CH461438A - Procédé pour la séparation de substances contenues dans un mélange de composés chimiques et colonne chromatographie gaz-solide par la mise en oeuvre du procédé - Google Patents

Procédé pour la séparation de substances contenues dans un mélange de composés chimiques et colonne chromatographie gaz-solide par la mise en oeuvre du procédé

Info

Publication number
CH461438A
CH461438A CH1669464A CH1669464A CH461438A CH 461438 A CH461438 A CH 461438A CH 1669464 A CH1669464 A CH 1669464A CH 1669464 A CH1669464 A CH 1669464A CH 461438 A CH461438 A CH 461438A
Authority
CH
Switzerland
Prior art keywords
separation
mixture
carrying
gas
chemical compounds
Prior art date
Application number
CH1669464A
Other languages
English (en)
Inventor
Burgess Rogers Lockhart
Giles Altenau Alan
Original Assignee
Wilkens Instr & Res Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wilkens Instr & Res Inc filed Critical Wilkens Instr & Res Inc
Publication of CH461438A publication Critical patent/CH461438A/fr

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/22—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the construction of the column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B11/00—Preparation of cellulose ethers
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid
    • G01N30/56—Packing methods or coating methods
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6004—Construction of the column end pieces
    • G01N30/6017—Fluid distributors
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6052—Construction of the column body
    • G01N30/6069—Construction of the column body with compartments or bed substructure
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/80—Fraction collectors
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/84—Preparation of the fraction to be distributed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/54—Sorbents specially adapted for analytical or investigative chromatography
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/84—Preparation of the fraction to be distributed
    • G01N2030/8411—Intermediate storage of effluent, including condensation on surface
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6034—Construction of the column joining multiple columns

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Pathology (AREA)
  • Physics & Mathematics (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Polymers & Plastics (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Gas Separation By Absorption (AREA)
  • Pyridine Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CH1669464A 1962-12-24 1964-12-24 Procédé pour la séparation de substances contenues dans un mélange de composés chimiques et colonne chromatographie gaz-solide par la mise en oeuvre du procédé CH461438A (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US24678262A 1962-12-24 1962-12-24
US349367A US3312042A (en) 1962-12-24 1964-03-04 Gas-solid chromatographic column
US540079A US3374607A (en) 1962-12-24 1966-04-04 Apparatus for and method of collecting gas chromatographic fractions

Publications (1)

Publication Number Publication Date
CH461438A true CH461438A (fr) 1968-08-31

Family

ID=34381878

Family Applications (3)

Application Number Title Priority Date Filing Date
CH1669464A CH461438A (fr) 1962-12-24 1964-12-24 Procédé pour la séparation de substances contenues dans un mélange de composés chimiques et colonne chromatographie gaz-solide par la mise en oeuvre du procédé
CH354265A CH430279A (fr) 1962-12-24 1965-03-15 Procédé pour la séparation chromatographique d'un fluide, appareil pour la mise en oeuvre de ce procédé et application de ce procédé
CH472067A CH483858A (fr) 1962-12-24 1967-04-04 Procédé de chromatographie gazeuse et appareil pour sa mise en oeuvre

Family Applications After (2)

Application Number Title Priority Date Filing Date
CH354265A CH430279A (fr) 1962-12-24 1965-03-15 Procédé pour la séparation chromatographique d'un fluide, appareil pour la mise en oeuvre de ce procédé et application de ce procédé
CH472067A CH483858A (fr) 1962-12-24 1967-04-04 Procédé de chromatographie gazeuse et appareil pour sa mise en oeuvre

Country Status (6)

Country Link
US (3) US3312042A (fr)
CH (3) CH461438A (fr)
DE (2) DE1221036B (fr)
FR (4) FR1430151A (fr)
GB (3) GB1028870A (fr)
NL (2) NL6502698A (fr)

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US3354619A (en) * 1963-08-23 1967-11-28 Continental Oil Co Vapor phase chromatography system
US3310932A (en) * 1964-12-14 1967-03-28 Atlantic Refining Co Gas chromatographic columns
US3374606A (en) * 1965-09-10 1968-03-26 Abcor Inc Method of and apparatus for chromatographic separations
FR1451420A (fr) * 1965-07-16 1966-01-07 Rech S Scient Et Ind E R S I E Colonne de chromatographie perfectionnée
US3422604A (en) * 1966-02-21 1969-01-21 Continental Oil Co Chromatography apparatus
US3398512A (en) * 1966-04-18 1968-08-27 Continental Oil Co Chromatography apparatus
US3422665A (en) * 1966-08-01 1969-01-21 Continental Oil Co Chromatography system
GB1202441A (en) * 1966-08-05 1970-08-19 Victor Pretious Improvements in liquid or gas chromatography
US3457705A (en) * 1967-04-20 1969-07-29 Continental Oil Co Gas chromatography process
US3491517A (en) * 1967-08-02 1970-01-27 Universal Oil Prod Co Separation process
US3453811A (en) * 1968-05-03 1969-07-08 Abcor Inc Chromatographic columns with partition elements therein
US3584674A (en) * 1969-05-22 1971-06-15 Fisher Scientific Co Sample concentration apparatus
AU476229B2 (en) * 1971-10-01 1976-09-16 Suomen Sokeri Osakeyhtio Liquid control apparatus for chromatography columns
US3782078A (en) * 1972-02-14 1974-01-01 J Jerpe Apparatus for chromatographic separations
US3879181A (en) * 1972-03-09 1975-04-22 Showa Denko Kk Gas chromatograph, specimen capsule for use therein and process for gas chromatography
US3841059A (en) * 1972-09-25 1974-10-15 W Mccabe Compressed and thermostated air regulated gas liquid chromatography oven with simultaneously operated multiple chromatography columns
US3928193A (en) * 1975-02-14 1975-12-23 Suomen Sokeri Oy Process for large scale chromatography
GB1578533A (en) * 1976-05-25 1980-11-05 Analytical Instr Ltd Apparatus for the separation of components in a multi-component sample
US4154583A (en) * 1977-10-25 1979-05-15 Phillips Petroleum Company Automated temperature programmed preparative chromatography
FR2412331A1 (fr) * 1977-12-20 1979-07-20 Elf Aquitaine Procede de recyclage du gaz vecteur utilise dans un procede de chromatographie
US4537759A (en) * 1981-08-24 1985-08-27 Eagle-Picher Industries, Inc. Production of elemental silicon from impure silane feed
US4536199A (en) * 1984-01-05 1985-08-20 Mobil Oil Corporation Gas chromatograph for reseparating a sampel into pure components
FR2560783B1 (fr) * 1984-03-06 1986-10-17 Centre Nat Rech Scient Procede et dispositif pour capter et recueillir des produits a la sortie d'un chromatographe, appareil de traitement d'un aerosol
FR2586811B1 (fr) * 1985-08-27 1987-12-18 Rhone Poulenc Rech Tube de piegeage adaptable a la sortie d'un chromatographe en phase gazeuse et dispositif de support et de presentation d'un tel tube
DE3864569D1 (de) * 1987-05-04 1991-10-10 Sulzer Ag Absorptionskolonne zum chromatographischen trennen von stoffgemischen.
FI97277C (fi) * 1993-01-25 1996-11-25 Suomen Sokeri Oy Kromatografinen erotuskolonni, sen sisärakenteet ja kromatografinen erotusmenetelmä
FI96225C (fi) 1993-01-26 1996-05-27 Cultor Oy Menetelmä melassin fraktioimiseksi
US6663780B2 (en) 1993-01-26 2003-12-16 Danisco Finland Oy Method for the fractionation of molasses
FR2708480B1 (fr) * 1993-08-02 1996-05-24 Inst Francais Du Petrole Distributeur-mélangeur-extracteur de fluide monophasique pour lits de solides granulaires.
US5795398A (en) 1994-09-30 1998-08-18 Cultor Ltd. Fractionation method of sucrose-containing solutions
DE69625769T2 (de) * 1995-10-20 2003-08-07 Institut Francais Du Petrole, Rueil Malmaison Verteiler zur unabhängigen Ein- und/oder Abführung von Fluiden
US6224776B1 (en) * 1996-05-24 2001-05-01 Cultor Corporation Method for fractionating a solution
US6413428B1 (en) * 1999-09-16 2002-07-02 Berger Instruments, Inc. Apparatus and method for preparative supercritical fluid chromatography
US6685828B2 (en) * 1999-09-16 2004-02-03 Berger Instruments, Inc. Automated sample collection in supercritical fluid chromatography
US6632353B2 (en) * 2000-06-26 2003-10-14 Berger Instruments, Inc. Rapid sample collection in supercritical fluid chromatography
FI20010977A (fi) 2001-05-09 2002-11-10 Danisco Sweeteners Oy Kromatografinen erotusmenetelmä
DE102008012798A1 (de) * 2008-03-05 2009-09-10 Dionex Softron Gmbh Kapillarartige Verbindung für die Flüssigkeitschromatographie, insbesondere für die Hochleistungsflüssigkeitschromatographie mit verminderter Dispersion und verbesserten thermischen Eigenschaften
US8021468B2 (en) * 2008-06-23 2011-09-20 Siemens Medical Solutions Usa, Inc. Room temperature chemical trap for the purification of gaseous methane
US9163618B2 (en) 2008-06-24 2015-10-20 Agilent Technologies, Inc. Automated conversion between SFC and HPLC
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US8419936B2 (en) * 2010-03-23 2013-04-16 Agilent Technologies, Inc. Low noise back pressure regulator for supercritical fluid chromatography
US9240253B2 (en) * 2010-04-07 2016-01-19 Ge-Hitachi Nuclear Energy Americas Llc Column geometry to maximize elution efficiencies for molybdenum-99
US11406916B2 (en) * 2015-03-18 2022-08-09 Francois Parmentier Method of power-efficient chromatographic separation
CN107615063B (zh) * 2015-04-10 2021-04-20 沃特世科技公司 气液分离后二氧化碳基色谱系统的冷却液体洗脱液
US20190227039A1 (en) * 2018-01-22 2019-07-25 Waters Technologies Corporation Systems and methods for compressible fluid chromatography
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US2242299A (en) * 1940-05-15 1941-05-20 Standard Oil Dev Co Vapor recovery system
US2723756A (en) * 1951-04-24 1955-11-15 John M Miller Apparatus with bonded adsorbent block and capillary chromatographic adsorption therewith
US2845136A (en) * 1955-09-12 1958-07-29 Cons Electrodynamics Corp Chromatography
US3002583A (en) * 1957-06-10 1961-10-03 Phillips Petroleum Co Fluid separation by gas chromatography
US3174326A (en) * 1958-02-24 1965-03-23 Beckman Instruments Inc Gas chromatograph
FR1203026A (fr) * 1958-05-09 1960-01-14 Air Liquide Perfectionnements aux procédés pour l'analyse de mélanges gazeux
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US3048029A (en) * 1959-03-19 1962-08-07 Jr Richard S Juvet Gas chromatographic analysis of inorganic materials
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US3038904A (en) * 1959-09-23 1962-06-12 Jefferson Chem Co Inc Method for separating amines
FR1258723A (fr) * 1960-06-03 1961-04-14 Perkin Elmer Corp Dispositif de colonne séparatrice pour appareil de chromatographie gazeuse

Also Published As

Publication number Publication date
FR1421737A (fr) 1965-12-17
GB1087246A (en) 1967-10-18
GB1028870A (en) 1966-05-11
FR1430151A (fr) 1966-03-04
CH483858A (fr) 1970-01-15
DE1598017A1 (de) 1969-10-02
NL6502698A (fr) 1965-09-06
NL6704796A (fr) 1967-10-05
FR1517537A (fr) 1968-03-15
US3312042A (en) 1967-04-04
GB1183189A (en) 1970-03-04
US3374607A (en) 1968-03-26
DE1221036B (de) 1966-07-14
FR1436825A (fr) 1966-04-29
CH430279A (fr) 1967-02-15
US3250058A (en) 1966-05-10

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