CH106075A - Process for the production of a new intermediate product. - Google Patents

Process for the production of a new intermediate product.

Info

Publication number
CH106075A
CH106075A CH106075DA CH106075A CH 106075 A CH106075 A CH 106075A CH 106075D A CH106075D A CH 106075DA CH 106075 A CH106075 A CH 106075A
Authority
CH
Switzerland
Prior art keywords
mole
cyanuric chloride
production
intermediate product
new intermediate
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH106075A publication Critical patent/CH106075A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/40—Nitrogen atoms
    • C07D251/42—One nitrogen atom
    • C07D251/44—One nitrogen atom with halogen atoms attached to the two other ring carbon atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Herstellung eines neuen Zwischenproduktes.    Es wurde gefunden, dass man ein neues  Zwischenprodukt, das primäre Kondensations  produkt von einem Mol. Cyanurchlorid mit  einem Mol. 2.8-Aminonaphthol-6-sulfosäure  erhält, wenn man auf ein Mol. Cyanurchlorid  ein Mol. 2 . 8-Aminonaphthol-6-sülfosäure ein  wirken lässt.  



  Diese Kondensation wird durch Zusam  menrühren der Komponenten in einem geeig  neten Verdünnungsmittel durchgeführt, und  es wurde gefunden, dass als solches     Wasser    in  überraschender Weise sehr gut geeignet ist.  Das primäre Kondensationsprodukt aus einem  Mol. Cyanurchlorid mit einem Mol.     2.8-          Aminonaphthol-6-sulfosäure    bildet ein in  Wasser leicht lösliches, kristallinisches, fast  farbloses Pulver. Es enthält noch zwei reak  tionsfähige Chloratome und stellt ein wert  volles Ausgangsmaterial zur Herstellung von  Farbstoffen dar.  



  Beispiel:  Eine fein verteilte Aufschlemmung von  18,5 Teilen Cyanurehlorid in 1000 Teilen  Wasser wird mit Salzsäure schwach sauer  gestellt und nach und nach bei 0  unter Rüh  ren mit einer Lösung von 26,2 Teilen 2.     8-          aminonaphthol-6-sulfosaurem    Natrium in 500    Teilen Wasser versetzt, wobei man durch Zu  g a be von Sodalösung (im ganzen 5,3 Teile)  die Reaktion immer schwach sauer hält. Die  so erhaltene klare Lösung enthält das     Kon-          densationsprodukt    von einem Mol.     Cyanur-          ehlorid    mit einem Mol. 2 .     8-Aminonaphthol-          6-sulfosäure,    das durch Kochsalz und Säure  zusatz gefällt wird.



  Process for the production of a new intermediate product. It has been found that a new intermediate product, the primary condensation product of one mole of cyanuric chloride with one mole of 2,8-aminonaphthol-6-sulfonic acid, is obtained if one mole of second cyanuric chloride is used for one mole of cyanuric chloride. 8-aminonaphthol-6-sulphonic acid can act.



  This condensation is carried out by stirring the components together in a suitable diluent, and it has been found that, surprisingly, water is very suitable as such. The primary condensation product of one mole of cyanuric chloride with one mole of 2,8-aminonaphthol-6-sulfonic acid forms a crystalline, almost colorless powder which is easily soluble in water. It still contains two reactive chlorine atoms and is a valuable starting material for the production of dyes.



  Example: A finely divided slurry of 18.5 parts of cyanuric chloride in 1000 parts of water is made weakly acidic with hydrochloric acid and gradually ren with a solution of 26.2 parts of 2. 8-aminonaphthol-6-sulfonic acid in sodium at 0 with stirring 500 parts of water are added, and the reaction is always kept slightly acidic by adding soda solution (5.3 parts in total). The clear solution thus obtained contains the condensation product of one mole of cyanuric chloride with one mole of 2. 8-aminonaphthol-6-sulfonic acid, which is precipitated by adding table salt and acid.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Zwischenproduktes, des primären Kondensa tionsproduktes von einem Mol. Cyanurchlorid mit einem Mol. 2.8-Aminonaphthol-6-sulfo- säure, dadurch gekennzeichnet, dass man auf ein Mol. Cyanurchlorid ein Mol. 2 . 8-Amino- naphthol-6-sulfosäure einwirken lässt. Das primäre Kondensationsprodukt aus einem Mol. Cyanurchlorid und einem Mol. 2 . 8-Aminonaphthol-6-sulfo,säure bildet ein in Wasser leicht lösliches, kristallinisches, fast farbloses Pulver. PATENT CLAIM: Process for the preparation of a new intermediate product, the primary condensation product of one mole of cyanuric chloride with one mole of 2,8-aminonaphthol-6-sulfonic acid, characterized in that one mole of cyanuric chloride is added to one mole of 2 8-amino-naphthol-6-sulfonic acid can act. The primary condensation product of one mole of cyanuric chloride and one mole of 2. 8-aminonaphthol-6-sulfo, acid forms a crystalline, almost colorless powder that is easily soluble in water. Es enthält noch zwei reak tionsfähige Chloratome und stellt ein wert volles Ausgangsmaterial zur Herstellung von Farbstoffen dar. It still contains two reactive chlorine atoms and is a valuable starting material for the production of dyes.
CH106075D 1922-09-07 1922-09-07 Process for the production of a new intermediate product. CH106075A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH103430T 1922-09-07
CH106075T 1922-09-07

Publications (1)

Publication Number Publication Date
CH106075A true CH106075A (en) 1924-08-01

Family

ID=25706374

Family Applications (1)

Application Number Title Priority Date Filing Date
CH106075D CH106075A (en) 1922-09-07 1922-09-07 Process for the production of a new intermediate product.

Country Status (1)

Country Link
CH (1) CH106075A (en)

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