CH166664A - Process for the preparation of an o-oxyazo dye. - Google Patents
Process for the preparation of an o-oxyazo dye.Info
- Publication number
- CH166664A CH166664A CH166664DA CH166664A CH 166664 A CH166664 A CH 166664A CH 166664D A CH166664D A CH 166664DA CH 166664 A CH166664 A CH 166664A
- Authority
- CH
- Switzerland
- Prior art keywords
- dye
- oxyazo
- preparation
- parts
- diazo
- Prior art date
Links
Landscapes
- Coloring (AREA)
Description
Verfahren zur Herstellung eines o-Oxyazofarbstoffes. Nach dem durch das Hauptpatent ge schützten Verfahren erhält man einen Wolle in Gegenwart von Chrombeizen echt anfär benden Farbstoff, wenn man 4-Clilor-2-diazo- 1-oxybenzol-6-sulfosäure mit 7, 8-Benzo-2.4- dioxychinolin kuppelt.
Wie nun weiter gefunden wurde, erhält man einen Farbstoff mit gleich guten Eigen schaften, wenn man als Diazokomponente die 4 Nitro-2-diazo-l-oxybenzol-6-sulfosäure wählt.
<I>Beispiel:</I> Eine aus 23,4 Teilen 4-Nitro-2-amirio-l- oxybenzol-6-sulfosäure, 6,9 Teilen Natrium nitrit und 5 Teilen Salzsäure von 120 B6 in etwa 500 Teilen Wasser bereitete Diazo- verbindung wird zu einer mit Eis versetzten Auflösung von 23 Teilen 7.8-Benzo-2.4- dioxychinolin und 20 Teilen Soda in<B>600</B> Teilen Wasser gegeben.
Der gebildete Farb stoff wird vollständig ausgesalzen und bildet getrocknet ein dunkles Pulver, welches sehr gut löslich ist und auf Wolle nach dem Einbad-Chromverfahren granatfarbene Töne von guter Walk- und Waschechtbeit erzeugt.
Process for the preparation of an o-oxyazo dye. After the process protected by the main patent ge one obtains a wool in the presence of chrome stains genuinely dyeing dye when 4-Clilor-2-diazo-1-oxybenzene-6-sulfonic acid is coupled with 7, 8-benzo-2.4-dioxyquinoline.
As has now been found further, a dye with equally good properties is obtained if the 4-nitro-2-diazo-1-oxybenzene-6-sulfonic acid is chosen as the diazo component.
<I> Example: </I> A prepared from 23.4 parts of 4-nitro-2-amirio-l-oxybenzene-6-sulfonic acid, 6.9 parts of sodium nitrite and 5 parts of hydrochloric acid of 120 B6 in about 500 parts of water Diazo compound is added to a solution, with ice, of 23 parts of 7.8-benzo-2.4-dioxyquinoline and 20 parts of soda in 600 parts of water.
The dyestuff formed is completely salted out and, when dried, forms a dark powder which is very soluble and produces garnet-colored tones of good fulling and washfastness on wool using the single-bath chrome process.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE166664X | 1932-04-18 | ||
CH164201T | 1932-11-11 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH166664A true CH166664A (en) | 1934-01-15 |
Family
ID=25717940
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH166664D CH166664A (en) | 1932-04-18 | 1932-11-11 | Process for the preparation of an o-oxyazo dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH166664A (en) |
-
1932
- 1932-11-11 CH CH166664D patent/CH166664A/en unknown
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