CH427308A - Process for joining graphite objects to one another or to objects made of other materials - Google Patents
Process for joining graphite objects to one another or to objects made of other materialsInfo
- Publication number
- CH427308A CH427308A CH1013762A CH1013762A CH427308A CH 427308 A CH427308 A CH 427308A CH 1013762 A CH1013762 A CH 1013762A CH 1013762 A CH1013762 A CH 1013762A CH 427308 A CH427308 A CH 427308A
- Authority
- CH
- Switzerland
- Prior art keywords
- objects
- weight
- graphite
- materials
- another
- Prior art date
Links
Classifications
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B7/00—Heating by electric discharge
- H05B7/02—Details
- H05B7/14—Arrangements or methods for connecting successive electrode sections
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/24—Selection of soldering or welding materials proper
- B23K35/30—Selection of soldering or welding materials proper with the principal constituent melting at less than 1550 degrees C
- B23K35/3013—Au as the principal constituent
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B37/00—Joining burned ceramic articles with other burned ceramic articles or other articles by heating
- C04B37/003—Joining burned ceramic articles with other burned ceramic articles or other articles by heating by means of an interlayer consisting of a combination of materials selected from glass, or ceramic material with metals, metal oxides or metal salts
- C04B37/006—Joining burned ceramic articles with other burned ceramic articles or other articles by heating by means of an interlayer consisting of a combination of materials selected from glass, or ceramic material with metals, metal oxides or metal salts consisting of metals or metal salts
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B37/00—Joining burned ceramic articles with other burned ceramic articles or other articles by heating
- C04B37/02—Joining burned ceramic articles with other burned ceramic articles or other articles by heating with metallic articles
- C04B37/023—Joining burned ceramic articles with other burned ceramic articles or other articles by heating with metallic articles characterised by the interlayer used
- C04B37/026—Joining burned ceramic articles with other burned ceramic articles or other articles by heating with metallic articles characterised by the interlayer used consisting of metals or metal salts
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C5/00—Alloys based on noble metals
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2237/00—Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
- C04B2237/02—Aspects relating to interlayers, e.g. used to join ceramic articles with other articles by heating
- C04B2237/12—Metallic interlayers
- C04B2237/125—Metallic interlayers based on noble metals, e.g. silver
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2237/00—Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
- C04B2237/02—Aspects relating to interlayers, e.g. used to join ceramic articles with other articles by heating
- C04B2237/12—Metallic interlayers
- C04B2237/126—Metallic interlayers wherein the active component for bonding is not the largest fraction of the interlayer
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2237/00—Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
- C04B2237/02—Aspects relating to interlayers, e.g. used to join ceramic articles with other articles by heating
- C04B2237/12—Metallic interlayers
- C04B2237/126—Metallic interlayers wherein the active component for bonding is not the largest fraction of the interlayer
- C04B2237/127—The active component for bonding being a refractory metal
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2237/00—Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
- C04B2237/50—Processing aspects relating to ceramic laminates or to the joining of ceramic articles with other articles by heating
- C04B2237/70—Forming laminates or joined articles comprising layers of a specific, unusual thickness
- C04B2237/704—Forming laminates or joined articles comprising layers of a specific, unusual thickness of one or more of the ceramic layers or articles
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2237/00—Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
- C04B2237/50—Processing aspects relating to ceramic laminates or to the joining of ceramic articles with other articles by heating
- C04B2237/70—Forming laminates or joined articles comprising layers of a specific, unusual thickness
- C04B2237/708—Forming laminates or joined articles comprising layers of a specific, unusual thickness of one or more of the interlayers
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2237/00—Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
- C04B2237/50—Processing aspects relating to ceramic laminates or to the joining of ceramic articles with other articles by heating
- C04B2237/76—Forming laminates or joined articles comprising at least one member in the form other than a sheet or disc, e.g. two tubes or a tube and a sheet or disc
- C04B2237/765—Forming laminates or joined articles comprising at least one member in the form other than a sheet or disc, e.g. two tubes or a tube and a sheet or disc at least one member being a tube
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/25—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Structural Engineering (AREA)
- Metallurgy (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Ceramic Products (AREA)
- Vessels And Coating Films For Discharge Lamps (AREA)
Description
Verfahren zum Verbinden von Graphitgegenständen miteinander oder mit Gegenständen aus anderen Materialien Die Erfindung betrifft ein Verfahren zum Ver binden von Graphitgegenständen miteinander oder reit Gegenständen aus anderen Materialien durch Löten.
Unter Graphit wird im nachfolenden nicht nur .in der Graphitform kristallisierter Kohlenstoff, sondern auch Material verstanden, das teilweise ans nicht kristallisiertem Kohlenstoff besteht, wie es zum Beispiel bei Handelsprodukten :der Fall sein kann, die, mit Elektrographit bezeichnet werden.
Für manche Anwendungen kommen die mit Hilfe eines Leims auf der Basis organischer Stoffe erzielten Verbindungen von Graphibgegenständen nicht in Frage, da solche Verbindungen nur gegen niedrigere Temperaturen beständig sind.
Da zur Zeit gas- und flüssigkeitsdichte Graphibarten verfügbar sind, ist die Erzielung dichter Verbindungen erwünscht. Mecha- nische Verbindungen, zum Beispiel Schrauben- oder Klemmverbindungen, sind .in diesem Fall nicht brauchbar.
Weiterhin ist es bekannt, dass Verbindungen zwi- schen Graphit und bestimmten Metallen mit Hilfe eines geschmolzenen Metallei hergestellt werden kön nen. Solche Verbindungen weisen im allgemeinen die obererwähnten Nachteile nicht oder in geringe rem Masse auf.
So ist es bekannt, dass solche Verbindungen mit Hilfe von Indium oder einer Indiumlegierung erzielt werden können. Weiterhin ist es zum Beispiel be kannt, dass Graphitkörper sich mit Aluminium mit Hilfe von Zinn verbinden lassen. Diese Verbindungen haben aber den Nachteil, dass Indium, Indmumlegie- rungen und Zinn einen niedrigen Schmelzpunkt auf- weisen.
Bekannt ist auch die Verwendung höher schmel- zender Metalle oder Legierungen, zum Beispiel Lot auf der Basis eines oder mehrerer der Metalle Kupfer, Silber und Gold zum Verbinden von Gegenständen -aus Graphit mit Gegenständen, (die völlig oder wenig stens an einer Oberfläche aus Titan,
Zirkon oder deren Legierungen bestehen. Zwar ergibt sich auf diese Weise eine verhältnismässig hochschmelzende Verbindung, aber die Anwendung beschränkt sich ,auf Verbindungen von Graphit mit den Metallen Titan und Zirkon.
Schliesslich ist es noch bekannt, Verbindungen von Graphit mit Metallen mit Hilfe von Oxyden herzustellen. So kann zum Beispiel eine Verbindung zwischen Eisen und Graphit,durch Erhitzung -in einer oxydierenden Atmosphäre erzielt werden,
wobei ent standenes Eisenoxyd die Verbindung herstellt. Die mechanische Festigkeit eines solchen Verbindung .ist verhältnismässig gering.
Die Erfindung bezweckt, die erwähnten Nach- ,teile zu vermeiden.
Nachdem Verfahren gemäss oder Erfindung wer den Graphitgegenstände miteinander oder mit Gegen ständen aus anderen Materialien durch Löten, ver- bunden, in :dem mit einer Legierung von Gold mit ,einem Gehalt an Tantal und/oder Niob von wenig stens 1 Gew. % im Vakuum oder mit einer Edel- gasatmosphäre gelötet wird.
Legierungen mit einem niedrigeren Gehalt -an Tantal und/oder Niob ergeben eine unzulängliche Benetzung der zu verbindenden Oberflächen.
Die Anwendung eines Tantalgehaltes über etwa 25 Gew. % oder eines Niobgehaltes über etwa 10 Gew.% bringt,den Nachteil mit sich, dass die Le gierungen einen zu hohen Schmelzpunkt für eine laichte Verarbeitung haben, oder spröde sind.
Die Legierungen mit einem Tantalgehalt bis 25 Gew.% und solche mit einem Niobgehalt bis 10 Gew.% haben einen Schmelzpunkt unter 1300 C und sind duktil. Die Legierungen können dadurch leicht in die Form von Draht oder Folie gebracht werden, was beim Löten vorteilhaft sein kann.
Sehr günstige Ergebnisse werden mit Legierungen erzielt, deren Tantalgehalt zwischen 5 und 10 Gew.% liegt. Der Gehalt -an Niob wird vorzugsweise nicht höher als etwa 5 Gew.% gewählt.
Die Legierungen von Gold mit Tontal und/oder Niob benetzen beim Löten Oberflächen von Graphit gegenständen besonders gut. Ausserdem werden die verschiedenartigsten anderen Materialien, wie Quarz, Keramik und Metalle, insbesondere Molybdän und Wolfram, gut benetzt.
In. allen diesen Fällen ergibt sich eine besonders gut haftende Verbindung, die für Temperaturschwan kungen wenig oder nicht empfindlich ist. Dies .hängt möglicherweise mit der besonderen Duktilität der betreffenden Legierungen zusammen, wodurch Span- nungen infolge .abweichender Ausdehnungskoeffizien ten der zu verbindenden Materialien und .der Le gierung leicht ausgeglichen werden können.
<I>Beispiele</I> 1. Zwei Graphitröhren mit einem Inneren Durch messer von 8 mm und einem äusseren Durchmesser von 10 mm werden mit Hilfe einer Legierung von 95 Gew.% Gold und 5 Gew.% Tontal verlötet. Dazu wird zwischen den Enden der Rohre .ein ringförmiges Drahtstückchen der Legierung in der Stärke von 200 Mikron angebracht. Anschliessend wird das Lot im Vakuum ,durch Hochfrequenzerhitzung auf etwa 1300 C zum Schmelzen gebracht.
2. Ein Graphitstab mit einem Durchmesser von 6 mm wird an einem Ende .mit Hilfe .einer Legierung von 97 Gew.% Gold und 3 Gew. % Niob auf eine Wol framplatte gelötet. Das Lot wird in Form einer kreis- förmigen Folie mit einem Durchmesser von 10, mm und einer Stärke von 150 Mikron zwischen dem Stab und der Platte angebracht. Anschliessend erfolgt eine Erhitzung auf etwa l300 C in einer Argonatmo sphäre.
3. Ein Graphitrohr und ;ein aus Aluminium oxyd bestehendes Keramikrohr mit Iden Abmessun gen wie im Beispiel 1 angegeben, werden mit Hilfe einer Legierung von 97 Gew. % Gold und 3 Gew. % Tontal miteinander verbunden. Die Rohre werden dazu an einem Ende derart konisch abgeschliffen, dass sie über eine Länge von einigen Millimetern inein anderpassen. Ein Folienstreifen in der Stärke von 150 Mikron der erwähnten Legierung wird zwischen den Enden der Röhre angebracht, worauf im Vakuum auf etwa 1300 C erhitzt wird.
Method for joining graphite objects to one another or to objects made of other materials. The invention relates to a method for joining graphite objects to one another or riding objects made of other materials by soldering.
In the following, graphite is understood to mean not only carbon crystallized in the graphite form, but also material that consists partly of non-crystallized carbon, as can be the case, for example, with commercial products that are referred to as electrographite.
For some applications, the connections of graphite objects achieved with the aid of a glue based on organic substances are out of the question, since such connections are only resistant to lower temperatures.
Since gas- and liquid-tight graphite types are currently available, it is desirable to achieve tight connections. Mechanical connections, for example screw or clamp connections, cannot be used in this case.
It is also known that connections between graphite and certain metals can be produced with the aid of a molten metal. Such compounds generally do not have the abovementioned disadvantages or only to a minor extent.
It is known that such compounds can be achieved with the aid of indium or an indium alloy. It is also known, for example, that graphite bodies can be connected to aluminum with the help of tin. However, these compounds have the disadvantage that indium, indium alloys and tin have a low melting point.
It is also known to use higher-melting metals or alloys, for example solder based on one or more of the metals copper, silver and gold for connecting objects made of graphite with objects (which are completely or at least on a surface made of titanium ,
Zircon or its alloys exist. Although this results in a relatively high-melting point connection, the application is limited to connections between graphite and the metals titanium and zirconium.
Finally, it is also known to produce compounds between graphite and metals with the aid of oxides. For example, a connection between iron and graphite can be achieved by heating in an oxidizing atmosphere,
whereby the iron oxide produced establishes the connection. The mechanical strength of such a connection is relatively low.
The invention aims to avoid the disadvantages mentioned, parts.
According to the method according to the invention or the invention, the graphite objects with each other or with objects made of other materials by soldering, connected in: with an alloy of gold with a content of tantalum and / or niobium of at least 1% by weight in a vacuum or is soldered with a noble gas atmosphere.
Alloys with a lower content of tantalum and / or niobium result in inadequate wetting of the surfaces to be connected.
The use of a tantalum content above about 25% by weight or a niobium content above about 10% by weight has the disadvantage that the alloys have a melting point that is too high for easy processing or are brittle.
The alloys with a tantalum content of up to 25% by weight and those with a niobium content of up to 10% by weight have a melting point below 1300 C and are ductile. The alloys can easily be brought into the form of wire or foil, which can be advantageous when soldering.
Very favorable results are achieved with alloys with a tantalum content between 5 and 10% by weight. The content of niobium is preferably not selected to be higher than about 5% by weight.
The alloys of gold with tonal and / or niobium wet surfaces of graphite objects particularly well when soldering. In addition, a wide variety of other materials, such as quartz, ceramics and metals, especially molybdenum and tungsten, are well wetted.
In. All of these cases result in a particularly well-adhering connection that is little or not sensitive to temperature fluctuations. This is possibly due to the particular ductility of the alloys in question, as a result of which stresses due to different expansion coefficients of the materials to be connected and the alloy can be easily compensated.
<I> Examples </I> 1. Two graphite tubes with an inner diameter of 8 mm and an outer diameter of 10 mm are soldered with the aid of an alloy of 95% by weight gold and 5% by weight Tontal. For this purpose, a ring-shaped piece of wire of the alloy with a thickness of 200 microns is attached between the ends of the tubes. The solder is then melted in a vacuum by high-frequency heating to around 1300 C.
2. A graphite rod with a diameter of 6 mm is soldered at one end to a tungsten plate using an alloy of 97% by weight gold and 3% by weight niobium. The solder is placed in the form of a circular foil with a diameter of 10 mm and a thickness of 150 microns between the rod and the plate. This is followed by heating to around 1300 C in an argon atmosphere.
3. A graphite tube and a ceramic tube made of aluminum oxide with dimensions as specified in Example 1 are connected to one another with the aid of an alloy of 97% by weight of gold and 3% by weight of Tontal. For this purpose, the tubes are ground conically at one end so that they fit into one another over a length of a few millimeters. A foil strip 150 microns thick of the alloy mentioned is placed between the ends of the tube, followed by heating to about 1300 ° C. in a vacuum.
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NL268735 | 1961-08-29 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH427308A true CH427308A (en) | 1966-12-31 |
Family
ID=19753258
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH1013762A CH427308A (en) | 1961-08-29 | 1962-08-27 | Process for joining graphite objects to one another or to objects made of other materials |
CH1013662A CH445267A (en) | 1961-08-29 | 1962-08-27 | Process for creating a bond between a diamond and metal |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH1013662A CH445267A (en) | 1961-08-29 | 1962-08-27 | Process for creating a bond between a diamond and metal |
Country Status (5)
Country | Link |
---|---|
US (1) | US3196536A (en) |
AT (1) | AT248834B (en) |
BE (2) | BE621794A (en) |
CH (2) | CH427308A (en) |
GB (1) | GB937947A (en) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR1355568A (en) * | 1962-12-17 | 1964-03-20 | Snecma | Process for soldering two parts, at least one of which is in graphite |
DE1671658B1 (en) * | 1966-03-25 | 1971-05-13 | Siemens Ag | Application of the process for the production of a firmly adhering coating consisting essentially of metal carbide of at least one of the metals from group IVa, Va and VIa on the surface of carbon bodies for the production of solderable coatings for the production of vacuum-tight metal-carbon- |
US3425116A (en) * | 1966-08-10 | 1969-02-04 | Us Navy | Brazing method |
US3725719A (en) * | 1970-11-30 | 1973-04-03 | Varian Associates | Method and aritcle for inhibiting gaseous permeation and corrosion of material |
US3813759A (en) * | 1971-09-09 | 1974-06-04 | English Electric Co Ltd | Method of brazing |
US4000026A (en) * | 1973-03-12 | 1976-12-28 | Union Carbide Corporation | Method and cement for bonding carbon articles |
ZA775521B (en) * | 1977-09-14 | 1979-01-31 | De Beers Ind Diamond | Wire drawing die composites |
US4180700A (en) * | 1978-03-13 | 1979-12-25 | Medtronic, Inc. | Alloy composition and brazing therewith, particularly for _ceramic-metal seals in electrical feedthroughs |
US5853661A (en) * | 1994-07-05 | 1998-12-29 | Cendres Et Metaux Sa | High gold content bio--compatible dental alloy |
US5972157A (en) * | 1995-11-20 | 1999-10-26 | Alliedsignal Inc. | Joining of rough carbon-carbon composites with high joint strength |
FR2751640B1 (en) * | 1996-07-23 | 1998-08-28 | Commissariat Energie Atomique | COMPOSITION AND METHOD FOR REACTIVE BRAZING OF CERAMIC MATERIALS CONTAINING ALUMINUM |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2739375A (en) * | 1952-09-12 | 1956-03-27 | Handy & Harman | Joining of non-metallic materials and brazing filler rods therefor |
US2979813A (en) * | 1956-09-28 | 1961-04-18 | Horizons Inc | Joining of graphite members |
-
0
- BE BE621795D patent/BE621795A/xx unknown
- BE BE621794D patent/BE621794A/xx unknown
-
1962
- 1962-07-23 US US211872A patent/US3196536A/en not_active Expired - Lifetime
- 1962-08-24 GB GB32652/62A patent/GB937947A/en not_active Expired
- 1962-08-27 CH CH1013762A patent/CH427308A/en unknown
- 1962-08-27 CH CH1013662A patent/CH445267A/en unknown
- 1962-08-27 AT AT686462A patent/AT248834B/en active
Also Published As
Publication number | Publication date |
---|---|
US3196536A (en) | 1965-07-27 |
AT248834B (en) | 1966-08-25 |
BE621794A (en) | 1900-01-01 |
CH445267A (en) | 1967-10-15 |
BE621795A (en) | 1900-01-01 |
GB937947A (en) | 1963-09-25 |
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