CH183876A - Process for the preparation of an azo dye. - Google Patents
Process for the preparation of an azo dye.Info
- Publication number
- CH183876A CH183876A CH183876DA CH183876A CH 183876 A CH183876 A CH 183876A CH 183876D A CH183876D A CH 183876DA CH 183876 A CH183876 A CH 183876A
- Authority
- CH
- Switzerland
- Prior art keywords
- azo dye
- dye
- preparation
- pyrazolone
- naphthol
- Prior art date
Links
Landscapes
- Coloring (AREA)
Description
Verfahren zur Herstellung eines Azofarbstoffes. Gegenstand des vorliegenden Zusatzpaten tes ist ein Verfahren zur Herstellung eines Azofarbstoffes, welches dadurch gekenn zeichnet ist, dass man dianotierte 1-Amino-2- naphtol-4-sulfonsäure mit 3-Phenyl-5-pyr- azolon kuppelt.
<I>Beispiel:</I> 25 Gewichtsteile der festen Diazoverbin- dung der 1-Amino-2-naphtol-4-sulfonsäure werden mit 100 Gewichtsteilen Wasser an gerührt und bei 20 in eine ätzn@Ltronalka- lische Lösung von 16 Gewichtsteilen 3-Phe- nyl-5-pyrazolon eingerührt. Der vollkommen in Lösung befindliche Farbstoff wird durch Ansäuren gefällt, filtriert und getrocknet.
Er stellt ein rotes Pulver dar, das Wolle aus saurem Bade in roten Tönen von sehr guter Wasch- und Lichtechtheit färbt. Durch Nachbehandlung mit Chromsalzen kann die Echtheit der Färbung noch verbessert wer den.
Process for the preparation of an azo dye. The subject of the present additional patent is a process for the production of an azo dye, which is characterized in that dianotated 1-amino-2-naphthol-4-sulfonic acid is coupled with 3-phenyl-5-pyrazolone.
<I> Example: </I> 25 parts by weight of the solid diazo compound of 1-amino-2-naphthol-4-sulfonic acid are stirred with 100 parts by weight of water and at 20 in a caustic solution of 16 parts by weight of 3 -Phenyl-5-pyrazolone stirred in. The dye, which is completely in solution, is precipitated by acidification, filtered and dried.
It is a red powder that dyes wool from an acid bath in red shades that are very washfast and lightfast. The fastness of the coloration can be further improved by post-treatment with chromium salts.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE183876X | 1933-12-01 | ||
CH180961T | 1934-11-29 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH183876A true CH183876A (en) | 1936-04-30 |
Family
ID=25720492
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH183876D CH183876A (en) | 1933-12-01 | 1934-11-29 | Process for the preparation of an azo dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH183876A (en) |
-
1934
- 1934-11-29 CH CH183876D patent/CH183876A/en unknown
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