solution consists of deionized water and a composition suitable for the parts to be cleaned. Washing is followed by rinsing with deionized water and then drying carried out under vacuum.

Le dispositif selon l'invention permet d'atteindre les deux objectifs :

  • éliminer les salissures polaires et non polaires dans une seule installation, et
  • augmenter notablement la durée de vie des solutions aqueuses et éviter une dégradation rapide et non contrôlée de leur pouvoir détergent.
The device according to the invention achieves two objectives:
  • remove polar and non-polar soiling in a single installation, and
  • significantly increase the life of aqueous solutions and avoid rapid and uncontrolled degradation of their detergent power.

Claims (3)

Dispositif de dégraissage et séchage de pièces métalliques, céramiques ou polymères utilisant dans une première phase de lavage un mélange de solvants isoparaffines à une température supérieure au point-éclair, sous vide ou à la température d'au moins 15°C en-dessous du point-éclair, lorsque l'installation ne travaille pas sous vide, puis dans une deuxième phase le dispositif utilise une solution aqueuse chauffée au-dessus de 45°C, constituée d'eau désionisée et de composition adaptée aux pièces à nettoyer, ledit lavage étant suivi d'un rinçage effectué avec de l'eau désionisée puis d'un séchage réalisé sous vide.Degreasing and drying device for metal parts, ceramics or polymers using in a first phase of washing a mixture of isoparaffin solvents at a temperature above flash point, vacuum or temperature at least 15 ° C below the flash point, when the installation does not work under vacuum, then in a second phase the device uses an aqueous solution heated above 45 ° C, consisting of deionized water and composition suitable for the parts to be cleaned, said washing being followed by rinsing with deionized water and then drying carried out under vacuum. Dispositif selon la revendication 1, comportant des réservoirs permettant d'utiliser une ou plusieurs solutions aqueuses différentes et une installation de production d'eau désionisée en circuit fermé.Device according to claim 1, comprising reservoirs allowing the use of one or more aqueous solutions different and a deionized water production facility in closed circuit. Dispositif selon la revendication 1, caractérisé en ce que l'on utilise un mélange de solvant isoparaffines C9 à C11.Device according to claim 1, characterized in that a mixture of isoparaffin solvents C 9 to C 11 is used .
EP02406032A 2002-02-22 2002-11-28 Apparatus for degreasing and drying metallic, ceramic or polymeric articles Expired - Lifetime EP1338680B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH3082002 2002-02-22
CH00308/02A CH696440A5 (en) 2002-02-22 2002-02-22 A method of degreasing, washing and drying of mechanical parts using non-halogenated hydrocarbons then detersive solvents in an installation monocuve vacuo

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EP1338680A1 true EP1338680A1 (en) 2003-08-27
EP1338680B1 EP1338680B1 (en) 2007-04-18

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2108464A1 (en) 2008-04-09 2009-10-14 Dow Global Technologies Inc. Process for cleaning articles
EP2260953A1 (en) * 2008-04-02 2010-12-15 Infinity Enterprises, Inc. Cleaning system
WO2022106886A1 (en) 2020-11-17 2022-05-27 Martin Ineichen Device and method for cleaning workpieces

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5397397A (en) * 1992-09-18 1995-03-14 Crestek, Inc. Method for cleaning and drying of metallic and nonmetallic surfaces
US5647143A (en) * 1992-10-30 1997-07-15 Japan Hayes Ltd. Vacuum-degreasing cleaning method
CH692084A5 (en) * 1998-03-27 2002-01-31 Egaclean Sa Device for degreasing and drying mechanical components using ultrasound and non-halogen hydrocarbon solvent comprises airtight enclosure under controlled pressure and temperature

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5397397A (en) * 1992-09-18 1995-03-14 Crestek, Inc. Method for cleaning and drying of metallic and nonmetallic surfaces
US5647143A (en) * 1992-10-30 1997-07-15 Japan Hayes Ltd. Vacuum-degreasing cleaning method
CH692084A5 (en) * 1998-03-27 2002-01-31 Egaclean Sa Device for degreasing and drying mechanical components using ultrasound and non-halogen hydrocarbon solvent comprises airtight enclosure under controlled pressure and temperature

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
"TIEFENWIRKUNG DIE KOHLENWASSERSTOFF-TECHNOLOGIE UNTER VAKUUM VERDRAENGT PERCHLORETHYLEN", MO METALLOBERFLACHE, CARL HANSER VERLAG. MUNCHEN, DE, vol. 56, no. 6, June 2002 (2002-06-01), pages 22 - 23, XP001114869, ISSN: 0043-2792 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2260953A1 (en) * 2008-04-02 2010-12-15 Infinity Enterprises, Inc. Cleaning system
EP2260953A4 (en) * 2008-04-02 2012-07-04 Infinity Entpr Inc Cleaning system
EP2108464A1 (en) 2008-04-09 2009-10-14 Dow Global Technologies Inc. Process for cleaning articles
US8066820B2 (en) 2008-04-09 2011-11-29 Dow Global Technologies Llc Process for cleaning articles
WO2022106886A1 (en) 2020-11-17 2022-05-27 Martin Ineichen Device and method for cleaning workpieces

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Publication number Publication date
CH696440A5 (en) 2007-06-15
DE60219591T2 (en) 2007-12-20
EP1338680B1 (en) 2007-04-18
DE60219591D1 (en) 2007-05-31

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