CH150924A - Process for the production of a vat dye. - Google Patents
Process for the production of a vat dye.Info
- Publication number
- CH150924A CH150924A CH150924DA CH150924A CH 150924 A CH150924 A CH 150924A CH 150924D A CH150924D A CH 150924DA CH 150924 A CH150924 A CH 150924A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- vat dye
- vat
- bromine
- dyed
- Prior art date
Links
Landscapes
- Coloring (AREA)
- Pyridine Compounds (AREA)
Description
Ycrfaliren zur Herstellung eines Küpenfarbstofes. Es wurde gefunden, dass man einen wert vollen Küpenfarbstoff erhält, wenn man Pyridinopyranthron, das nach dem Verfahren des schweiz. Patentes Nr. 149413 erhalten werden kann, mit einem bromierend wirken den Mittel bis zur Aufnahme von 2 Atomen Brom behandelt. Man kann hierbei in Gegen- #art von Katalysatoren, wie Jod, Eisen, Alu ininiumchlorid, Schwefel etc., arbeiten.
Das Reaktionsprodukt löst sich in kon zentrierter Schwefelsäure mit blauer Farbe und liefert eine violette Küpe, aus der die pflanzliche Faser in klaren, kräftigen, bor- clea,uxroten Tönen von sehr guter Echtheit gefärbt wird. Beispiel: 460 Teile des gemäss -des Patentes 149413 dargestellten Pyridinopyranthrons werden in :1000 Teilen Chlorsulfonsäure unter Rühren gelöst und nach Zugabe von 40 Teilen Schwe fel und 200 Teilen Brom langsam auf 60 bis<B>6 5</B> C erhitzt.
Man hält bei dieser Tem peratur so lange, bis alles Brom aufgenom men, lässt dann erkalten und arbeitet in der üblichen Weise auf.
Ycrfaliren for making a vat dye. It has been found that a valuable vat dye is obtained if one uses pyridinopyranthrone, which is produced using the Swiss method. Patent No. 149413 can be obtained, treated with a brominating agent up to the absorption of 2 atoms of bromine. You can work in the opposite #art of catalysts such as iodine, iron, aluminum chloride, sulfur, etc.
The reaction product dissolves in concentrated sulfuric acid with a blue color and yields a violet vat from which the vegetable fiber is dyed in clear, strong, borclea, ux-red shades of very good fastness. Example: 460 parts of the pyridinopyranthrone shown according to patent 149413 are dissolved in: 1000 parts of chlorosulfonic acid with stirring and, after the addition of 40 parts of sulfur and 200 parts of bromine, slowly heated to 60 to 65.degree.
You hold at this temperature until all the bromine is absorbed, then let it cool down and work up in the usual way.
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE150924X | 1929-06-21 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH150924A true CH150924A (en) | 1931-11-30 |
Family
ID=5674191
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH150924D CH150924A (en) | 1929-06-21 | 1930-06-20 | Process for the production of a vat dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH150924A (en) |
-
1930
- 1930-06-20 CH CH150924D patent/CH150924A/en unknown
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